CN105238089A - Novel deodorant natural fiber material and preparation method thereof - Google Patents
Novel deodorant natural fiber material and preparation method thereof Download PDFInfo
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- CN105238089A CN105238089A CN201510780004.0A CN201510780004A CN105238089A CN 105238089 A CN105238089 A CN 105238089A CN 201510780004 A CN201510780004 A CN 201510780004A CN 105238089 A CN105238089 A CN 105238089A
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Abstract
The invention discloses a novel deodorant natural fiber material and a preparation method thereof. The novel deodorant natural fiber material is prepared from the following components in parts by weight: 85-90 parts of natural fibers, 15-18 parts of polyvinyl alcohol, 12-18 parts of columbianetin acetate, 7-10 parts of bornyl isovalerate, 5-7 parts of bergapten, 3-5 parts of starch phosphate monoester, 1-2 parts of phenylalanine, 0.5-1 part of eucalyptus citriodora alcohol, 0.5-0.8 part of fumaric acid and 0.2-0.8 part of cnidium lactone. The invention also provides a preparation method of the deodorant natural fiber material.
Description
Technical field
The invention belongs to filamentary material field, particularly a kind of New deodouring natural fiber material and preparation method thereof.
Background technology
Along with people require more and more higher to the comfortableness of fabric, health, security and the feature of environmental protection etc. day by day, the textile material of exploitation moisture absorption, perspire and deodorizing class function has become a large Main Trends of The Development.The performance of fiber depends primarily on its chemical constitution and physical structure.
The natural fiber that nature exists mainly contains cotton, crudefiber crop, silk and animal wool, the wherein molecular constituents of cotton and crudefiber crop mainly Mierocrystalline cellulose, and the molecular constituents of silk and hairs mainly protein.By natural fiber through chemical treatment, do not change its chemical structure, only change the physical structure of natural cellulose, thus create the fiber with various new function, this technology is called regenerated fiber technology.
Summary of the invention
For above-mentioned demand, invention especially provides a kind of New deodouring natural fiber material and preparation method thereof.
Object of the present invention can be achieved through the following technical solutions:
A kind of New deodouring natural fiber material, be made up of the component comprising following weight part:
Natural fiber 85-90 part,
Polyvinyl alcohol 15-18 part,
Columbianetin acetic ester 12-18 part,
Bornival 7-10 part,
Bergapton 5-7 part,
Starch phosphate monoester 3-5 part,
Phenylalanine 1-2 part,
Lemon eucalyptus alcohol 0.5-1 part,
FUMARIC ACID TECH GRADE 0.5-0.8 part,
Osthole 0.2-0.8 part.
Described natural fiber is selected from the mixing of one or more in cotton fibre, flaxen fiber, bamboo fibers or silky fibre.
Described component also comprises nano zine oxide 0-0.3 weight part.
A preparation method for New deodouring natural fiber material, the method comprises the following steps:
(1) weighing polyvinyl alcohol 15-18 weight part, Columbianetin acetic ester 12-18 weight part, bornival 7-10 weight part, bergapton 5-7 weight part, starch phosphate monoester 3-5 weight part, phenylalanine 1-2 weight part, lemon eucalyptus alcohol 0.5-1 weight part, FUMARIC ACID TECH GRADE 0.5-0.8 weight part and osthole 0.2-0.8 weight part, stir at 120-140 DEG C;
(2) add natural fiber 85-90 weight part and nano zine oxide 0-0.3 weight part, mix 10-20 minute, twist in high pressure homogenizer, cooling, pelletizing, obtains deodorizing natural fiber material.
Mixing temperature in described high pressure homogenizer is 80-100 DEG C, and blend pressure is 12-16MPa.
Compared with prior art, its beneficial effect is in the present invention:
(1) the deodorizing natural fiber material that the present invention obtains take natural fiber as main raw material, by adding polyvinyl alcohol, Columbianetin acetic ester, bornival, bergapton, starch phosphate monoester, phenylalanine, lemon eucalyptus alcohol, FUMARIC ACID TECH GRADE and osthole, obtained deodorizing natural fiber material has good deodorizing and anti-microbial property, and this deodorizing natural fiber material has good kindliness and mechanical strength.
(2) properties of deodorizing natural fiber material that the present invention obtains has stability.
(3) deodorizing natural fiber material of the present invention, its preparation method is simple, is easy to suitability for industrialized production.
Embodiment
Below in conjunction with embodiment, the present invention is further illustrated.
Embodiment 1
(1) weighing polyvinyl alcohol 15kg, Columbianetin acetic ester 12kg, bornival 7kg, bergapton 5kg, starch phosphate monoester 3kg, phenylalanine 1kg, lemon eucalyptus alcohol 0.5kg, FUMARIC ACID TECH GRADE 0.5kg and osthole 0.2kg, stir at 120 DEG C;
(2) add flaxen fiber 85kg, 80 DEG C, mixing 20 minutes under 16MPa in high pressure homogenizer, twist, cooling, pelletizing, obtains deodorizing natural fiber material.
The performance test results of obtained deodorizing natural fiber material is as shown in table 1.
Embodiment 2
(1) weighing polyvinyl alcohol 15kg, Columbianetin acetic ester 12kg, bornival 7kg, bergapton 5kg, starch phosphate monoester 3kg, phenylalanine 1kg, lemon eucalyptus alcohol 0.5kg, FUMARIC ACID TECH GRADE 0.5kg and osthole 0.2kg, stir at 120 DEG C;
(2) add flaxen fiber 85kg and nano zine oxide 0.3kg, 80 DEG C, mixing 20 minutes under 16MPa in high pressure homogenizer, twist, cooling, pelletizing, obtains deodorizing natural fiber material.
The performance test results of obtained deodorizing natural fiber material is as shown in table 1.
Embodiment 3
(1) weighing polyvinyl alcohol 18kg, Columbianetin acetic ester 18kg, bornival 10kg, bergapton 7kg, starch phosphate monoester 5kg, phenylalanine 2kg, lemon eucalyptus alcohol 1kg, FUMARIC ACID TECH GRADE 0.8kg and osthole 0.8kg, stir at 140 DEG C;
(2) add silky fibre 90kg and nano zine oxide 0.3kg, 100 DEG C, mixing 10 minutes under 12MPa in high pressure homogenizer, twist, cooling, pelletizing, obtains deodorizing natural fiber material.
The performance test results of obtained deodorizing natural fiber material is as shown in table 1.
Embodiment 4
(1) weighing polyvinyl alcohol 18kg, Columbianetin acetic ester 18kg, bornival 10kg, bergapton 7kg, starch phosphate monoester 5kg, phenylalanine 2kg, lemon eucalyptus alcohol 0.5kg, FUMARIC ACID TECH GRADE 0.5kg and osthole 0.2kg, stir at 140 DEG C;
(2) add silky fibre 90kg and nano zine oxide 0.3kg, 100 DEG C, mixing 10 minutes under 12MPa in high pressure homogenizer, twist, cooling, pelletizing, obtains deodorizing natural fiber material.
The performance test results of obtained deodorizing natural fiber material is as shown in table 1.
Embodiment 5
(1) weighing polyvinyl alcohol 17kg, Columbianetin acetic ester 16kg, bornival 8kg, bergapton 6kg, starch phosphate monoester 4kg, phenylalanine 1kg, lemon eucalyptus alcohol 0.8kg, FUMARIC ACID TECH GRADE 0.6kg and osthole 0.5kg, stir at 130 DEG C;
(2) add silky fibre 88kg and nano zine oxide 0.2kg, 90 DEG C, mixing 15 minutes under 14MPa in high pressure homogenizer, twist, cooling, pelletizing, obtains deodorizing natural fiber material.
The performance test results of obtained deodorizing natural fiber material is as shown in table 1.
Comparative example 1
(1) weighing polyvinyl alcohol 18kg, Columbianetin acetic ester 18kg, bornival 10kg, bergapton 7kg, starch phosphate monoester 5kg, lemon eucalyptus alcohol 1kg and osthole 0.8kg, stir at 140 DEG C;
(2) add silky fibre 90kg, 100 DEG C, mixing 10 minutes under 12MPa in high pressure homogenizer, twist, cooling, pelletizing, obtains deodorizing natural fiber material.
The performance test results of obtained deodorizing natural fiber material is as shown in table 1.
Comparative example 2
(1) weighing polyvinyl alcohol 18kg, Columbianetin acetic ester 18kg, bornival 10kg, starch phosphate monoester 5kg, phenylalanine 2kg, lemon eucalyptus alcohol 1kg and FUMARIC ACID TECH GRADE 0.8kg, stir at 140 DEG C;
(2) add silky fibre 90kg, 100 DEG C, mixing 10 minutes under 12MPa in high pressure homogenizer, twist, cooling, pelletizing, obtains deodorizing natural fiber material.
The performance test results of obtained deodorizing natural fiber material is as shown in table 1.
Comparative example 3
(1) weighing polyvinyl alcohol 18kg, Columbianetin acetic ester 18kg, bergapton 7kg, starch phosphate monoester 5kg, phenylalanine 2kg, FUMARIC ACID TECH GRADE 0.8kg and osthole 0.8kg, stir at 140 DEG C;
(2) add silky fibre 90kg, 100 DEG C, mixing 10 minutes under 12MPa in high pressure homogenizer, twist, cooling, pelletizing, obtains deodorizing natural fiber material.
The performance test results of obtained deodorizing natural fiber material is as shown in table 1.
Table 1
| Test event | Tensile strength (N) | Acarid survival rate (%) |
| Embodiment 1 | 68 | 1 |
| Embodiment 2 | 72 | 0.5 |
| Embodiment 3 | 77 | 0.5 |
| Embodiment 4 | 80 | 0.1 |
| Embodiment 5 | 75 | 0.2 |
| Comparative example 1 | 36 | 58 |
| Comparative example 2 | 30 | 69 |
| Comparative example 3 | 33 | 72 |
The invention is not restricted to embodiment here, those skilled in the art, according to announcement of the present invention, do not depart from improvement that scope makes and amendment all should within protection scope of the present invention.
Claims (5)
1. a New deodouring natural fiber material, is characterized in that, is made up of the component comprising following weight part:
2. New deodouring natural fiber material according to claim 1, is characterized in that, described natural fiber is selected from the mixing of one or more in cotton fibre, flaxen fiber, bamboo fibers or silky fibre.
3. New deodouring natural fiber material according to claim 1, is characterized in that, described component also comprises nano zine oxide 0-0.3 weight part.
4. a preparation method for New deodouring natural fiber material, is characterized in that, the method comprises the following steps:
(1) weighing polyvinyl alcohol 15-18 weight part, Columbianetin acetic ester 12-18 weight part, bornival 7-10 weight part, bergapton 5-7 weight part, starch phosphate monoester 3-5 weight part, phenylalanine 1-2 weight part, lemon eucalyptus alcohol 0.5-1 weight part, FUMARIC ACID TECH GRADE 0.5-0.8 weight part and osthole 0.2-0.8 weight part, stir at 120-140 DEG C;
(2) add natural fiber 85-90 weight part and nano zine oxide 0-0.3 weight part, mix 10-20 minute, twist in high pressure homogenizer, cooling, pelletizing, obtains deodorizing natural fiber material.
5. the preparation method of New deodouring natural fiber material according to claim 4, is characterized in that, the mixing temperature in described high pressure homogenizer is 80-100 DEG C, and blend pressure is 12-16MPa.
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| Application Number | Priority Date | Filing Date | Title |
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| CN201510780004.0A CN105238089A (en) | 2015-11-13 | 2015-11-13 | Novel deodorant natural fiber material and preparation method thereof |
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| CN201510780004.0A CN105238089A (en) | 2015-11-13 | 2015-11-13 | Novel deodorant natural fiber material and preparation method thereof |
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Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN110194886A (en) * | 2019-06-18 | 2019-09-03 | 郑颖 | A kind of preparation method of bamboo fiber-based degradable environment-friendly material |
Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JP2003072854A (en) * | 2001-09-03 | 2003-03-12 | Sony Corp | Packaging cushioning body, and manufacturing method thereof |
| CN103655960A (en) * | 2013-12-05 | 2014-03-26 | 山东富山集团有限公司 | Traditional Chinese medicine composition for preparing male health viscose fibers, prepared health viscose fibers and preparation method thereof |
| CN104069525A (en) * | 2013-03-25 | 2014-10-01 | 理研香料工业株式会社 | Deodorant |
-
2015
- 2015-11-13 CN CN201510780004.0A patent/CN105238089A/en active Pending
Patent Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JP2003072854A (en) * | 2001-09-03 | 2003-03-12 | Sony Corp | Packaging cushioning body, and manufacturing method thereof |
| CN104069525A (en) * | 2013-03-25 | 2014-10-01 | 理研香料工业株式会社 | Deodorant |
| CN103655960A (en) * | 2013-12-05 | 2014-03-26 | 山东富山集团有限公司 | Traditional Chinese medicine composition for preparing male health viscose fibers, prepared health viscose fibers and preparation method thereof |
Non-Patent Citations (3)
| Title |
|---|
| 张文富: "《新型化工小产品制造技术（第三集）》", 30 April 2001 * |
| 李少华: "《植物农药》", 31 May 2013 * |
| 王本祥: "《现代中药药理与临床》", 1 June 2004 * |
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN110194886A (en) * | 2019-06-18 | 2019-09-03 | 郑颖 | A kind of preparation method of bamboo fiber-based degradable environment-friendly material |
| CN110194886B (en) * | 2019-06-18 | 2021-04-13 | 青岛中宝塑业有限公司 | Preparation method of bamboo fiber based degradable environment-friendly material |
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