CN103655960A - Traditional Chinese medicine composition for preparing male health viscose fibers, prepared health viscose fibers and preparation method thereof - Google Patents
Traditional Chinese medicine composition for preparing male health viscose fibers, prepared health viscose fibers and preparation method thereof Download PDFInfo
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Abstract
The present invention discloses a traditional Chinese medicine composition for preparing male health viscose fibers, the prepared health viscose fibers and a preparation method thereof. The traditional Chinese medicine composition comprises the following traditional Chinese medicine components, by weight, 25-45% of common cnidium fruit, 25-45% of common curculigo rhizome, 20-40% of beautiful sweetgum fruit, and 10-30% of wild chrysanthemum flower. The method for preparing the health viscose fibers by using the traditional Chinese medicine composition comprises: dissolving traditional Chinese medicine composition extract powder to obtain an antibacterial health solution; heating borneol until being melted, and emulsifying to obtain an emulsifying solution; adopting a cellulose pulp as a raw material to prepare a spinning viscose, and adding the antibacterial health solution to the viscose solution in any steps from the end of yellowing to spinning to obtain an antibacterial health blending viscose solution; and carrying out spinning forming, strand drafting and post-treating on the antibacterial health blending viscose solution to obtain the health viscose fibers, wherein the borneol emulsifying solution is added in the oiling step of post-treating.
Description
Technical field
The present invention relates to functional fiber cellulose fiber technical field, be specifically related to a kind of the have Chinese medicine composition of male health care performance and the health fiber cellulose fiber of preparation thereof.
Background technology
Existing conventional viscose rayon is regenerated celulose fibre, and it is good that its goods have sucting wet air permeability, feature comfortable and easy to wear, but do not possess the function of plant amedica antibiotic health care.Along with the raising of people's living standard and the change of philosophy of life, people more and more pay attention to antibacterial, the health care of textile, wish that existing viscose rayon textile improves at aspects such as antibacterial and health cares.Moreover, due to running down and the increase of human survival pressure of environment for human survival, the mankind bear the puzzlement of various diseases, therefore, in order to make people nurse one's health health by inner disease outer treat in daily life, develop this characteristic both with natural fiber, the functional viscose fiber of health care of having again just seems very necessary.Chinese medicine external medicine treatment disease is that China working people is for thousands of years at same disease struggle middle summary a set of uniqueness out, effective Therapeutic Method.It is to take basic theory of tcm as guidance, all Chinese herbal and crude drugs preparationses are except oral, can also impose on the positions such as skin, hole key, acupuncture points on the human body and pathological changes part, to bring into play the effects such as its dredging the meridian, QI and blood regulating, eliminating toxic substances to remove stasis, strengthening vital QI to eliminate pathogenic factors, make unbalanced internal organs negative and positive be readjusted and improve, thereby reach the object of curing the disease.
In existing antibacterial fiber product, the antibacterial using is divided into three major types substantially, i.e. natural antibacterial agent, organic antibacterial agent and inorganic antiseptic; Organic antibacterial agent bacteriostasis and sterilization rapidly, efficient, but human body is had to side effect, antibacterial easily produces drug resistance, and poor in timeliness, non-refractory; Mineral-type antibacterial is mainly metal inorganic salt and the antibacterial zeolite particles with antibacterial action.Heavy metal ion in this type of antibacterial, very easily by contacting and be absorbed by the body with human body skin, causes very large potential hazard to the health of human body; Traditional Chinese Medicine Anti microbial inoculum in natural antibacterial agent has antibacterial efficient, and to human-body safety, antibacterial does not produce the advantages such as drug resistance, and environmental protection, therefore, in application, is day by day subject to people's attention.But in prior art, but do not use up to now the viscose rayon with antimicrobial health care function of Chinese medicine spinning to emerge.
Summary of the invention
First technical problem to be solved by this invention is: for common viscose fiber in prior art, do not possess antibacterial and deficiency health-care effect, a kind of Chinese medicine composition for the preparation of male health care viscose rayon is provided, and the viscose rayon of preparing with this Chinese medicine composition and cellulose viscose glue blending has the function of antibiotic health care to man.
Second technical problem to be solved by this invention is: for common viscose fiber in prior art, do not possess antibacterial and deficiency health-care effect, the viscose rayon with botanical herbs male health care function that provides a kind of extract of take botanical herbs compositions to prepare as man's antimicrobial health care function material and viscose rayon blend.
The 3rd technical problem to be solved by this invention is: for common viscose fiber in prior art, do not possess antibacterial and deficiency health-care effect, provide a kind of extract of take botanical herbs compositions to prepare the production method with botanical herbs antimicrobial health care function viscose rayon as antimicrobial health care function material and viscose rayon blend.
For solving above-mentioned first technical problem, technical scheme of the present invention is:
For the preparation of a Chinese medicine composition for male health care viscose rayon, the Chinese medicinal components that described Chinese medicine composition contains following percentage by weight: Fructus Cnidii 25～45%, Rhizoma Curculiginis 25～45%, Fructus Liquidambaris 20～40% and Flos Chrysanthemi Indici 10～30%.
In described Chinese medicine composition, the pharmacological action of each Chinese medicine ingredients is:
Fructus Cnidii has another name called Serpentis rice, Radix Habenariae Dentatae, is the fruit of samphire cnidium monnieri, and it is warm in nature, and acrid in the mouth is bitter, enters kidney, spleen two warps.According to surveying and determination, fruit is containing volatile oil, be mainly pinene, bank alkene, isoborneol, bergapton and angelate etc., there is warming the kidney to activate YANG, dispel the wind, the effect of dampness, parasite killing, be used for the treatment of the cards such as impotence in male, scrotum pruritus due to damp pathogen, woman's leukorrhagia pudendal pruritus, cold uterus are infertile, rheumatic arthralgia, scabies eczema.The newly organized > > of < < book on Chinese herbal medicine claims its " function is quite strange, inside and outsidely all can treat, and external treatment is especially good ".Fructus Cnidii fruit is containing volatile oil 1.3wt%, and its main component is left-handed pinene, left-handed camphene, bornyl isovaleriate, isoborneol etc. the Coumarins composition such as, o-acetyl columbianectin fixed containing osthole, isopimpinellin, bergapton, Archie angelicone, columbianetin, coffee human relations, o-isovaleryl columbianetin, cnidiadin, cnidimine again.
Rhizoma Curculiginis (Curculigo orchioides Gaertn.), < < Haiyao Bencao, Oversea Materia Medica > > begins to be loaded in, its leaf is like thatch, and root stock takes for a long time benefit essence and mends marrow, increases spirit, therefore there is the title of Rhizoma Curculiginis, another name ground palm fibre (Sichuan, Guizhou), Rhizoma Curculiginis (Sichuan), mountain Radix Codonopsis (Fujian), Radix Scorzonerae Albicaulis (Yunnan), Radix Glehniae (Hainan).The rhizome of amrallid Rhizoma Curculiginis is the Chinese medicine Rhizoma Curculiginis that < < Pharmacopoeia of People's Republic of China > > version First in 2005 records, there is the effect of reinforcing the kidney and supporting YANG, benefiting essence-blood, bone and muscle strengthening and promoting the circulation of blood detumescence, be mainly used in the diseases such as insufficiency of kidney-YANG, impotence and seminal emission, chronic consumptive disease internal injury and bones and muscles pain.
Fructus Liquidambaris, the property of Fructus Liquidambaris tool tonneau, function promoting the circulation of QI to alleviate the stagnation in middle-JIAO and pain relieving, for abdominal distention, the disease such as not well of defecating, can be equal to use with the Radix Aucklandiae, the Radix Linderae, Fructus Aurantii, for abdominal distention clinically.Again can promoting blood circulation to remove obstruction in the collateral, to menoxenia, Hypomenorrhea and abdominal distention person, can with the compatibilities such as Rhizoma Cyperi, Fructus Leonuri; To diseases such as rheumatic arthralgia, waist and leg ache, grain contractures, can be equal to use with Radix Angelicae Sinensis, Rhizoma Chuanxiong, Radix Angelicae Pubescentis, Herba Taxilli, can be used for rheumatic arthralgia, use through uncomfortable.In addition, have again the effect of inducing diuresis to remove edema, for edema, can with the compatibilities such as Cortex Sclerotii Poriae, Cortex Mori, Exocarpium Benincasae, can be used for the diseases such as edema, dysuria.The property of its tonneau also can catharsis milk, for stagnation of QI-blood, galactostasis.
Flos Chrysanthemi Indici, is Compositae herbaceos perennial, and the capitate profile of Flos Chrysanthemi Indici is similar to Flos Chrysanthemi, wild in wild areas such as patana, limit, field, roadsides.Take yellow skin without stalk, complete, gas is fragrant, flower not standard-sized sheet person as good.Flos Chrysanthemi Indici can be widely used in treatment furuncle carbuncle, laryngopharynx swelling and pain, wind-fire acute conjunctivitis, the disease such as dizzy of having a headache.There is again good hypotensive effect, can be used for the auxiliary treatment of hypertension simultaneously.
For solving above-mentioned second technical problem, technical scheme of the present invention is:
The male health care viscose rayon that uses described Chinese medicine composition to prepare, content of alphacellulose >=90wt%, the Content of Osthole >=0.02mg/Kg in described male health care viscose rayon, curculigoside content >=0.02mg/Kg, fruit keto acid and styracin content >=0.015mg/Kg, yejuhua lactone and chrysanthemol content >=0.01mg/Kg.
Described male health care viscose rayon is to bacteriostasis rate >=98.8% of staphylococcus aureus, to colibacillary suppression ratio >=98.6%, suppression ratio >=88.0% to Candida albicans.
For solving above-mentioned the 3rd technical problem, technical scheme of the present invention is:
Use described Chinese medicine composition to prepare the method for health care viscose fiber, comprise the following steps:
(1) prepare antibiotic health care solution: by the powder of described Chinese medicine composition extract, according to the addition of 100～500g/1000mL, join in the water of 30～60 ℃, be stirred well to powder and dissolve completely, obtain described antibiotic health care solution.
(2) prepare Borneolum Syntheticum emulsion: Borneolum Syntheticum is heated to fusing, then, under stirring, adds distilled water and the emulsifying agent of 70～90 ℃, fast homogeneous emulsifying is emulsion, is incubated standby.
(3) preparation of viscose glue: employing cellulose pulp is raw material, through comprising that dipping, squeezing, pulverizing, experienced, yellow step make cellulose viscose solution, and then make spinning viscose through dissolving, deaeration and filtration step.
(4) prepare antibiotic health care blend viscose solution: the antibiotic health care solution that step (1) is obtained is the addition with respect to first fibre 2～8wt% in viscose solution according to Chinese medicine composition, after joining yellow in step (3) and finishing, to the viscose solution in the arbitrary step before spinning, obtain described antibiotic health care blend viscose solution.
(5) antibiotic health care viscose rayon spinning moulding: spinning moulding in the coagulating bath by described antibiotic health care blend viscose solution through containing sulphuric acid, sodium sulfate, zinc sulfate and/or aluminum sulfate, through strand drawing-off, obtain nascent short fiber or the nascent filament fiber of described health care viscose fiber simultaneously.
(6) post processing: the post-processing step through comprising washing, desulfurization, oiling, dry by described nascent short fiber or nascent filament fiber, before the described step that oils or oil in step, described Borneolum Syntheticum emulsion, according to 0.1～0.5% use amount of cellulose quality content, is infiltrated described Borneolum Syntheticum emulsion and is penetrated into the surface of described health care viscose fiber and inner.
Borneolum Syntheticum, have another name called sheet brain, Fructus Citri tangerinae sheet, Borneolum Syntheticum, MEIHUA BINGPIAN, Dipterocarpus pilosus, Flos Mume brain, Borneolum Syntheticum brain, Mei Bing etc., the resin and the volatile oil processed goods that are Spore density Borneolum Syntheticum extract the crystallization obtaining, and are near pure dextro Borneolum Syntheticum, have very strong penetration.Also useful chemical method is synthetic.Its nature and flavor are arduous, are slightly cold.Can be used for excess syndrome of stroke coma, for conjunctival congestion and swelling pain, sore throat aphtha, for skin infection, swell and ache, after bursting, do not hold back etc.
As a kind of preferred, the powder of described Chinese medicine composition extract, is to use decoction and alcohol sedimentation technique to extract the solution that obtains effective ingredient described Chinese medicine composition, then the dry powder obtaining.
As a kind of improvement, in step (2), described while preparing Borneolum Syntheticum emulsion, described in Borneolum Syntheticum mass content in the Borneolum Syntheticum emulsion for preparing be 50～60%; The described emulsifying agent adding is at least one in arabic gum and sodium alkyl benzene sulfonate, 30～40wt% that the addition of described emulsifying agent is described Borneolum Syntheticum, 40～50wt% that the addition of described distilled water is described Borneolum Syntheticum.
As a kind of preferred, described while preparing antibiotic health care blend viscose glue, the antibiotic health care solution that step (1) is obtained joins in the viscose solution before the middle filtration step of step (3), through mix homogeneously, obtains described antibiotic health care blend viscose solution after spinning front filtration again.
As a kind of preferred, the total stretch ratio of strand drawing-off during the nascent staple fiber spinning molding of described health care viscose fiber is 50～180%, and spinning speed is 30～100m/min; Strand drawing-off during the nascent filament fiber spinning moulding of described health care viscose fiber comprise shower nozzle draw ratio between spinning head and drawing-off dish for-10～30%, drawing-off dish and to solidify draw ratio between the dish between roller be 10～20%, solidify that coagulating bath draw ratio between roller and acid removing roller is 0～15%, spinning speed is 50～120m/min.
As a kind of preferred, in described coagulating bath, sulfuric acid concentration is that 40～160g/L, sodium sulfate concentration are 80～320g/L, and zinc sulfate and/or aluminum sulfate concentration are 1～20g/L, and the temperature of described coagulating bath is 30～60 ℃.
As further preferred, in coagulating bath during the nascent staple fiber spinning molding of described health care viscose fiber, sulfuric acid concentration is that 40～160g/L, sodium sulfate concentration are 80～320g/L, and aluminum sulfate concentration is 1～20g/L, and the temperature of described coagulating bath is 30～60 ℃; In coagulating bath during the nascent filament fiber spinning moulding of described health care viscose fiber, sulfuric acid concentration is that 50～160g/L, sodium sulfate concentration are 100～320g/L, and aluminum sulfate concentration is 10～20g/L, and the temperature of described coagulating bath is 30～50 ℃.
Owing to having adopted technique scheme, the invention has the beneficial effects as follows:
The Chinese medicinal components that the Chinese medicine composition that the present invention adopts contains following percentage by weight: Fructus Cnidii 25～45%, Rhizoma Curculiginis 25～45%, Fructus Liquidambaris 20～40% and Flos Chrysanthemi Indici 10～30%, wherein, Fructus Cnidii is our monarch drug, and bitter in the mouth is warm in nature, can warming the kidney to invigorate YANG, kindly again dispel the wind, dampness, parasite killing, be treatment chronic prostatitis good merchantable brand; Rhizoma Curculiginis is warm in nature, and acrid in the mouth is micro-salty, have regulate immunity, antioxidation, protect the liver, the effect such as hyperglycemia, kidney invigorating and YANG supporting and osteoporosis, antiinflammatory and adaptation former state; Fructus Liquidambaris is bitter, flat.Return liver, kidney channel.There is dispelling, collateral-activating, the diuretic effect of stimulating the menstrual flow.For arthralgia, numbness contracture, edema distension, the few amenorrhea of breast; Flos Chrysanthemi Indici cold nature, bitter in the mouth, pungent, function heat-clearing and toxic substances removing, detumescence, to staphylococcus aureus, diphtheria corynebacterium, streptococcus, bacillus pyocyaneus, puncture Shigella, influenza virus, all has inhibitory action.Owing to thinking through Long-term clinical test and study, the pathogenesis of chronic prostatitis is the result of comprehensive functions such as " suffer from a deficiency of the kidney, blood stasis, expectorant knot, damp and hot, poisonous insect ", therefore above several Chinese medicine share, there is warming the kidney to invigorate YANG, supplementing QI and nourishing YIN, heat clearing and damp drying, blood circulation promoting and blood stasis dispelling, killing parasites for relieving itching, promoting the circulation of QI and reducing phlegm texts.Chronic prostatitis, scrotum pruritus due to damp pathogen and the sexual hypofunction that causes are had to good therapeutical effect.
Use content of alphacellulose >=90wt%, Content of Osthole >=0.02mg/Kg, curculigoside content >=0.02mg/Kg, fruit keto acid and styracin content >=0.015mg/Kg, yejuhua lactone and chrysanthemol content >=0.01mg/Kg in male health care viscose rayon prepared by above-mentioned Chinese medicine composition.After testing to bacteriostasis rate >=98.8% of staphylococcus aureus, to colibacillary suppression ratio >=98.6%, suppression ratio >=88.0% to Candida albicans.Therefore the male health care viscose rayon of preparing with the present invention has very excellent antibiotic health care performance, existing antibacterial and health-care effect, there is again viscose rayon moisture absorption to breathe freely, take comfortable characteristic, and antibiotic health care medicine is uniformly distributed in the inside of fiber, make this fibre antibacterial function lasting, with this antibiotic health care viscose rayon, make underwear, other clothing and bedding textile, male prostatitis is had to good prevention and health-care effect.
The present invention uses described Chinese medicine composition to prepare health care viscose fiber, use antibiotic health care solution and the spinning of viscose rayon solution blending of Chinese medicine extract, in the antiseptic health care fiber of producing, antibiotic health care medicine is uniformly distributed in the inside of fiber, make this fibre antibacterial function lasting, because Chinese medicine extract is the natural materials extracting from plant, human body is had no side effect; And use Borneolum Syntheticum emulsion to infiltrate and be penetrated into the surperficial and inner of described antibiotic health care viscose rayon in the step that oils, Borneolum Syntheticum can be used as " Percutaneous absorption enhancer ", there is good promotion osmosis, coordinate with other drug and greatly improved medicine for external use therapeutic effect.The preparation method with the viscose rayon of botanical herbs antimicrobial health care function provided by the invention, has the advantages that technique is reasonable, be applicable to suitability for industrialized production.
The specific embodiment
Below in conjunction with specific embodiment, further set forth the present invention.
Embodiment 1
For the preparation of a Chinese medicine composition for male health care viscose rayon, the Chinese medicinal components that contains following percentage by weight: Fructus Cnidii 25%, Rhizoma Curculiginis 40%, Fructus Liquidambaris 20% and Flos Chrysanthemi Indici 15%.
Embodiment 2
For the preparation of a Chinese medicine composition for male health care viscose rayon, the Chinese medicinal components that contains following percentage by weight: Fructus Cnidii 30%, Rhizoma Curculiginis 30%, Fructus Liquidambaris 30% and Flos Chrysanthemi Indici 10%.
Embodiment 3
For the preparation of a Chinese medicine composition for male health care viscose rayon, the Chinese medicinal components that contains following percentage by weight: Fructus Cnidii 35%, Rhizoma Curculiginis 25%, Fructus Liquidambaris 20% and Flos Chrysanthemi Indici 20%.
Embodiment 4
For the preparation of a Chinese medicine composition for male health care viscose rayon, the Chinese medicinal components that contains following percentage by weight: Fructus Cnidii 32%, Rhizoma Curculiginis 28%, Fructus Liquidambaris 28% and Flos Chrysanthemi Indici 12%.
Embodiment 5
The male health care viscose rayon that described in use embodiment 1 prepared by Chinese medicine composition, the content of alphacellulose 92.5wt% in described male health care viscose rayon, Content of Osthole 0.09mg/Kg, curculigoside content 0.18mg/Kg, fruit keto acid and styracin content 0.018mg/Kg, yejuhua lactone and chrysanthemol content 0.012mg/Kg.
Embodiment 6
The male health care viscose rayon that described in use embodiment 3 prepared by Chinese medicine composition, the content of alphacellulose 92wt% in described male health care viscose rayon, Content of Osthole 0.20mg/Kg, curculigoside content 0.025mg/Kg, fruit keto acid and styracin content 0.016mg/Kg, yejuhua lactone and chrysanthemol content 0.018mg/Kg.
Described male health care viscose rayon is to bacteriostasis rate >=98.8% of staphylococcus aureus, to colibacillary suppression ratio >=98.7%, suppression ratio >=88.02% to Candida albicans.
Embodiment 7
The male health care viscose rayon that described in use embodiment 4 prepared by Chinese medicine composition, the content of alphacellulose 92.3wt% in described male health care viscose rayon, Content of Osthole 0.35mg/Kg, curculigoside content 0.22mg/Kg, fruit keto acid and styracin content 0.02mg/Kg, yejuhua lactone and chrysanthemol content 0.011mg/Kg.
Described male health care viscose rayon is to bacteriostasis rate >=99.1% of staphylococcus aureus, to colibacillary suppression ratio >=98.75%, suppression ratio >=88.4% to Candida albicans.
Embodiment 8
(1) by percentage by weight, be the powder of the Chinese medicine composition extract of Fructus Cnidii 25%, Rhizoma Curculiginis 32%, Fructus Liquidambaris 25% and Flos Chrysanthemi Indici 18%, according to the addition of 100/1000mL, join in the water of 35 ℃, be stirred well to powder and dissolve completely, obtain described antibiotic health care solution.
(2) Borneolum Syntheticum is heated to fusing, then, under stirring, adds distilled water and the emulsifying agent of 75 ℃, fast homogeneous emulsifying is emulsion, is incubated standby.
(3) adopting cellulose pulp is raw material, through comprising that dipping, squeezing, pulverizing, experienced, yellow step make cellulose viscose solution, and then make spinning viscose through dissolving, deaeration and filtration step.
(4) antibiotic health care solution step (1) being obtained is the addition with respect to the fine 3wt% of first in viscose solution according to Chinese medicine composition, joins in the viscose solution after the middle yellow of step (3) finishes, and obtains described antibiotic health care blend viscose solution.
(5) spinning moulding in the coagulating bath through containing sulphuric acid, sodium sulfate, aluminum sulfate by described antibiotic health care blend viscose solution, simultaneously through strand drawing-off, obtains nascent short fiber or the nascent filament fiber of described health care viscose fiber.
(6) by described nascent short fiber or nascent filament fiber through washing, desulfurization, oil, baking operation, obtain described health care viscose fiber, in the step that oils, by described Borneolum Syntheticum emulsion according to 0.2% use amount of cellulose quality content in fiber, join in oil bath, described Borneolum Syntheticum emulsion is infiltrated and be penetrated into described health care viscose fiber surface and inner.
Embodiment 9
(1) by percentage by weight, be the Chinese medicine composition of Fructus Cnidii 40%, Rhizoma Curculiginis 25%, Fructus Liquidambaris 20% and Flos Chrysanthemi Indici 15%, use decoction and alcohol sedimentation technique to extract the solution that obtains effective ingredient, be dried again the extract powder obtaining, according to the addition of 300g/1000mL, join in the water of 45 ℃, be stirred well to powder and dissolve completely, obtain described antibiotic health care solution.
(2) Borneolum Syntheticum is heated to fusing, then, under stirring, adds distilled water and the emulsifying agent of 80 ℃, fast homogeneous emulsifying is emulsion, be incubated standby, described in the emulsifying agent that adds be arabic gum, the 30wt% that the addition of described arabic gum is described Borneolum Syntheticum.
(3) adopting bamboo pulp is raw material, through comprising that dipping, squeezing, pulverizing, experienced, yellow step make cellulose viscose solution, and then make spinning viscose through dissolving, deaeration and filtration step.
(4) antibiotic health care solution step (1) being obtained is the addition with respect to the fine 5wt% of first in viscose solution according to Chinese medicine composition, join in the viscose solution in the middle dissolving step of step (3), then obtain described antibiotic health care blend viscose solution through deaeration and filtration step.
(5) spinning moulding in the coagulating bath through containing sulphuric acid, sodium sulfate, zinc sulfate by described antibiotic health care blend viscose solution, simultaneously through strand drawing-off and cut-out, obtain the nascent short fiber of described health care viscose fiber, in described coagulating bath, sulfuric acid concentration is that 100g/L, sodium sulfate concentration are 220g/L, zinc sulfate concentration is 5g/L, and the temperature of described coagulating bath is 50 ℃.
(6) by described nascent short fiber through washing, desulfurization, oil, baking operation, obtain described health care viscose fiber, described desulfurization and washing after, oil before step, by described Borneolum Syntheticum emulsion according to 0.40% use amount of cellulose quality content, described Borneolum Syntheticum emulsion is infiltrated and be penetrated into described health care viscose fiber surface and inner, and then through oiling and baking step, obtain described health care viscose fiber.
Embodiment 10
(1) by percentage by weight, be the Chinese medicine composition of Fructus Cnidii 30%, Rhizoma Curculiginis 25%, Fructus Liquidambaris 25% and Flos Chrysanthemi Indici 20%, use decoction and alcohol sedimentation technique to extract the solution that obtains effective ingredient, be dried again the extract powder obtaining, according to the addition of 450g/1000mL, join in the water of 50 ℃, be stirred well to powder and dissolve completely, obtain described antibiotic health care solution.
(2) Borneolum Syntheticum is heated to fusing, then under stirring, the distilled water and the emulsifying agent that add 85 ℃, fast homogeneous emulsifying is that Borneolum Syntheticum mass content is 52% emulsion, 70～90 ℃ of insulations are standby, the described emulsifying agent adding is sodium alkyl benzene sulfonate, the 38wt% that the addition of described sodium alkyl benzene sulfonate is described Borneolum Syntheticum.
(3) adopting bamboo pulp is raw material, through comprising that dipping, squeezing, pulverizing, experienced, yellow step make cellulose viscose solution, and then make spinning viscose through dissolving, deaeration and filtration step.
(4) antibiotic health care solution step (1) being obtained is the addition with respect to the fine 6wt% of first in viscose solution according to Chinese medicine composition, joins in the viscose solution before the middle filtration of step (3), obtains after filtration described antibiotic health care blend viscose solution.
(5) spinning moulding in the coagulating bath through containing sulphuric acid, sodium sulfate, aluminum sulfate by described antibiotic health care blend viscose solution, simultaneously through strand drawing-off and cut-out, obtain the nascent short fiber of described antibiotic health care viscose rayon, in coagulating bath during described molding, sulfuric acid concentration is that 60g/L, sodium sulfate concentration are 300g/L, aluminum sulfate concentration is 10g/L, and the temperature of described coagulating bath is 40 ℃; The total stretch ratio of strand drawing-off during the nascent staple fiber spinning molding of described antibiotic health care viscose glue as-spun fibre is 120%, and spinning speed is 100m/min.
(6) by described nascent short fiber through washing, desulfurization, oil, baking operation, obtain described health care viscose fiber, in the step that oils, described Borneolum Syntheticum emulsion is joined in oil bath according to 0.3% use amount of cellulose quality content, described Borneolum Syntheticum emulsion is infiltrated and be penetrated into the surface of described health care viscose fiber and inner.
Embodiment 11
(1) by percentage by weight, be the Chinese medicine composition of Fructus Cnidii Fructus Cnidii 30%, Rhizoma Curculiginis 30%, Fructus Liquidambaris 25% and Flos Chrysanthemi Indici 15%, use decoction and alcohol sedimentation technique to extract the solution that obtains effective ingredient, be dried again the extract powder obtaining, according to the addition of 500g/1000mL, join in the water of 60 ℃, be stirred well to powder and dissolve completely, obtain described antibiotic health care solution.
(2) Borneolum Syntheticum is heated to fusing, then under stirring, the distilled water and the emulsifying agent that add 90 ℃, fast homogeneous emulsifying is that Borneolum Syntheticum mass content is 58% emulsion, 90 ℃ of insulations are standby, the described emulsifying agent adding is arabic gum, the 35wt% that the addition of described arabic gum is described Borneolum Syntheticum.
(3) adopting Cotton Pulp is raw material, through comprising that dipping, squeezing, pulverizing, experienced, yellow step make cellulose viscose solution, and then make spinning viscose through dissolving, deaeration and filtration step.
(4) antibiotic health care solution step (1) being obtained is the addition with respect to the fine 8wt% of first in viscose solution according to Chinese medicine composition, join in the viscose solution in the middle dissolving step of step (3), then obtain described antibiotic health care blend viscose solution through deaeration and filtration step.
(5) spinning moulding in the coagulating bath through containing sulphuric acid, sodium sulfate, zinc sulfate and aluminum sulfate by described antibiotic health care blend viscose solution, simultaneously through strand drawing-off, obtain the nascent filament fiber of described antibiotic health care viscose rayon, in coagulating bath during described nascent filament fiber spinning moulding, sulfuric acid concentration is that 120g/L, sodium sulfate concentration are 260g/L, aluminum sulfate concentration is 15g/L, and the temperature of described coagulating bath is 45 ℃; Strand drawing-off during nascent filament fiber spinning moulding comprises that the shower nozzle draw ratio between spinning head and drawing-off dish is 5%, drawing-off dish and to solidify draw ratio between the dish between roller be 12%, solidify that coagulating bath draw ratio between roller and acid removing roller is 5%, spinning speed is 75m/min.
(6) by described nascent filament fiber through washing, desulfurization, oil, baking operation, obtain described health care viscose fiber, in the step that oils, described Borneolum Syntheticum emulsion is joined in oil bath according to 0.5% use amount of cellulose quality content, in the process of oiling, described Borneolum Syntheticum emulsion infiltrated and be penetrated into the surface of described health care viscose fiber and inner.
Health care viscose fiber prepared by above embodiment 8-11, utilize respectively Chinese medicine ingredients that ethanol contains it to extract and obtain Chinese medicine ingredients solid, respectively contained different Chinese medicine ingredients is tested to (adopting high performance liquid chromatography method of testing), the results are shown in Table 1.
Table 1
As can be seen from Table 1, in health care viscose fiber, contain a certain amount of Chinese medicine ingredients, there is antimicrobial health care function.
Health care viscose fiber sample prepared by embodiment 8-11 has carried out respectively antibacterial test, the results are shown in Table 2.
Table 2
As can be seen from Table 2, health care viscose fiber has all surpassed national standard to the bacteriostasis rate of three kinds of bacterium, has good antibiotic property.
Health care viscose fiber sample prepared by embodiment 8-11 carries out respectively the test of key property with conventional viscose rayon, the results are shown in Table 3.
Table 3
As can be seen from Table 3, the key property of health care viscose fiber key property and conventional viscose rayon does not relatively have significant difference.
Claims (10)
1. for the preparation of a Chinese medicine composition for male health care viscose rayon, it is characterized in that the Chinese medicinal components that described Chinese medicine composition contains following percentage by weight: Fructus Cnidii 25～45%, Rhizoma Curculiginis 25～45%, Fructus Liquidambaris 20～40% and Flos Chrysanthemi Indici 10～30%.
2. the male health care viscose rayon that uses Chinese medicine composition as claimed in claim 1 to prepare, is characterized in that: content of alphacellulose >=90wt%, the Content of Osthole >=0.02mg/Kg in described male health care viscose rayon, curculigoside content >=0.02mg/Kg, fruit keto acid and styracin content >=0.015mg/Kg, yejuhua lactone and chrysanthemol content >=0.01mg/Kg.
3. male health care viscose rayon as claimed in claim 2, is characterized in that: described male health care viscose rayon is to bacteriostasis rate >=98.8% of staphylococcus aureus, to colibacillary suppression ratio >=98.6%, suppression ratio >=88.0% to Candida albicans.
4. use Chinese medicine composition as claimed in claim 1 to prepare the method for health care viscose fiber, it is characterized in that comprising the following steps:
(1) prepare antibiotic health care solution: by the powder of described Chinese medicine composition extract, according to the addition of 100～500g/1000mL, join in the water of 30～60 ℃, be stirred well to powder and dissolve completely, obtain described antibiotic health care solution;
(2) prepare Borneolum Syntheticum emulsion: Borneolum Syntheticum is heated to fusing, then, under stirring, adds distilled water and the emulsifying agent of 70～90 ℃, fast homogeneous emulsifying is emulsion, is incubated standby;
(3) preparation of viscose glue: employing cellulose pulp is raw material, through comprising that dipping, squeezing, pulverizing, experienced, yellow step make cellulose viscose solution, and then make spinning viscose through dissolving, deaeration and filtration step;
(4) prepare antibiotic health care blend viscose solution: the antibiotic health care solution that step (1) is obtained is the addition with respect to first fibre 2～8wt% in viscose solution according to Chinese medicine composition, after joining yellow in step (3) and finishing, to the viscose solution in the arbitrary step before spinning, obtain described antibiotic health care blend viscose solution;
(5) antibiotic health care viscose rayon spinning moulding: spinning moulding in the coagulating bath by described antibiotic health care blend viscose solution through containing sulphuric acid, sodium sulfate, zinc sulfate and/or aluminum sulfate, through strand drawing-off, obtain nascent short fiber or the nascent filament fiber of described health care viscose fiber simultaneously;
(6) post processing: the post-processing step through comprising washing, desulfurization, oiling, dry by described nascent short fiber or nascent filament fiber, obtain described health care viscose fiber, before the described step that oils or oil in step, described Borneolum Syntheticum emulsion, according to 0.1～0.5% use amount of cellulose quality content, is infiltrated described Borneolum Syntheticum emulsion and is penetrated into the surface of described health care viscose fiber and inner.
5. the preparation method of health care viscose fiber as claimed in claim 4, is characterized in that: the powder of described Chinese medicine composition extract is to use decoction and alcohol sedimentation technique to extract the solution that obtains effective ingredient described Chinese medicine composition, then the dry powder obtaining.
6. the preparation method of health care viscose fiber as claimed in claim 4, is characterized in that: in step (2), described while preparing Borneolum Syntheticum emulsion, the Borneolum Syntheticum mass content in the Borneolum Syntheticum emulsion preparing is 50～60%; The described emulsifying agent adding is at least one in arabic gum and sodium alkyl benzene sulfonate, 30～40wt% that the addition of described emulsifying agent is described Borneolum Syntheticum.
7. the preparation method of health care viscose fiber as claimed in claim 4, it is characterized in that: described while preparing antibiotic health care blend viscose glue, the antibiotic health care solution that step (1) is obtained joins in the viscose solution before the middle filtration step of step (3), after mixing, filtering, obtains described antibiotic health care blend viscose solution.
8. the preparation method of health care viscose fiber as claimed in claim 4, is characterized in that: the total stretch ratio of strand drawing-off during the nascent staple fiber spinning molding of described health care viscose fiber is 50～180%, and spinning speed is 30～100m/min; Strand drawing-off during the nascent filament fiber spinning moulding of described health care viscose fiber comprises that draw ratio is 10～20% to shower nozzle draw ratio for-10～30%, between dish, coagulating bath draw ratio is 0～15%, spinning speed is 50～120m/min.
9. the preparation method of the health care viscose fiber as described in claim as arbitrary in claim 4 to 8, it is characterized in that: in described coagulating bath, sulfuric acid concentration is that 40～160g/L, sodium sulfate concentration are 80～320g/L, zinc sulfate and/or aluminum sulfate concentration are 1～20g/L, and the temperature of described coagulating bath is 30～60 ℃.
10. the preparation method of health care viscose fiber as claimed in claim 9, it is characterized in that: in coagulating bath during the nascent staple fiber spinning molding of described health care viscose fiber, sulfuric acid concentration is that 40～160g/L, sodium sulfate concentration are 80～320g/L, aluminum sulfate concentration is 1～20g/L, and the temperature of described coagulating bath is 30～60 ℃; In coagulating bath during the nascent filament fiber spinning moulding of described health care viscose fiber, sulfuric acid concentration is that 50～160g/L, sodium sulfate concentration are 100～320g/L, and aluminum sulfate concentration is 10～20g/L, and the temperature of described coagulating bath is 30～50 ℃.
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