CN104480716A - Novel anti-pilling softener for fabrics and preparation method of softener - Google Patents
Novel anti-pilling softener for fabrics and preparation method of softener Download PDFInfo
- Publication number
- CN104480716A CN104480716A CN201410815749.1A CN201410815749A CN104480716A CN 104480716 A CN104480716 A CN 104480716A CN 201410815749 A CN201410815749 A CN 201410815749A CN 104480716 A CN104480716 A CN 104480716A
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- CN
- China
- Prior art keywords
- softener
- weight portion
- parts
- antipilling
- polyvinyl alcohol
- Prior art date
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- 239000004744 fabric Substances 0.000 title claims abstract description 31
- 238000002360 preparation method Methods 0.000 title claims abstract description 9
- BAPJBEWLBFYGME-UHFFFAOYSA-N Methyl acrylate Chemical compound COC(=O)C=C BAPJBEWLBFYGME-UHFFFAOYSA-N 0.000 claims abstract description 18
- 239000004372 Polyvinyl alcohol Substances 0.000 claims abstract description 12
- 229920002451 polyvinyl alcohol Polymers 0.000 claims abstract description 12
- WXZMFSXDPGVJKK-UHFFFAOYSA-N pentaerythritol Chemical compound OCC(CO)(CO)CO WXZMFSXDPGVJKK-UHFFFAOYSA-N 0.000 claims abstract description 10
- DBMJMQXJHONAFJ-UHFFFAOYSA-M Sodium laurylsulphate Chemical compound [Na+].CCCCCCCCCCCCOS([O-])(=O)=O DBMJMQXJHONAFJ-UHFFFAOYSA-M 0.000 claims abstract description 9
- 239000008367 deionised water Substances 0.000 claims abstract description 9
- 229910021641 deionized water Inorganic materials 0.000 claims abstract description 9
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Chemical compound O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims abstract description 9
- 238000000034 method Methods 0.000 claims abstract description 3
- 239000003109 Disodium ethylene diamine tetraacetate Substances 0.000 claims description 8
- ZGTMUACCHSMWAC-UHFFFAOYSA-L EDTA disodium salt (anhydrous) Chemical compound [Na+].[Na+].OC(=O)CN(CC([O-])=O)CCN(CC(O)=O)CC([O-])=O ZGTMUACCHSMWAC-UHFFFAOYSA-L 0.000 claims description 8
- -1 Poly-methyl cyclotetrasiloxane Chemical compound 0.000 claims description 8
- 150000001412 amines Chemical group 0.000 claims description 8
- 125000000118 dimethyl group Chemical group [H]C([H])([H])* 0.000 claims description 8
- 235000019301 disodium ethylene diamine tetraacetate Nutrition 0.000 claims description 8
- 229920005573 silicon-containing polymer Polymers 0.000 claims description 8
- KRKNYBCHXYNGOX-UHFFFAOYSA-N citric acid Chemical compound OC(=O)CC(O)(C(O)=O)CC(O)=O KRKNYBCHXYNGOX-UHFFFAOYSA-N 0.000 claims description 6
- 239000000203 mixture Substances 0.000 abstract description 2
- BDOYKFSQFYNPKF-UHFFFAOYSA-N 2-[2-[bis(carboxymethyl)amino]ethyl-(carboxymethyl)amino]acetic acid;sodium Chemical compound [Na].[Na].OC(=O)CN(CC(O)=O)CCN(CC(O)=O)CC(O)=O BDOYKFSQFYNPKF-UHFFFAOYSA-N 0.000 abstract 1
- 238000001914 filtration Methods 0.000 abstract 1
- 150000003839 salts Chemical class 0.000 abstract 1
- 239000000835 fiber Substances 0.000 description 7
- 244000248349 Citrus limon Species 0.000 description 5
- 235000005979 Citrus limon Nutrition 0.000 description 5
- 239000002253 acid Substances 0.000 description 5
- 239000004753 textile Substances 0.000 description 4
- 239000000463 material Substances 0.000 description 3
- 210000002268 wool Anatomy 0.000 description 3
- 230000000694 effects Effects 0.000 description 2
- 238000005516 engineering process Methods 0.000 description 2
- 229920004934 Dacron® Polymers 0.000 description 1
- 238000005299 abrasion Methods 0.000 description 1
- 238000010521 absorption reaction Methods 0.000 description 1
- 230000000844 anti-bacterial effect Effects 0.000 description 1
- 238000005452 bending Methods 0.000 description 1
- 230000009286 beneficial effect Effects 0.000 description 1
- 230000002349 favourable effect Effects 0.000 description 1
- 239000008187 granular material Substances 0.000 description 1
- 238000005470 impregnation Methods 0.000 description 1
- 230000001965 increasing effect Effects 0.000 description 1
- 238000004519 manufacturing process Methods 0.000 description 1
- 231100000252 nontoxic Toxicity 0.000 description 1
- 230000003000 nontoxic effect Effects 0.000 description 1
- 239000005020 polyethylene terephthalate Substances 0.000 description 1
- 239000002994 raw material Substances 0.000 description 1
- 230000001105 regulatory effect Effects 0.000 description 1
- 238000005406 washing Methods 0.000 description 1
Abstract
The invention discloses a novel anti-pilling softener for fabrics and a preparation method of the softener. The anti-pilling softener for the fabrics is prepared from components in parts by weight as follows: 15-20 parts of polyvinyl alcohol, 5-7 parts of pentaerythritol, 4-7 parts of methyl acrylate, 2-3 parts of ethylenediaminetetraacetic acid disodium, 0.8-1.4 parts of polymethylcyclotetrasiloxane, 0.5-2 parts of sodium dodecyl sulfate, 0.5-1 part of polydimethylsiloxanebiquaternaryammonium salt and 110-120 parts of deionized water. The method comprises steps as follows: evenly mixing the components, adjusting the pH to range from 5.5 to 6, and filtering the mixture with a filter net with 100-200 meshes to obtain the anti-pilling softener for the fabrics.
Description
Technical field
The invention belongs to textile material field, particularly a kind of novel fabric ANTIPILLING softener and preparation method thereof.
Background technology
Along with the development of science and technology, improving constantly of people's quality of life, people not only rest on good-looking and comfort aspect for the demand of textiles, and original single textile material can not meet the demand of people.
Fiber be a class extensively by people's favorable comment and the material that accepts by masses, mainly because the intensity of its fiber is high, ability of extending is large, particularly tired, the resistance to torsional fatigue of resist bending and ABRASION RESISTANCE good.But its fabric is in reality dress, use and washing process, constant standing is rubbed, thus fluffing, balling-up, the fiber of fabric face is made to be exposed to fabric, if the fiber exposed can not come off in time in continuing to wear, with regard to mutual tied up in knots, be kneaded into many spherical granules, be commonly referred to the aesthetic feeling of ball impact outward appearance.
The factor affecting pilling affect gigging, balling-up factor a lot, the reason of fabric pilling and the proterties of fiber have substantial connection, how to reduce dacron balling-up, fluffing, are the directions that we study always.
Summary of the invention
For above-mentioned demand, the object of this invention is to provide a kind of novel fabric ANTIPILLING softener and preparation method thereof.
Object of the present invention can be achieved through the following technical solutions:
A kind of novel fabric ANTIPILLING softener, be made up of the component comprising following weight portion:
Described component also comprises toner 0-1 weight portion.
The mean molecule quantity of described polyvinyl alcohol is 1000-2500.
A preparation method for novel fabric ANTIPILLING softener, the method comprises the following steps:
(1) polyvinyl alcohol 15-20 weight portion, pentaerythrite 5-7 weight portion, methyl acrylate 4-7 weight portion, disodium ethylene diamine tetraacetate 2-3 weight portion, poly-methyl cyclotetrasiloxane 0.8-1.4 weight portion, dodecyl sodium sulfate 0.5-2 weight portion, dimethyl silicone polymer two quaternary amine 0.5-1 weight portion, deionized water 110-120 weight portion and toner 0-1 weight portion;
(2) said components is mixed, regulate pH to 5.5-6, filter with 100-200 mesh filter screen, obtained fabric ANTIPILLING softener.
PH is regulated to be by adding citric acid described in step 2.
Beneficial effect:
(1) fabric ANTIPILLING softener of the present invention, its raw material be nontoxic can directly and human contact.
(2) fabric ANTIPILLING softener of the present invention, with the addition of polyvinyl alcohol and pentaerythrite especially, adding of these two kinds of compositions not only can make product have certain viscosity, and can obtain good contact between product and fabric, plays the effect increasing effect of impregnation.
(3) fabric ANTIPILLING softener of the present invention, has the effect of antibacterial, ventilative, good springiness and comfortable moisture absorption.
(4) fabric ANTIPILLING softener of the present invention, its preparation method is simple, is easy to suitability for industrialized production.
Detailed description of the invention
Below in conjunction with embodiment, the present invention is further illustrated.
Embodiment 1
(1) mean molecule quantity be 1000 polyvinyl alcohol 15kg, pentaerythrite 5kg, methyl acrylate 4kg, disodium ethylene diamine tetraacetate 2kg, poly-methyl cyclotetrasiloxane 0.8kg, dodecyl sodium sulfate 0.5kg, dimethyl silicone polymer two quaternary amine 0.5kg and deionized water 110kg;
(2) said components is mixed, add lemon acid for adjusting pH to 5.5, filter with 100 mesh filter screens, obtained fabric ANTIPILLING softener.
Embodiment 2
(1) mean molecule quantity be 2500 polyvinyl alcohol 15kg, pentaerythrite 5kg, methyl acrylate 4kg, disodium ethylene diamine tetraacetate 2kg, poly-methyl cyclotetrasiloxane 0.8kg, dodecyl sodium sulfate 0.5kg, dimethyl silicone polymer two quaternary amine 0.5kg and deionized water 110kg;
(2) said components is mixed, add lemon acid for adjusting pH to 5.5, filter with 100 mesh filter screens, obtained fabric ANTIPILLING softener.
Embodiment 3
(1) mean molecule quantity be 2500 polyvinyl alcohol 20kg, pentaerythrite 7kg, methyl acrylate 7kg, disodium ethylene diamine tetraacetate 3kg, poly-methyl cyclotetrasiloxane 1.4kg, dodecyl sodium sulfate 2kg, dimethyl silicone polymer two quaternary amine 1kg, deionized water 120kg;
(2) said components is mixed, add lemon acid for adjusting pH to 6, filter with 200 mesh filter screens, obtained fabric ANTIPILLING softener.
Embodiment 4
(1) mean molecule quantity be 2500 polyvinyl alcohol 20kg, pentaerythrite 7kg, methyl acrylate 4kg, disodium ethylene diamine tetraacetate 2kg, poly-methyl cyclotetrasiloxane 1kg, dodecyl sodium sulfate 2kg, dimethyl silicone polymer two quaternary amine 1kg and deionized water 110kg;
(2) said components is mixed, add lemon acid for adjusting pH to 6, filter with 200 mesh filter screens, obtained fabric ANTIPILLING softener.
Embodiment 5
(1) mean molecule quantity be 2000 polyvinyl alcohol 18kg, pentaerythrite 6kg, methyl acrylate 5kg, disodium ethylene diamine tetraacetate 3kg, poly-methyl cyclotetrasiloxane 1kg, dodecyl sodium sulfate 1kg, dimethyl silicone polymer two quaternary amine 0.8kg, deionized water 115kg and toner 1kg;
(2) said components is mixed, add lemon acid for adjusting pH to 5.5, filter with 100 mesh filter screens, obtained fabric ANTIPILLING softener.
By the fabric of embodiment 1-5 ANTIPILLING softener, add wool fibre, after being dried by wool fibre, the concrete condition recording wool textile electrostatic half-life according to GB18401-2010 asks for an interview table 1.
Table 1
The invention is not restricted to embodiment here, those skilled in the art, according to announcement of the present invention, do not depart from improvement that scope makes and amendment all should within protection scope of the present invention.
Claims (5)
1. a novel fabric ANTIPILLING softener, is characterized in that, is made up of the component comprising following weight portion:
Polyvinyl alcohol 15-20 part,
Pentaerythrite 5-7 part,
Methyl acrylate 4-7 part,
Disodium ethylene diamine tetraacetate 2-3 part,
Poly-methyl cyclotetrasiloxane 0.8-1.4 part,
Dodecyl sodium sulfate 0.5-2 part,
Dimethyl silicone polymer two quaternary amine 0.5-1 part,
Deionized water 110-120 part.
2. novel fabric ANTIPILLING softener according to claim 1, is characterized in that, described component also comprises toner 0-1 weight portion.
3. novel fabric ANTIPILLING softener according to claim 1, is characterized in that, the mean molecule quantity of described polyvinyl alcohol is 1000-2500.
4. a novel fabric preparation method for ANTIPILLING softener, it is characterized in that, the method comprises the following steps:
(1) polyvinyl alcohol 15-20 weight portion, pentaerythrite 5-7 weight portion, methyl acrylate 4-7 weight portion, disodium ethylene diamine tetraacetate 2-3 weight portion, poly-methyl cyclotetrasiloxane 0.8-1.4 weight portion, dodecyl sodium sulfate 0.5-2 weight portion, dimethyl silicone polymer two quaternary amine 0.5-1 weight portion, deionized water 110-120 weight portion and toner 0-1 weight portion;
(2) said components is mixed, regulate pH to 5.5-6, filter with 100-200 mesh filter screen, obtained fabric ANTIPILLING softener.
5. the preparation method of novel fabric ANTIPILLING softener according to claim 4, is characterized in that, regulates pH to be by adding citric acid described in step 2.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201410815749.1A CN104480716B (en) | 2014-12-24 | 2014-12-24 | A kind of fabric anti pilling softener and preparation method thereof |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201410815749.1A CN104480716B (en) | 2014-12-24 | 2014-12-24 | A kind of fabric anti pilling softener and preparation method thereof |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| CN104480716A true CN104480716A (en) | 2015-04-01 |
| CN104480716B CN104480716B (en) | 2016-11-02 |
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Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
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| CN201410815749.1A Active CN104480716B (en) | 2014-12-24 | 2014-12-24 | A kind of fabric anti pilling softener and preparation method thereof |
Country Status (1)
| Country | Link |
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| CN (1) | CN104480716B (en) |
Cited By (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN105350333A (en) * | 2015-12-07 | 2016-02-24 | 常熟市永新印染有限公司 | Real silk fabric after finishing process |
| CN106480717A (en) * | 2016-10-13 | 2017-03-08 | 无锡市华诚印染剂厂 | Anti pilling fabric softener |
| CN109440467A (en) * | 2018-10-11 | 2019-03-08 | 苏州市职业大学 | A kind of finishing agent and preparation method thereof and application method preventing embroidery fluffing |
| CN112252040A (en) * | 2020-11-03 | 2021-01-22 | 上海锐鲨高新材料有限公司 | Antibacterial fluffy softening agent for fabric and preparation method thereof |
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| CN101935949A (en) * | 2010-08-27 | 2011-01-05 | 上海制皂有限公司 | Clothes softener |
| WO2011101857A2 (en) * | 2010-02-19 | 2011-08-25 | Khandelwal, Sanjeev | Multifunctional textile |
| CN103643484A (en) * | 2013-11-22 | 2014-03-19 | 江苏波波熊纺织品有限公司 | Knitted fabric anti-pilling finishing agent and preparation method thereof |
| CN103669000A (en) * | 2013-11-22 | 2014-03-26 | 南通市通州区川姜镇盛世王朝家用纺织品设计工作室 | Antistatic garment softener and preparation method thereof |
| CN103866567A (en) * | 2012-12-11 | 2014-06-18 | 罗莱家纺股份有限公司 | Pilling resistant liquid, and method for improving pilling of woven cotton fabric |
| CN104088143A (en) * | 2014-07-16 | 2014-10-08 | 上海制皂(集团)如皋有限公司 | Woolen clothes softening agent and preparation method thereof |
-
2014
- 2014-12-24 CN CN201410815749.1A patent/CN104480716B/en active Active
Patent Citations (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| WO2011101857A2 (en) * | 2010-02-19 | 2011-08-25 | Khandelwal, Sanjeev | Multifunctional textile |
| CN101935949A (en) * | 2010-08-27 | 2011-01-05 | 上海制皂有限公司 | Clothes softener |
| CN103866567A (en) * | 2012-12-11 | 2014-06-18 | 罗莱家纺股份有限公司 | Pilling resistant liquid, and method for improving pilling of woven cotton fabric |
| CN103643484A (en) * | 2013-11-22 | 2014-03-19 | 江苏波波熊纺织品有限公司 | Knitted fabric anti-pilling finishing agent and preparation method thereof |
| CN103669000A (en) * | 2013-11-22 | 2014-03-26 | 南通市通州区川姜镇盛世王朝家用纺织品设计工作室 | Antistatic garment softener and preparation method thereof |
| CN104088143A (en) * | 2014-07-16 | 2014-10-08 | 上海制皂(集团)如皋有限公司 | Woolen clothes softening agent and preparation method thereof |
Cited By (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN105350333A (en) * | 2015-12-07 | 2016-02-24 | 常熟市永新印染有限公司 | Real silk fabric after finishing process |
| CN106480717A (en) * | 2016-10-13 | 2017-03-08 | 无锡市华诚印染剂厂 | Anti pilling fabric softener |
| CN109440467A (en) * | 2018-10-11 | 2019-03-08 | 苏州市职业大学 | A kind of finishing agent and preparation method thereof and application method preventing embroidery fluffing |
| CN109440467B (en) * | 2018-10-11 | 2021-05-04 | 苏州市职业大学 | Finishing agent for preventing embroidery from fluffing and preparation method and using method thereof |
| CN112252040A (en) * | 2020-11-03 | 2021-01-22 | 上海锐鲨高新材料有限公司 | Antibacterial fluffy softening agent for fabric and preparation method thereof |
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| Publication number | Publication date |
|---|---|
| CN104480716B (en) | 2016-11-02 |
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| C41 | Transfer of patent application or patent right or utility model | ||
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Inventor after: Zhang Xinxing Inventor before: Shen Xuyuan |
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Effective date of registration: 20160902 Address after: 362417 Quanzhou province Anxi County Peach boat Township, South pit street, No. 19 Applicant after: Zhang Xinxing Address before: 313026 Zhejiang Province, Huzhou city Nanxun District Hefu town re trillion Industrial Park Applicant before: Huzhou Linghu Zhongzhao Jinhui Silk Weaving Factory |
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Inventor after: Yin Shuangquan Inventor before: Zhang Xinxing |
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Effective date of registration: 20170407 Address after: 510635 Guangdong province Guangzhou Science City, Guangzhou hi tech Industrial Development Zone, No. 31 Southern China Ke Feng Lu Park G7 building materials innovation No. 109 (to plant) Patentee after: Guangzhou Asahi Mstar Technology Ltd Address before: 362417 Quanzhou province Anxi County Peach boat Township, South pit street, No. 19 Patentee before: Zhang Xinxing |
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