CN103553731B - Organic compound foliage fertilizer and preparation method thereof - Google Patents
Organic compound foliage fertilizer and preparation method thereof Download PDFInfo
- Publication number
- CN103553731B CN103553731B CN201310545137.0A CN201310545137A CN103553731B CN 103553731 B CN103553731 B CN 103553731B CN 201310545137 A CN201310545137 A CN 201310545137A CN 103553731 B CN103553731 B CN 103553731B
- Authority
- CN
- China
- Prior art keywords
- foliage fertilizer
- amino acid
- organic compound
- compound
- preparation
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired - Fee Related
Links
Abstract
The invention discloses an organic compound foliage fertilizer and a preparation method thereof. The preparation method comprises the steps of preparing compound amino acid from kitchen wastes through adopting a sulfuric acid hydrolysis method, preparing a nicotine extract from waste tobacco leaves through adopting a hydrochloric acid extraction method, and mixing the compound amino acid with the nicotine extract according to different proportions, wherein the mass proportion of the compound amino acid to the nicotine extract is (1:0.5)-(1:1.5). The organic compound foliage fertilizer is beneficial to promoting the germination of Chinese cabbage seeds and improving the germination rate and germination index; the organic compound foliage fertilizer can obviously promote the growth of leaf mustards and improve the production and quality of the leaf mustards; the organic compound foliage fertilizer plays a role in well promoting the growth of swamp cabbages; the organic compound foliage fertilizer can enhance the resistance of bitter gourds, and relieve the diseases and pests, thus being a desirable foliage fertilizer for producing green food.
Description
Technical field
The invention belongs to organic fertilizer field, be specifically related to a kind of Organic compound foliage fertilizer and preparation method thereof.
Background technology
Kitchen castoff, refers to the waste products produced in human diet process.Kitchen castoff is primarily of remaining discarded object and food processing discarded object two parts form after the meal.After the meal remaining discarded object refer to the mankind have dinner after the remnants that abandon, comprise and again the grease of processing and eating and profit can not mix thing in a large number; Food processing discarded object refers to the waste material produced before and after food processing process.In China, kitchen castoff is the main component in municipal refuse.Kitchen castoff moisture content is higher, easily rots and distributes dense stink, having a strong impact on social environment health.But kitchen castoff chemically composition is analyzed, containing a large amount of organic substances, and containing abundant trace element, have nutrient various, reclaim the high advantage of value added again.According to correlative study analysis, in the organic waste of meal kitchen, 85.3% is moisture; About have 1/4 after kitchen castoff drying for crude fat, total energy level reaches 20 MJ/kg, and crude protein accounts for 1/4, is two times of corn.As can be seen here, kitchen castoff has good recycling meaning.Have their own characteristics each for kitchen castoff recovery and reuse technology mode and means in current global range, comprising landfill method, burning disposal, anaerobic fermentation biogas, fodder, machine process, biological treatment composting material.Biological treatment refers to necessarily artificially under operating condition, utilizing relevant microorganism species, is dried by kitchen castoff residue and pulverizes, and uses some specific disposal options to form fertilizer.The organic fertilizer prepared by biological treatment mode has can provide multiple nutrients material, uses the advantages such as convenient, is the fertilizer that peasant's acceptance is higher instantly.Renewable resource in kitchen castoff makes full use of by the mode therefore seeking to be applicable to, and both can protect human ecological environment, saves social resources, can make full use of again the value of kitchen castoff, create certain economic benefit.
China is tobacco planting big country, annual yield of tobacco about 2,500,000 tons, but has the leftover bits and pieces of about 1/4 to be dropped, serious environment pollution.Comprise a lot of different chemical composition in tobacco, determined at present and comprised about 300 kinds of materials such as nicotine, protein.And protein and nicotine are the main matter that can recycle.Therefore be nowadays that protein is separated with the lixiviate of nicotine to the recycling major way of tobacco leaf discarded object; other recycling mode and technology are still weaker; so pay attention to the research of the recycling of waste tobacco leaf resource; not only tobacco waste can be turned waste into wealth; also can be increase economic benefit; protection of the environment, has important practical significance.
Summary of the invention
The object of the invention is to, for the recycling present situation of kitchen castoff, tobacco leaf discarded object, provide a kind of Organic compound foliage fertilizer and preparation method thereof.The present invention, by materials such as extraction nicotines from waste tobacco leaf, prepares compound amino acid, carries out compatibility by different proportion, make Organic compound foliage fertilizer from kitchen castoff.From environmental protection and economic benefit, there is double meaning.
For achieving the above object, the present invention adopts following technical scheme:
A kind of Organic compound foliage fertilizer, the quality proportioning consisting of compound amino acid and nicotine extract is: 1:0.5 ~ 1:1.5; Described compound amino acid is obtained from kitchen castoff through sulphuric acid hydrolysis; Described nicotine extract is obtained from waste tobacco leaf through lixiviation method.
The quality proportioning of compound amino acid and nicotine extract is: 1:1.
The preparation method of described a kind of Organic compound foliage fertilizer, comprises the following steps:
(1) preparation of compound amino acid: take 100g through the kitchen castoff sample of drying, pulverize, adds sulfuric acid solution 350 mL ~ 550 mL that mass fraction is 20% ~ 45%, adds a small amount of zeolite, stir, at 85 DEG C ~ 100 DEG C hydrolysis 8 ~ 12h.After hydrolysis terminates, be cooled to room temperature.Hydrolyzate mass fraction is the Ca (OH) of 30%
2it is 7 that solution is neutralized to pH value, filters, the impurity removed calcium sulfate and be not hydrolyzed, and gained filtrate is Moriamin S, and in the insulating box of rearmounted 45 ~ 50 DEG C of evaporation and concentration, dry 3 ~ 5 h, obtain compounded amino acid product.
(2) preparation of nicotine extract: take waste tobacco leaf 20g and move in the volumetric flask of 250ml, add hydrochloric acid solution 150 ~ 200 ml that mass concentration is 0.03 ~ 0.05g/ml, after fully shaking up concussion 10min, put into the water bath with thermostatic control of 70 ~ 85 DEG C, lixiviate 0.5 ~ 1.5h.After lixiviate terminates, regulate solution ph to be 7, filter with the sodium hydroxide solution that mass concentration is 0.04g/ml, filtrate is dry 3 ~ 5 h in the insulating box of rearmounted 45 ~ 50 DEG C of evaporation and concentration, obtain nicotine extract.
(3) compound amino acid and nicotine extract compatibility: compatibility compound amino acid and nicotine extract being carried out different proportion, according to the impact of different compatibility foliage fertilizer solution on germination rate of vegetable seeds and germination index, filters out Organic compound foliage fertilizer formula.
Beneficial effect of the present invention is: Organic compound foliage fertilizer provided by the invention, is conducive to promoting pakchoi germination, improves germination percentage and germination index; The growth of leaf mustard can be promoted significantly, improve leaf mustard yield and quality.The present invention extracts the Organic compound foliage fertilizer prepared from kitchen castoff and waste tobacco leaf, is the desirable foliar fertilizer of pollution-free food production.From environmental protection and economic benefit, there is double meaning.
Accompanying drawing explanation
Fig. 1 is the impact that in embodiment 1, Organic compound foliage fertilizer is germinateed on pakchoi; In figure, filled squares represents germination index, and hollow triangle represents germination percentage.
Fig. 2 sprays the impact of variable concentrations Organic compound foliage fertilizer on leaf mustard plant height in embodiment 2.
Fig. 3 sprays the impact of variable concentrations Organic compound foliage fertilizer on mustard leaf number in embodiment 2.
Detailed description of the invention
The present invention's the following example further illustrates the present invention, but protection scope of the present invention is not limited to the following example.
Embodiment 1
1. the preparation of compound amino acid
Take 100g through the kitchen castoff sample of drying, pulverize, add sulfuric acid solution 550 mL that mass fraction is 20%, add 2-3g zeolite, stir, at 85 DEG C of hydrolysis 12h.After hydrolysis terminates, be cooled to room temperature.Hydrolyzate mass fraction is the Ca (OH) of 30%
2it is 7 that solution is neutralized to pH value, filters, and the impurity removed calcium sulfate and be not hydrolyzed, gained filtrate is Moriamin S, and in the insulating box of rearmounted 45 DEG C of evaporation and concentration, dry 5 h, obtain compounded amino acid product.
2. the preparation of nicotine extract
Take waste tobacco leaf 20g to move in the volumetric flask of 250ml, add hydrochloric acid solution 200 ml that mass concentration is 0.03g/ml, after fully shaking up concussion 10min, put into the water bath with thermostatic control of 70 DEG C, lixiviate 1.5h.After lixiviate terminates, regulate solution ph to be 7 with the sodium hydroxide solution that mass concentration is 0.04g/ml, filter, filtrate is dry 5 h in the insulating box of rearmounted 45 DEG C of evaporation and concentration, obtain nicotine extract.
3. the screening of organic foliage fertilizer formula
Nicotine extract prepared by the compound amino acid prepare kitchen castoff and waste tobacco leaf, carries out the compatibility of different proportion, according to the impact of different compatibility foliage fertilizer solution on germination rate of vegetable seeds and germination index, filters out the organic foliage fertilizer formulation of compound.
With pakchoi (the black leaf of short pin) seed for subjects, by the compound amino acid that extracts from kitchen castoff and the nicotine extract that extracts from waste tobacco leaf by different proportion compatibility, the germination percentage of observation pakchoi seed.Result shows, when compound amino acid and nicotine extract press 1:1.5,1:1 and 1:0.5 compatibility, pakchoi percentage of seedgermination result is respectively 85.30%, 92.50% and 89.60%; And in other ratio compatibilities, pakchoi percentage of seedgermination is all lower than 80%.Therefore, determine the quality proportioning 1:0.5 ~ 1:1.5 of compound amino acid and nicotine extract in Organic compound foliage fertilizer, wherein, preferably quality proportioning is 1:1.
4. Organic compound foliage fertilizer is for soaking pakchoi seed
With pakchoi (the black leaf of short pin) seed for subjects, control group (CK) is that clear water soaks, to be respectively quality proportioning that formula is compound amino acid and nicotine extract be that the dilution that the Organic compound foliage fertilizer of 1:1 dilutes 100 times, 300 times, 500 times, 700 times, 900 times soaks to test group.Test repetition 3 times.
Experimental procedure:
(1) first with the NaClO solution of 1% concentration, seed used for test, filter paper and culture dish are carried out sterilization processing;
(2) with the Organic compound foliage fertilizer dilution of variable concentrations, seed soaking is carried out to seed respectively, control group clear water process, soak seed 10 hours, respectively getting 20 seeds processed is laid in the culture dish of filter paper, and culture dish is placed in 25 DEG C of constant incubators the conventional vernalization carried out 48 hours, keep the skin wet in time in the training period, take a breath, and record chitting piece number;
(3), after vernalization is cultivated, average germination percentage and the germination index of seed in variable concentrations solution is added up.
Main mensuration project and method
Bud is long: measure with common ruler;
Germinative number: all directly observed afterwards at the 2nd day;
The softwares such as all data acquisition Excel, SPSS carry out processing and statistical analysis.
Interpretation:
Fig. 1 is the impact of compound organic foliar fertilizer on pakchoi percentage of seedgermination, and abscissa is the extension rate of Organic compound foliage fertilizer, and ordinate is germination percentage.Can as apparent from Fig. 1, the germination percentage and the germination index that soak pakchoi seed after Organic compound foliage fertilizer are all greater than clear water control group, illustrate that Organic compound foliage fertilizer can impel pakchoi seed to have better growth tendency and stronger vigor in the development stage, wherein may be relevant with certain nutriment promoting seed embryo blastogenesis long contained in Organic compound foliage fertilizer.Pakchoi seed dilute with compound organic foliar fertilizer 500 times soak germination percentages and germination index all the highest, germination percentage is 87%, and germination index is 92.44%, and significant difference.Although when diluting 100 times and 300 times of process germination percentage and germination index higher than the value of control group, difference is remarkable, and reason may be too large due to compound organic foliar fertilizer concentration, and some nutriment suppresses pakchoi germination.When diluting 700 times and 900 times of process germination percentage and germination index relatively high, also in significant difference, but effect is inferior to the process of 500 times of dilutions.So after utilizing compound organic foliar fertilizer to soak pakchoi seed, be conducive to promoting pakchoi germination, improve germination percentage and germination index, diluting 500 times by Organic compound foliage fertilizer, to soak effects best.
Embodiment 2
1. the preparation of compound amino acid
Take 100g through the kitchen castoff sample of drying, pulverize, add sulfuric acid solution 350 mL that mass fraction is 45%, add 2-3g zeolite, stir, at 100 DEG C of hydrolysis 8 h; After hydrolysis terminates, be cooled to room temperature; Hydrolyzate mass fraction is the Ca (OH) of 30%
2it is 7 that solution is neutralized to pH value, filters, the impurity removed calcium sulfate and be not hydrolyzed, and gained filtrate is Moriamin S, and in the insulating box of rearmounted 50 DEG C of evaporation and concentration, dry 3 h, obtain compounded amino acid product;
2. the preparation of nicotine extract
Take waste tobacco leaf 20g to move in the volumetric flask of 250ml, add hydrochloric acid solution 150 ml that mass concentration is 0.05g/ml, after fully shaking up concussion 10min, put into the water bath with thermostatic control of 85 DEG C, lixiviate 0.5h; After lixiviate terminates, regulate solution ph to be 7 with the sodium hydroxide solution that mass concentration is 0.04g/ml, filter, filtrate is dry 3 h in the insulating box of rearmounted 50 DEG C of evaporation and concentration, obtain nicotine extract;
3. the screening of organic foliage fertilizer formula
Nicotine extract prepared by the compound amino acid prepare kitchen castoff and waste tobacco leaf, carries out the compatibility of different proportion, according to the impact of different compatibility foliage fertilizer solution on germination rate of vegetable seeds and germination index, filters out the organic foliage fertilizer formulation of compound.
With pakchoi (the black leaf of short pin) for subjects, by the compound amino acid that extracts from kitchen castoff and the nicotine extract that extracts from waste tobacco leaf by different proportion compatibility, the germination percentage of observation pakchoi seed.Result shows, when compound amino acid and nicotine extract press 1:1.5,1:1 and 1:0.5 compatibility, pakchoi percentage of seedgermination result is respectively 86.30%, 93.00% and 88.60%; And in other ratio compatibilities, pakchoi percentage of seedgermination is all lower than 80%.Therefore, determine the quality proportioning 1:0.5 ~ 1:1.5 of compound amino acid and nicotine extract in Organic compound foliage fertilizer, wherein, preferably quality proportioning is 1:1.
4. Organic compound foliage fertilizer is used for leaf mustard
It is potted plant that this test with leaf mustard is that test material carries out, and every basin fills air-dry soil 6Kg, establishes 10 process altogether, 1 control group, 9 test group, and experiment repetition 3 times, selects the Organic compound foliage fertilizer of better quality proportioning 1:1.
Table 1 experimental design scheme
Table 2 is for the basic physicochemical character of examination soil
Sieved by soil after process, every basin applies 0.19g/kg urea and 0.25g/kg phosphorus element potassium dihydrogen makes base manure, and fertilizer and soil mix, dress basin, test basin random alignment.Then plant leaf mustard seedling, interval sprays once in 5 days, and with being sprayed onto blade face to having drop to drip when spraying, within first 10 days, stop spray fertile to gathering, all the other manage routinely.Gather after 30 days.Complete half an hour at 105 DEG C, fresh sample, then dry at 65 DEG C.
Test determination project and method:
Test determination project: leaf mustard individual plant plant yield, Vc content, nitrate content.
Test determination method: leaf mustard Vc content 2,6-dichloroindophenol titration; Nitrate content ultraviolet spectrophotometry.
All data all adopt the softwares such as Excel, SPSS to carry out processing and statistical analysis.
Interpretation:
(1) variable concentrations compound organic foliar fertilizer is sprayed on the impact of leaf mustard plant height
Fig. 2 abscissa is variable concentrations compound organic foliar fertilizer, and ordinate is leaf mustard plant height.As seen from Figure 2, be compared to clear water control treatment, the organic Foliar Spraying of variable concentrations compound is all significantly increased in leaf mustard plant height proterties, the plant height wherein processing spray 500 times 2 times is 32.245cm, plant height increases 49.98%, for the highest in all process, illustrate and spray the growth that compound organic foliar fertilizer can promote leaf mustard.
(2) impact of variable concentrations Organic compound foliage fertilizer on mustard leaf number is sprayed
Fig. 3 abscissa is variable concentrations compound organic foliar fertilizer, and ordinate is mustard leaf number.As can be seen from Figure 3, compared with control group, the blade spraying variable concentrations Organic compound foliage fertilizer leaf mustard there is no significant difference, about being mostly 5 blades.And compare from same concentrations different disposal, the process average leaf number spraying twice foliage fertilizer is all the highest, the average leaf number spraying three compound organic foliar fertilizers is all less slightly than spraying secondary, may be because Foliar Spraying amount increases, and does not continue the effect of the leaf growth promoting leaf mustard.Therefore, illustrate that compound organic Foliar Spraying secondary is the suitableeest.
(3) impact of Organic compound foliage fertilizer on leaf mustard output is sprayed
Table 3 sprays variable concentrations compound organic foliar fertilizer to the impact of leaf mustard output
Note: show significant difference (p<0.05) with different lowercase alphabet attached after column data, alphabetical identical table differential is different not significantly (p>0.05).
Can obviously be found out by table 3, after spraying compound organic foliar fertilizer, leaf mustard output significantly improves, and illustrates that this fertilizer can promote that leaf mustard grows, and improves leaf mustard output.Compare with control group, after spraying dilution 900 times of NEW TYPE OF COMPOSITE organic foliar fertilizers, leaf mustard output on average improves 3.8%, but difference is not remarkable, and the foliage fertilizer output average mark spraying dilution 500 times and dilution 700 times you can well imagine high 20.66% and 12.09%, significant difference.Leaf mustard sprays in variable concentrations NEW TYPE OF COMPOSITE organic foliar fertilizer, dilutes 500 times of foliage fertilizers the most remarkable for the output increased of leaf mustard, and in dilution 500 times of three different disposal.The output spraying twice is maximum, output is 39.52g, output recruitment is 29.74%, reason may be that NEW TYPE OF COMPOSITE organic foliar fertilizer contains the material promoting leaf mustard growth, for the growth of leaf mustard, there is good facilitation in certain concentration, and spraying after three times, the amount spraying foliage fertilizer increases, and the growth for leaf mustard there is no obvious facilitation effect.
(4) impact of compound organic foliar fertilizer on leaf mustard Vc, nitrate is sprayed
Table 4 sprays the impact of compound organic foliar fertilizer on leaf mustard Vc, nitrate
Note: show significant difference (p<0.05) with different lowercase alphabet attached after column data, alphabetical identical table differential is different not significantly (p>0.05).
Table 4 is that pot experiment sprays the impact of variable concentrations Organic compound foliage fertilizer on leaf mustard Vc content and nitrate content.Vitamin content in vegetables is the key index weighing vegetable nutrient quality, because vegetables are important sources of human consumption's vitamin.For Vc content, as can be seen from Table 4, and control group compares, after spraying compound organic foliar fertilizer, the Vc content of leaf mustard increases all to some extent, and the process of diluting 900 times increases by 4.14%, and difference is not remarkable, reason may be that foliage fertilizer concentration is too low, provides not enough to leaf mustard desired nutritional.Dilute 500 times and 700 times of increases by 32.26% and 21.44%, significant difference, and two groups are compared, the successful diluting 500 times is better than dilution 700 times.Therefore compound organic foliar fertilizer is at raising leaf mustard Vc content successful.
For nitrate content, compare with control group, after spraying compound organic foliar fertilizer, the nitrate content of leaf mustard reduces all to some extent, and significant difference.. general Nitrate Accumulation in Vegetables increases with nitrogen fertilizer amount and increases, but as can be seen from Table 4, after leaf mustard sprays compound organic foliar fertilizer, nitrate content reduces, may due in compound organic foliar fertilizer containing simple organic nitrogens such as the free amine group acid-state that directly can be absorbed by leaf mustard, participate in metabolism after absorption immediately, Promoting plant growth is grown, thus make it absorb the minimizing of nitrified nitrogen in soil amount, thus nitrate is reduced in its cylinder accumulation amount.Wherein nitrate content reduces is spray compound organic foliar fertilizer to dilute 500 times of 2 process the most significantly, nitrate content is 720.67mg/kg, reduce by 23.74%, this may be because Vc content and nitrate content have certain relation, the Vc of high-load can react rapidly with nitrous acid, generate nitric oxide, itself is oxidized to hydroascorbic acid, thus reduces Nitrate in Vegetable.Therefore compound organic foliar fertilizer has good effect improving in leaf mustard nitrate, also meets the requirement to green agricultural product.
Embodiment 3
1. the preparation of compound amino acid
Take 100g through the kitchen castoff sample of drying, pulverize, add sulfuric acid solution 450 mL that mass fraction is 30%, add 2-3g zeolite, stir, at 90 DEG C of hydrolysis 10h; After hydrolysis terminates, be cooled to room temperature; Hydrolyzate mass fraction is the Ca (OH) of 30%
2it is 7 that solution is neutralized to pH value, filters, the impurity removed calcium sulfate and be not hydrolyzed, and gained filtrate is Moriamin S, and in the insulating box of rearmounted 48 DEG C of evaporation and concentration, dry 4 h, obtain compounded amino acid product;
2. the preparation of nicotine extract
Take waste tobacco leaf 20g to move in the volumetric flask of 250ml, add hydrochloric acid solution 180 ml that mass concentration is 0.04g/ml, after fully shaking up concussion 10min, put into the water bath with thermostatic control of 78 DEG C, lixiviate 1h; After lixiviate terminates, regulate solution ph to be 7 with the sodium hydroxide solution that mass concentration is 0.04g/ml, filter, filtrate dry 4h in the insulating box of rearmounted 48 DEG C of evaporation and concentration, obtains nicotine extract;
3. the screening of organic foliage fertilizer formula
Nicotine extract prepared by the compound amino acid prepare kitchen castoff and waste tobacco leaf, carries out the compatibility of different proportion, according to the impact of different compatibility foliage fertilizer solution on germination rate of vegetable seeds and germination index, filters out the organic foliage fertilizer formulation of compound.
With pakchoi (the black leaf of short pin) for subjects, by the compound amino acid that extracts from kitchen castoff and the nicotine extract that extracts from waste tobacco leaf by different proportion compatibility, the germination percentage of observation pakchoi seed.Result shows, when compound amino acid and nicotine extract press 1:1.5,1:1 and 1:0.5 compatibility, pakchoi percentage of seedgermination result is respectively 83.30%, 93.70% and 88.90%; And in other ratio compatibilities, pakchoi percentage of seedgermination is all lower than 80%.Therefore, determine the quality proportioning 1:0.5 ~ 1:1.5 of compound amino acid and nicotine extract in Organic compound foliage fertilizer, wherein, preferably quality proportioning is 1:1.
4. Organic compound foliage fertilizer is used for water spinach
By the experimental result of embodiment 1 and 2, choose the Organic compound foliage fertilizer of dilution 700 times and 500 times, in field test, 2 times are sprayed to water spinach.And observe the effect that NEW TYPE OF COMPOSITE organic foliar fertilizer sprays in field thus.
The water spinach biological character of table 5 different disposal
Record according to field observation, spray after the process of NEW TYPE OF COMPOSITE organic foliar fertilizer compared to control group,, Ye Kuan, leaf look, growth potential thick from plant height, stem and these indexs of biomass, all higher than control group, can infer that NEW TYPE OF COMPOSITE organic foliar fertilizer has good facilitation for the growth of water spinach thus.Wherein spray 500 times of NEW TYPE OF COMPOSITE organic foliar fertilizers, 2 plant heights and increase by 30.51%, stem slightly increases by 37.5%, and biomass increases by 20.41%, and sprays 2 the plant heights increases by 40% of 700 times of NEW TYPE OF COMPOSITE organic foliar fertilizers, and stem slightly increases by 47.92%, and biomass increases by 30.61%.Comprehensive each factor, the effect spraying 500 times of NEW TYPE OF COMPOSITE organic foliar fertilizers is more better than 700 times.
Table 6 different disposal water spinach output condition
Note: show significant difference (p<0.05) with different lowercase alphabet attached after column data, different capitalization represents that difference is extremely significantly (p<0.01).
Table 6 is different fertilization on the impact of water spinach output and the output value, as can be seen from the table, after spraying NEW TYPE OF COMPOSITE organic foliar fertilizer, the output of water spinach and the output value increase significantly, wherein spray 700 times of compound organic foliar fertilizer output recruitments and improve 13.97% than control group, 500 times then improve 27.57%.Show to spray the volume increase of special-effect NEW TYPE OF COMPOSITE organic foliar fertilizer has to(for) water spinach field planting, wherein spray 500 times of 2 effects best.From the output value, output increases, and the output value improves naturally thereupon, therefore, sprays NEW TYPE OF COMPOSITE organic foliar fertilizer and has good economic benefit.
5. Organic compound foliage fertilizer is used for balsam pear
(1) on the impact of quantity production of bitter melon
Observe according to field test and record, the balsam pear spraying 500 times of liquid 2 times process is more prosperous than the growing way of control treatment, and leaf look more dark green, initial bloom stage and just knot melon phase early 1 day, 3 days respectively, and the knot melon phase extends 3 days, 5 days.
More greatly and slightly straight, color of the leather is more emerald green glossy, and outward appearance is more attractive in appearance, and meat is thicker, and matter is more crisp, and taste is sweetness and bitterness comparatively, and product are of fine quality, average long 24cm, shoulder breadth 6cm, single fruit weight 335g for the fruit spraying 500 times of liquid 2 times process; Than increase respectively 3cm, 0.5cm, 73g of control treatment; 2.5cm, 0.4cm, 45g is increased respectively than spraying the average of 700 times of liquid, 2 process.
Test is surveyed and is produced result Analysis of variance in table 7.By there and then balsam pear market price 2 yuan/kg.
Table 7 different disposal is on the impact of quantity production of bitter melon and the output value
Note: show significant difference (p<0.05) with different lowercase alphabet attached after column data, different capitalization represents that difference is extremely significantly (p<0.01).
As can be seen from the impact of table 7 on quantity production of bitter melon and the output value, compare with control group, after spraying NEW TYPE OF COMPOSITE organic foliar fertilizer, output and the output value of balsam pear all increase.Wherein output recruitment, spray 700 times 2 times be 8.97%, spraying 500 times is for 2 times 11.45%, and output increases, and the output value also can improve, and therefore, sprays NEW TYPE OF COMPOSITE organic foliar fertilizer and the output increased of balsam pear is had to good effect and has certain economic benefit.
(2) on the impact of balsam pear disease and pest
In on September 15th, 2013,20 days, the incidence investigating downy mildew, root knot nematode disease and droop respectively on the 30th.Each process is continuous observation 100 strain droop and root knot nematode disease incidence in each furrow, under the field management conditions such as the identical prevention and control of plant diseases, pest control, balsam pear sprays the withered diseased plant incidence of disease 2.7% of 500 times of liquid, 2 process, than the withered diseased plant incidence of disease 4.5% of control treatment, alleviate 1.8 percentage points; Balsam pear sprays the sick leaf rate 4.9% of downy mildew of 500 times of liquid, 2 process, and leaf rate 7.6% more sick than the downy mildew of control treatment, alleviates 2.7 percentage points.The root knot nematode disease morbidity hypopathia strain symptom spraying 500 times of liquid 2 times process is not obvious, plant withered only 0.2%; And it is heavier to contrast the root-knot nematode state of an illness, disease plant knot melon is bad, and plant is withered up to 4% in advance.The root knot nematode disease spraying 700 times of liquid 2 times process fall ill plant withered be 4.1%, with contrast close.Therefore, can think that spraying 500 times of liquid can strengthen balsam pear resistance 2 times, suppress the generation of root knot nematode disease, alleviate disease and pest and cause harm.
Claims (2)
1. a preparation method for Organic compound foliage fertilizer, is characterized in that: step is as follows:
(1) preparation of compound amino acid: take 100g through the kitchen castoff sample of drying, pulverize, adds sulfuric acid solution 350 mL ~ 550 mL that mass fraction is 20% ~ 45%, adds 2-3g zeolite, stir, at 85 DEG C ~ 100 DEG C hydrolysis 8 ~ 12h; After hydrolysis terminates, be cooled to room temperature; Hydrolyzate mass fraction is the Ca (OH) of 30%
2it is 7 that solution is neutralized to pH value, filters, the impurity removed calcium sulfate and be not hydrolyzed, and gained filtrate is Moriamin S, and in the insulating box of rearmounted 45 ~ 50 DEG C of evaporation and concentration, dry 3 ~ 5 h, obtain compounded amino acid product;
(2) preparation of nicotine extract: take waste tobacco leaf 20g and move in the volumetric flask of 250ml, add hydrochloric acid solution 150 ~ 200 ml that mass concentration is 0.03 ~ 0.05g/ml, after fully shaking up concussion 10min, put into the water bath with thermostatic control of 70 ~ 85 DEG C, lixiviate 0.5 ~ 1.5h; After lixiviate terminates, regulate solution ph to be 7, filter with the sodium hydroxide solution that mass concentration is 0.04g/ml, filtrate is dry 3 ~ 5 h in the insulating box of rearmounted 45 ~ 50 DEG C of evaporation and concentration, obtain nicotine extract
;
(3) by compound amino acid and nicotine extract in mass ratio 1:0.5 ~ 1:1.5 mix obtained composite foliage fertilizer.
2. the preparation method of Organic compound foliage fertilizer according to claim 1, is characterized in that: in step (3), the quality proportioning of compound amino acid and nicotine extract is: 1:1.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201310545137.0A CN103553731B (en) | 2013-11-07 | 2013-11-07 | Organic compound foliage fertilizer and preparation method thereof |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201310545137.0A CN103553731B (en) | 2013-11-07 | 2013-11-07 | Organic compound foliage fertilizer and preparation method thereof |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| CN103553731A CN103553731A (en) | 2014-02-05 |
| CN103553731B true CN103553731B (en) | 2015-04-29 |
Family
ID=50008150
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201310545137.0A Expired - Fee Related CN103553731B (en) | 2013-11-07 | 2013-11-07 | Organic compound foliage fertilizer and preparation method thereof |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN103553731B (en) |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN105850424A (en) * | 2016-04-07 | 2016-08-17 | 固镇县玉鹏蔬菜开发有限责任公司 | High-calcium pepper planting method |
Families Citing this family (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN107188743A (en) * | 2017-05-29 | 2017-09-22 | 句容市农业技术推广中心 | A kind of method that foliar fertilizer is prepared by base-material of waste tobacco leaf |
| CN107759326A (en) * | 2017-11-03 | 2018-03-06 | 常州市鑫嘉生物科技有限公司 | A kind of preparation method of micro-capsule foliar fertilizer |
| CN108849324B (en) * | 2018-06-08 | 2021-05-11 | 四川农业大学 | Cultivation method for improving quality and yield of intercropping corn |
| CN110199754A (en) * | 2019-05-27 | 2019-09-06 | 宜宾市南溪区陆零农业发展有限责任公司 | A kind of Chinese prickly ash and tuber of pinellia method for interplanting cultivation |
| CN112341270A (en) * | 2020-11-02 | 2021-02-09 | 云南中烟再造烟叶有限责任公司 | Method for preparing water-soluble organic carbon fertilizer from tobacco waste |
Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN102531785A (en) * | 2012-01-06 | 2012-07-04 | 云南金星化工有限公司 | Method for producing biogenic insecticide fertilizer by abandoned tobacco |
| CN102603391A (en) * | 2012-03-30 | 2012-07-25 | 广西宇鑫生物科技有限公司 | Compound amino acid organic fertilizer and production method of compound amino acid organic fertilizer |
| CN103102340A (en) * | 2012-11-28 | 2013-05-15 | 江南大学 | Preparation method of nicotine |
-
2013
- 2013-11-07 CN CN201310545137.0A patent/CN103553731B/en not_active Expired - Fee Related
Patent Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN102531785A (en) * | 2012-01-06 | 2012-07-04 | 云南金星化工有限公司 | Method for producing biogenic insecticide fertilizer by abandoned tobacco |
| CN102603391A (en) * | 2012-03-30 | 2012-07-25 | 广西宇鑫生物科技有限公司 | Compound amino acid organic fertilizer and production method of compound amino acid organic fertilizer |
| CN103102340A (en) * | 2012-11-28 | 2013-05-15 | 江南大学 | Preparation method of nicotine |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN105850424A (en) * | 2016-04-07 | 2016-08-17 | 固镇县玉鹏蔬菜开发有限责任公司 | High-calcium pepper planting method |
Also Published As
| Publication number | Publication date |
|---|---|
| CN103553731A (en) | 2014-02-05 |
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| CN103553731B (en) | Organic compound foliage fertilizer and preparation method thereof | |
| CN102786362B (en) | Biological pesticidal organic fertilizer | |
| CN103864511B (en) | A kind of synergy composite organic-inorganic fertilizer | |
| CN101302124B (en) | Multi-element biofertilizer | |
| CN103864510A (en) | Controlled-release compound pesticide fertilizer | |
| CN103086771B (en) | Bioorganic fertilizer preparation method, bioorganic fertilizer and application of bioorganic fertilizer | |
| CN106748247A (en) | A kind of selenium-enriched foliage fertilizer and preparation method thereof | |
| CN104193533A (en) | Organic fertilizer | |
| CN109180323A (en) | A kind of bio-organic fertilizer and its preparation method for agricultural plant | |
| CN102010245B (en) | Concentrated amino acid liquid fertilizer and preparation method thereof | |
| CN102503643A (en) | Fertilizer special for honeysuckle flower and preparation method and application method thereof | |
| CN107188749A (en) | A kind of high-yield planting base manure of passion fruit and preparation method thereof | |
| CN104649812A (en) | Bio-organic fertilizer for eggplant fruits and vegetables and preparation method of bio-organic fertilizer | |
| CN106365893A (en) | Preparation method of special organic fertilizer for grapes | |
| CN107509584A (en) | A kind of selenium-rich Yunan seedless wampee implantation methods | |
| CN104370595A (en) | Preparation method and application of multi-effect organic foliage conditioner | |
| CN106348865A (en) | Organic-inorganic compound fertilizer with silkworm excrement and tobacco stems as organic raw materials and preparation method of organic-inorganic compound fertilizer | |
| CN105198655A (en) | Organic compound fertilizer for areca catechu | |
| CN107285961A (en) | A kind of organic fertilizer for improveing grape soil and preparation method thereof | |
| CN106365894A (en) | Production method of organic fertilizer for grapes | |
| CN103493644B (en) | Fertilizing method for improving Chinese wampee fruit yield and quality | |
| CN106233962A (en) | A kind of cultural method of rich iron oxide red potato | |
| CN108610192A (en) | A kind of bio-organic fertilizer and preparation method thereof | |
| CN108840752A (en) | A kind of biological organic fertilizer containing complex micro organism fungicide | |
| CN109197429A (en) | A method of using sugar refinery give up material production wormcast cultivation Brassica rapa L |
Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| C06 | Publication | ||
| PB01 | Publication | ||
| SE01 | Entry into force of request for substantive examination | ||
| SE01 | Entry into force of request for substantive examination | ||
| C14 | Grant of patent or utility model | ||
| GR01 | Patent grant | ||
| CF01 | Termination of patent right due to non-payment of annual fee | ||
| CF01 | Termination of patent right due to non-payment of annual fee |
Granted publication date: 20150429 Termination date: 20171107 |