CN110693767A - Glacier mineral mud film with skin cleaning effect and preparation method thereof - Google Patents

Abstract

The invention discloses a glacier mineral mud film with a skin cleaning effect and a preparation method thereof, wherein the mud film comprises a pore convergence component, an anti-inflammatory repair component, a humectant, a skin feel regulator and a film forming agent; wherein the mud film comprises the pore astringing components in percentage by mass as follows: 0.1-30% of natural glacier sea mud, 0.1-5% of pseudoalteromonas fermentation product extract, 0.1-20% of Jizhou island lava water and 0.01-20% of hamamelis virginiana flower water; the mud film is quick-dried for 8-10 minutes, easy to absorb and easy to clean; the natural glacier sea mud is adopted as a main component, can provide sufficient application for skin, is compounded with a plurality of effective components, and can show the anti-allergy and anti-inflammation, relieving and repairing, brightening skin color and astringing pores of each component, thereby achieving the long-acting effect of balancing oil and water; the preparation method of the glacier mineral mud film is simple and convenient, and the glacier mineral mud film product which can effectively control oil, astringe pores and smooth skin can be provided.

Description

Glacier mineral mud film with skin cleaning effect and preparation method thereof

Technical Field

The invention belongs to the field of daily chemicals, relates to a mud film, and particularly relates to a glacier mineral mud film with a skin cleaning effect and a preparation method thereof.

Background

The facial mask is a common skin care product, and the facial mask mainly has four types, namely a paste type, a tearing type, a jelly type and a wet tissue type. Among them, the mud-paste type mask is usually a seaweed mask, a slime mask, etc. The mud mask is a mud-shaped mask, and can achieve a certain effect by directly smearing the mud-shaped mask on the face, incubating for a period of time and then washing with water.

The mud mask does not use powder such as kaolin for emphasizing fat absorption, but uses natural raw materials such as sea mud, volcanic mud and the like, contains natural mineral components and various nutrient components, has low irritation, and can be cleaned and maintained simultaneously. Most of the mud film products in the market rarely use natural glacier sea mud, and use more volcanic mud and dead sea mud. The Canadian glacier sea mud is superior to other beauty mud in purity, components and functions, is rich in more than 60 mineral substances and rare earth elements, has complex natural components and has unique physical and beauty characteristics.

Disclosure of Invention

The invention aims to design a mud film formula adopting Canada glacier sea mud, and in order to realize the aim, the invention adopts the technical scheme that: a glacial mineral mud film with skin cleaning effect comprises pore astringing component, antiinflammatory and repairing component, humectant, skin feeling regulator, and film forming agent; wherein the mud film comprises the pore astringing components in percentage by mass as follows: 0.1-30% of natural glacier sea mud, 0.1-5% of pseudoalteromonas fermentation product extract, 0.1-20% of Jizhou island lava water and 0.01-20% of hamamelis virginiana flower water.

Natural glacier sea mud, bred over one million years ago and produced during the last age of glacier, contains almost all elements present in the ocean, has strong ion exchange capacity, high astringency, provides skin cleansing and astringency, and can effectively promote repair and moisturization, and has the following advantages over other mud film substrates:

1. rich in minerals: this natural glacier sea mud has matured over thousands of years of incubation on the west coast of canada and is unique in this area of the world as it is formed by the movement of glaciers and contains over 60 minerals.

2. Magnetic purification: impurities on the skin are positively charged, while sea mud particles are negatively charged. When applied to the skin, negatively charged ions in the sea mud will adsorb skin impurities. When you wash their face, the impurities are washed away along with the sea mud, thus ensuring deep cleaning.

3. Pore shrinking: the natural glacier sea mud can help reduce pores and make skin smooth like porcelain while removing impurities such as grease and dirt in pores.

4. Natural moisturizing: the natural glacier sea mud can bring the water in the deep tissue inside to the surface layer by utilizing the osmotic pressure of the natural glacier sea mud to moisten the skin. The use of the natural glacier sea mud for cleaning the skin does not cause the skin to be dehydrated and dried as other skin cleaning products.

5. Removing impurities: the fine natural glacier sea mud particles act like an emulsifier to form a barrier around the oil particles of your skin, effectively removing the oil when washing the face.

6. Therapeutic properties: the natural glacier sea mud, like the skin protection shield with anti-inflammatory properties, is cooled by various procedures to soothe the skin.

7. Equilibrium pH: natural glacier sea mud helps maintain a balanced PH and possesses strong buffering capacity. It can also help to enhance the barrier function of the skin to maintain its healthy beauty.

UV protection: the minerals in the natural glacier sea mud act together to form a natural, durable protective layer against UVB, UVA and UVC radiation.

Most of east China island is covered by lava flow, and the water permeability of the earth surface is particularly good; the underground geology is a surface layer formed by basalt, the molten rock water of the Jizhou island is pure low-temperature seawater which is rich in mineral substances and is obtained after being filtered by the geological structures, and the low-temperature seawater contains other mineral substances which are not possessed by common seawater and deep seawater, and has the effects of resisting inflammation, removing free radicals, preserving moisture, promoting cell proliferation, resisting acnes and the like. Available from IRONWOOD CLAY COMPANY INC under the JMSWED trade name.

The pseudoalteromonas fermentation product extract is extracellular polymeric substances (ECPS) obtained from the marine pseudoalteromonas through a biotechnology, can reduce the protein level of MC5-R (related to sebaceous gland cell differentiation), reduce the maturation and lipid peroxidation of sebaceous gland cells, and simultaneously can greatly increase the synthesis of type I collagen, thereby relieving the skin symptoms of oily and mixed skin and tightening the skin; the biological component can reduce excessive oil and sebum, shrink pores, and reduce speckle.

The peculiar allergy-relieving factor in the witch hazel has excellent effects of calming and soothing, and can mildly relieve sensitive skin and balance metabolism. The irritated skin is alleviated, the skin regeneration can be effectively helped, and the wound can be healed. Has good improvement effect on eczema, sunburn and rhagadia. The Hamamelis virginiana water can regulate skin balance and oil secretion from inside to outside, has astringent and antibacterial effects, can rapidly permeate into skin, obviously astringe large pores, and prevent blackheads and acnes. Skin care ingredients are preferred for adolescent or skin with severe oil-producing condition.

The pseudoalteromonas fermentation product extract, the Jizhou island lava water, the Hamamelis virginiana water and the natural glacier sea mud can be synergized, and the effects of inhibiting grease secretion and astringing pores by a mud film are obviously improved.

As a preferred implementation method of the invention, the mud film comprises the following anti-inflammatory repair components in percentage by mass: 0.1-5% of composite plant extract, 0.01-5% of glycyrrhiza glabra root extract and 0.01-2% of lavender oil; the plant composite extract is a mixture consisting of centella asiatica extract, polygonum cuspidatum root extract, scutellaria baicalensis extract, glycyrrhiza glabra root extract, chamomile flower extract, tea extract and rosemary leaf extract.

The functional components with strong antioxidant activity for skin decolorization and color spot lightening exist in the root and rhizome tissue cells of the glycyrrhiza glabra, and the functional components are main components, namely glycyrrhiza glabra and glycyrrhiza glabra, and are called whitening gold. It has effects in whitening skin, killing bacteria, removing mottle, and relieving skin.

The composite plant extract is a combination of multiple plant extracts, and is available from Korean BioSpectrum under the trade name of BioSpectrumHas anti-allergic, anti-inflammatory, and repairing effects.

The natural glacier sea mud and the glycyrrhiza glabra root extract have synergistic effect and play a role in brightening the skin;the glycyrrhiza glabra root extract and the natural glacier sea mud are synergistic, so that the anti-allergy, anti-inflammation, and relieving and repairing effects of the mud film can be further improved.

As a preferred implementation method of the invention, the mud film comprises the following moisture-preserving components in percentage by mass: trehalose 0.1-10%, glycerol 0.1-20%, 1, 3-propanediol 0.1-10%, 1, 2-hexanediol 0.01-2%, and 1, 2-pentanediol 0.01-2%.

As a preferred implementation method of the invention, the mud film comprises the following skin feel conditioning agents in percentage by mass: 0.1-30% of mung bean-like mud mixture, 0.1-30% of kaolin and 0.01-2% of xanthan gum.

The mung bean paste-like mixture is a mixture consisting of sea sludge, salt mine slurry and iron oxide, and is purchased from Shanghai Longxin chemical technology Co., Ltd, and has a trade name of NTS-711 mung bean paste.

As a preferable implementation method of the invention, the mud film comprises a film forming agent with the mass percentage of 0.1-4%.

As a preferred method of carrying out the present invention, the film forming agent is a mixture of polyacrylamide, C13-14 isoparaffin, and laureth-7.

As a preferable implementation method of the invention, the mud film further comprises 0.01-0.4% by mass of a preservative and 0.01-2% by mass of an antioxidant.

As a preferred method of carrying out the present invention, the preservative is methylparaben; the antioxidant is p-hydroxyacetophenone.

As a preferred implementation method of the invention, the mud film comprises the following components in percentage by mass: 20% of natural glacier sea mud, 1% of pseudoalteromonas ferment product extract, 2% of jizhou island lava water, 5% of hamamelis virginiana water, 0.5% of compound plant extract, 0.3% of glycyrrhiza glabra root extract, 0.02% of lavender oil, 2% of trehalose, 5% of glycerol, 3% of 1, 3-propylene glycol, 1% of 1, 2-hexanediol, 1% of 1, 2-pentanediol, 8% of mung bean-like mud mixture, 10% of kaolin, 0.4% of xanthan gum, 2% of polyacrylamide, a mixture of C13-14 isoparaffin and laureth-7, 0.2% of methylparaben, 0.5% of p-hydroxyacetophenone, and the balance of water.

The invention also provides a preparation method of the mud film, which comprises the following steps:

(1) sequentially adding water, trehalose, glycerol, 1, 3-propylene glycol, a preservative, an antioxidant, a skin feel regulator and natural glacier sea mud into an emulsifying pot, heating and stirring, heating to 85-90 ℃, and homogenizing;

(2) cooling the mixture in the step (1) to 60 ℃, adding a film-forming agent, homogenizing, and then vacuumizing for defoaming;

(3) cooling to 45-50 ℃, adding 1, 2-hexanediol, 1, 2-pentanediol, hamamelis virginiana water, Jizhou island lava water, pseudoalteromonas ferment product extract, composite plant extract and glycyrrhiza glabra root extract, and stirring uniformly;

(4) cooling to 42-45 ℃, adding lavender oil, and stirring uniformly;

(5) and filtering and discharging after sampling detection is qualified.

As a preferred method for carrying out the present invention, in the step (1), the mixture is homogeneously stirred for 30 minutes; the homogenization time in the step (2) is 10 minutes; the step (3) is stirred for at least 30 minutes; the step (4) was stirred for 10 minutes.

The mud film is quick-dried for 8-10 minutes, easy to absorb and easy to clean; the natural glacial sea mud is used as a main component, has the effect of instantly shrinking pores and provides a cool and refreshing feeling for the product, and after the natural glacial sea mud is used, the grease on the surface of the skin is obviously reduced by 95% on average; the composition is combined with pseudoalteromonas ferment product extract, Jizhou island lava water and Hamamelis virginiana flower water, and has the effects of inhibiting grease secretion and astringing pores in a synergistic manner, so that the effects of balancing oil and water for a long time and improving skin smoothness are achieved. The preparation method of the glacier mineral mud film is simple and convenient, and the glacier mineral mud film product which can effectively control oil and astringe pores can be provided.

Detailed Description

To better illustrate the objects, aspects and advantages of the present invention, the present invention will be further described with reference to specific examples.

Examples 1 to 13

The formulations of the glacier mineral mud films having a skin cleansing effect in examples 1 to 13 of the present invention are shown in table 1.

Table 1 weight percentages of the components of the mud film of examples 1-13

The preparation method of the mud film in each example is as follows:

(1) sequentially adding water, trehalose, glycerol, 1, 3-propylene glycol, a preservative, an antioxidant, a skin feel regulator and natural glacier sea mud into an emulsifying pot, heating and stirring for 30 minutes, heating to 85-90 ℃, and homogenizing;

(2) cooling the mixture in the step (1) to 60 ℃, adding a film-forming agent, homogenizing for 10 minutes, and then vacuumizing for defoaming;

(3) cooling to 45-50 ℃, adding 1, 2-hexanediol, 1, 2-pentanediol, hamamelis virginiana water, Jizhou island lava water, pseudoalteromonas ferment product extract, composite plant extract and glycyrrhiza glabra root extract, and stirring for at least 30 minutes until the mixture is uniform;

(4) cooling to 42-45 ℃, adding lavender oil, and stirring for 10 minutes until the mixture is uniform;

(5) and filtering and discharging after sampling detection is qualified.

Comparative example 1

Comparative example 1 except that the natural glacier sea mud is not contained, the kaolin accounts for 30% of the total mass (the balance is made up by adjusting water according to the components), and the other components and the preparation method are basically consistent with those in example 1.

Comparative example 2

Comparative example 2 the components and preparation method were substantially the same as in example 1 except that the extract of the fermentation product of pseudoalteromonas was not contained (water was adjusted to make up the balance depending on the components).

Comparative example 3

Comparative example 3 the components and preparation method were substantially the same as those of example 1 except that the water for melting rock in Jizhou island was not contained (the water was adjusted to make up the balance according to the components).

Comparative example 4

Comparative example 4 the ingredients and preparation method were substantially the same as in example 1 except that hamamelis virginiana water was not contained (water was adjusted to make up the balance according to the ingredients).

Oil control performance test

Female volunteers between the ages of 28-50 were found and randomly divided into 17 groups of 10 people each. After face washing, the forehead grease is detected on the face at 1 hour, 3 hours, 5 hours and 7 hours by using examples 1-13, comparative examples 1-4 and a control group, the grease variation of a positioning part is comprehensively obtained by adopting a German CK grease tester SM 815 test, and the average value is taken, wherein the lower the grease variation data value is, the better the oil control performance is. The test results are shown in Table 2.

TABLE 2 oil control Performance test results of examples 1 to 13 and comparative examples 1 to 4

From the experimental results, the proportion of the example 1 is optimal in the examples 1 to 13; in comparative examples 1-4, after the pseudoalteromonas ferment product extract, the Jizhou island lava water, the Hamamelis virginiana water and the natural glacier sea mud are lack of part of components, the oil control effect is remarkably reduced, and the pseudoalteromonas ferment product extract, the Jizhou island lava water, the Hamamelis virginiana water and the natural glacier sea mud have the effects of synergy and inhibition of oil secretion.

Second, skin smoothness change rate test

Female volunteers between 18-50 years of age were found and divided into 17 groups of 10 persons each according to age and skin condition. The test subjects were used once a day for 30 days without any other product during the test period using examples 1 to 13 and comparative examples 1 to 4 on the face. Under the conditions that the ambient temperature is 25 +/-1 ℃ and the humidity is 50 +/-5%, a VISIA facial image analyzer is adopted for testing, smoothness data are comprehensively obtained, and the higher the data value is, the worse the skin smoothness is. The test results are given in table 3 below.

TABLE 3 skin smoothness test results for examples 1-13 and comparative examples 1-4

From the above experimental results, the best mixture ratio of example 1 is found in examples 1 to 13; and after the comparative example lacks part of components of the pseudoalteromonas ferment product extract, the Jizhou island lava water, the Hamamelis virginiana water and the natural glacier sea mud, the skin smoothness is obviously reduced, which indicates that the pseudoalteromonas ferment product extract, the Jizhou island lava water, the Hamamelis virginiana water and the natural glacier sea mud have the synergistic effect and the effect of improving the skin smoothness.

Finally, it should be noted that the above embodiments are only used for illustrating the technical solutions of the present invention and not for limiting the protection scope of the present invention, and although the present invention is described in detail with reference to the preferred embodiments, it should be understood by those skilled in the art that modifications or equivalent substitutions can be made on the technical solutions of the present invention without departing from the spirit and scope of the technical solutions of the present invention.

Claims (10)

1. An glacial mineral mud film with a skin cleaning effect is characterized by comprising a pore astringing component, an anti-inflammatory repairing component, a humectant, a skin feel regulator and a film forming agent; wherein the mud film comprises the pore astringing components in percentage by mass as follows: 0.1-30% of natural glacier sea mud, 0.1-5% of pseudoalteromonas fermentation product extract, 0.1-20% of Jizhou island lava water and 0.01-20% of hamamelis virginiana flower water.

2. The mud film of claim 1, wherein the mud film comprises the following anti-inflammatory repair components in percentage by mass: 0.1-5% of composite plant extract, 0.01-5% of glycyrrhiza glabra root extract and 0.01-2% of lavender oil; the plant composite extract is a mixture consisting of centella asiatica extract, polygonum cuspidatum root extract, scutellaria baicalensis extract, glycyrrhiza glabra root extract, chamomile flower extract, tea extract and rosemary leaf extract.

3. The mud film as claimed in claim 1, wherein the mud film comprises the following moisture retention components in percentage by mass: trehalose 0.1-10%, glycerol 0.1-20%, 1, 3-propanediol 0.1-10%, 1, 2-hexanediol 0.01-2%, and 1, 2-pentanediol 0.01-2%.

4. The mud film of claim 1, wherein the mud film comprises the following skin-feel modifiers in mass percent: 0.1-30% of mung bean-like mud mixture, 0.1-30% of kaolin and 0.01-2% of xanthan gum; the mung bean-like mud mixture is a mixture consisting of sea mud, salt mine mud and iron oxide.

5. The mud film of claim 1, wherein the mud film comprises 0.1-4% by mass of a film forming agent.

6. The mud film of claim 5, wherein the film forming agent is a mixture of polyacrylamide, C13-14 isoparaffin, and laureth-7.

7. The mud film as claimed in claim 1, further comprising 0.01-0.4% by mass of a preservative and 0.01-2% by mass of an antioxidant.

8. The mud film of claim 7, wherein the preservative is methylparaben; the antioxidant is p-hydroxyacetophenone.

9. The mud film as claimed in claim 1, which is characterized by comprising the following components in percentage by mass: 20% of natural glacier sea mud, 1% of pseudoalteromonas ferment product extract, 2% of jizhou island lava water, 5% of hamamelis virginiana water, 0.5% of compound plant extract, 0.3% of glycyrrhiza glabra root extract, 0.02% of lavender oil, 2% of trehalose, 5% of glycerol, 3% of 1, 3-propylene glycol, 1% of 1, 2-hexanediol, 1% of 1, 2-pentanediol, 8% of mung bean-like mud mixture, 10% of kaolin, 0.4% of xanthan gum, 2% of polyacrylamide, a mixture of C13-14 isoparaffin and laureth-7, 0.2% of methylparaben, 0.5% of p-hydroxyacetophenone, and the balance of water.

10. A method for preparing a mudfilm according to claim 9, characterized by comprising the following steps:

(1) sequentially adding water, trehalose, glycerol, 1, 3-propylene glycol, a preservative, an antioxidant, a skin feel regulator and natural glacier sea mud into an emulsifying pot, heating and stirring, heating to 85-90 ℃, and homogenizing;

(2) cooling the mixture in the step (1) to 60 ℃, adding a film-forming agent, homogenizing, and then vacuumizing for defoaming;

(3) cooling to 45-50 ℃, adding 1, 2-hexanediol, 1, 2-pentanediol, hamamelis virginiana water, Jizhou island lava water, pseudoalteromonas ferment product extract, composite plant extract and glycyrrhiza glabra root extract, and uniformly stirring;

(4) cooling to 42-45 ℃, adding lavender oil, and uniformly stirring;

(5) and filtering and discharging after sampling detection is qualified.