CN104695229B - A kind of fabric inorganic agent and preparation method thereof - Google Patents
A kind of fabric inorganic agent and preparation method thereof Download PDFInfo
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- CN104695229B CN104695229B CN201510099180.8A CN201510099180A CN104695229B CN 104695229 B CN104695229 B CN 104695229B CN 201510099180 A CN201510099180 A CN 201510099180A CN 104695229 B CN104695229 B CN 104695229B
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- inorganic agent
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- polyethylene glycol
- methylisothiazolinone
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Abstract
The invention discloses a kind of fabric inorganic agent and preparation method thereof.This fabric inorganic agent, is made up of the component comprising following weight portion: Polyethylene Glycol 25 42 parts, Acidic phosphates ethylene oxidic ester 35 parts, 0.5 2 parts of EDTA tetra-sodium, propyl hydroxybenzoate 1.5 1.8 parts, hydroxypropyl starch sodium phosphate 24 parts, Methylisothiazolinone 0.8 1.8 parts, organic acid 0.05 0.9 parts, polyvinylpyrrolidone 0.5 1 parts and 95 105 parts of water.Present invention also offers the preparation method of above-mentioned fabrics inorganic agent.
Description
Technical field
The invention belongs to inorganic agent field, particularly to a kind of fabric inorganic agent and preparation method thereof.
Background technology
Countries in the world all using development new material as developing the economy, the importance of Promote Technology, various Novel Spinnings
Textured fiber becomes the important materials of current high-tech sector.
Fiber be a class extensively by people's favorable comment with by the most well-established material, mainly because the intensity of its fiber is high, elongation
Ability is big, and particularly resist bending torsional fatigue tired, resistance to is good with wearability.But fabric is worn in reality, is used and washed
Cheng Zhong, constant is rubbed, thus fluff, balling-up, make the fiber of fabric face be exposed to fabric, if the fiber exposed exists
Can not come off in time in continuing to wear, with regard to mutual tied up in knots, be kneaded into many spherical granules, commonly referred to balling-up, balling-up
Then can affect the aesthetic feeling of outward appearance.
Chinese patent CN 1553978A discloses a kind of fabric-treating agent, comprises a kind of aqueous dispersion, this aqueous dispersion master
Will be made up of the polyurethane of a kind of closing and a kind of hydrophobic solvent, the inorganic agent prepared the most still has good stablizing
Property, make the textile processed through the fabric-treating agent of the present invention possess feel and the resistance to contractility of improvement of softness.
Summary of the invention
For above-mentioned demand, it is an object of the invention to provide a kind of fabric inorganic agent and preparation method thereof.
The purpose of the present invention can be achieved through the following technical solutions:
A kind of fabric inorganic agent, is made up of the component comprising following weight portion:
Described organic acid is lauric acid or myristic acid.
The mean molecule quantity of described Polyethylene Glycol is 1200-2000.
A kind of preparation method of fabric inorganic agent, the method comprises the following steps:
(1) by Polyethylene Glycol 25-42 part, Acidic phosphates ethylene oxidic ester 3-5 part, EDTA tetra-sodium 0.5-2 part, oxybenzene third
Ester 1.5-1.8 part, hydroxypropyl starch sodium phosphate 2-4 part, Methylisothiazolinone 0.8-1.8 part, polyvinylpyrrolidone 0.5-1
Part mix homogeneously, adds ultrafine crusher, sieves;
(2) add organic acid 0.05-0.9 part and water 95-105 part, after mix homogeneously, at 90-100 DEG C, stir 20-25
Minute, obtain fabric inorganic agent.
The described screen cloth sieved is 200 mesh.
Compared with prior art, beneficial effects of the present invention:
(1) textile fiber material of the present invention add Acidic phosphates ethylene oxidic ester, hydroxypropyl starch sodium phosphate and
Methylisothiazolinone, prepared fibrous material has good processability, and mechanical strength is high.
(2) textile fiber material of the present invention, its preparation method is simple, it is easy to industrialized production.
Detailed description of the invention
Below in conjunction with embodiment, the present invention is further illustrated.
Embodiment 1
(1) by Polyethylene Glycol 25kg that mean molecule quantity is 1200, Acidic phosphates ethylene oxidic ester 3kg, EDTA tetra-sodium
0.5kg, propyl hydroxybenzoate 1.5kg, hydroxypropyl starch sodium phosphate 2kg, Methylisothiazolinone 0.8kg, polyvinylpyrrolidone
0.5kg mix homogeneously, adds ultrafine crusher, sieves;
(2) add lauric acid 0.05kg and water 95kg, after mix homogeneously, stir 20 minutes at 90 DEG C, obtain fabric and use
Inorganic agent.
The performance test results preparing fabric inorganic agent is as shown in table 1.
Embodiment 2
(1) by Polyethylene Glycol 25kg that mean molecule quantity is 2000, Acidic phosphates ethylene oxidic ester 3kg, EDTA tetra-sodium
0.5kg, propyl hydroxybenzoate 1.5kg, hydroxypropyl starch sodium phosphate 2kg, Methylisothiazolinone 0.8kg, polyvinylpyrrolidone
0.5kg mix homogeneously, adds ultrafine crusher, sieves;
(2) add lauric acid 0.05kg and water 95kg, after mix homogeneously, stir 20 minutes at 90 DEG C, obtain fabric and use
Inorganic agent.
The performance test results preparing fabric inorganic agent is as shown in table 1.
Embodiment 3
(1) by Polyethylene Glycol 42kg that mean molecule quantity is 2000, Acidic phosphates ethylene oxidic ester 5kg, EDTA tetra-sodium
2kg, propyl hydroxybenzoate 1.8kg, hydroxypropyl starch sodium phosphate 4kg, Methylisothiazolinone 1.8kg, polyvinylpyrrolidone 1kg mix
Close uniformly, add ultrafine crusher, sieve;
(2) add myristic acid 0.9kg and water 105kg, after mix homogeneously, stir 25 minutes at 100 DEG C, obtain fabric
Use inorganic agent.
The performance test results preparing fabric inorganic agent is as shown in table 1.
Embodiment 4
(1) by Polyethylene Glycol 25kg that mean molecule quantity is 2000, Acidic phosphates ethylene oxidic ester 3kg, EDTA tetra-sodium
2kg, propyl hydroxybenzoate 1.8kg, hydroxypropyl starch sodium phosphate 4kg, Methylisothiazolinone 1.8kg, polyvinylpyrrolidone 1kg mix
Close uniformly, add ultrafine crusher, sieve;
(2) add myristic acid 0.9kg and water 105kg, after mix homogeneously, stir 25 minutes at 100 DEG C, obtain fabric
Use inorganic agent.
The performance test results preparing fabric inorganic agent is as shown in table 1.
Embodiment 5
(1) by Polyethylene Glycol 30kg that mean molecule quantity is 1800, Acidic phosphates ethylene oxidic ester 4kg, EDTA tetra-sodium
1kg, propyl hydroxybenzoate 1.5kg, hydroxypropyl starch sodium phosphate 3kg, Methylisothiazolinone 1kg, polyvinylpyrrolidone 0.8kg mix
Close uniformly, add ultrafine crusher, sieve;
(2) add myristic acid 0.1kg and water 105kg, after mix homogeneously, stir 25 minutes at 100 DEG C, obtain fabric and use
Inorganic agent.
The performance test results preparing fabric inorganic agent is as shown in table 1.
Embodiment 6
(1) by Polyethylene Glycol 25kg that mean molecule quantity is 1200, Acidic phosphates ethylene oxidic ester 3kg, EDTA tetra-sodium
2kg, propyl hydroxybenzoate 1.5kg, hydroxypropyl starch sodium phosphate 4kg, Methylisothiazolinone 1.8kg, polyvinylpyrrolidone 1kg mix
Close uniformly, add ultrafine crusher, filter with 200 eye mesh screens;
(2) add myristic acid 0.4kg and water 100kg, after mix homogeneously, stir 22 minutes at 95 DEG C, obtain fabric
Use inorganic agent.
The performance test results preparing fabric inorganic agent is as shown in table 1.
Comparative example
By Polyethylene Glycol 30kg, tristerin 3kg, EDTA tetra-sodium 2kg and polyvinylpyrrolidone 1kg mixing all
Even, add ultrafine crusher, filter with 200 eye mesh screens;Add citric acid 0.4kg and water 100kg, after mix homogeneously, at 95 DEG C
Lower stirring 22 minutes, obtains fabric inorganic agent.
Table 1
Claims (1)
1. a fabric inorganic agent, it is characterised in that be made up of the component comprising following weight portion:
Polyethylene Glycol 25-42 part,
Acidic phosphates ethylene oxidic ester 3-5 part,
Hydroxypropyl starch sodium phosphate 2-4 part,
Propyl hydroxybenzoate 1.5-1.8 part,
Methylisothiazolinone 0.8-1.8 part,
EDTA tetra-sodium 0.5-2 part,
Polyvinylpyrrolidone 0.5-1 part,
Organic acid 0.05-0.9 part,
Water 95-105 part;
Described organic acid is lauric acid or myristic acid;
The mean molecule quantity of described Polyethylene Glycol is 1200-2000;
Described a kind of fabric inorganic agent is prepared by following preparation method:
(1) by Polyethylene Glycol 25-42 part, Acidic phosphates ethylene oxidic ester 3-5 part, EDTA tetra-sodium 0.5-2 part, propyl hydroxybenzoate
1.5-1.8 part, hydroxypropyl starch sodium phosphate 2-4 part, Methylisothiazolinone 0.8-1.8 part, polyvinylpyrrolidone 0.5-1 part
Mix homogeneously, adds ultrafine crusher, sieves;
(2) add organic acid 0.05-0.9 part and water 95-105 part, after mix homogeneously, stir 20-25 minute at 90-100 DEG C,
Obtain fabric inorganic agent;
The described screen cloth sieved is 200 mesh.
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CN104695229A CN104695229A (en) | 2015-06-10 |
CN104695229B true CN104695229B (en) | 2017-01-04 |
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CN110106691A (en) * | 2019-05-28 | 2019-08-09 | 苏州凯美斯化学材料有限公司 | A kind of environmentally friendly nylon yarn desizing agent |
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US2853451A (en) * | 1955-03-04 | 1958-09-23 | Celanese Corp | Lubricating agents |
CN103668975A (en) * | 2012-09-21 | 2014-03-26 | 青岛道合生物科技有限公司 | Rot resistant finishing agent special for textiles |
CN103981713B (en) * | 2014-05-21 | 2016-08-17 | 吴江市英力达塑料包装有限公司 | A kind of fabric maintenance softener and preparation method thereof |
CN104294600A (en) * | 2014-10-20 | 2015-01-21 | 苏州富美纺织科技有限公司 | Ultraviolet-protective finishing agent for fabrics |
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Effective date of registration: 20200519 Address after: 215200 east side of Weiming village, FenHu high tech Industrial Development Zone, Suzhou City, Jiangsu Province Patentee after: Suzhou ed home furnishing Co., Ltd Address before: Wujiang District of Suzhou City, Jiangsu province 215200 Song Ling Zhen Heng Shan Bridge Road Patentee before: SUZHOU AILIFANG CLOTHING Co.,Ltd. |
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