CN103549653B - The application of fragrant plantain lily flower ethanol extract in cigarette - Google Patents
The application of fragrant plantain lily flower ethanol extract in cigarette Download PDFInfo
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- CN103549653B CN103549653B CN201310583791.0A CN201310583791A CN103549653B CN 103549653 B CN103549653 B CN 103549653B CN 201310583791 A CN201310583791 A CN 201310583791A CN 103549653 B CN103549653 B CN 103549653B
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Abstract
The application of a kind of fragrant plantain lily flower ethanol extract in cigarette, it is characterized in that: fragrant plantain lily flower ethanol extract is applied in production of cigarettes as tobacco aromatics, the property sent out thoroughly of flue gas when cigarette burns and sucks can be increased, improve aroma quality, reduce dry sensation, cover assorted gas, improve mouthfeel, and give cigarette a kind of special alcohol Flavor.Described fragrant plantain lily flower ethanol extract is prepared from by the following method: a. gets dry fragrant plantain lily flower, and removal of impurities, is crushed to 10 ~ 60 orders; B. under 20 ~ 85 DEG C of conditions, extract fragrant plantain lily flower dry mash with ethanol, solid-liquid ratio is 1:5 ~ 1:20; C. leach leaching liquor, after reduced pressure concentration, be fragrant plantain lily flower ethanol extract.The present invention does not change original performance and the processing technology of cigarette, improves the flavouring essence quality of cigarette, improves sense organ comfort level during cigarette smoking, and abundant raw material is easy to get, production technology is simple to operation, and production cost is lower, therefore has more the meaning and value of actual production.
Description
Technical field
The present invention relates to cigarette additive, be specifically related to the application of a kind of fragrant plantain lily flower ethanol extract in cigarette.The application of this technology does not change the existing processing technology of cigarette, can improve suction quality and the sense organ comfort level of cigarette.
Background technology
Along with the tar content of domestic cigarette product constantly reduces, cause the problems such as the decline of cigarette flavor amount, style and features reduction, comfortableness variation to some extent.For improving the overall quality of cigarette product, the Novel tobacco flavor of exploitation bright characteristic, stay in grade is a main solution route.This wherein, natural perfume material is because of its note enriches, the advantage such as fragrance is true to nature, safety and environmental protection becomes recent researches exploitation emphasis.
Vast territory and abundant resources in China, and floristics is various, and the composition of contained active ingredient also respectively has feature, for the exploitation of natural perfume material provides rich in natural resources.By different modes method, extraction and isolation is carried out to effective ingredients in plant, and for the feature of cigarette product, extract is applied in cigarette in different forms, to improving the overall quality of cigarette.
Jade hairpin (
hosta plantaginea) be Liliaceae herbaceos perennial, complete stool is all pharmaceutically acceptable; Its dried floral, nature and flavor are sweet cool, there is effect of clearing heat and detoxicating, cough-relieving, throat, be used for the treatment of lung heat, abscess of throat, hoarse, chest is warm, scorchingly hot etc., for Inner Mongol local people commonly use a kind of there is definite clinical efficacy medicine pharmacopoeia commission of Ministry of Health of the People's Republic of China. Drug Standard of Ministry of Public Health of the Peoples Republic of China. anaesthetic fascicle [M]. 1998:10.}.Can do after its fresh flower removes stamen vegetables edible the Chinese Academy of Sciences's " Chinese Plants will " editorial board edits. Chinese Plants will [M]. Beijing: Science Press publishes, 1980,14:49.}.The main component of fragrant plantain lily flower has: steroid sapogenin and saponins, flavonols and glycoside thereof, alkaloids, ester class, carbohydrate and amino acid etc. Li Wenyuan. and the chemical composition of anaesthetic fragrant plantain lily flower and biologically active Primary Study [D]. the Central China University of Science and Technology, Wuhan, 2009.}.
Fragrant plantain lily flower all has cultivation in China various places, and its petal is like hairpin, and look white as a jade, and delicate fragrance is pleasant, positive so-called " jade hairpin perfume (or spice) fortunately, open by several, corner ".It is used for ornamental plantation, is also the common medicine simply of anti-inflammatory in anaesthetic, removing toxic substances simultaneously.Domestic correlative study mainly, in the Propogation and culture, medicinal efficacy, chemical composition qualification etc. of fragrant plantain lily flower, there is not yet the application of its extract in tobacco.
Summary of the invention
The present invention studies fragrant plantain lily flower based on above-mentioned present Research just, sets up the ethanol extraction process of fragrant plantain lily flower, puts in cigarette by fragrant plantain lily flower ethanol extract, and object is the suction quality and the sense organ comfort level that improve cigarette.
Object of the present invention realizes by following technical scheme:
The application of a kind of fragrant plantain lily flower ethanol extract in cigarette, that fragrant plantain lily flower ethanol extract is applied in production of cigarettes as tobacco aromatics, the property sent out thoroughly of flue gas when cigarette burns and sucks can be increased, improve aroma quality, reduce dry sensation, cover assorted gas, improve mouthfeel, and give cigarette a kind of special alcohol Flavor.Described fragrant plantain lily flower ethanol extract is prepared from by the following method:
A. get dry fragrant plantain lily flower, removal of impurities, is crushed to 10 ~ 60 orders;
B. under 20 ~ 85 DEG C of conditions, extract fragrant plantain lily flower dry mash with ethanol, concentration of alcohol is 80 % ~ 95 %(
v/
v, lower same), solid-liquid ratio is 1:5 ~ 1:20;
C. leach leaching liquor, after reduced pressure concentration, be fragrant plantain lily flower ethanol extract.
The present invention, when extracting fragrant plantain lily flower powder with ethanol, can adopt following various ways to extract: as lixiviate under room temperature, every batch materials lixiviate 2 times, each 7 ~ 10 days; Under 60 ~ 85 DEG C of conditions, heating extraction 2 times, each 1 ~ 3 hour; Ultrasonic assistant extracts, ultrasonic frequency 30 ~ 60 kHz, power 100 ~ 1000 W, extraction time 30 ~ 60 min, extraction temperature 25 ~ 50 DEG C; Also other prior aries such as microwave radiation exaraction can be adopted.
Be rufous liquid or liquid extract under the fragrant plantain lily flower ethanol extract room temperature adopting said method to prepare, there is mellow sauce perfume and spend fragrant and sweet, soluble in water or certain density alcohol solution.
Fragrant plantain lily flower ethanol extract of the present invention is applied on cigarette shreds as tobacco aromatics after water or the dilution of finite concentration ethanol.When burning and sucking cigarette, the flue gas property sent out thoroughly can be increased, promote aroma quality, reduce dry sensation, cover assorted gas, improve mouthfeel, and give cigarette a kind of special alcohol Flavor.Concrete usage ratio is 0.01 ~ 0.1 ‰ of tobacco quality, can be used alone or be deployed into essence with other spices to use.
The present invention is as a kind of new cigarette additive, do not change original performance of cigarette, do not change the original processing technology of cigarette, improve the quality defect that cigarette humid keeping performance is poor, flue gas drying, comfort level are poor that China's cigarette product exists to a certain extent, improve the suction quality of cigarette; And abundant raw material is easy to get, production technology is simple to operation, and production cost is not high, therefore has more the meaning and value of actual production.
Detailed description of the invention
Below in conjunction with embodiment, the present invention is described further, but does not limit the present invention.
embodiment 1
Get dried fragrant plantain lily flower 200 g, about being crushed to 20 orders; Be heated to 65 DEG C with 95 % ethanol extract 2 times, each 3 hours, solid-liquid ratio was followed successively by 1:9 and 1:8.Filter to obtain leaching liquor totally 2800 mL; Reduced pressure concentration, within the scope of vacuum degree control – 0.090～– 0.095 MPa, bath temperature is no more than 45 DEG C, is condensed into flowing soaking paste, is fragrant plantain lily flower ethanol extract of the present invention, is total to obtain product 100.24 g.After testing, product acid number is 20.84, refraction index n
d 20be 1.482, relative density (25 DEG C) is 1.268 g/cm
3.
Take the above-mentioned fragrant plantain lily flower ethanol extract of 0.005 g, add distilled water to 5.000 g, spray equably with micro sprayer after mixing and be added on the blank pipe tobacco of 100 g (feeding quantity is 0.05 ‰).Loaded by pipe tobacco in sealing bag, place 80 DEG C of constant temperature 30 min in baking oven, then shake pipe tobacco rapidly, moisture in cut tobacco controls, at about 12 %, to roll into cigarette, puts into constant temperature (22 ± 1 DEG C) constant humidity (relative humidity 60 ± 2 %) case inner equilibrium 48 more than h.Blank reference cigarette is under similarity condition, adds identical deal distilled water, roll into contrast cigarette with same pipe tobacco spray.Smoke panel test through the above judging panel of 7 people, result shows: soft, the saturating property of cigarette smoke exquisiteness of applying fragrant plantain lily flower ethanol extract is good, contrasts with reference cigarette, and dry sensation reduction, assorted gas minimizing, time sweet sense increase, improve the suction quality of cigarette.
embodiment 2
Get dry fragrant plantain lily flower 100 g, pulverize and cross 40 eye mesh screens, at room temperature adopt ultrasonic and circulated extraction machine, add 80 % alcohol extracts, solid-liquid ratio is 1:15, ultrasonic frequency 40 kHz, power 750 W, extract total time 50 min, ultrasonic time and interval time are 2 s/1 s, mixing speed 1300 rpm.Extraction terminates rear use 400 order filter cloth and leaches leaching liquor, and namely 20 % being evaporated to original volume obtain fragrant plantain lily flower ethanol extract of the present invention.After testing, product acid number is 19.96, refraction index n
d 20be 1.423, relative density (25 DEG C) is 1.236 g/cm
3.
Take 0.020 g fragrant plantain lily flower ethanol extract, add 70 % ethanol and be diluted to 1.000 g, mixing, to inject 4 μ L(perfuming amounts be 0.1 ‰ to often propping up in blank cigarette to adopt perfuming cigarette injector); Separately get partial blank cigarette, often prop up injection 4 μ L 70 % ethanol as reference cigarette.Cigarette after perfuming and reference cigarette are put into respectively constant temperature (22 ± 1 DEG C) constant humidity (relative humidity 60 ± 2 %) case inner equilibrium 48 more than h.Smoking result shows: the cigarette flavor matter after perfuming and perfume quantity promote, and assorted gas reduces, and have Hui Tian to promote the production of body fluid sense, pleasant impression is comfortable.
Claims (3)
1. the application of fragrant plantain lily flower ethanol extract in cigarette, it is characterized in that: fragrant plantain lily flower ethanol extract is applied in production of cigarettes as tobacco aromatics, the property sent out thoroughly of flue gas when cigarette burns and sucks can be increased, improve aroma quality, reduce dry sensation, cover assorted gas, improve mouthfeel, and give cigarette a kind of special alcohol Flavor, the adding proportion of fragrant plantain lily flower ethanol extract is the 0.01-0.1 ‰ of tobacco quality, and fragrant plantain lily flower ethanol extract can add separately and uses or be deployed into essence mixture with other spices and use; Described fragrant plantain lily flower ethanol extract is prepared from by the following method:
A. get dry fragrant plantain lily flower, removal of impurities, is crushed to 10 ~ 60 orders;
B. under 20 ~ 85 DEG C of conditions, extract fragrant plantain lily flower dry mash with ethanol, solid-liquid ratio is 1:5 ~ 1:20;
C. leach leaching liquor, after reduced pressure concentration, be fragrant plantain lily flower ethanol extract.
2. the application of fragrant plantain lily flower ethanol extract according to claim 1 in cigarette, it is characterized in that: when fragrant plantain lily flower powder being extracted with ethanol, any one mode following is adopted to carry out: lixiviate under (1) room temperature, every batch materials lixiviate 2 times, each 7 ~ 10 days; (2) under 60 ~ 85 DEG C of conditions, with ethanol heating extraction 2 times, each 1 ~ 3 hour; (3) ultrasonic assistant extracts, ultrasonic frequency 30 ~ 60 kHz, power 100 ~ 1000 W, extraction time 30 ~ 60 min, extraction temperature 25 ~ 50 DEG C; (4) microwave radiation exaraction.
3. the application of fragrant plantain lily flower ethanol extract according to claim 1 and 2 in cigarette, is characterized in that: described concentration of alcohol is 80 % ~ 95 %.
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| JPS6136257A (en) * | 1984-07-26 | 1986-02-20 | Japan Tobacco Inc | Cembrene derivative and flavor taste improver consisting of said compound |
| CN101376870B (en) * | 2008-10-10 | 2012-07-18 | 黄毓星 | Chinese herbal medicine wine capable of activating blood circulation, removing stasis, expelling toxin and relieving itching |
| CN102166039B (en) * | 2011-04-08 | 2013-06-12 | 深圳波顿香料有限公司 | Method for extracting roselle extractive and application in cigarettes as well as cigarettes |
| CN102225168A (en) * | 2011-06-20 | 2011-10-26 | 奥·乌力吉 | Mongolian medicine for treating pharyngitis |
| CN102579908B (en) * | 2012-03-19 | 2013-09-11 | 常熟华港制药有限公司 | Traditional Chinese medicine preparation for toxin expelling, refreshment and beautifying |
| CN103190693B (en) * | 2013-04-19 | 2015-03-25 | 安徽中烟工业有限责任公司 | Extracting method for tobacco flower extract and application thereof |
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