A kind of copper algae powder facial film and preparation method thereof
Technical field
The invention belongs to cosmetic field, particularly a kind of copper algae powder facial film and preparation method thereof.
Background technology
Facial film is a kind of facial cosmetics and skincare product that spreads on, utilization covers the blink of face, extraneous air and the pollution of temporary transient isolation, promote sweat gland secretion and metabolism, make the oxygen content of skin increase, be conducive to skin and get rid of the oil substances of the metabolic product of epidermis cell and accumulation, improve elasticity, pliability and the brightness of skin.The kind of facial film is a lot, and wherein seaweed mask, with the mineral composition of Sargassum extract, can be controlled oily Peppermint Extract, and moisture is provided, and calm tired, rough skin makes skin remain fine and smooth, glossy.But the moistening effect of plant seaweed mask of the prior art is not the most desirable, and use inconvenience, the shelf-life is short, expensive.
Sargassum phyllocystum Tseng et Lu,Sargassum horneri (Turn.) C. Ag. (Fucus horneri (Turn.)C.Ag.,Spongocarpus horneri Kutz.), claim again post capsule Alga Sgrgassi Enerves, grass madder, the alizarin dish of bamboo, that one is distributed in Japan, Korea S and north of China marine site, the normal common temperate zone Alga Sgrgassi Enerves that forms seaweed woods, can be at the beginning of annual winter end, spring amount reproduction, algae plant height can reach 7 meters, single-strain fresh weight is more than 3 kilograms, flourishing, swim in flakes the water surface.Due to Sargassum phyllocystum Tseng et Lu,Sargassum horneri (Turn.) C. Ag. (Fucus horneri (Turn.)C.Ag.,Spongocarpus horneri Kutz.) fast growth, Biomass is large, has caused Marine Biologist and Sargassum worker's concern.Spring, north Taiwan seashore often has Sargassum phyllocystum Tseng et Lu,Sargassum horneri (Turn.) C. Ag. (Fucus horneri (Turn.)C.Ag.,Spongocarpus horneri Kutz.) from marine site, temperate zone, to float, be deposited in bank and bay, 2013 because of ocean temperature lower, there is more Sargassum phyllocystum Tseng et Lu,Sargassum horneri (Turn.) C. Ag. (Fucus horneri (Turn.)C.Ag.,Spongocarpus horneri Kutz.) successfully to float to Taiwan, make Sargassum phyllocystum Tseng et Lu,Sargassum horneri (Turn.) C. Ag. (Fucus horneri (Turn.)C.Ag.,Spongocarpus horneri Kutz.) amount compared with being former years many, each scenic spot is all initiated the activity of clean beach a large amount of Sargassum phyllocystum Tseng et Lu,Sargassum horneri (Turn.) C. Ag. (Fucus horneri (Turn.)C.Ag.,Spongocarpus horneri Kutz.)s is picked up and destroyed by fire, has spent a large amount of energy and material resources.In recent years, along with progressively going deep into that Sargassum phyllocystum Tseng et Lu,Sargassum horneri (Turn.) C. Ag. (Fucus horneri (Turn.)C.Ag.,Spongocarpus horneri Kutz.) chemical composition is studied, its medical mechanism is also illustrated gradually, and the step of drug development is constantly accelerated.
Utilize Sargassum phyllocystum Tseng et Lu,Sargassum horneri (Turn.) C. Ag. (Fucus horneri (Turn.)C.Ag.,Spongocarpus horneri Kutz.) to prepare facial film for raw material, in existing document and report, record not yet to some extent.If people can constantly research and develop the effect of Sargassum phyllocystum Tseng et Lu,Sargassum horneri (Turn.) C. Ag. (Fucus horneri (Turn.)C.Ag.,Spongocarpus horneri Kutz.), utilize its characteristic, be developed to there is whitening, the facial film of the effect such as moisturizing, turn waste into wealth, it is fully utilized, in environmental improvement, also increased economic benefit, kill two birds with one stone.
Summary of the invention
The object of this invention is to provide a kind of copper algae powder facial film, this facial film can increase epiderm skin moisture, and moistening effect excellence also has the effect of whitening, antiinflammatory, reduce wrinkle, and uses simple, low price.
Another object of the present invention is to provide a kind of preparation method of above-mentioned copper algae powder facial film.
Object of the present invention can be achieved through the following technical solutions:
A kind of copper algae powder facial film, is characterized in that, comprises following percentage by weight and count the raw material of meter:
Sargassum phyllocystum Tseng et Lu,Sargassum horneri (Turn.) C. Ag. (Fucus horneri (Turn.)C.Ag.,Spongocarpus horneri Kutz.) powder 10-20%, wetting agent 6-13%, tackifier 1.5-3%, antioxidant 1-5%, metal ion chelation agent 2-15%, antiseptic 0.05-1%, brightening agent 1.5-5%, deodorizer 1-5%, sebum inhibitor 0.1-1%, keratin-lytic agent 1-5%, antibacterial 1-5%, anti-allergic agent 0.6-2.5%, nourishing additive agent 1.2-8%, surplus are deionized water.
The preparation method of described Sargassum phyllocystum Tseng et Lu,Sargassum horneri (Turn.) C. Ag. (Fucus horneri (Turn.)C.Ag.,Spongocarpus horneri Kutz.) powder is, by Sargassum phyllocystum Tseng et Lu,Sargassum horneri (Turn.) C. Ag. (Fucus horneri (Turn.)C.Ag.,Spongocarpus horneri Kutz.) remove impurity, washing, dry and become fragile to frond till, by dry Sargassum phyllocystum Tseng et Lu,Sargassum horneri (Turn.) C. Ag. (Fucus horneri (Turn.)C.Ag.,Spongocarpus horneri Kutz.) coarse pulverization to graininess; Then Sargassum phyllocystum Tseng et Lu,Sargassum horneri (Turn.) C. Ag. (Fucus horneri (Turn.)C.Ag.,Spongocarpus horneri Kutz.) grain regrinding is extremely Powdered, sieve, obtain Sargassum phyllocystum Tseng et Lu,Sargassum horneri (Turn.) C. Ag. (Fucus horneri (Turn.)C.Ag.,Spongocarpus horneri Kutz.) powder.
Described wetting agent is one or more the mixture in glycerol, amino acid humectant, propylene glycol, butanediol, hyaluronate sodium.Preferably, described wetting agent is the mixture of glycerol, amino acid humectant, propylene glycol, butanediol, hyaluronate sodium; The weight ratio of glycerol, amino acid humectant, propylene glycol, butanediol, hyaluronate sodium is 1:0.5-1:0.05-0.15:0.05-0.15:0.04-0.08.
Described tackifier is one or both the mixture in high molecular cellulose or HANSHENGJIAO.Preferably, described tackifier is the mixture of high molecular cellulose and HANSHENGJIAO, and the weight ratio of high molecular cellulose and HANSHENGJIAO is 3-4:1.
Described metal ion chelation agent is one or both the mixture in L-vitamin C or citric acid, and preferred described metal ion chelation agent is the mixture of L-vitamin C and citric acid, and wherein the weight ratio of L-vitamin C and citric acid is 1-3:1.
Described antiseptic is one or both the mixture in phenoxyethanol or Sang Pu K15.Preferably, described antiseptic is the mixture of phenoxyethanol and Sang Pu K15, and wherein, the volume ratio of phenoxyethanol and Sang Pu K15 is 1-2:1.
Described brightening agent is one or more the mixture in arbutin, nicotiamide or Trenaxmine.Preferably, described brightening agent is the mixture of arbutin, nicotiamide and Trenaxmine, and wherein, the weight ratio of arbutin, nicotiamide and Trenaxmine is 1:1-3:1.
Described anti-allergic agent is one or both the mixture in water solublity a-bisabolol or glycyrrhizic acid dipotassium.Preferably, described anti-allergic agent is the mixture of water solublity a-bisabolol and glycyrrhizic acid dipotassium, and wherein, the weight ratio of water solublity a-bisabolol and glycyrrhizic acid dipotassium is 2-6:1.
Described nourishing additive agent is one or more the mixture in ceramide, silk fibroin powder, collagen protein powder, avenabeta glucosan, polymerization almond protein, Argireline and Margarita hydrolyzed solution.
Described antioxidant is red wine polyphenols; Described deodorizer is trehalose; Described sebum inhibitor is vitamin B6; Described keratin-lytic agent is glycolic acid; Described antibacterial is azelaic acid.
The preparation method of above-mentioned copper algae powder facial film, its step comprises:
(1), by Sargassum phyllocystum Tseng et Lu,Sargassum horneri (Turn.) C. Ag. (Fucus horneri (Turn.)C.Ag.,Spongocarpus horneri Kutz.) remove impurity, washing, dry and become fragile to frond till, by dry Sargassum phyllocystum Tseng et Lu,Sargassum horneri (Turn.) C. Ag. (Fucus horneri (Turn.)C.Ag.,Spongocarpus horneri Kutz.) coarse pulverization to graininess; Then Sargassum phyllocystum Tseng et Lu,Sargassum horneri (Turn.) C. Ag. (Fucus horneri (Turn.)C.Ag.,Spongocarpus horneri Kutz.) grain regrinding is extremely Powdered, sieve, obtain Sargassum phyllocystum Tseng et Lu,Sargassum horneri (Turn.) C. Ag. (Fucus horneri (Turn.)C.Ag.,Spongocarpus horneri Kutz.) powder;
(2), according to formula, weigh good various raw materials;
(3), will in load weighted Sargassum phyllocystum Tseng et Lu,Sargassum horneri (Turn.) C. Ag. (Fucus horneri (Turn.)C.Ag.,Spongocarpus horneri Kutz.) powder, add deionized water and stirring swelling; Moisturizing, antioxidant, metal ion chelation agent, antiseptic, brightening agent, deodorizer, sebum inhibitor, keratin-lytic agent, antibacterial, anti-allergic agent, nourishing additive agent are dissolved in deionized water, then add and stir swelling good Sargassum phyllocystum Tseng et Lu,Sargassum horneri (Turn.) C. Ag. (Fucus horneri (Turn.)C.Ag.,Spongocarpus horneri Kutz.) mud continuation stirring, add while stirring tackifier and deionized water, after stirring, obtain copper algae powder facial film.
In described step (1), by Sargassum phyllocystum Tseng et Lu,Sargassum horneri (Turn.) C. Ag. (Fucus horneri (Turn.)C.Ag.,Spongocarpus horneri Kutz.) oven dry to the baking temperature becoming fragile, be 55-65 ℃.
In described step (1), Sargassum phyllocystum Tseng et Lu,Sargassum horneri (Turn.) C. Ag. (Fucus horneri (Turn.)C.Ag.,Spongocarpus horneri Kutz.) coarse pulverization is to the graininess that is less than 5mm, and then that Sargassum phyllocystum Tseng et Lu,Sargassum horneri (Turn.) C. Ag. (Fucus horneri (Turn.)C.Ag.,Spongocarpus horneri Kutz.) grain regrinding is extremely Powdered, 50 orders sieve.
Compared with prior art, beneficial effect of the present invention is:
1, the moisture retention of described copper algae powder facial film is good, and the skin moisture content rate of increase applying after 20 minutes through facial film face of the present invention is more than 25%, and can obviously improve the colour of skin, Glycerin, effectively prevents skin aging, reduces wrinkle.And adjuvant that this facial film adds is hydrophilic or water solublity, be easy to skin and absorb, with after can directly wash, easy to use.
2, the preparation method of described copper algae powder facial film is simple, easy to operate, and raw material is easy to get, cost is low, low price, and the medicine adding in preparation process does not only injure skin, and environmentally safe, green, environmental protection.
Accompanying drawing explanation
Fig. 1 is the skin lines comparison diagram that has applied the copper algae powder facial film front and back that make in embodiment 1.
The specific embodiment
Below in conjunction with embodiment, the invention will be further described:
Embodiment 1
(1) preparation of Sargassum phyllocystum Tseng et Lu,Sargassum horneri (Turn.) C. Ag. (Fucus horneri (Turn.)C.Ag.,Spongocarpus horneri Kutz.) powder
The Sargassum phyllocystum Tseng et Lu,Sargassum horneri (Turn.) C. Ag. (Fucus horneri (Turn.)C.Ag.,Spongocarpus horneri Kutz.) gathering is removed to assorted algae and other non-algae substances, and fresh water washes away salinity and sea mud, and distilled water is washed till electrical conductivity and drops to below 0.02MS; Till drying in the baking oven of 60 ℃ and becoming fragile to frond; Smash to pieces to the Sargassum phyllocystum Tseng et Lu,Sargassum horneri (Turn.) C. Ag. (Fucus horneri (Turn.)C.Ag.,Spongocarpus horneri Kutz.) algae grain that is shorter in length than 5mm with medicine bruisher; And then Sargassum phyllocystum Tseng et Lu,Sargassum horneri (Turn.) C. Ag. (Fucus horneri (Turn.)C.Ag.,Spongocarpus horneri Kutz.) algae grain is fully ground, obtain Sargassum phyllocystum Tseng et Lu,Sargassum horneri (Turn.) C. Ag. (Fucus horneri (Turn.)C.Ag.,Spongocarpus horneri Kutz.) powder with 50 order rustless steel sieve filtering screenings.
(2) preparation process of facial film
Get the Sargassum phyllocystum Tseng et Lu,Sargassum horneri (Turn.) C. Ag. (Fucus horneri (Turn.)C.Ag.,Spongocarpus horneri Kutz.) powder 10g in step (1), add the swelling stirring of 30mL deionized water, standby.
Following adjuvant is dissolved in the deionized water of 20mL:
Glycerol 5g, amino acid humectant 3g, propylene glycol 0.5g, butanediol 0.5g, hyaluronate sodium 0.3g(wherein, molecular weight 20-40 ten thousand, 90-120 ten thousand, the each 0.1g of 120-160 ten thousand), red wine polyphenols 1g, L-vitamin C1g, citric acid 2g, phenoxyethanol 0.025g, Sang Pu K15 is 0.025g, arbutin 0.5g, nicotiamide 1g, Trenaxmine 0.5g, trehalose 2g, vitamin B6 is 0.5g, glycolic acid 1g, azelaic acid 1g, water solublity a-bisabolol 0.5g, glycyrrhizic acid dipotassium 0.1g, ceramide 0.2g, silk fibroin powder 0.2g, collagen protein powder 0.2g, avenabeta glucosan 0.2g, polymerization almond protein 0.2g, Argireline 0.1g, Margarita hydrolyzed solution 0.2g.
Sargassum phyllocystum Tseng et Lu,Sargassum horneri (Turn.) C. Ag. (Fucus horneri (Turn.)C.Ag.,Spongocarpus horneri Kutz.) mud after swelling stirring is mixed homogeneously with above-mentioned adjuvant, add while stirring even mixed 1.4g high molecular cellulose and 0.4g HANSHENGJIAO, add to 100g total amount with deionized water, obtain copper algae powder facial film.
(3) testing result
For the moistening effect of the copper algae powder facial film for preparing in test implementation example 1, respectively by green tea powder facial film, lavandula angustifolia facial film in contrast.Wherein the preparation method of green tea powder facial film and lavandula angustifolia facial film, according to the formula preparation in the present embodiment 1, only replaces Sargassum phyllocystum Tseng et Lu,Sargassum horneri (Turn.) C. Ag. (Fucus horneri (Turn.)C.Ag.,Spongocarpus horneri Kutz.) powder by the green tea powder of equivalent and lavandula angustifolia powder (all purchased from Chhnang daily use chemicals, Guangdong), and other raw materials and addition thereof are all constant.
Before test: experimenter's arm of cleaning inner side, and with wet gauze (with deionized water) scrub, water temperature is room temperature, after cleaning, inside experimenter's both hands forearm, carries out measurement markers, within before tested position 2-3 days, can not use any cosmetic product; In test: use latex finger cot that test products and reference product are evenly applied in arm trial zone, smearing thickness is 2mm, carries out measurement and the observation of tested region and control zone after 20min, each region parallel assay five times according to the order of sequence, draw meansigma methods, shown in table 1 specific as follows:
Table 1 skin moisture content rate of increase
With 2,000,000 pixel CCD50X portable high-definition intelligent skin detection instrument (EH-800U) observation, applied the skin of the copper algae powder facial film in the present embodiment 1, as shown in Figure 1, wherein Fig. 1 a does not apply the skin observation figure of copper algae powder facial film, Fig. 1 b is the skin observation figure that has applied copper algae powder facial film, from comparative observation, figure shows, the facial film of preparing in the present embodiment all can improve the colour of skin, Glycerin, the moisture content of raising epiderm skin.
Embodiment 2
(1) preparation of Sargassum phyllocystum Tseng et Lu,Sargassum horneri (Turn.) C. Ag. (Fucus horneri (Turn.)C.Ag.,Spongocarpus horneri Kutz.) powder
The Sargassum phyllocystum Tseng et Lu,Sargassum horneri (Turn.) C. Ag. (Fucus horneri (Turn.)C.Ag.,Spongocarpus horneri Kutz.) gathering is removed to assorted algae and other non-algae substances, and fresh water washes away salinity and sea mud, and distilled water is washed till electrical conductivity and drops to below 0.02MS; Till drying in the baking oven of 60 ℃ and becoming fragile to frond; Smash to pieces to the Sargassum phyllocystum Tseng et Lu,Sargassum horneri (Turn.) C. Ag. (Fucus horneri (Turn.)C.Ag.,Spongocarpus horneri Kutz.) algae grain that is shorter in length than 5mm with medicine bruisher; And then Sargassum phyllocystum Tseng et Lu,Sargassum horneri (Turn.) C. Ag. (Fucus horneri (Turn.)C.Ag.,Spongocarpus horneri Kutz.) algae grain is fully ground, obtain Sargassum phyllocystum Tseng et Lu,Sargassum horneri (Turn.) C. Ag. (Fucus horneri (Turn.)C.Ag.,Spongocarpus horneri Kutz.) powder with 50 order rustless steel sieve filtering screenings.
(2) preparation process of facial film
Get the Sargassum phyllocystum Tseng et Lu,Sargassum horneri (Turn.) C. Ag. (Fucus horneri (Turn.)C.Ag.,Spongocarpus horneri Kutz.) powder 15g in step (1), add the swelling stirring of 30mL deionized water, standby.
Following adjuvant is dissolved in the deionized water of 20mL:
Glycerol 4g, amino acid humectant 4g, propylene glycol 0.5g, butanediol 0.5g, hyaluronate sodium 0.3g(wherein, molecular weight 20-40 ten thousand, 90-120 ten thousand, the each 0.1g of 120-160 ten thousand), red wine polyphenols 2g, L-vitamin C2g, citric acid 2g, phenoxyethanol 0.025g, Sang Pu K150.025g, arbutin 0.5g, nicotiamide 1g, Trenaxmine 0.5g, trehalose 1.5g, vitamin B6 0.5g, glycolic acid 1g, azelaic acid 1g, water solublity a-bisabolol 0.5g, glycyrrhizic acid dipotassium 0.1g, ceramide 0.2g, silk fibroin powder 0.2g, collagen protein powder 0.2g, avenabeta glucosan 0.2g, polymerization almond protein 0.2g, Argireline 0.1g, Margarita hydrolyzed solution 0.2g.
Sargassum phyllocystum Tseng et Lu,Sargassum horneri (Turn.) C. Ag. (Fucus horneri (Turn.)C.Ag.,Spongocarpus horneri Kutz.) mud after swelling stirring is mixed homogeneously with above-mentioned adjuvant, add while stirring even mixed 1.5g high molecular cellulose and 0.5g HANSHENGJIAO, add to 100g total amount with deionized water, obtain copper algae powder facial film.
(3) testing result
Method of testing is with embodiment 1, and concrete test result is as shown in table 2 below:
Table 2 skin moisture content rate of increase
In sum, use the moisture content that can obviously improve skin epidermis after copper algae powder facial film, improved the colour of skin, Glycerin.
The above is preferred embodiment of the present invention, but the present invention should not be confined to the disclosed content of this embodiment.So every, do not depart from the equivalence completing under spirit disclosed in this invention or revise, all falling into the scope of protection of the invention.