CN103549653A - Application of hosta plantaginea flower ethanol extract to cigarettes - Google Patents
Application of hosta plantaginea flower ethanol extract to cigarettes Download PDFInfo
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- CN103549653A CN103549653A CN201310583791.0A CN201310583791A CN103549653A CN 103549653 A CN103549653 A CN 103549653A CN 201310583791 A CN201310583791 A CN 201310583791A CN 103549653 A CN103549653 A CN 103549653A
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- ethanol extract
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- lily flower
- plantain lily
- fragrant plantain
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Abstract
An application of a hosta plantaginea flower ethanol extract to cigarettes is characterized in that the hosta plantaginea flower ethanol extract is applied to cigarette production as a cigarette flavor, the permeability of smoke during burning of the cigarettes can be increased, the fragrance quality can be improved, the dry sensation can be reduced, offensive odors can be covered up, the taste can be improved, and a special mellow flavor is endowed to the cigarettes. A preparation method of the hosta plantaginea flower ethanol extract comprises the steps as follows: a, taking dried hosta plantaginea flowers, removing impurities, and crushing the dried hosta plantaginea flowers into the fineness of 10-60 meshes; b, extracting dried hosta plantaginea flower powder with ethanol at the temperature of 20-85 DEG C, wherein the power-liquid ratio is 1:5-1:20; and c, filtering out a leach liquor and obtaining the hosta plantaginea flower ethanol extract after vacuum concentration. According to the hosta plantaginea flower ethanol extract, original performances and processing technologies of the cigarettes are unchanged, the fragrance quality of the cigarettes is improved, the sensory comfort of the cigarettes during smoking is improved, raw materials are rich and easy to obtain, the production process is simple and easy to operate, and the production cost is low, so that the application has practical production significance and values.
Description
Technical field
The present invention relates to cigarette additive, be specifically related to the application of a kind of fragrant plantain lily flower ethanol extract in cigarette.The application of this technology does not change the existing processing technology of cigarette, can improve suction quality and the sense organ comfort level of cigarette.
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Background technology
Along with the tar content of domestic cigarette product constantly reduces, the problems such as the decline of cigarette flavor amount, style and features reduction, comfortableness variation have been caused to some extent.For improving the overall quality of cigarette product, the Novel tobacco flavor of exploitation bright characteristic, stay in grade is a main solution route.This wherein, natural perfume material becomes the emphasis of recent researches exploitation because of advantages such as its note is abundant, fragrance is true to nature, safety and environmental protections.
Vast territory and abundant resources in China, and floristics is various, and the composition of contained active ingredient also respectively has feature, for the exploitation of natural perfume material provides rich in natural resources.Can to effective ingredients in plant, extract separation by different modes method, and for the feature of cigarette product, extract is applied in cigarette with multi-form, to improving the overall quality of cigarette.
Jade hairpin (
hosta plantaginea) be Liliaceae herbaceos perennial, complete stool is all pharmaceutically acceptable; Its dried floral, nature and flavor are sweet cool, the effect with clearing heat and detoxicating, cough-relieving, throat, be used for the treatment of lung heat, abscess of throat, hoarse, chest is warm, scorchingly hot etc., a kind of medicine with definite clinical efficacy of commonly using for the Inner Mongol local people pharmacopoeia commission of Ministry of Health of the People's Republic of China. Drug Standard of Ministry of Public Health of the Peoples Republic of China. anaesthetic fascicle [M]. 1998:10.}.Its fresh flower remove can do after stamen vegetables edible the Chinese Academy of Sciences " chief editor of Chinese Plants Zhi” editorial board. Chinese Plants will [M]. Beijing: Science Press publishes, 1980,14:49.}.The main component of fragrant plantain lily flower has: steroid sapogenin and saponins thereof, flavonols and glycoside thereof, alkaloids, ester class, carbohydrate and amino acid etc. Li Wenyuan. and the chemical composition of anaesthetic fragrant plantain lily flower and biologically active Primary Study [D]. the Central China University of Science and Technology, Wuhan, 2009.}.
Fragrant plantain lily flower all has cultivation in China various places, and its petal is like hairpin, and look white as a jade, and delicate fragrance is pleasant, positive so-called " jade hairpin perfume (or spice) fortunately, open by several, corner ".It is used for ornamental plantation, is also the common medicine simply of anti-inflammatory in anaesthetic, removing toxic substances simultaneously.Domestic correlative study mainly, at aspects such as the Propogation and culture of fragrant plantain lily flower, medicinal efficacy, chemical composition evaluations, there is not yet the application of its extract in tobacco.
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Summary of the invention
The present invention studies fragrant plantain lily flower based on above-mentioned present Research just, sets up the alcohol extract technique of fragrant plantain lily flower, and fragrant plantain lily flower ethanol extract is put in cigarette, and object is to improve suction quality and the sense organ comfort level of cigarette.
Object of the present invention can be achieved through the following technical solutions:
The application of a kind of fragrant plantain lily flower ethanol extract in cigarette, to be applied in production of cigarettes fragrant plantain lily flower ethanol extract as tobacco aromatics using, in the time of increasing cigarette and burn and suck, flue gas sends out property thoroughly, improve aroma quality, reduce dry sensation, cover assorted gas, improve mouthfeel, and give cigarette a kind of special alcohol Flavor.Described fragrant plantain lily flower ethanol extract is prepared from by the following method:
A. get dry fragrant plantain lily flower, removal of impurities, is crushed to 10～60 orders;
B. under 20～85 ℃ of conditions, with ethanol, fragrant plantain lily flower dry mash is extracted, concentration of alcohol is 80 %～95 %(
v/
v, lower same), solid-liquid ratio is 1:5～1:20;
C. leach leaching liquor, after reduced pressure concentration, be fragrant plantain lily flower ethanol extract.
The present invention, when fragrant plantain lily flower powder being extracted with ethanol, can adopt following various ways to extract: as lixiviate under room temperature, and every batch materials lixiviate 2 times, each 7～10 days; Under 60～85 ℃ of conditions, heating is extracted 2 times, each 1～3 hour; Ultrasonic wave assisted extraction, ultrasonic frequency 30～60 kHz, power 100～1000 W, extraction times 30～60 min, 25～50 ℃ of extraction temperatures; Also can adopt Microwave-assisted Extraction other prior art such as to get.
Adopting under fragrant plantain lily flower ethanol extract room temperature prepared by said method is rufous liquid or liquid extract, have mellow sauce fragrant and spend fragrant and sweet, soluble in water or certain density alcohol solution.
Fragrant plantain lily flower ethanol extract of the present invention is applied on cigarette shreds as tobacco aromatics using after water or the dilution of finite concentration ethanol.While burning and sucking cigarette, can increase the flue gas property sent out thoroughly, promote aroma quality, reduce dry sensation, cover assorted gas, improve mouthfeel, and give cigarette a kind of special alcohol Flavor.Concrete usage ratio is tobacco quality 0.01～0.1 ‰, can be used alone or is deployed into essence with other spices and use.
The present invention is as a kind of new cigarette additive, do not change original performance of cigarette, do not change the original processing technology of cigarette, improved to a certain extent that the cigarette humid keeping performance that China's cigarette product exists is poor, flue gas drying, comfort level poor quality defect, improved the suction quality of cigarette; And abundant raw material is easy to get, production technology is simple to operation, and production cost is not high, therefore has more the meaning and value of actual production.
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The specific embodiment
Below in conjunction with embodiment, the present invention is described further, but does not limit the present invention.
embodiment 1
Get dried fragrant plantain lily flower 200 g, be crushed to 20 order left and right; With 95 % ethanol, be heated to 65 ℃ and extract 2 times, each 3 hours, solid-liquid ratio was followed successively by 1:9 and 1:8.Filter to obtain leaching liquor totally 2800 mL; Reduced pressure concentration, within the scope of vacuum degree control – 0.090～– 0.095 MPa, bath temperature is no more than 45 ℃, is condensed into flowing soaking paste, is fragrant plantain lily flower ethanol extract of the present invention, is total to obtain product 100.24 g.After testing, product acid number is 20.84, refraction index n
d 20be 1.482, relative density (25 ℃) is 1.268 g/cm
3.
Take the above-mentioned fragrant plantain lily flower ethanol extract of 0.005 g, add distilled water to 5.000 g, mix and with micro sprayer, spray equably and be added on the blank pipe tobaccos of 100 g (feeding quantity is 0.05 ‰) afterwards.Pipe tobacco is packed in sealing bag, place 80 ℃ of constant temperature 30 min in baking oven, then shake rapidly pipe tobacco, moisture in cut tobacco is controlled at 12 % left and right, rolls into cigarette, puts into constant temperature (22 ± 1 ℃) constant humidity (relative humidity 60 ± 2 %) more than case inner equilibrium 48 h.Blank reference cigarette is under similarity condition, with same pipe tobacco spray, adds identical deal distilled water, rolls into contrast cigarette.Through the above judging panel of 7 people, smoke panel test, result shows: the cigarette smoke exquisiteness that applies fragrant plantain lily flower ethanol extract is soft, the property sent out is good thoroughly, contrast with reference cigarette, and dry sensation reduces, assorted gas reduces, returns sweet sense increase, has improved the suction quality of cigarette.
embodiment 2
Get dry fragrant plantain lily flower 100 g, pulverize and cross 40 eye mesh screens, at room temperature adopt ultrasonic circulation extractor, add 80 % alcohol extracts, solid-liquid ratio is 1:15, ultrasonic frequency 40 kHz, power 750 W, extract total times 50 min, ultrasonic time and interval time are 2 s/1 s, mixing speed 1300 rpm.Extraction finishes rear use 400 order filter clothes and leaches leaching liquor, and 20 % that are evaporated to original volume obtain fragrant plantain lily flower ethanol extract of the present invention.After testing, product acid number is 19.96, refraction index n
d 20be 1.423, relative density (25 ℃) is 1.236 g/cm
3.
Take 0.020 g fragrant plantain lily flower ethanol extract, add 70 % ethanol to be diluted to 1.000 g, mix, adopting perfuming cigarette injector is 0.1 ‰ to injecting 4 μ L(perfuming amounts in every blank cigarette); Separately get the blank cigarette of part, every injection 4 μ L 70 % ethanol are as reference cigarette.Cigarette after perfuming and reference cigarette are put into respectively to constant temperature (22 ± 1 ℃) constant humidity (relative humidity 60 ± 2 %) more than case inner equilibrium 48 h.Smoking result shows: the cigarette flavor matter after perfuming and perfume quantity promote, and assorted gas reduces, and has the Hui Tian sense of promoting the production of body fluid, and pleasant impression is comfortable.
Claims (5)
1. the fragrant plantain lily flower ethanol extract application in cigarette, it is characterized in that: using fragrant plantain lily flower ethanol extract as tobacco aromatics using, be applied in production of cigarettes, in the time of increasing cigarette and burn and suck, flue gas sends out property thoroughly, improve aroma quality, reduce dry sensation, cover assorted gas, improve mouthfeel, and give cigarette a kind of special alcohol Flavor, described fragrant plantain lily flower ethanol extract is prepared from by the following method:
A. get dry fragrant plantain lily flower, removal of impurities, is crushed to 10～60 orders;
B. under 20～85 ℃ of conditions, with ethanol, fragrant plantain lily flower dry mash is extracted, solid-liquid ratio is 1:5～1:20;
C. leach leaching liquor, after reduced pressure concentration, be fragrant plantain lily flower ethanol extract.
2. the application of fragrant plantain lily flower ethanol extract according to claim 1 in cigarette, is characterized in that: the 0.01-0.1 ‰ that the adding proportion of fragrant plantain lily flower ethanol extract is tobacco quality.
3. the application of fragrant plantain lily flower ethanol extract according to claim 1 in cigarette, is characterized in that: fragrant plantain lily flower ethanol extract can add separately and uses or be deployed into the essence use that is mixed with other spices.
4. the application of fragrant plantain lily flower ethanol extract according to claim 1 in cigarette, it is characterized in that: when fragrant plantain lily flower powder is extracted with ethanol, adopt following any one mode to carry out: lixiviate under (1) room temperature, every batch materials lixiviate 2 times, each 7～10 days; (2), under 60～85 ℃ of conditions, with ethanol heating, extract 2 times each 1～3 hour; (3) ultrasonic wave assisted extraction, ultrasonic frequency 30～60 kHz, power 100～1000 W, extraction times 30～60 min, 25～50 ℃ of extraction temperatures; (4) Microwave-assisted Extraction is got.
5. the application in cigarette according to the fragrant plantain lily flower ethanol extract described in claim 1 or 4, is characterized in that: described concentration of alcohol is 80 %～95 %.
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Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN105154235A (en) * | 2015-07-15 | 2015-12-16 | 河南中烟工业有限责任公司 | Cigarette Chinese photinia perfume, and preparation method and application thereof |
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| JPS6214550B2 (en) * | 1984-07-26 | 1987-04-02 | Nippon Tabako Sangyo Kk | |
| CN101376870A (en) * | 2008-10-10 | 2009-03-04 | 黄毓星 | Chinese herbal medicine wine capable of activating blood circulation, removing stasis, expelling toxin and relieving itching |
| CN102166039A (en) * | 2011-04-08 | 2011-08-31 | 深圳波顿香料有限公司 | Method for extracting roselle extractive and application in cigarettes as well as cigarettes |
| CN102225168A (en) * | 2011-06-20 | 2011-10-26 | 奥·乌力吉 | Mongolian medicine for treating pharyngitis |
| CN102579908A (en) * | 2012-03-19 | 2012-07-18 | 常熟华港制药有限公司 | Traditional Chinese medicine preparation for toxin expelling, refreshment and beautifying |
| CN103190693A (en) * | 2013-04-19 | 2013-07-10 | 安徽中烟工业有限责任公司 | Extracting method for tobacco flower extract and application thereof |
-
2013
- 2013-11-20 CN CN201310583791.0A patent/CN103549653B/en active Active
Patent Citations (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JPS6214550B2 (en) * | 1984-07-26 | 1987-04-02 | Nippon Tabako Sangyo Kk | |
| CN101376870A (en) * | 2008-10-10 | 2009-03-04 | 黄毓星 | Chinese herbal medicine wine capable of activating blood circulation, removing stasis, expelling toxin and relieving itching |
| CN102166039A (en) * | 2011-04-08 | 2011-08-31 | 深圳波顿香料有限公司 | Method for extracting roselle extractive and application in cigarettes as well as cigarettes |
| CN102225168A (en) * | 2011-06-20 | 2011-10-26 | 奥·乌力吉 | Mongolian medicine for treating pharyngitis |
| CN102579908A (en) * | 2012-03-19 | 2012-07-18 | 常熟华港制药有限公司 | Traditional Chinese medicine preparation for toxin expelling, refreshment and beautifying |
| CN103190693A (en) * | 2013-04-19 | 2013-07-10 | 安徽中烟工业有限责任公司 | Extracting method for tobacco flower extract and application thereof |
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN105154235A (en) * | 2015-07-15 | 2015-12-16 | 河南中烟工业有限责任公司 | Cigarette Chinese photinia perfume, and preparation method and application thereof |
| CN105154235B (en) * | 2015-07-15 | 2019-03-08 | 河南中烟工业有限责任公司 | A kind of cigarette Chinese photinia fragrance, preparation method and applications |
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| CN103549653B (en) | 2015-08-19 |
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