CN103750182A - 蜜柚果粉口含片及其制备方法 - Google Patents
蜜柚果粉口含片及其制备方法 Download PDFInfo
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- CN103750182A CN103750182A CN201310647079.2A CN201310647079A CN103750182A CN 103750182 A CN103750182 A CN 103750182A CN 201310647079 A CN201310647079 A CN 201310647079A CN 103750182 A CN103750182 A CN 103750182A
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- Prior art keywords
- sweet shaddock
- honey pomelo
- fruit powder
- sweet
- normal juice
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Abstract
本发明公开一种蜜柚果粉口含片及其制备方法,其成分包括脱苦蜜柚果粉,麦芽糊精,白砂糖,果葡糖浆,一水柠檬酸,山梨酸钾,甘草和维生素C;其制备方法包括制备脱苦蜜柚果粉步骤、配方调配步骤、制软材步骤、造粒步骤、压片步骤。该蜜柚果粉口含片软硬适度,崩解性好,既蜜柚香味浓郁、口感甜而不腻,且蜜柚原料的脱苦效果好、所含柚皮苷的含量低。
Description
技术领域
本发明公开一种口含片,特别是一种柚香风味的口含片。
背景技术
口含片指含于口腔内缓慢溶解的压制片。口含片因其优良的口感及方便的服用方法而受到广大患者的欢迎。在国内市场上,有联邦阿莫仙、江中草珊瑚、华素片等许多品种都有着不俗的销售业绩。
口含片不仅用于对口腔及咽部产生持久的药效,如草珊瑚含片用于局部的消炎、消毒;还有更多用于保健食品等其他用途。例如,专利CN101791096A公开了一种沙枣甘饴口含片,以沙枣为主要原料,辅以甘草等原料,按下述的步骤制备:沙枣粉末或沙枣水提物粉末的制备、甘草粉末的制备、配料、混合、湿法制料、干燥、压片和包装等步骤。该种沙枣甘饴口含片质量好、不易回潮变质,色、香、味俱佳,含片硬度高,味道沙枣独特和营养价值极高,并为大众接受。专利CN102342515A公开了一种柿子口含片,由柿子浓缩浆、中药浓缩浆、食用淀粉、甘露醇、蔗糖和硬脂酸镁混合压片制成;各组分质量配比为:柿子浓缩浆31-35%,中药浓缩浆12-16%,食用淀粉34-38%,甘露醇5-8%,蔗糖4-7%和硬脂酸镁0.7-1.5%;该种柿子口含片具有生产效率高,设备利用率高,便于机械化生产等优点;产品风味独特、口感纯正、色泽优良,易于成型,具有抗氧化作用,质量符合国家相关产品质量标准要求。专利CN102488815A发明公开一种降糖口含片,由如下重量份的组分制成:青钱柳提取物16-20份、肉桂提取物15-19份、苦瓜提取物11-15份、牛磺酸8-12份、山药提取物10-14份、葛根提取物10-14份、交联羧甲基纤维素钠5-10份、阿斯巴坦2-5份、硬脂酸镁6-9份、薄荷香精0.2-0.5份,该口含片具有服用方便、易储存和便于携带的优势,且生物利用度比普通制剂明显提高,为适应现在快节奏的生活需求和不断提升的生活品味又提供了一项便利的给药途径。
口含片已经大规模产业化,而且应用领域越来越广,其加工工艺非常成熟,其流程常见为:原料处理→配方调配→制软材→造粒→烘干、整粒→压片→包装。其中造粒是片剂工艺中的一个关键操作点:可防止粉状食品加工时粉尘飞扬,也可以提高填充效率,防止片剂吸水。一般情况下,为了使各原料成分有效粘结成片,须在制片过程中添加粘合剂;为使口含片易从模板上脱落,可在混合后的物料中加入润滑剂。
专利CN1339310A公开了一种柚子含片及其制作方法,包括以下重量配比的原料:柚子粉83-87%,甘草粉3-7%,枇杷叶粉3-7%,桔梗粉3-7%,甜菊糖甙1-5%,薄荷脑0.5-1.5%。其制作工艺为:将整柚粉碎至糊状,果胶与果碎分离;分别干燥果胶和果碎,含水量控制7%以下;果胶和果碎分别过筛后,混合均匀;分别将甘草、枇杷叶、桔梗粉碎,过筛后,干燥;将果胶粉、果碎粉、甘草粉、枇杷叶粉和桔梗粉再加入甜菊糖甙、薄荷脑,混合均匀,用压片机压成片。该口含片以柚子粉为主体成分,但柚子果皮果肉未经脱苦处理,口含片涩味明显;其甜味剂主要依赖高比例的甘草,其甜度过甜,而且营养成分缺失。
为满足喜欢蜜柚风味的蜜柚口含片的消费者,还急需一款以蜜柚为原料的口含片产品。既要求它蜜柚香味浓郁、口感甜而不腻,又要求其所含柚皮苷的含量低(也即脱苦效果良好)。
发明内容
本发明的目的在于提供一种蜜柚果粉口含片,以蜜柚为主要原料制备而成的,可满足喜欢蜜柚风味口含片的消费者。该口含片软硬适度,崩解性好,既蜜柚香味浓郁、口感甜而不腻,且蜜柚原料的脱苦效果良好、所含柚皮苷的含量低。
本发明的另一个目的在于提供一种制备蜜柚果粉口含片的方法,该方法工艺过程简单,适合产业化生产,蜜柚原料中的柚皮苷脱除效果良好。
本发明提供一种蜜柚果粉口含片,包括如下重量份的组分:脱苦蜜柚果粉45-55份,麦芽糊精19-23份,白砂糖14-16份,果葡糖浆13-15份,一水柠檬酸0.2-0.4份,山梨酸钾0.02-0.04份,甘草0.1-0.3份和维生素C0.06-0.1份。
其中,所述的脱苦蜜柚果粉由下述的步骤制备得到:
A1.去皮取肉步骤:将蜜柚鲜果分切成瓣鲜果,并成瓣鲜果的蜜柚果皮和蜜柚果肉分离,取其蜜柚果肉;
A2.制备蜜柚原汁步骤:将蜜柚果肉进行破碎,过滤,取滤液得蜜柚原汁;
A3.蜜柚原汁脱苦步骤:通过离子交换树脂脱除蜜柚原汁中的苦味素,将脱苦后的蜜柚原汁与离子交换树脂分离,制得脱苦蜜柚汁;
A4.制粉步骤:将脱苦蜜柚汁浓缩结晶,研磨成粉,制得脱苦蜜柚果粉。
优选的,所述的蜜柚原汁脱苦步骤的工艺条件为:蜜柚原汁与离子交换树脂的重量比为6-10:1,室温下混匀静置2-10分钟。
该蜜柚果粉口含片由下述步骤制备得到:
A.制备脱苦蜜柚果粉;
B.配方调配步骤:将下述重量份的组分原料混合均匀:脱苦蜜柚果粉45-55份,麦芽糊精19-23份,白砂糖14-16份,果葡糖浆13-15份,一水柠檬酸0.2-0.4份,山梨酸钾0.02-0.04份,甘草0.1-0.3份和维生素C0.06-0.1份;
C.制软材步骤:将混合均匀的配方原料与食用乙醇混合,制得软材;
D.造粒步骤:将所得软材过16-24目筛进行制粒,并在45-65℃下烘干,使其水分含量小于5%,再过35-45目筛进行整粒;
E.压片步骤:送入压片机进行压片,制得蜜柚果粉口含片。
由于甘草的甜度是蔗糖的百倍,添加微量的甘草后,可在不影响蜜柚果粉口含片的糖分含量情况下,大幅度增加蜜柚果粉口含片的甜味、改善其酸甜度;同时甘草中含有甘草甜素、甘草次酸、甘草甙、异甘草甙、新甘草甙、新异甘草甙、甘草素、异甘草素以及甘草西定、甘草醇、异甘草醇、7-甲基香豆精、伞形花内酯等数十种化合物,可以起到调和其他组分的作用。
在甜味剂的选择上,采用白砂糖和果葡糖浆的配合,而且配比在控制1:1左右,又添加微量的甘草,既可以保证蜜柚果粉口含片的适口的甜味,又可以相对节约成本;还可以较好协调加入的脱苦蜜柚果粉的天然柚香风味。白砂糖用量需要适应控制,其不仅影响蜜柚口含片成品的酸甜度,若用量不足则会导致压片过程中出现裂片问题。
麦芽糊精是以淀粉为原料,经酶法工艺控制水解转化而成的,是一种价格低廉、口感滑腻、没有任何味道的营养性多糖。它的溶解性能良好,有适度的粘度;吸湿性低,不易结团。有较好的载体作用,是各种甜味剂、香味剂、填充剂等的优良载体;还有很好的乳化作用和增稠效果,便于促进片剂产品成型;成膜性能好,既能防止片剂产品变形又能改善产品外观;同时还极易被人体吸收,特别适宜作病人和婴幼儿童食品。该蜜柚果粉口含片选择麦芽糊精作为填充剂,它不仅避免了传统的糖粉类填充剂易引湿、易造成龋齿等缺点,而且还能与脱苦蜜柚果粉等主要原料融合良好。
本发明的口含片中,白砂糖既做稀释剂,又起到矫味和粘合作用,同时还作为甜味剂。主体成分、糖粉和可溶性淀粉的配比控制为:脱苦蜜柚果粉:白砂糖:麦芽糊精=(9-11):3:4左右,既保护了蜜柚口含片的蜜柚天然风味,又保证了片剂成品的硬度、含化时间等性能指标,还克服了加工过程中易出现的松片、裂片、花片等问题。
一水柠檬酸作为酸性调味剂,用于协调脱苦蜜柚果粉的酸甜度,同时还可改善口含片的感官性状,增强食欲和促进体内钙、磷物质的消化吸收。
离子交换树脂对蜜柚原汁进行脱苦时,也会吸附果汁中的维生素C和部分还原糖,在配置糖液时加入微量的维生素C进行增补,保证了蜜柚果粉的维生素C含量。
本发明还提供一种制备蜜柚果粉口含片的方法,包括下述步骤:
A.制备脱苦蜜柚果粉;
B.配方调配步骤:将下述重量份的组分原料混合均匀:脱苦蜜柚果粉45-55份,麦芽糊精19-23份,白砂糖14-16份,果葡糖浆13-15份,一水柠檬酸0.2-0.4份,山梨酸钾0.02-0.04份,甘草0.1-0.3份和维生素C0.06-0.1份;
C.制软材步骤:将混合均匀的配方原料与食用乙醇混合,制得软材;
D.造粒步骤:将所得软材过16-24目筛进行制粒,并在45-65℃下烘干,使其水分含量小于5%,再过35-45目筛进行整粒;
E.压片步骤:送入压片机进行压片,制得蜜柚果粉口含片。
颗粒太潮则会在压片过程中产生粘冲问题;而颗粒水分含量过低则会导致压片过程中出现松片问题。同时,造粒步骤中的烘干处理的终点控制对口含片成品的崩解性有较大的影响,需要适宜控制:使干燥终点的软材水分含量小于5%为宜,此时软材的软硬度以手捏成团(且手感干脆、不粘手)、轻压则散。较佳的,干燥终点控制宜在软材的水分含量为2-4%。
润滑剂的添加不仅需要考虑其离型、脱模效果,还要考虑其引入后的残留问题,以及对口含片的表面花点问题和口含片的崩解性的影响。优选的,在所述的压片步骤中,在经造粒步骤后的颗粒中添加重量百分比1-2%的硬脂酸镁。硬脂酸镁不溶于水、乙醇或乙醚,可用作润滑剂,便于口含片易从模板上脱落;同时对该蜜柚果粉口含片的表面花点问题和口含片的崩解性影响较小。
其中,制备脱苦蜜柚果粉的步骤包括:
A1.去皮取肉步骤:将蜜柚鲜果分切成瓣鲜果,并成瓣鲜果的蜜柚果皮和蜜柚果肉分离,取其蜜柚果肉;
A2.制备蜜柚原汁步骤:将蜜柚果肉进行破碎,过滤,取滤液得蜜柚原汁;
A3.蜜柚原汁脱苦步骤:通过离子交换树脂脱除蜜柚原汁中的苦味素,将脱苦后的蜜柚原汁与离子交换树脂分离,制得脱苦蜜柚汁;
A4.制粉步骤:将脱苦蜜柚汁浓缩结晶,研磨成粉,制得脱苦蜜柚果粉。
优选的,所述的蜜柚原汁脱苦步骤的工艺条件为:蜜柚原汁与离子交换树脂的重量比为6-10:1,室温下混匀静置2-10分钟。
为便于产业化生产时更好的控制蜜柚果粉口含片的质量的稳定性和口感的一致性,可在制备脱苦蜜柚果粉的去皮取肉步骤之前,增加清洗消毒的步骤:采用浓度为10-500mg/L的二氧化氯水溶液对蜜柚鲜果进行清洗消毒,从而可以较好清洁蜜柚鲜果在生长、采收及运输过程中表面附着的尘土、泥沙、害虫、微生物等。若去除蜜柚鲜表皮残存的农药或重油等,可以先用0.5%-1.5%(重量)盐酸水溶液进行清洗,再用1%(重量)碳酸钠水溶液清洗;或者,先用0.03%-0.1%(重量)的高锰酸钾溶液或0.04%-0.06%的漂白粉溶液浸泡10-15分钟,再用清水漂洗。
本发明的有益效果有:蜜柚果粉口含片以脱苦蜜柚果粉为主要原料,通过配方调配、制软材、造粒、压片步骤制得,其保持了适宜的酸甜度,保证了维生素C的含量,所含柚皮苷的含量控制较低水平。该口含片软硬适度,崩解性好,既蜜柚香味浓郁、口感甜而不腻,且蜜柚辅料的脱苦效果良好、所含柚皮苷的含量低。
具体实施方式
通过下面给出的本发明的具体实施例和比较实施例可以进一步清楚地了解本发明,但它们不是对本发明的限定。具体实施例和比较实施例中没有详细叙述的部分是采用现有技术、公知技术手段和行业标准获得的。
除非另有说明,本发明中所采用的百分数均为重量百分数。
实施例1
按如下的步骤方法制备蜜柚果粉口含片:
(1)制备脱苦蜜柚果粉:
去皮取肉步骤:将蜜柚鲜果分切成瓣鲜果,并成瓣鲜果的蜜柚果皮和蜜柚果肉分离,取其蜜柚果肉;
制备蜜柚原汁步骤:将蜜柚果肉进行破碎,使用200目过滤网进行过滤,取滤液得蜜柚原汁;
蜜柚原汁脱苦步骤:蜜柚原汁与离子交换树脂的重量比为6:1,室温下混合均匀,静置2分钟,将脱苦后的蜜柚原汁与离子交换树脂分离,制得脱苦蜜柚汁。
制粉步骤:将脱苦蜜柚汁在105℃下加热浓缩结晶,再将其研磨成粉末,并过100目筛,保证颗粒粒径小于0.15mm,制得脱苦蜜柚果粉。
(2)配方调配步骤:将下述重量份的组分原料:脱苦蜜柚果粉50份,麦芽糊精21份,白砂糖15份,一水柠檬酸0.2份,山梨酸钾0.03份,甘草0.2份,维生素C0.08份,经粉碎机粉碎后再过100目筛,保证颗粒度小于0.15mm;再混入14重量份的果葡糖浆搅拌均匀;
(3)制软材步骤:缓慢加入作为润湿剂的乙醇,混合均匀,调整原料湿度,制成软材;其中,乙醇的质量浓度会间接影响糖粉的混合均匀性,进而影响片剂成品的表面花点问题,较佳的,乙醇浓度控制在30-50%为宜;本实施例中乙醇的质量百分浓度为40%。
(4)造粒步骤:将所得软材过20目筛,在55℃条件下干燥1-3小时,干燥的终点为:软材的软硬度以手捏能成团(手感干脆、不粘手)、轻压则散为宜,使其含水量为2-4%,再过40目筛整粒;
(5)压片步骤:在颗粒中添加重量百分比1%的硬脂酸镁,送入压片机进行压片,制得蜜柚果粉口含片。
实施例2
该实施例的过程与实施例1基本相同,其区别在于:
①制备脱苦蜜柚果粉步骤中,在去皮取肉步骤之前增加清洗消毒的步骤:蜜柚鲜果于45℃热水中自动清洗2分钟,进入洁净水冷却漂洗,在浓度为100mg/L二氧化氯溶液中常温消毒以及吹干。
②配方调配和工艺参数的调整具体详见表1、表2。
实施例3
该实施例的过程与实施例1基本相同,配方调配和工艺参数的调整详见表1、表2。
比较例1
按如下的步骤方法制备柿子口含片。
(1)制备柿子浓缩浆:将新鲜成熟的柿果冲洗、沥干后迅速打浆,按柿浆量1-3mL/kg添加果胶酶、50-55℃酶解90-150min,静置澄清30-40min、过滤,60-80℃蒸发浓缩至可溶性固形物含量达到75%成柿子浓缩浆;
(2)制备中药浓缩浆:按重量比3:1:1:1:1取金银花、薄荷、竹叶、淡豆豉和牛蒡子,冷水浸泡40min、煎制50min,80℃蒸发,按体积6:1浓缩成中药浓缩浆;
(3)按质量比将柿子浓缩浆35%、中药浓缩浆16%、食用淀粉38%、甘露醇8%、蔗糖7%配料混合、制软材,混合充分的软材投入颗粒机中进行造粒,过20目筛,将湿颗粒放入干燥箱中干燥、温度控制在40-50℃,颗粒水分控制在3~5%;
(4)将1.5%的硬脂酸镁加入上述干燥好的颗粒中、混匀,颗粒放入压片机中压片、成型,制得柿子口含片。
比较例2
该实施例的过程与实施例1基本相同,配方调配和工艺参数的调整详见表1、表2。
比较例3
该实施例的过程与实施例1基本相同,配方调配和工艺参数的调整详见表1、表2。
比较例4
该实施例的过程与实施例1基本相同,配方调配和工艺参数的具体调整详见表1、表2。
表1配方调配
实施例1 | 实施例2 | 实施例3 | 比较例2 | 比较例3 | 比较例4 | |
脱苦蜜柚果粉 | 50 | 45 | 55 | 30 | 20 | 50 |
麦芽糊精 | 21 | 19 | 23 | 20 | 40 | 30 |
白砂糖 | 15 | 14 | 16 | 5 | 10 | 25 |
果葡糖浆 | 14 | 15 | 13 | 25 | 20 | 14 |
一水柠檬酸 | 0.2 | 0.3 | 0.4 | 2.2 | 0.2 | 0.2 |
甘草 | 0.2 | 0.1 | 0.3 | 0.3 | 1 | 0.2 |
维生素C | 0.08 | 0.06 | 0.1 | 0.08 | 0.08 | 0.08 |
山梨酸钾 | 0.03 | 0.02 | 0.04 | 0.03 | 0.03 | 0.03 |
表2工艺参数
表3给出了实施例1至3和比较例1至4制得的口含片的十人小组的感官评定结果;表4给出了实施例1至3和比较例1至4制得的口含片的性能指标,其中,柚皮苷含量采用《中国药典2005版》中的枳壳的柚皮苷含量的测定方法,硬度采用片剂四用测定仪测定。
表3十人小组感官评定结果
实施例1 | 实施例2 | 实施例3 | 比较例1 | 比较例2 | 比较例3 | 比较例4 | |
风味 | 柚香浓郁 | 柚香浓郁 | 柚香浓郁 | 柿子风味 | 柚香浓郁 | 柚香浓郁 | 柚香浓郁 |
酸甜度 | 酸甜适口 | 酸甜适口 | 酸甜适口 | 偏甜 | 过酸 | 过甜 | 涩味 |
口感 | 口感细腻 | 口感细腻 | 口感细腻 | 口感粗糙 | 口感粗糙 | 口感粗糙 | 口感细腻 |
质地 | 质地均匀 | 质地均匀 | 质地均匀 | 质地不均 | 质地均匀 | 质地不均 | 质地不均 |
表面花点 | 少,均匀 | 少,均匀 | 少,均匀 | 多,不均 | 少,均匀 | 多,不匀 | 多,不匀 |
崩解性 | 好 | 好 | 好 | 好 | 差 | 较好 | 较好 |
表4性能指标
实施例1 | 实施例2 | 实施例3 | 比较例1 | 比较例2 | 比较例3 | 比较例4 | |
柚皮苷含量 | 0.19% | 0.21% | 0.20% | — | 0.20% | 0.21% | 1.12% |
硬度kg/20片 | 8.3 | 8.1 | 8.2 | 6.4 | 6.9 | 6.3 | 6.5 |
含化时间/min | 20 | 18 | 20 | 10 | 15 | 11 | 12 |
以上所揭露的仅为本发明的优选实施例而已,当然不能以此来限定本发明之权利范围,因此依本发明申请专利范围所作的等同变化,仍属本发明所涵盖的范围。
Claims (9)
1.一种蜜柚果粉口含片,其特征在于:包括如下重量份的组分:脱苦蜜柚果粉45-55份,麦芽糊精19-23份,白砂糖14-16份,果葡糖浆13-15份,一水柠檬酸0.2-0.4份,山梨酸钾0.02-0.04份,甘草0.1-0.3份和维生素C0.06-0.1份。
2.根据权利要求1所述的蜜柚果粉口含片,其特征在于:由下述步骤制备得到:
A.制备脱苦蜜柚果粉;
B.配方调配步骤:将下述重量份的组分原料混合均匀:脱苦蜜柚果粉45-55份,麦芽糊精19-23份,白砂糖14-16份,果葡糖浆13-15份,一水柠檬酸0.2-0.4份,山梨酸钾0.02-0.04份,甘草0.1-0.3份和维生素C0.06-0.1份;
C.制软材步骤:将混合均匀的配方原料与食用乙醇混合,制得软材;
D.造粒步骤:将所得软材过16-24目筛进行制粒,并在45-65℃下烘干,使其水分含量小于5%,再过35-45目筛进行整粒;
E.压片步骤:送入压片机进行压片,制得蜜柚果粉口含片。
3.根据权利要求1或2所述的蜜柚果粉口含片,其特征在于:所述的脱苦蜜柚果粉由下述步骤制备得到:
A1.去皮取肉步骤:将蜜柚鲜果分切成瓣鲜果,并成瓣鲜果的蜜柚果皮和蜜柚果肉分离,取其蜜柚果肉;
A2.制备蜜柚原汁步骤:将蜜柚果肉进行破碎,过滤,取滤液得蜜柚原汁;
A3.蜜柚原汁脱苦步骤:通过离子交换树脂脱除蜜柚原汁中的苦味素,将脱苦后的蜜柚原汁与离子交换树脂分离,制得脱苦蜜柚汁;
A4.制粉步骤:将脱苦蜜柚汁浓缩结晶,研磨成粉,制得脱苦蜜柚果粉。
4.根据权利要求3所述的蜜柚果粉口含片,其特征在于:所述的蜜柚原汁脱苦步骤的工艺条件为:蜜柚原汁与离子交换树脂的重量比为6-10:1,室温下混匀静置2-10分钟。
5.一种制备蜜柚果粉口含片的方法,其特征在于:包括下列步骤:
A.制备脱苦蜜柚果粉;
B.配方调配步骤:将下述重量份的组分原料混合均匀:脱苦蜜柚果粉45-55份,麦芽糊精19-23份,白砂糖14-16份,果葡糖浆13-15份,一水柠檬酸0.2-0.4份,山梨酸钾0.02-0.04份,甘草0.1-0.3份和维生素C0.06-0.1份;
C.制软材步骤:将混合均匀的配方原料与食用乙醇混合,制得软材;
D.造粒步骤:将所得软材过16-24目筛进行制粒,并在45-65℃下烘干,使其水分含量小于5%,再过35-45目筛进行整粒;
E.压片步骤:送入压片机进行压片,制得蜜柚果粉口含片。
6.根据权利要求5所述的方法,其特征在于:制备脱苦蜜柚果粉的步骤包括:
A1.去皮取肉步骤:将蜜柚鲜果分切成瓣鲜果,并成瓣鲜果的蜜柚果皮和蜜柚果肉分离,取其蜜柚果肉;
A2.制备蜜柚原汁步骤:将蜜柚果肉进行破碎,过滤,取滤液得蜜柚原汁;
A3.蜜柚原汁脱苦步骤:通过离子交换树脂脱除蜜柚原汁中的苦味素,将脱苦后的蜜柚原汁与离子交换树脂分离,制得脱苦蜜柚汁;
A4.制粉步骤:将脱苦蜜柚汁浓缩结晶,研磨成粉,制得脱苦蜜柚果粉。
7.根据权利要求5或6所述的方法,其特征在于:在所述的去皮取肉步骤之前,增加清洗消毒步骤:采用浓度为10-500mg/L的二氧化氯水溶液对蜜柚鲜果进行清洗消毒。
8.根据权利要求6所述的方法,其特征在于:所述的蜜柚原汁脱苦步骤的工艺条件为:蜜柚原汁与离子交换树脂的重量比为6-10:1,室温下混匀静置2-10分钟。
9.根据权利要求5至8中任一项所述的方法,其特征在于:在所述的压片步骤中,在经造粒步骤后的颗粒中添加重量百分比1-2%的硬脂酸镁。
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