CN103468004B - 负载纳米石墨烯的蜡浆及其制备方法和用途 - Google Patents
负载纳米石墨烯的蜡浆及其制备方法和用途 Download PDFInfo
- Publication number
- CN103468004B CN103468004B CN201310440876.3A CN201310440876A CN103468004B CN 103468004 B CN103468004 B CN 103468004B CN 201310440876 A CN201310440876 A CN 201310440876A CN 103468004 B CN103468004 B CN 103468004B
- Authority
- CN
- China
- Prior art keywords
- wax
- graphene
- slurry
- nano
- preparation
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Active
Links
- 229910021389 graphene Inorganic materials 0.000 title claims abstract description 82
- 239000002002 slurry Substances 0.000 title claims abstract description 64
- OKTJSMMVPCPJKN-UHFFFAOYSA-N Carbon Chemical compound [C] OKTJSMMVPCPJKN-UHFFFAOYSA-N 0.000 title claims abstract description 63
- 238000004519 manufacturing process Methods 0.000 title abstract description 5
- 238000002360 preparation method Methods 0.000 claims abstract description 32
- 239000002245 particle Substances 0.000 claims abstract description 31
- 239000006185 dispersion Substances 0.000 claims abstract description 23
- 238000000576 coating method Methods 0.000 claims abstract description 19
- 239000007787 solid Substances 0.000 claims abstract description 19
- 239000011248 coating agent Substances 0.000 claims abstract description 17
- 239000000976 ink Substances 0.000 claims abstract description 16
- 239000010985 leather Substances 0.000 claims abstract description 5
- 239000001993 wax Substances 0.000 claims description 142
- 239000012530 fluid Substances 0.000 claims description 29
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 19
- 239000003595 mist Substances 0.000 claims description 12
- 239000008367 deionised water Substances 0.000 claims description 10
- 229910021641 deionized water Inorganic materials 0.000 claims description 10
- 239000002904 solvent Substances 0.000 claims description 10
- XEKOWRVHYACXOJ-UHFFFAOYSA-N Ethyl acetate Chemical compound CCOC(C)=O XEKOWRVHYACXOJ-UHFFFAOYSA-N 0.000 claims description 9
- 239000007788 liquid Substances 0.000 claims description 9
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 claims description 7
- 238000013019 agitation Methods 0.000 claims description 7
- ZMXDDKWLCZADIW-UHFFFAOYSA-N N,N-Dimethylformamide Chemical compound CN(C)C=O ZMXDDKWLCZADIW-UHFFFAOYSA-N 0.000 claims description 6
- CTQNGGLPUBDAKN-UHFFFAOYSA-N O-Xylene Chemical compound CC1=CC=CC=C1C CTQNGGLPUBDAKN-UHFFFAOYSA-N 0.000 claims description 6
- 239000000839 emulsion Substances 0.000 claims description 6
- 238000000227 grinding Methods 0.000 claims description 5
- -1 polyethylene Polymers 0.000 claims description 5
- 239000013543 active substance Substances 0.000 claims description 4
- 239000000203 mixture Substances 0.000 claims description 4
- 238000002525 ultrasonication Methods 0.000 claims description 4
- 239000004698 Polyethylene Substances 0.000 claims description 3
- 235000011114 ammonium hydroxide Nutrition 0.000 claims description 3
- 239000003849 aromatic solvent Substances 0.000 claims description 3
- 238000010438 heat treatment Methods 0.000 claims description 3
- 229920000573 polyethylene Polymers 0.000 claims description 3
- BFKJFAAPBSQJPD-UHFFFAOYSA-N tetrafluoroethene Chemical group FC(F)=C(F)F BFKJFAAPBSQJPD-UHFFFAOYSA-N 0.000 claims description 3
- MKYLOMHWHWEFCT-UHFFFAOYSA-N Manthidine Natural products C1C2=CC=3OCOC=3C=C2C2C3=CC(OC)C(O)CC3N1C2 MKYLOMHWHWEFCT-UHFFFAOYSA-N 0.000 claims description 2
- SNFRINMTRPQQLE-JQWAAABSSA-N Montanin Chemical compound O[C@H]([C@@]1(CO)O[C@H]1[C@H]1[C@H]2O3)[C@]4(O)C(=O)C(C)=C[C@H]4[C@]11OC3(CCCCCCCCCCC)O[C@@]2(C(C)=C)C[C@H]1C SNFRINMTRPQQLE-JQWAAABSSA-N 0.000 claims description 2
- SNFRINMTRPQQLE-OFGNMXNXSA-N Montanin Natural products O=C1[C@@]2(O)[C@@H](O)[C@@]3(CO)O[C@H]3[C@@H]3[C@H]4[C@@]5(C(=C)C)O[C@](CCCCCCCCCCC)(O4)O[C@@]3([C@H](C)C5)[C@@H]2C=C1C SNFRINMTRPQQLE-OFGNMXNXSA-N 0.000 claims description 2
- 239000004952 Polyamide Substances 0.000 claims description 2
- 239000004743 Polypropylene Substances 0.000 claims description 2
- QTZPBQMTXNEKRX-UHFFFAOYSA-N Voacristine pseudoindoxyl Natural products N1C2=CC=C(OC)C=C2C(=O)C21CCN(C1)C3C(C(C)O)CC1CC32C(=O)OC QTZPBQMTXNEKRX-UHFFFAOYSA-N 0.000 claims description 2
- 239000004203 carnauba wax Substances 0.000 claims description 2
- 235000013869 carnauba wax Nutrition 0.000 claims description 2
- 238000009833 condensation Methods 0.000 claims description 2
- 230000005494 condensation Effects 0.000 claims description 2
- 238000003801 milling Methods 0.000 claims description 2
- 239000011259 mixed solution Substances 0.000 claims description 2
- 238000002156 mixing Methods 0.000 claims description 2
- 229920002647 polyamide Polymers 0.000 claims description 2
- 229920001155 polypropylene Polymers 0.000 claims description 2
- 239000004170 rice bran wax Substances 0.000 claims description 2
- 235000019384 rice bran wax Nutrition 0.000 claims description 2
- 238000005299 abrasion Methods 0.000 abstract description 2
- 230000005672 electromagnetic field Effects 0.000 abstract description 2
- 239000002861 polymer material Substances 0.000 abstract description 2
- 238000000034 method Methods 0.000 description 8
- 230000010355 oscillation Effects 0.000 description 6
- 238000005516 engineering process Methods 0.000 description 4
- 239000000843 powder Substances 0.000 description 4
- 239000000243 solution Substances 0.000 description 4
- 239000002253 acid Substances 0.000 description 3
- 239000012736 aqueous medium Substances 0.000 description 3
- 238000006243 chemical reaction Methods 0.000 description 3
- 238000001816 cooling Methods 0.000 description 3
- 229960000935 dehydrated alcohol Drugs 0.000 description 3
- 238000004945 emulsification Methods 0.000 description 3
- 229910002804 graphite Inorganic materials 0.000 description 3
- 239000010439 graphite Substances 0.000 description 3
- 238000005498 polishing Methods 0.000 description 3
- 239000012286 potassium permanganate Substances 0.000 description 3
- 238000003756 stirring Methods 0.000 description 3
- CSCPPACGZOOCGX-UHFFFAOYSA-N Acetone Chemical compound CC(C)=O CSCPPACGZOOCGX-UHFFFAOYSA-N 0.000 description 2
- 229920002472 Starch Polymers 0.000 description 2
- 230000002776 aggregation Effects 0.000 description 2
- 239000013068 control sample Substances 0.000 description 2
- 239000000463 material Substances 0.000 description 2
- 239000003960 organic solvent Substances 0.000 description 2
- 230000003647 oxidation Effects 0.000 description 2
- 238000007254 oxidation reaction Methods 0.000 description 2
- 239000003973 paint Substances 0.000 description 2
- 235000019698 starch Nutrition 0.000 description 2
- 238000003860 storage Methods 0.000 description 2
- 238000012360 testing method Methods 0.000 description 2
- 230000008719 thickening Effects 0.000 description 2
- 238000005054 agglomeration Methods 0.000 description 1
- 238000004220 aggregation Methods 0.000 description 1
- 230000000694 effects Effects 0.000 description 1
- 229960004756 ethanol Drugs 0.000 description 1
- 239000008187 granular material Substances 0.000 description 1
- 238000009830 intercalation Methods 0.000 description 1
- 230000002687 intercalation Effects 0.000 description 1
- 239000002609 medium Substances 0.000 description 1
- 230000035515 penetration Effects 0.000 description 1
- 239000003208 petroleum Substances 0.000 description 1
- 239000000523 sample Substances 0.000 description 1
- 238000007711 solidification Methods 0.000 description 1
- 230000008023 solidification Effects 0.000 description 1
- 239000008107 starch Substances 0.000 description 1
- 238000010792 warming Methods 0.000 description 1
Abstract
Description
Claims (13)
Priority Applications (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
CN201310440876.3A CN103468004B (zh) | 2013-09-25 | 2013-09-25 | 负载纳米石墨烯的蜡浆及其制备方法和用途 |
Applications Claiming Priority (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
CN201310440876.3A CN103468004B (zh) | 2013-09-25 | 2013-09-25 | 负载纳米石墨烯的蜡浆及其制备方法和用途 |
Publications (2)
Publication Number | Publication Date |
---|---|
CN103468004A CN103468004A (zh) | 2013-12-25 |
CN103468004B true CN103468004B (zh) | 2015-12-23 |
Family
ID=49793057
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
CN201310440876.3A Active CN103468004B (zh) | 2013-09-25 | 2013-09-25 | 负载纳米石墨烯的蜡浆及其制备方法和用途 |
Country Status (1)
Country | Link |
---|---|
CN (1) | CN103468004B (zh) |
Families Citing this family (16)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US10927267B2 (en) | 2014-03-31 | 2021-02-23 | Ppg Industries Ohio, Inc. | Infrared fluorescent coatings |
CN105885439A (zh) * | 2014-08-26 | 2016-08-24 | 闫立群 | 一种基于表面改性石墨烯的保护蜡及其制备方法 |
CN104371412A (zh) * | 2014-12-16 | 2015-02-25 | 东莞市隆海新材料科技有限公司 | 一种耐磨蜡浆及其制备方法 |
CN105131730A (zh) * | 2015-08-13 | 2015-12-09 | 蚌埠市时代电子有限公司 | 一种环保散热涂料及其制备方法 |
CN105219266B (zh) * | 2015-11-03 | 2017-11-07 | 海宁皮革研究院 | 一种皮革用耐磨抗撕裂涂饰助剂及其制备方法 |
MX2018008032A (es) | 2015-12-29 | 2018-11-12 | Ppg Ind Ohio Inc | Recubrimientos fluorescentes infrarrojos. |
CN106498782A (zh) * | 2016-11-07 | 2017-03-15 | 苏州市兴丰强纺织科技有限公司 | 一种石墨烯发热面料及其制备方法 |
CN108641506B (zh) * | 2018-04-19 | 2021-02-26 | 苏州诺升功能高分子材料股份有限公司 | 一种基于聚四氟乙烯的复合纳米抗菌分散剂的制备方法 |
CN109853237A (zh) * | 2019-01-28 | 2019-06-07 | 上海矽联新材料科技有限公司 | 一种石墨烯改性氧化聚乙烯蜡乳液及其制备方法 |
CN109868651A (zh) * | 2019-01-28 | 2019-06-11 | 上海矽联新材料科技有限公司 | 一种石墨烯改性马来酸酐化聚乙烯蜡乳液及其制备方法 |
CN110684314B (zh) * | 2019-09-06 | 2020-11-10 | 东莞理工学院 | 一种精密铸造蜡及其制备方法 |
IT201900017942A1 (it) * | 2019-10-04 | 2021-04-04 | Leather Plus S R L | Metodo di trattamento funzionalizzante per pelli e simili. |
CN110643205B (zh) * | 2019-10-17 | 2021-04-06 | 江苏华光粉末有限公司 | 核壳结构有机改性石墨烯的制备方法、防腐粉末涂料及其制备方法 |
CN110655809B (zh) * | 2019-10-29 | 2021-02-05 | 江苏华光粉末有限公司 | 聚酰胺蜡改性海胆形石墨烯及其制备方法和防腐粉末涂料及其制备工艺 |
CN113382623B (zh) * | 2021-06-18 | 2022-10-28 | 西安交通大学 | 一种热、电磁多功能防护器及其制备方法 |
CN115232443A (zh) * | 2022-08-17 | 2022-10-25 | 安徽宇航派蒙健康科技股份有限公司 | 一种用石墨烯和聚合物制备导热复合材料的方法 |
Citations (7)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN102502593A (zh) * | 2011-10-11 | 2012-06-20 | 中国石油大学(北京) | 一种石墨烯、掺杂石墨烯或石墨烯复合物的制备方法 |
CN102532563A (zh) * | 2012-02-21 | 2012-07-04 | 南京天诗新材料科技有限公司 | 一种制备聚合物蜡水性分散体的方法 |
CN102636549A (zh) * | 2012-02-27 | 2012-08-15 | 苏州科技学院 | 胶束识别的人体血清中多巴胺的电化学传感器及测定方法 |
CN102732037A (zh) * | 2011-04-08 | 2012-10-17 | 中国科学院金属研究所 | 石墨烯泡沫∕聚合物高导电复合材料及其制备方法和应用 |
CN102816442A (zh) * | 2012-07-31 | 2012-12-12 | 华南理工大学 | 一种高导热复合材料 |
CN102838857A (zh) * | 2012-09-21 | 2012-12-26 | 南京天诗新材料科技有限公司 | 一种可生物降解的聚合物类蜡超细粉体及用途 |
CN103113786A (zh) * | 2013-03-07 | 2013-05-22 | 苏州牛剑新材料有限公司 | 一种石墨烯导电油墨及其制备方法 |
Family Cites Families (1)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
JP2013001882A (ja) * | 2011-06-21 | 2013-01-07 | Ulvac Japan Ltd | グラフェンインク及びその製造方法 |
-
2013
- 2013-09-25 CN CN201310440876.3A patent/CN103468004B/zh active Active
Patent Citations (7)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN102732037A (zh) * | 2011-04-08 | 2012-10-17 | 中国科学院金属研究所 | 石墨烯泡沫∕聚合物高导电复合材料及其制备方法和应用 |
CN102502593A (zh) * | 2011-10-11 | 2012-06-20 | 中国石油大学(北京) | 一种石墨烯、掺杂石墨烯或石墨烯复合物的制备方法 |
CN102532563A (zh) * | 2012-02-21 | 2012-07-04 | 南京天诗新材料科技有限公司 | 一种制备聚合物蜡水性分散体的方法 |
CN102636549A (zh) * | 2012-02-27 | 2012-08-15 | 苏州科技学院 | 胶束识别的人体血清中多巴胺的电化学传感器及测定方法 |
CN102816442A (zh) * | 2012-07-31 | 2012-12-12 | 华南理工大学 | 一种高导热复合材料 |
CN102838857A (zh) * | 2012-09-21 | 2012-12-26 | 南京天诗新材料科技有限公司 | 一种可生物降解的聚合物类蜡超细粉体及用途 |
CN103113786A (zh) * | 2013-03-07 | 2013-05-22 | 苏州牛剑新材料有限公司 | 一种石墨烯导电油墨及其制备方法 |
Also Published As
Publication number | Publication date |
---|---|
CN103468004A (zh) | 2013-12-25 |
Similar Documents
Publication | Publication Date | Title |
---|---|---|
CN103468004B (zh) | 负载纳米石墨烯的蜡浆及其制备方法和用途 | |
Song et al. | Synthesis of CeO2-coated SiO2 nanoparticle and dispersion stability of its suspension | |
CN104470644B (zh) | 用于化学机械平坦化浆料的接触释放胶囊 | |
CN103351651B (zh) | 一种纳米二硫化钼有机分散液的制备方法 | |
Wang et al. | Synthesis of silica-coated ZnO nanocomposite: the resonance structure of polyvinyl pyrrolidone (PVP) as a coupling agent | |
CN103788402B (zh) | 一种碳量子点/锂皂石乳液稳定体系及制备石蜡乳液的方法 | |
CN109079154A (zh) | 一种纳米银及其合成方法 | |
CN103467829A (zh) | 负载纳米二氧化硅的蜡水性分散体及其制备方法和用途 | |
CN103979612A (zh) | 一种制备四氧化三铁纳米粒子的方法 | |
Grzelczak et al. | A general approach toward polymer-coated plasmonic nanostructures | |
CN110551486A (zh) | 一种含气凝胶的相变膜的制备方法 | |
Yang et al. | Preparation and tribological properties of dual-coated CuO nanoparticles as water based lubricant additives | |
CN106744738A (zh) | 一种制备六方氮化硼纳米层片的方法 | |
CN107768061B (zh) | 一种包硅纳米磁球的制备方法 | |
Zheng et al. | High performance shear thickening fluid based on calcinated colloidal silica microspheres | |
CN102181126B (zh) | 一种低表面能聚合物微胶囊及其制备方法 | |
Antosik et al. | Effect of SiO2 particle size and length of polypropylene glycol) chain on rheological properties of shear thickening fluids | |
CN103301763B (zh) | 一种在水溶液中分散纳米碳酸钙粉体材料的方法 | |
CN108822738B (zh) | 一种琉璃化学抛光液 | |
CN107384544A (zh) | 一种长效防锈的气相防锈材料及其制备方法 | |
CN104445333A (zh) | 一种纳米沉淀法生产碳酸钙工艺 | |
CN106673072A (zh) | 一种用于磁性液体的纳米Fe3O4颗粒及其制备方法 | |
CN113880081B (zh) | 石墨烯的制备方法 | |
CN103194096A (zh) | 一种纳米材料表面改性方法 | |
CN102516820A (zh) | 溶剂型纳米硫酸钡分散液及其制备方法 |
Legal Events
Date | Code | Title | Description |
---|---|---|---|
C06 | Publication | ||
PB01 | Publication | ||
C10 | Entry into substantive examination | ||
SE01 | Entry into force of request for substantive examination | ||
C14 | Grant of patent or utility model | ||
GR01 | Patent grant | ||
EE01 | Entry into force of recordation of patent licensing contract | ||
EE01 | Entry into force of recordation of patent licensing contract |
Application publication date: 20131225 Assignee: Yangzhou Tianshi new Mstar Technology Ltd Assignor: Nanjing Tianshi New Material Technology Co., Ltd. Contract record no.: 2017320000206 Denomination of invention: Nano-graphene loaded wax liquor, and preparation method and use thereof Granted publication date: 20151223 License type: Common License Record date: 20171218 |
|
PE01 | Entry into force of the registration of the contract for pledge of patent right |
Denomination of invention: Nano-graphene loaded wax liquor, and preparation method and use thereof Effective date of registration: 20191028 Granted publication date: 20151223 Pledgee: Jiangsu Zijin rural commercial bank Limited by Share Ltd branch of science and technology Pledgor: Nanjing Tianshi New Material Technology Co., Ltd. Registration number: Y2019320000227 |
|
PE01 | Entry into force of the registration of the contract for pledge of patent right | ||
PC01 | Cancellation of the registration of the contract for pledge of patent right |
Date of cancellation: 20200903 Granted publication date: 20151223 Pledgee: Jiangsu Zijin rural commercial bank Limited by Share Ltd. branch of science and technology Pledgor: NANJING TIANSHI NEW MATERIAL TECHNOLOGY Co.,Ltd. Registration number: Y2019320000227 |
|
PC01 | Cancellation of the registration of the contract for pledge of patent right | ||
PE01 | Entry into force of the registration of the contract for pledge of patent right |
Denomination of invention: Preparation and application of nano graphene supported wax slurry Effective date of registration: 20200909 Granted publication date: 20151223 Pledgee: Jiangsu Zijin rural commercial bank Limited by Share Ltd. branch of science and technology Pledgor: NANJING TIANSHI NEW MATERIAL TECHNOLOGY Co.,Ltd. Registration number: Y2020980005857 |
|
PE01 | Entry into force of the registration of the contract for pledge of patent right |