CN103689487A - Pomegranate bark and Chinese yam dispersible tablet and preparation method thereof - Google Patents
Pomegranate bark and Chinese yam dispersible tablet and preparation method thereof Download PDFInfo
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- 235000006536 Dioscorea esculenta Nutrition 0.000 title claims abstract description 61
- 240000001811 Dioscorea oppositifolia Species 0.000 title claims abstract description 61
- 235000003416 Dioscorea oppositifolia Nutrition 0.000 title claims abstract description 61
- 238000002360 preparation method Methods 0.000 title claims description 12
- 244000294611 Punica granatum Species 0.000 title abstract 4
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- 239000007919 dispersible tablet Substances 0.000 title abstract 3
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 claims abstract description 41
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- ZZZCUOFIHGPKAK-UHFFFAOYSA-N D-erythro-ascorbic acid Natural products OCC1OC(=O)C(O)=C1O ZZZCUOFIHGPKAK-UHFFFAOYSA-N 0.000 claims abstract description 15
- 229930003268 Vitamin C Natural products 0.000 claims abstract description 15
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- VYPSYNLAJGMNEJ-UHFFFAOYSA-N Silicium dioxide Chemical compound O=[Si]=O VYPSYNLAJGMNEJ-UHFFFAOYSA-N 0.000 claims abstract description 14
- FPIPGXGPPPQFEQ-UHFFFAOYSA-N 13-cis retinol Natural products OCC=C(C)C=CC=C(C)C=CC1=C(C)CCCC1(C)C FPIPGXGPPPQFEQ-UHFFFAOYSA-N 0.000 claims abstract description 13
- 229920002134 Carboxymethyl cellulose Polymers 0.000 claims abstract description 13
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- WHMDKBIGKVEYHS-IYEMJOQQSA-L Zinc gluconate Chemical compound [Zn+2].OC[C@@H](O)[C@@H](O)[C@H](O)[C@@H](O)C([O-])=O.OC[C@@H](O)[C@@H](O)[C@H](O)[C@@H](O)C([O-])=O WHMDKBIGKVEYHS-IYEMJOQQSA-L 0.000 claims abstract description 13
- FPIPGXGPPPQFEQ-OVSJKPMPSA-N all-trans-retinol Chemical compound OC\C=C(/C)\C=C\C=C(/C)\C=C\C1=C(C)CCCC1(C)C FPIPGXGPPPQFEQ-OVSJKPMPSA-N 0.000 claims abstract description 13
- 235000010948 carboxy methyl cellulose Nutrition 0.000 claims abstract description 13
- 150000004676 glycans Chemical class 0.000 claims abstract description 13
- 235000020717 hawthorn extract Nutrition 0.000 claims abstract description 13
- 235000019813 microcrystalline cellulose Nutrition 0.000 claims abstract description 13
- 229920001282 polysaccharide Polymers 0.000 claims abstract description 13
- 239000005017 polysaccharide Substances 0.000 claims abstract description 13
- 239000011734 sodium Substances 0.000 claims abstract description 13
- 229910052708 sodium Inorganic materials 0.000 claims abstract description 13
- 235000019698 starch Nutrition 0.000 claims abstract description 13
- 235000019408 sucralose Nutrition 0.000 claims abstract description 13
- 235000019155 vitamin A Nutrition 0.000 claims abstract description 13
- 239000011719 vitamin A Substances 0.000 claims abstract description 13
- 229940045997 vitamin a Drugs 0.000 claims abstract description 13
- 235000011478 zinc gluconate Nutrition 0.000 claims abstract description 13
- 239000011670 zinc gluconate Substances 0.000 claims abstract description 13
- 229960000306 zinc gluconate Drugs 0.000 claims abstract description 13
- 239000004376 Sucralose Substances 0.000 claims abstract description 8
- 239000001768 carboxy methyl cellulose Substances 0.000 claims abstract description 8
- 239000008112 carboxymethyl-cellulose Substances 0.000 claims abstract description 8
- RQFQJYYMBWVMQG-IXDPLRRUSA-N chitotriose Chemical compound O[C@@H]1[C@@H](N)[C@H](O)O[C@H](CO)[C@H]1O[C@H]1[C@H](N)[C@@H](O)[C@H](O[C@H]2[C@@H]([C@@H](O)[C@H](O)[C@@H](CO)O2)N)[C@@H](CO)O1 RQFQJYYMBWVMQG-IXDPLRRUSA-N 0.000 claims abstract description 8
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- 229940016286 microcrystalline cellulose Drugs 0.000 claims abstract description 8
- 239000008107 starch Substances 0.000 claims abstract description 8
- BAQAVOSOZGMPRM-QBMZZYIRSA-N sucralose Chemical compound O[C@@H]1[C@@H](O)[C@@H](Cl)[C@@H](CO)O[C@@H]1O[C@@]1(CCl)[C@@H](O)[C@H](O)[C@@H](CCl)O1 BAQAVOSOZGMPRM-QBMZZYIRSA-N 0.000 claims abstract description 8
- 239000002994 raw material Substances 0.000 claims description 21
- 239000000203 mixture Substances 0.000 claims description 17
- 238000004108 freeze drying Methods 0.000 claims description 14
- 235000009508 confectionery Nutrition 0.000 claims description 12
- 239000000741 silica gel Substances 0.000 claims description 12
- 229910002027 silica gel Inorganic materials 0.000 claims description 12
- 238000002156 mixing Methods 0.000 claims description 10
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- 241001570521 Lonicera periclymenum Species 0.000 claims description 9
- RZVAJINKPMORJF-UHFFFAOYSA-N Acetaminophen Chemical compound CC(=O)NC1=CC=C(O)C=C1 RZVAJINKPMORJF-UHFFFAOYSA-N 0.000 claims description 7
- 108010073178 Glucan 1,4-alpha-Glucosidase Proteins 0.000 claims description 7
- 239000007864 aqueous solution Substances 0.000 claims description 7
- 238000009835 boiling Methods 0.000 claims description 7
- 239000000706 filtrate Substances 0.000 claims description 7
- 238000001914 filtration Methods 0.000 claims description 7
- 238000002791 soaking Methods 0.000 claims description 7
- 239000007787 solid Substances 0.000 claims description 7
- PTHCMJGKKRQCBF-UHFFFAOYSA-N Cellulose, microcrystalline Chemical compound OC1C(O)C(OC)OC(CO)C1OC1C(O)C(O)C(OC)C(CO)O1 PTHCMJGKKRQCBF-UHFFFAOYSA-N 0.000 claims description 5
- 229920001661 Chitosan Polymers 0.000 claims description 5
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- 235000004879 dioscorea Nutrition 0.000 claims description 5
- 238000001035 drying Methods 0.000 claims description 5
- 238000005469 granulation Methods 0.000 claims description 5
- 230000003179 granulation Effects 0.000 claims description 5
- 239000012535 impurity Substances 0.000 claims description 5
- 229920001542 oligosaccharide Polymers 0.000 claims description 5
- 150000002482 oligosaccharides Chemical class 0.000 claims description 5
- 238000011084 recovery Methods 0.000 claims description 5
- 239000000126 substance Substances 0.000 claims description 5
- 238000001291 vacuum drying Methods 0.000 claims description 5
- 229930003231 vitamin Natural products 0.000 claims description 5
- 235000013343 vitamin Nutrition 0.000 claims description 5
- 239000011782 vitamin Substances 0.000 claims description 5
- 229940088594 vitamin Drugs 0.000 claims description 5
- 150000003722 vitamin derivatives Chemical class 0.000 claims description 5
- 206010012735 Diarrhoea Diseases 0.000 abstract description 7
- 210000000952 spleen Anatomy 0.000 abstract description 3
- HQKMJHAJHXVSDF-UHFFFAOYSA-L magnesium stearate Chemical compound [Mg+2].CCCCCCCCCCCCCCCCCC([O-])=O.CCCCCCCCCCCCCCCCCC([O-])=O HQKMJHAJHXVSDF-UHFFFAOYSA-L 0.000 abstract 2
- 241000205585 Aquilegia canadensis Species 0.000 abstract 1
- FBPFZTCFMRRESA-KVTDHHQDSA-N D-Mannitol Chemical compound OC[C@@H](O)[C@@H](O)[C@H](O)[C@H](O)CO FBPFZTCFMRRESA-KVTDHHQDSA-N 0.000 abstract 1
- 208000019637 Infantile Diarrhea Diseases 0.000 abstract 1
- 229930195725 Mannitol Natural products 0.000 abstract 1
- 235000019441 ethanol Nutrition 0.000 abstract 1
- 235000019359 magnesium stearate Nutrition 0.000 abstract 1
- 239000000594 mannitol Substances 0.000 abstract 1
- 235000010355 mannitol Nutrition 0.000 abstract 1
- 239000000377 silicon dioxide Substances 0.000 abstract 1
- 208000037265 diseases, disorders, signs and symptoms Diseases 0.000 description 6
- 201000010099 disease Diseases 0.000 description 5
- 241000894006 Bacteria Species 0.000 description 2
- 235000005911 diet Nutrition 0.000 description 2
- 230000000378 dietary effect Effects 0.000 description 2
- 238000005516 engineering process Methods 0.000 description 2
- 239000000047 product Substances 0.000 description 2
- 206010000087 Abdominal pain upper Diseases 0.000 description 1
- 241000589875 Campylobacter jejuni Species 0.000 description 1
- 241000305071 Enterobacterales Species 0.000 description 1
- 241000709661 Enterovirus Species 0.000 description 1
- 241000588724 Escherichia coli Species 0.000 description 1
- 241000233866 Fungi Species 0.000 description 1
- 241000617996 Human rotavirus Species 0.000 description 1
- 206010020751 Hypersensitivity Diseases 0.000 description 1
- 241000293869 Salmonella enterica subsp. enterica serovar Typhimurium Species 0.000 description 1
- 241000700605 Viruses Species 0.000 description 1
- 206010047700 Vomiting Diseases 0.000 description 1
- 241000607447 Yersinia enterocolitica Species 0.000 description 1
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- 239000003242 anti bacterial agent Substances 0.000 description 1
- 229940088710 antibiotic agent Drugs 0.000 description 1
- 230000009286 beneficial effect Effects 0.000 description 1
- 230000013872 defecation Effects 0.000 description 1
- 239000003814 drug Substances 0.000 description 1
- 239000003792 electrolyte Substances 0.000 description 1
- 230000000369 enteropathogenic effect Effects 0.000 description 1
- 230000000688 enterotoxigenic effect Effects 0.000 description 1
- 235000013402 health food Nutrition 0.000 description 1
- 238000010438 heat treatment Methods 0.000 description 1
- 230000007774 longterm Effects 0.000 description 1
- 235000016709 nutrition Nutrition 0.000 description 1
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- 208000024891 symptom Diseases 0.000 description 1
- 229940126672 traditional medicines Drugs 0.000 description 1
- 230000008673 vomiting Effects 0.000 description 1
- 229940098232 yersinia enterocolitica Drugs 0.000 description 1
Classifications
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23L—FOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
- A23L33/00—Modifying nutritive qualities of foods; Dietetic products; Preparation or treatment thereof
- A23L33/10—Modifying nutritive qualities of foods; Dietetic products; Preparation or treatment thereof using additives
- A23L33/105—Plant extracts, their artificial duplicates or their derivatives
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23L—FOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
- A23L19/00—Products from fruits or vegetables; Preparation or treatment thereof
- A23L19/09—Mashed or comminuted products, e.g. pulp, purée, sauce, or products made therefrom, e.g. snacks
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23L—FOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
- A23L19/00—Products from fruits or vegetables; Preparation or treatment thereof
- A23L19/10—Products from fruits or vegetables; Preparation or treatment thereof of tuberous or like starch containing root crops
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23L—FOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
- A23L29/00—Foods or foodstuffs containing additives; Preparation or treatment thereof
- A23L29/30—Foods or foodstuffs containing additives; Preparation or treatment thereof containing carbohydrate syrups; containing sugars; containing sugar alcohols, e.g. xylitol; containing starch hydrolysates, e.g. dextrin
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23L—FOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
- A23L33/00—Modifying nutritive qualities of foods; Dietetic products; Preparation or treatment thereof
- A23L33/10—Modifying nutritive qualities of foods; Dietetic products; Preparation or treatment thereof using additives
- A23L33/15—Vitamins
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- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23L—FOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
- A23L33/00—Modifying nutritive qualities of foods; Dietetic products; Preparation or treatment thereof
- A23L33/10—Modifying nutritive qualities of foods; Dietetic products; Preparation or treatment thereof using additives
- A23L33/16—Inorganic salts, minerals or trace elements
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23L—FOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
- A23L33/00—Modifying nutritive qualities of foods; Dietetic products; Preparation or treatment thereof
- A23L33/20—Reducing nutritive value; Dietetic products with reduced nutritive value
- A23L33/21—Addition of substantially indigestible substances, e.g. dietary fibres
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23V—INDEXING SCHEME RELATING TO FOODS, FOODSTUFFS OR NON-ALCOHOLIC BEVERAGES AND LACTIC OR PROPIONIC ACID BACTERIA USED IN FOODSTUFFS OR FOOD PREPARATION
- A23V2002/00—Food compositions, function of food ingredients or processes for food or foodstuffs
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- Life Sciences & Earth Sciences (AREA)
- Chemical & Material Sciences (AREA)
- Health & Medical Sciences (AREA)
- Food Science & Technology (AREA)
- Nutrition Science (AREA)
- Engineering & Computer Science (AREA)
- Polymers & Plastics (AREA)
- Mycology (AREA)
- Botany (AREA)
- Molecular Biology (AREA)
- Inorganic Chemistry (AREA)
- Medicinal Preparation (AREA)
- Medicines Containing Plant Substances (AREA)
Abstract
The invention discloses a pomegranate bark and Chinese yam dispersible tablet which comprises the following components in parts by weight: 100-300 parts of pomegranate bark, 100-300 parts of Chinese yam, 80-120 parts of honeysuckle, 1.75-3.75 parts of vitamin C, 0.01-0.02 part of vitamin A, 0.15-0.35 part of zinc gluconate, 40-60 parts of microcrystalline cellulose, 0.12-0.32 part of hawthorn extract, 0.12-0.32 part of American ginseng extract, 100-170 parts of mannitol, 1.2-3.2 parts of chitosan oligosaccharide, 1.2-3.2 parts of crude polysaccharide, 10-15 parts of sucralose, 10-50 parts of superfine silica powder, 3-5 parts of carboxymethyl cellulose, 55-80 parts of sodium carboxymethyl starch, 4-6 parts of magnesium stearate, appropriate amount of purified water, and an appropriate amount of 75% ethyl alcohol. The pomegranate bark and Chinese yam dispersible tablet has the effects of tonifying spleen and checking diarrhea and is suitable for infantile diarrhea.
Description
Technical field
The invention belongs to nutritional health food field, be specially a kind of granatum Chinese yam dispersing tablet and preparation method.
Background technology
Baby diarrhea be many cause of diseases, multifactor cause take diarrhoea as one group of main disease.Main feature is that times of defecation increases and proterties changes, can be with the symptoms such as heating, vomiting, stomachache and water, electrolyte, disturbance of acid-base balance in various degree.Cause of disease can be by virus, bacterium, is mainly human rotavirus and other enteroviruses, enteropathogenic E．Coli, enterotoxigenic E．Coli, Enterohemorrhagic E.coli, aggressive is large
Parasite, the fungies etc. such as enterobacteria and salmonella typhimurium, campylobacter jejuni, yersinia enterocolitica, golden Portugal bacterium cause.Enteron aisle infects outward, enteric flora disturbance, allergy, improper feeding and climatic factor due to abuse of antibiotics also can be caused a disease.It is the common disease of 2 years old Infants Below.Although also have Chinese Traditional Medicines or the formula of a lot of baby diarrhea diseases at present, although treatment prescribed preparation is a lot, be all the form appearance with medicine, be applicable to the dietary product of long-term edible auxiliary curing seldom.Therefore the dietary product of researching and developing a kind of safe auxiliary curing is very with practical value.
Summary of the invention
For above-mentioned situation, technical problem solved by the invention is to provide a kind of granatum Chinese yam dispersing tablet and preparation method of invigorating the spleen to arrest diarrhea, to solve the problem proposing in above-mentioned background technology.
For achieving the above object, the invention provides following technical scheme:
A kind of granatum Chinese yam dispersing tablet, comprise following weight portion composition: red granatum 100-300 part, Chinese yam 100-300 part, honeysuckle 80-120 part, vitamin C 1.75-3.75 part, vitamin A 0.01-0.02 part, zinc gluconate 0.15-0.35 part, microcrystalline cellulose 40-60 part, haw thorn extract 0.12-0.32 part, American ginseng extract 0.12-0.32 part, sweet mellow wine 100-170 part, chitosan oligosaccharide 1.2-3.2 part, thick polysaccharide 1.2-3.2 part, Sucralose 10-15 part, superfine silica gel powder 10-50 part, carboxymethyl cellulose 3-5 part, sodium carboxymethyl starch 55-80 part, dolomol 4-6 part, purified water is appropriate, 75% concentration ethanol is appropriate.
As preferably, described a kind of granatum Chinese yam dispersing tablet, comprise following weight portion composition: 200 parts of red granatums, 200 parts of Chinese yams, 100 parts of honeysuckles, 2.75 parts of vitamin Cs, 0.015 part of vitamin A, 0.25 part of zinc gluconate, 50 parts of microcrystalline celluloses, 0.22 part of haw thorn extract, 0.22 part of American ginseng extract, 135 parts, sweet mellow wine, 2.2 parts of chitosan oligosaccharides, 2.2 parts of thick polysaccharide, 12.5 parts of Sucraloses, 30 parts of superfine silica gel powders, 4 parts of carboxymethyl celluloses, 67.5 parts of sodium carboxymethyl starches, 5 parts of dolomols, purified water is appropriate, 75% concentration ethanol is appropriate.
A preparation method for granatum Chinese yam dispersing tablet, comprises the following steps:
(1) get after fresh Chinese yam is cleaned and soak 15-20min in 0.1% the vitamin C aqueous solution, Chinese yam after soaking is put into and in freeze drier, carries out freeze drying, first open refrigerator and freeze, be chilled to raw material Chinese yam temperature within the scope of-20 to-30 ℃, and maintain 8-10h and be dried, then open vacuum, and be heated to 95-100 ℃, and continue dry 1-3h, the resulting solid matter of above-mentioned freeze drying is pulverized, make Chinese yam freeze-dried powder, standby;
(2) getting the red granatum of raw material, honeysuckle cleans, add the 4-5 of above-mentioned raw materials gross weight doubly to measure purified water and decoct 2-2.5h within the scope of 90-100 ℃, filter, the dregs of a decoction after filtering are added to the purified water that 2-4 doubly measures and within the scope of 90-100 ℃, decoct 1-1.5h, filter, filter residue is discharged, merge filtrate twice, and be concentrated into the gamma amylase that adds 1-2 ‰ when proportion is 1-1.5, within the scope of 35-45 ℃, be incubated 5-10h, after finally boiling 25-35min, filter, obtain mixed extract, standby;
(3) gained mixed extract in step (1) gained Chinese yam freeze-dried powder and step (2) is uniformly mixed, mixer speed is 50-75r/min, and the time is 10-15min, obtains mixture I, standby;
(4) to the middle gained mixture I of step (3), add ethanol to make determining alcohol reach 75%, after standing 8-16h, filter, impurity is discharged, after recovery ethanol, at temperature 40-60 ℃, under vacuum 0.58-0.68MPa condition, Vacuum Concentration to dry substance reaches 50-70%, carry out again vacuum drying, within the scope of baking temperature 40-60 ℃, obtain dry extract, standby;
(5) after being pulverized, step (4) gained dry extract add vitamin C, vitamin A, zinc gluconate, carboxymethyl cellulose, microcrystalline cellulose, haw thorn extract, American ginseng extract, sweet mellow wine, chitosan oligosaccharide, thick polysaccharide, Sucralose, superfine silica gel powder to mix granulation with mixing machine, rotating speed is 10-15r/min, time is 6-8min, by the particle after mixing 50-60 ℃ of scope inner drying to water content between 1-3%, standby;
(6) to the middle gained particle of step (5), add sodium carboxymethyl starch, dolomol to mix, compacting in flakes, obtains granatum Chinese yam dispersing tablet.
In described step (1), get after fresh Chinese yam is cleaned and soak 20min in 0.1% the vitamin C aqueous solution, Chinese yam after soaking is put into and in freeze drier, carries out freeze drying, first opening refrigerator freezes, while being chilled to raw material Chinese yam temperature for-26 ℃, maintain 8h dry, then open vacuum, and continue dry 2.5h while being heated to 95 ℃, and the resulting solid matter of above-mentioned freeze drying is pulverized, make Chinese yam freeze-dried powder.
In described step (2), getting the red granatum of raw material, honeysuckle cleans, add 6 times of amount purified water of above-mentioned raw materials gross weight to decoct 2h under 90 ℃ of conditions, filter, the purified water that the dregs of a decoction after filtering is added to 3 times of amounts decocts 1.5h under 90 ℃ of conditions, filters, filter residue is discharged, merge filtrate twice, and to be concentrated into proportion be to add 2 ‰ gamma amylase at 1 o'clock, under 45 ℃ of conditions, be incubated 6h, after finally boiling 35min, filter, obtain mixed extract.
In sum, beneficial effect of the present invention:
The present invention has invigorating the spleen to arrest diarrhea, is applicable to baby diarrhea.
The specific embodiment
Below in conjunction with the embodiment of the present invention, gained technical scheme in the embodiment of the present invention is clearly and completely described, obviously, described embodiment is only the present invention's part embodiment, rather than whole embodiment.Based on gained embodiment in the present invention, those of ordinary skills, not making the every other embodiment obtaining under creative work prerequisite, belong to the scope of protection of the invention.
Embodiment 1
A granatum Chinese yam dispersing tablet, comprises following weight portion composition: 100 parts of red granatums, 100 parts of Chinese yams, 80 parts of honeysuckles, 1.75 parts of vitamin Cs, 0.01 part of vitamin A, zinc gluconate 0.15-0.35 part, 40 parts of microcrystalline celluloses, 0.12 part of haw thorn extract, 0.12 part of American ginseng extract, 100 parts, sweet mellow wine, 1.2 parts of chitosan oligosaccharides, 1.2 parts of thick polysaccharide, 10 parts of Sucraloses, 10 parts of superfine silica gel powders, 3 parts of carboxymethyl celluloses, 55 parts of sodium carboxymethyl starches, 4 parts of dolomols, purified water is appropriate, 75% concentration ethanol is appropriate.
A preparation method for granatum Chinese yam dispersing tablet, comprises the following steps:
(1) get after fresh Chinese yam is cleaned and soak 15-20min in 0.1% the vitamin C aqueous solution, Chinese yam after soaking is put into and in freeze drier, carries out freeze drying, first open refrigerator and freeze, be chilled to raw material Chinese yam temperature within the scope of-20 to-30 ℃, and maintain 8-10h and be dried, then open vacuum, and be heated to 95-100 ℃, and continue dry 1-3h, the resulting solid matter of above-mentioned freeze drying is pulverized, make Chinese yam freeze-dried powder, standby;
(2) getting the red granatum of raw material, honeysuckle cleans, add the 4-5 of above-mentioned raw materials gross weight doubly to measure purified water and decoct 2-2.5h within the scope of 90-100 ℃, filter, the dregs of a decoction after filtering are added to the purified water that 2-4 doubly measures and within the scope of 90-100 ℃, decoct 1-1.5h, filter, filter residue is discharged, merge filtrate twice, and be concentrated into the gamma amylase that adds 1-2 ‰ when proportion is 1-1.5, within the scope of 35-45 ℃, be incubated 5-10h, after finally boiling 25-35min, filter, obtain mixed extract, standby;
(3) gained mixed extract in step (1) gained Chinese yam freeze-dried powder and step (2) is uniformly mixed, mixer speed is 50-75r/min, and the time is 10-15min, obtains mixture I, standby;
(4) to the middle gained mixture I of step (3), add ethanol to make determining alcohol reach 75%, after standing 8-16h, filter, impurity is discharged, after recovery ethanol, at temperature 40-60 ℃, under vacuum 0.58-0.68MPa condition, Vacuum Concentration to dry substance reaches 50-70%, carry out again vacuum drying, within the scope of baking temperature 40-60 ℃, obtain dry extract, standby;
(5) after being pulverized, step (4) gained dry extract add vitamin C, vitamin A, zinc gluconate, carboxymethyl cellulose, microcrystalline cellulose, haw thorn extract, American ginseng extract, sweet mellow wine, chitosan oligosaccharide, thick polysaccharide, Sucralose, superfine silica gel powder to mix granulation with mixing machine, rotating speed is 10-15r/min, time is 6-8min, by the particle after mixing 50-60 ℃ of scope inner drying to water content between 1-3%, standby;
(6) to the middle gained particle of step (5), add sodium carboxymethyl starch, dolomol to mix, compacting in flakes, obtains granatum Chinese yam dispersing tablet.
Embodiment 2
A granatum Chinese yam dispersing tablet, comprises following weight portion composition: 200 parts of red granatums, 200 parts of Chinese yams, 100 parts of honeysuckles, 2.75 parts of vitamin Cs, 0.015 part of vitamin A, 0.25 part of zinc gluconate, 50 parts of microcrystalline celluloses, 0.22 part of haw thorn extract, 0.22 part of American ginseng extract, 135 parts, sweet mellow wine, 2.2 parts of chitosan oligosaccharides, 2.2 parts of thick polysaccharide, 12.5 parts of Sucraloses, 30 parts of superfine silica gel powders, 4 parts of carboxymethyl celluloses, 67.5 parts of sodium carboxymethyl starches, 5 parts of dolomols, purified water is appropriate, 75% concentration ethanol is appropriate.
A preparation method for granatum Chinese yam dispersing tablet, comprises the following steps:
(1) get after fresh Chinese yam is cleaned and soak 15-20min in 0.1% the vitamin C aqueous solution, Chinese yam after soaking is put into and in freeze drier, carries out freeze drying, first open refrigerator and freeze, be chilled to raw material Chinese yam temperature within the scope of-20 to-30 ℃, and maintain 8-10h and be dried, then open vacuum, and be heated to 95-100 ℃, and continue dry 1-3h, the resulting solid matter of above-mentioned freeze drying is pulverized, make Chinese yam freeze-dried powder, standby;
(2) getting the red granatum of raw material, honeysuckle cleans, add the 4-5 of above-mentioned raw materials gross weight doubly to measure purified water and decoct 2-2.5h within the scope of 90-100 ℃, filter, the dregs of a decoction after filtering are added to the purified water that 2-4 doubly measures and within the scope of 90-100 ℃, decoct 1-1.5h, filter, filter residue is discharged, merge filtrate twice, and be concentrated into the gamma amylase that adds 1-2 ‰ when proportion is 1-1.5, within the scope of 35-45 ℃, be incubated 5-10h, after finally boiling 25-35min, filter, obtain mixed extract, standby;
(3) gained mixed extract in step (1) gained Chinese yam freeze-dried powder and step (2) is uniformly mixed, mixer speed is 50-75r/min, and the time is 10-15min, obtains mixture I, standby;
(4) to the middle gained mixture I of step (3), add ethanol to make determining alcohol reach 75%, after standing 8-16h, filter, impurity is discharged, after recovery ethanol, at temperature 40-60 ℃, under vacuum 0.58-0.68MPa condition, Vacuum Concentration to dry substance reaches 50-70%, carry out again vacuum drying, within the scope of baking temperature 40-60 ℃, obtain dry extract, standby;
(5) after being pulverized, step (4) gained dry extract add vitamin C, vitamin A, zinc gluconate, carboxymethyl cellulose, microcrystalline cellulose, haw thorn extract, American ginseng extract, sweet mellow wine, chitosan oligosaccharide, thick polysaccharide, Sucralose, superfine silica gel powder to mix granulation with mixing machine, rotating speed is 10-15r/min, time is 6-8min, by the particle after mixing 50-60 ℃ of scope inner drying to water content between 1-3%, standby;
(6) to the middle gained particle of step (5), add sodium carboxymethyl starch, dolomol to mix, compacting in flakes, obtains granatum Chinese yam dispersing tablet.
Embodiment 3
A granatum Chinese yam dispersing tablet, comprises following weight portion composition: 300 parts of red granatums, 300 parts of Chinese yams, 120 parts of honeysuckles, 3.75 parts of vitamin Cs, 0.02 part of vitamin A, 0.35 part of zinc gluconate, 60 parts of microcrystalline celluloses, 0.32 part of haw thorn extract, 0.32 part of American ginseng extract, 170 parts, sweet mellow wine, 3.2 parts of chitosan oligosaccharides, 3.2 parts of thick polysaccharide, 15 parts of Sucraloses, 50 parts of superfine silica gel powders, 5 parts of carboxymethyl celluloses, 80 parts of sodium carboxymethyl starches, 6 parts of dolomols, purified water is appropriate, 75% concentration ethanol is appropriate.
A preparation method for granatum Chinese yam dispersing tablet, comprises the following steps:
(1) get after fresh Chinese yam is cleaned and soak 15-20min in 0.1% the vitamin C aqueous solution, Chinese yam after soaking is put into and in freeze drier, carries out freeze drying, first open refrigerator and freeze, be chilled to raw material Chinese yam temperature within the scope of-20 to-30 ℃, and maintain 8-10h and be dried, then open vacuum, and be heated to 95-100 ℃, and continue dry 1-3h, the resulting solid matter of above-mentioned freeze drying is pulverized, make Chinese yam freeze-dried powder, standby;
(2) getting the red granatum of raw material, honeysuckle cleans, add the 4-5 of above-mentioned raw materials gross weight doubly to measure purified water and decoct 2-2.5h within the scope of 90-100 ℃, filter, the dregs of a decoction after filtering are added to the purified water that 2-4 doubly measures and within the scope of 90-100 ℃, decoct 1-1.5h, filter, filter residue is discharged, merge filtrate twice, and be concentrated into the gamma amylase that adds 1-2 ‰ when proportion is 1-1.5, within the scope of 35-45 ℃, be incubated 5-10h, after finally boiling 25-35min, filter, obtain mixed extract, standby;
(3) gained mixed extract in step (1) gained Chinese yam freeze-dried powder and step (2) is uniformly mixed, mixer speed is 50-75r/min, and the time is 10-15min, obtains mixture I, standby;
(4) to the middle gained mixture I of step (3), add ethanol to make determining alcohol reach 75%, after standing 8-16h, filter, impurity is discharged, after recovery ethanol, at temperature 40-60 ℃, under vacuum 0.58-0.68MPa condition, Vacuum Concentration to dry substance reaches 50-70%, carry out again vacuum drying, within the scope of baking temperature 40-60 ℃, obtain dry extract, standby;
(5) after being pulverized, step (4) gained dry extract add vitamin C, vitamin A, zinc gluconate, carboxymethyl cellulose, microcrystalline cellulose, haw thorn extract, American ginseng extract, sweet mellow wine, chitosan oligosaccharide, thick polysaccharide, Sucralose, superfine silica gel powder to mix granulation with mixing machine, rotating speed is 10-15r/min, time is 6-8min, by the particle after mixing 50-60 ℃ of scope inner drying to water content between 1-3%, standby;
(6) to the middle gained particle of step (5), add sodium carboxymethyl starch, dolomol to mix, compacting in flakes, obtains granatum Chinese yam dispersing tablet.
To those skilled in the art, obviously the invention is not restricted to the details of above-mentioned one exemplary embodiment, and in the situation that not deviating from spirit of the present invention or essential characteristic, can realize the present invention with other concrete form.Therefore, no matter from which point, all should regard embodiment as exemplary, and be nonrestrictive, scope of the present invention is limited by claims rather than above-mentioned explanation, is therefore intended to include in the present invention dropping on the implication that is equal to important document of claim and all changes in scope.
In addition, be to be understood that, although this description is described according to embodiment, but not each embodiment only comprises an independently technical scheme, this narrating mode of description is only for clarity sake, those skilled in the art should make description as a whole, and in each embodiment, gained technical scheme also can, through appropriately combined, form other embodiments that it will be appreciated by those skilled in the art that.
Claims (5)
1. a granatum Chinese yam dispersing tablet, it is characterized in that: comprise following weight portion composition: red granatum 100-300 part, Chinese yam 100-300 part, honeysuckle 80-120 part, vitamin C 1.75-3.75 part, vitamin A 0.01-0.02 part, zinc gluconate 0.15-0.35 part, microcrystalline cellulose 40-60 part, haw thorn extract 0.12-0.32 part, American ginseng extract 0.12-0.32 part, sweet mellow wine 100-170 part, chitosan oligosaccharide 1.2-3.2 part, thick polysaccharide 1.2-3.2 part, Sucralose 10-15 part, superfine silica gel powder 10-50 part, carboxymethyl cellulose 3-5 part, sodium carboxymethyl starch 55-80 part, dolomol 4-6 part, purified water is appropriate, 75% concentration ethanol is appropriate.
2. a kind of granatum Chinese yam dispersing tablet according to claim 1, it is characterized in that: comprise following weight portion composition: 200 parts of red granatums, 200 parts of Chinese yams, 100 parts of honeysuckles, 2.75 parts of vitamin Cs, 0.015 part of vitamin A, 0.25 part of zinc gluconate, 50 parts of microcrystalline celluloses, 0.22 part of haw thorn extract, 0.22 part of American ginseng extract, 135 parts, sweet mellow wine, 2.2 parts of chitosan oligosaccharides, 2.2 parts of thick polysaccharide, 12.5 parts of Sucraloses, 30 parts of superfine silica gel powders, 4 parts of carboxymethyl celluloses, 67.5 parts of sodium carboxymethyl starches, 5 parts of dolomols, purified water is appropriate, 75% concentration ethanol is appropriate.
3. a preparation method for granatum Chinese yam dispersing tablet, is characterized in that: comprise the following steps:
(1) get after fresh Chinese yam is cleaned and soak 15-20min in 0.1% the vitamin C aqueous solution, Chinese yam after soaking is put into and in freeze drier, carries out freeze drying, first open refrigerator and freeze, be chilled to raw material Chinese yam temperature within the scope of-20 to-30 ℃, and maintain 8-10h and be dried, then open vacuum, and be heated to 95-100 ℃, and continue dry 1-3h, the resulting solid matter of above-mentioned freeze drying is pulverized, make Chinese yam freeze-dried powder, standby;
(2) getting the red granatum of raw material, honeysuckle cleans, add the 4-5 of above-mentioned raw materials gross weight doubly to measure purified water and decoct 2-2.5h within the scope of 90-100 ℃, filter, the dregs of a decoction after filtering are added to the purified water that 2-4 doubly measures and within the scope of 90-100 ℃, decoct 1-1.5h, filter, filter residue is discharged, merge filtrate twice, and be concentrated into the gamma amylase that adds 1-2 ‰ when proportion is 1-1.5, within the scope of 35-45 ℃, be incubated 5-10h, after finally boiling 25-35min, filter, obtain mixed extract, standby;
(3) gained mixed extract in step (1) gained Chinese yam freeze-dried powder and step (2) is uniformly mixed, mixer speed is 50-75r/min, and the time is 10-15min, obtains mixture I, standby;
(4) to the middle gained mixture I of step (3), add ethanol to make determining alcohol reach 75%, after standing 8-16h, filter, impurity is discharged, after recovery ethanol, at temperature 40-60 ℃, under vacuum 0.58-0.68MPa condition, Vacuum Concentration to dry substance reaches 50-70%, carry out again vacuum drying, within the scope of baking temperature 40-60 ℃, obtain dry extract, standby;
(5) after being pulverized, step (4) gained dry extract add vitamin C, vitamin A, zinc gluconate, carboxymethyl cellulose, microcrystalline cellulose, haw thorn extract, American ginseng extract, sweet mellow wine, chitosan oligosaccharide, thick polysaccharide, Sucralose, superfine silica gel powder to mix granulation with mixing machine, rotating speed is 10-15r/min, time is 6-8min, by the particle after mixing 50-60 ℃ of scope inner drying to water content between 1-3%, standby;
(6) to the middle gained particle of step (5), add sodium carboxymethyl starch, dolomol to mix, compacting in flakes, obtains granatum Chinese yam dispersing tablet.
4. the preparation method of a kind of granatum Chinese yam dispersing tablet according to claim 3, it is characterized in that: in described step (1), get after fresh Chinese yam is cleaned and soak 20min in 0.1% the vitamin C aqueous solution, Chinese yam after soaking is put into and in freeze drier, carries out freeze drying, first opening refrigerator freezes, while being chilled to raw material Chinese yam temperature for-26 ℃, maintain 8h dry, then open vacuum, and continue dry 2.5h while being heated to 95 ℃, the resulting solid matter of above-mentioned freeze drying is pulverized, made Chinese yam freeze-dried powder.
5. the preparation method of a kind of granatum Chinese yam dispersing tablet according to claim 3, it is characterized in that: in described step (2), get the red granatum of raw material, honeysuckle is cleaned, add 6 times of amount purified water of above-mentioned raw materials gross weight to decoct 2h under 90 ℃ of conditions, filter, the purified water that the dregs of a decoction after filtering is added to 3 times of amounts decocts 1.5h under 90 ℃ of conditions, filter, filter residue is discharged, merge filtrate twice, and to be concentrated into proportion be to add 2 ‰ gamma amylase at 1 o'clock, under 45 ℃ of conditions, be incubated 6h, after finally boiling 35min, filter, obtain mixed extract.
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| CN104757464A (en) * | 2015-04-30 | 2015-07-08 | 黄馨莹 | Haw flake tablet making method |
| CN113041181A (en) * | 2019-12-27 | 2021-06-29 | 广州市科能化妆品科研有限公司 | Toner, preparation method thereof and collagenase inhibitor |
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