CN103619754B - 制备二氢二氰基硼酸盐的方法 - Google Patents

制备二氢二氰基硼酸盐的方法 Download PDF

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Publication number
CN103619754B
CN103619754B CN201280026802.9A CN201280026802A CN103619754B CN 103619754 B CN103619754 B CN 103619754B CN 201280026802 A CN201280026802 A CN 201280026802A CN 103619754 B CN103619754 B CN 103619754B
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China
Prior art keywords
atoms
branched
linear
substituted
formula
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Expired - Fee Related
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CN201280026802.9A
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English (en)
Chinese (zh)
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CN103619754A (zh
Inventor
N·(M)·艾格纳缇弗
M·舒尔特
E·波恩哈特
V·波恩哈特-皮彻欧吉纳
H·威尔纳
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Merck Patent GmbH
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Merck Patent GmbH
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Publication of CN103619754A publication Critical patent/CN103619754A/zh
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Expired - Fee Related legal-status Critical Current
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Classifications

    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07F—ACYCLIC, CARBOCYCLIC OR HETEROCYCLIC COMPOUNDS CONTAINING ELEMENTS OTHER THAN CARBON, HYDROGEN, HALOGEN, OXYGEN, NITROGEN, SULFUR, SELENIUM OR TELLURIUM
    • C07F5/00—Compounds containing elements of Groups 3 or 13 of the Periodic Table
    • C07F5/02—Boron compounds
    • C07F5/027—Organoboranes and organoborohydrides
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B6/00—Hydrides of metals including fully or partially hydrided metals, alloys or intermetallic compounds ; Compounds containing at least one metal-hydrogen bond, e.g. (GeH3)2S, SiH GeH; Monoborane or diborane; Addition complexes thereof
    • C01B6/06—Hydrides of aluminium, gallium, indium, thallium, germanium, tin, lead, arsenic, antimony, bismuth or polonium; Monoborane; Diborane; Addition complexes thereof
    • C01B6/10—Monoborane; Diborane; Addition complexes thereof
    • C01B6/13—Addition complexes of monoborane or diborane, e.g. with phosphine, arsine or hydrazine
    • C01B6/15—Metal borohydrides; Addition complexes thereof
    • C01B6/19—Preparation from other compounds of boron
    • C01B6/21—Preparation of borohydrides of alkali metals, alkaline earth metals, magnesium or beryllium; Addition complexes thereof, e.g. LiBH4.2N2H4, NaB2H7
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B35/00—Boron; Compounds thereof
    • C01B35/08—Compounds containing boron and nitrogen, phosphorus, oxygen, sulfur, selenium or tellurium
    • C01B35/10—Compounds containing boron and oxygen
    • C01B35/12—Borates
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B35/00—Boron; Compounds thereof
    • C01B35/08—Compounds containing boron and nitrogen, phosphorus, oxygen, sulfur, selenium or tellurium
    • C01B35/10—Compounds containing boron and oxygen
    • C01B35/12—Borates
    • C01B35/121—Borates of alkali metal
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B35/00—Boron; Compounds thereof
    • C01B35/08—Compounds containing boron and nitrogen, phosphorus, oxygen, sulfur, selenium or tellurium
    • C01B35/14—Compounds containing boron and nitrogen, phosphorus, sulfur, selenium or tellurium
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B35/00—Boron; Compounds thereof
    • C01B35/08—Compounds containing boron and nitrogen, phosphorus, oxygen, sulfur, selenium or tellurium
    • C01B35/14—Compounds containing boron and nitrogen, phosphorus, sulfur, selenium or tellurium
    • C01B35/146—Compounds containing boron and nitrogen, e.g. borazoles
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01C—AMMONIA; CYANOGEN; COMPOUNDS THEREOF
    • C01C3/00—Cyanogen; Compounds thereof
    • C01C3/08—Simple or complex cyanides of metals
    • C01C3/11—Complex cyanides
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
    • C01P2002/00—Crystal-structural characteristics
    • C01P2002/80—Crystal-structural characteristics defined by measured data other than those specified in group C01P2002/70
    • C01P2002/86—Crystal-structural characteristics defined by measured data other than those specified in group C01P2002/70 by NMR- or ESR-data

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  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Inorganic Chemistry (AREA)
  • Health & Medical Sciences (AREA)
  • General Health & Medical Sciences (AREA)
  • Toxicology (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • General Life Sciences & Earth Sciences (AREA)
  • Geology (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
  • Pyridine Compounds (AREA)
CN201280026802.9A 2011-05-31 2012-05-23 制备二氢二氰基硼酸盐的方法 Expired - Fee Related CN103619754B (zh)

Applications Claiming Priority (3)

Application Number Priority Date Filing Date Title
DE102011103754A DE102011103754A1 (de) 2011-05-31 2011-05-31 Verfahren zur Herstellung von Dihydridodicyanoborat-Salzen
DE102011103754.7 2011-05-31
PCT/EP2012/002178 WO2012163488A1 (de) 2011-05-31 2012-05-23 Verfahren zur herstellung von dihydridodicyanoborat-salzen

Publications (2)

Publication Number Publication Date
CN103619754A CN103619754A (zh) 2014-03-05
CN103619754B true CN103619754B (zh) 2016-01-20

Family

ID=46172763

Family Applications (1)

Application Number Title Priority Date Filing Date
CN201280026802.9A Expired - Fee Related CN103619754B (zh) 2011-05-31 2012-05-23 制备二氢二氰基硼酸盐的方法

Country Status (7)

Country Link
US (1) US8927714B2 (enExample)
EP (1) EP2714586B1 (enExample)
JP (1) JP2014518888A (enExample)
KR (1) KR20140043908A (enExample)
CN (1) CN103619754B (enExample)
DE (1) DE102011103754A1 (enExample)
WO (1) WO2012163488A1 (enExample)

Families Citing this family (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
DE102013009959A1 (de) 2013-06-14 2014-12-31 Julius-Maximilians-Universität Würzburg Verfahren zur Herstellung von Salzen mit Hydridocyanoborat-Anionen
DE102014008131A1 (de) 2014-06-06 2015-12-17 Julius-Maximilians-Universität Würzburg Verfahren zur Herstellung von Salzen mit Monoydridocyanoborat-Anionen
DE102014011089A1 (de) 2014-07-30 2016-02-04 Julius-Maximilians-Universität Würzburg Verfahren zur Herstellung von Salzen mit Hydridocyanoborat-Anionen
DE102014016681A1 (de) 2014-11-12 2016-05-12 Julius-Maximilians-Universität Würzburg Verfahren zur Herstellung von Salzen mit Hydridocyanoborat-Anionen
DE102016009846A1 (de) 2016-08-16 2018-02-22 Julius-Maximilians-Universität Würzburg Fluoralkylhydrido- und Fluoralkylcyanohydridoborate

Family Cites Families (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CA978980A (en) 1969-06-16 1975-12-02 Ventron Corporation Solvated cyanoborohydrides and method for the preparation thereof
US3697232A (en) 1969-06-16 1972-10-10 Ventron Corp Preparation of potassium cyanoborohydride
DE10306617A1 (de) * 2003-02-14 2004-08-26 Merck Patent Gmbh Salze mit Cyanoborat-Anionen
JPWO2008102661A1 (ja) 2007-02-03 2010-05-27 東洋化成工業株式会社 トリアルキルシリルニトリルの製造方法
US9243013B2 (en) * 2008-08-22 2016-01-26 Nippon Shokubai Co., Ltd. Ionic compound, method for producing the same, and ion-conductive material comprising the same

Non-Patent Citations (2)

* Cited by examiner, † Cited by third party
Title
"Preparation and properties of novel cyano and isocyano derivatives of borane and the tetrahydroborate anion";Bela Gyori et al.;《Journal of Organometallic Chemistry》;19831231;第255卷;第17-28页 *
"Synthesis of Sodium and Tetra-n-butylammonium Dicyanodihydroborates";Bernard F. Spielvogel et al.;《Inorganic chemistry》;19841231;第23卷(第20期);第3263－3265页 *

Also Published As

Publication number Publication date
EP2714586A1 (de) 2014-04-09
WO2012163488A1 (de) 2012-12-06
US8927714B2 (en) 2015-01-06
US20140114074A1 (en) 2014-04-24
CN103619754A (zh) 2014-03-05
DE102011103754A1 (de) 2012-12-06
EP2714586B1 (de) 2015-07-22
KR20140043908A (ko) 2014-04-11
JP2014518888A (ja) 2014-08-07

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Granted publication date: 20160120

Termination date: 20170523

CF01 Termination of patent right due to non-payment of annual fee