CN103463655A - Natural lavender incense piece and preparation method thereof - Google Patents
Natural lavender incense piece and preparation method thereof Download PDFInfo
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- CN103463655A CN103463655A CN201310400807XA CN201310400807A CN103463655A CN 103463655 A CN103463655 A CN 103463655A CN 201310400807X A CN201310400807X A CN 201310400807XA CN 201310400807 A CN201310400807 A CN 201310400807A CN 103463655 A CN103463655 A CN 103463655A
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Abstract
The invention discloses a natural lavender incense piece and a preparation method thereof. The natural lavender incense piece comprises the following components in percent by weight: 59-79 percent of a matrix body, 20-40 percent of natural lavender microcapsules and 1 percent of auxiliary additives, wherein the matrix body is all-tree lavender powder which can pass through a 40-80-mesh sieve; the natural lavender microcapsules are spherical natural lavender microcapsules formed by using natural lavender essential oil as a core material and beta-cyclodextrin as a wall material, and the particle diameter of each natural lavender microcapsule is 5-10 microns; the auxiliary additives refer to carrageenan, konjac glucomannan, pectin or xanthan gum. The preparation method comprises the steps: firstly, preparing the natural lavender microcapsules, then uniformly mixing the natural lavender microcapsules, the matrix body and the auxiliary additives to obtain a mixture, placing the mixture in a mould, extruding and forming the mixture on a preforming machine to obtain the natural lavender incense pieces. The natural lavender incense piece disclosed by the invention is purely natural in adopted raw materials, and has the advantages of uniformity in fragrance releasing, durability in fragrance holding, and non toxicity; the preparation method is simple, economic and efficient.
Description
Technical field
What the present invention relates to is a kind of natural lavandula angustifolia incense sheet and preparation method thereof.
Background technology
Because the effective ingredient of most of mosquito incenses is pyrethrin insecticides.Contain harmful material ultrafine dust (diameter is less than the particulate matter of 2.5 μ m) in the cigarette of mosquito incense burning.Therefore, may cause asthma in a short time, for a long time may cause cancer, they are mosquito incense base material products of incomplete combustion for polycyclic aromatic hydrocarbons (PAHs), belong to possibility carcinogen carbonyl compound (as formaldehyde and acetaldehyde), this compounds can stimulate upper respiratory tract.In addition, burning can produce a small amount of benzene, and benzene to be a kind of meeting make neurotoxic and carcinogenic material Long Term Contact can affect bone marrow.
Although electric mosquito repellent has replaced traditional mosquito incense gradually, the anophelifuge principle of electric mosquito repellent is by the suction anti-mosquito incense sheets such as pyrethrin, after heating, evaporates, and discharges insecticide substance to reach continuous heating, although use conveniently.But, because the insect killing substance used has certain toxicity, as used for a long time, may produce untoward reaction to human body in closed room.
Herba Lysimachiae foenum-graeci quintessence oil is to be refined and to be formed by lavandula angustifolia, can heat-clearing and toxic substances removing, cleaning skin, control oil content, freckle removing and whitening, wrinkle removal skin care, eye haustra-dsipelling black eye, also can promote skin-protecting function such as damaged tissues regeneration recoverys grade.It can purify, pacify soul, alleviates indignation and used-up sensation, makes the people can face life even-tempered and good-humouredly.Heart is had to sedation effect, can reduce hypertension, pacify cardiopalmus, helpful for insomnia.It is one of best pain relieving quintessence oil, can effectively improve muscle spasm, to spraining, muscle overuses and rheumatalgia also has good mitigation.But Herba Lysimachiae foenum-graeci quintessence oil is volatile, fragrance is short release time, and inhomogeneous, and this can have a strong impact on its effect in use.
Through retrieval, not yet find to utilize Herba Lysimachiae foenum-graeci quintessence oil to replace in mosquito incense the noxious substances such as Pyrethrum, reaching fresh air, except the relevant report of mosquito, deinsectization.
Summary of the invention
One of purpose of the present invention is in order to overcome the deficiency of existing mosquito incense and some incense sheets, to propose a kind of natural lavandula angustifolia incense sheet.This natural lavandula angustifolia incense sheet has the safety non-toxic to people, has the effect except mosquito, deinsectization fresh air simultaneously.
Two of purpose of the present invention is to provide the preparation method of above-mentioned a kind of natural lavandula angustifolia incense sheet.
Know-why of the present invention
A kind of natural lavandula angustifolia incense sheet of the present invention, utilize the inclusion complexation method, take beta-schardinger dextrin-as the wall material, prepares natural Lavender microcapsule.Give natural Lavender microcapsule odor characteristic by natural Herba Lysimachiae foenum-graeci quintessence oil, utilize hollow structure and the spatial volume matching effect of beta-schardinger dextrin-, adsorb natural Herba Lysimachiae foenum-graeci quintessence oil.
The inclusion complexation method is to take the microcapsule preparation method of beta-schardinger dextrin-as the wall material.Beta-schardinger dextrin-is that 7 Glucopyranose .s connect into by α-Isosorbide-5-Nitrae glycosidic bond, has the material of ring shaped molecule structure.Its molecule becomes oil cake shape, and the structure ，Ta center with hollow has hydrophobicity, and skin is hydrophilic.Simultaneously, beta-schardinger dextrin-has the spatial volume matching effect, and has the interaction by non-covalent bond of suitable size, shape and hydrophobic molecule and forms stable clathrate.Therefore, many hydrophobic essence materials, pigment and vitamin can replace the hydrone at its center and and its strong complexation.
Technical scheme of the present invention
A kind of natural lavandula angustifolia incense sheet, calculate by mass percentage, and its raw material composition and content are as follows:
Matrix 59～79%
Natural Lavender microcapsule 20～40%
Auxiliary agent 1%;
The Herb lavandula angustifolia powder that described matrix was 40～80 mesh sieves;
Described natural Lavender microcapsule, the natural Lavender microcapsule of the spherical form that the natural Herba Lysimachiae foenum-graeci quintessence oil of take forms as the wall material as core, the beta-schardinger dextrin-of take, its particle diameter is preferably 5～10 μ m;
In described natural Lavender microcapsule, core and wall material are calculated by mass percentage, and its content is as follows:
Wall material 50～90%
Core 10～50%;
Described auxiliary agent is carrageenan, Konjac glucomannan, pectin or xanthan gum, is preferably Konjac glucomannan or pectin.
The preparation method of above-mentioned a kind of natural lavandula angustifolia incense sheet, specifically comprise the steps:
(1), the preparation of natural Lavender microcapsule
Be dissolved in dehydrated alcohol and ultrasonic being uniformly dispersed by natural Herba Lysimachiae foenum-graeci quintessence oil, obtain the natural Herba Lysimachiae foenum-graeci quintessence oil alcoholic solution of 200-400g/L;
Beta-schardinger dextrin-is dissolved in the distilled water of 50 ℃, obtains the beta-schardinger dextrin-aqueous solution of 40g/L;
Utilize under the mixing speed that magnetic stirring apparatus is 400～2000rpm at rotating speed, controlling drop rate is that 2-4ml/min joins resulting natural Herba Lysimachiae foenum-graeci quintessence oil alcoholic solution in the beta-schardinger dextrin-aqueous solution, and standing 24h after stirring 2h, sucking filtration, the gained filter cake, in 50 ℃ of lower forced air dryings of air dry oven, is obtained to natural Lavender microcapsule;
(2), after the natural Lavender microcapsule of step (1) gained, matrix and auxiliary agent mix homogeneously, be put in mould, carry out extrusion modling on tablet machine, obtain natural lavandula angustifolia incense sheet.
Beneficial effect of the present invention
A kind of natural lavandula angustifolia incense sheet of the present invention, owing to having adopted the essence microcapsule coating technology, the raw material pure natural used, nontoxic.Therefore, in the time of not only can improving direct use Herba Lysimachiae foenum-graeci quintessence oil, volatile, fragrance remaining time is short, fragrance discharges the shortcomings such as inhomogeneous, can also avoid using in the mosquito incense electric mosquito repellent the harmful drawbacks of insect killing substance such as pyrethrin.In addition, the effect that also there is fresh air.
The specific embodiment
Below by specific embodiment, the present invention is further set forth, but do not limit the present invention.
In various embodiments of the present invention, the information of the specification of various raw materials used or reagent and manufacturer is as follows:
The Herb lavandula angustifolia, Xinjiang Yili of China lavandula angustifolia villa garden;
Dehydrated alcohol, analytical pure, Chemical Reagent Co., Ltd., Sinopharm Group;
Beta-schardinger dextrin-, analytical pure, Chemical Reagent Co., Ltd., Sinopharm Group;
Konjac glucomannan, analytical pure, Chemical Reagent Co., Ltd., Sinopharm Group;
Carrageenan, analytical pure, Chemical Reagent Co., Ltd., Sinopharm Group;
Pectin, analytical pure, Chemical Reagent Co., Ltd., Sinopharm Group;
Xanthan gum, analytical pure, Chemical Reagent Co., Ltd., Sinopharm Group;
Herba Lysimachiae foenum-graeci quintessence oil, Xinjiang Yili of China lavandula angustifolia villa garden.
In various embodiments of the present invention, the information of the model of instrument and equipment used and manufacturer is as follows:
Tablet machine, Chengdu bright brightness machinery company limited;
Electronic balance, PL403, prunus mume (sieb.) sieb.et zucc. Teller-Tuo benefit Instrument Ltd.;
Constant temperature blender with magnetic force, 524G, Mei Ying Pu, Shanghai instrument and meter Manufacturing Co., Ltd;
The multiplex vacuum pump of circulating water type, SHZ-D III, the Shanghai special instrument and equipment company limited of shining;
The digital display blast drier, 101, the Shanghai leaf is opened up the instrument and meter company limited.
embodiment 1
A kind of natural lavandula angustifolia incense sheet, calculate by mass percentage, and its raw material composition and content are as follows:
Matrix 15g (74%)
Natural Lavender microcapsule 5g (25%)
Auxiliary agent 0.2g (1%);
The Herb lavandula angustifolia powder that described matrix was 40～80 mesh sieves;
Described natural Lavender microcapsule, the natural Lavender microcapsule of the spherical form that the natural Herba Lysimachiae foenum-graeci quintessence oil of take forms as core and beta-schardinger dextrin-as the wall material, its particle diameter is preferably 5～10 μ m;
In described natural Lavender microcapsule, core and wall material are calculated by mass percentage, and its content is as follows:
Wall material 8g (67%)
Core 4g (33%);
Described auxiliary agent is Konjac glucomannan.
The preparation method of above-mentioned a kind of natural lavandula angustifolia incense sheet, specifically comprise the steps:
(1), in 20mL dehydrated alcohol that 4g lavandula angustifolia type quintessence oil is dissolved in and ultrasonic being uniformly dispersed, obtain the natural Herba Lysimachiae foenum-graeci quintessence oil alcoholic solution of 200g/L;
The 8g beta-schardinger dextrin-is dissolved in to 200mL, the deionized water of 50 ℃ under magnetic agitation, obtains the beta-schardinger dextrin-aqueous solution of 40g/L;
Utilizing magnetic stirring apparatus is under 50 ℃, the rotating speed mixing speed that is 600rpm in temperature, controlling drop rate is that 3ml/min joins resulting natural Herba Lysimachiae foenum-graeci quintessence oil alcoholic solution in the beta-schardinger dextrin-aqueous solution, and standing 24h after stirring 2h, sucking filtration, and by the gained filter cake in 50 ℃ of lower forced air dryings of air dry oven, obtaining particle diameter is the natural Lavender microcapsule of 5～10 μ m;
(2), the preparation of lavandula angustifolia incense sheet:
Natural Lavender microcapsule, 15g matrix gained in 5g step (1), after 0.2g auxiliary agent mix homogeneously, at ambient temperature, be put into it in preset mould, carries out extrusion modling on tablet machine, obtains natural lavandula angustifolia incense sheet.
For making it more attractive in appearance, can be finally in the one side of the natural lavandula angustifolia incense sheet of gained, be sprinkled into a certain amount of lavandula angustifolia dry flower, make it stick to natural lavandula angustifolia incense sheet surface.
The natural lavandula angustifolia incense sheet of above-mentioned gained, special fragrance with natural lavandula angustifolia, the empirical tests natural lavandula angustifolia incense sheet that the present embodiment is prepared is positioned in confined chamber, indoor lavandula angustifolia fragrance is sustainable more than 8 hours, and aroma strength is good, can reach the standard that substitutes electric mosquito repellent.
embodiment 2
A kind of natural lavandula angustifolia incense sheet, calculate by mass percentage, and its raw material composition and content are as follows:
Matrix 20g (79%)
Natural Lavender microcapsule 5g (20%)
Auxiliary agent 0.25g (1%);
The Herb that described matrix was 40～80 mesh sieves smokes the clothing powder;
Described natural Lavender microcapsule, the natural Lavender microcapsule of the spherical form that the natural Herba Lysimachiae foenum-graeci quintessence oil of take forms as core and beta-schardinger dextrin-as the wall material, its particle diameter is preferably 5～10 μ m;
In described natural Lavender microcapsule, core and wall material are calculated by mass percentage, and its content is as follows:
Wall material 4g (50%)
Core 4g (50%);
Described auxiliary agent is pectin.
The preparation method of above-mentioned a kind of natural lavandula angustifolia incense sheet, specifically comprise the steps:
(1), in 10mL dehydrated alcohol that 4g lavandula angustifolia type quintessence oil is dissolved in and ultrasonic being uniformly dispersed, obtain the natural Herba Lysimachiae foenum-graeci quintessence oil alcoholic solution of 400g/L;
The 4g beta-schardinger dextrin-is dissolved in to 100mL, the deionized water of 50 ℃ under magnetic agitation, obtains the beta-schardinger dextrin-aqueous solution of 40g/L;
Utilizing magnetic stirring apparatus is under 50 ℃, the rotating speed mixing speed that is 600rpm in temperature, controlling drop rate is that 2ml/min joins resulting natural Herba Lysimachiae foenum-graeci quintessence oil alcoholic solution in the beta-schardinger dextrin-aqueous solution, and standing 24h after stirring 2h, sucking filtration, and by the gained filter cake in 50 ℃ of lower forced air dryings of air dry oven, obtaining particle diameter is the natural Lavender microcapsule of 5～10 μ m;
(2), the preparation of lavandula angustifolia incense sheet
Natural Lavender microcapsule, 20g matrix gained in 5g step (1), after 0.25g auxiliary agent mix homogeneously, at ambient temperature, be put into it in preset mould, carries out extrusion modling on tablet machine, obtains natural lavandula angustifolia incense sheet.
For making it more attractive in appearance, can be finally in the one side of the natural lavandula angustifolia incense sheet of gained, be sprinkled into a certain amount of lavandula angustifolia dry flower, make it stick to natural lavandula angustifolia incense sheet surface.
The natural lavandula angustifolia incense sheet of above-mentioned gained, special fragrance with natural lavandula angustifolia, the empirical tests natural lavandula angustifolia incense sheet that the present embodiment is prepared is positioned in confined chamber, indoor lavandula angustifolia fragrance is sustainable more than 8 hours, and aroma strength is good, can reach the standard that substitutes electric mosquito repellent.
embodiment 3
A kind of natural lavandula angustifolia incense sheet, calculate by mass percentage, and its raw material composition and content are as follows:
Matrix 7.5g (59%)
Natural Lavender microcapsule 5g (40%)
Auxiliary agent 0.12g (1%);
The Herb lavandula angustifolia powder that described matrix was 40～80 mesh sieves;
Described natural Lavender microcapsule, the natural Lavender microcapsule of the spherical form that the natural Herba Lysimachiae foenum-graeci quintessence oil of take forms as core and beta-schardinger dextrin-as the wall material, its particle diameter is preferably 5～10 μ m;
In described natural Lavender microcapsule, core and wall material are calculated by mass percentage, and its content is as follows:
Wall material 18g(90%)
Core 2g(10%);
Described auxiliary agent is Konjac glucomannan.
The preparation method of above-mentioned a kind of natural lavandula angustifolia incense sheet, specifically comprise the steps:
(1), in 10mL dehydrated alcohol that 2g lavandula angustifolia type quintessence oil is dissolved in and ultrasonic being uniformly dispersed, obtain the natural Herba Lysimachiae foenum-graeci quintessence oil alcoholic solution of 200g/L;
The 18g beta-schardinger dextrin-is dissolved in to 450mL, the deionized water of 50 ℃ under magnetic agitation, obtains the beta-schardinger dextrin-aqueous solution of 40g/L;
Utilizing magnetic stirring apparatus is under 50 ℃, the rotating speed mixing speed that is 600rpm in temperature, controlling drop rate is that 4ml/min joins resulting natural Herba Lysimachiae foenum-graeci quintessence oil alcoholic solution in the beta-schardinger dextrin-aqueous solution, and standing 24h after stirring 2h, sucking filtration, and by the gained filter cake in 50 ℃ of lower forced air dryings of air dry oven, obtaining particle diameter is the natural Lavender microcapsule of 5～10 μ m;
(2), the preparation of lavandula angustifolia incense sheet:
Natural Lavender microcapsule, 7.5g matrix gained in 5g step (1), after 0.12g auxiliary agent mix homogeneously, at ambient temperature, be put into it in preset mould, carries out extrusion modling on tablet machine, obtains natural lavandula angustifolia incense sheet.
For making it more attractive in appearance, can be finally in the one side of the natural lavandula angustifolia incense sheet of gained, be sprinkled into a certain amount of lavandula angustifolia dry flower, make it stick to natural lavandula angustifolia incense sheet surface.
Foregoing is the basic explanation under conceiving for the present invention only, and, according to any equivalent transformation that technical scheme of the present invention is done, all should belong to protection scope of the present invention.
Claims (4)
1. a natural lavandula angustifolia incense sheet, is characterized in that calculating by mass percentage, and its raw material composition and content are as follows:
Matrix 59～79%
Natural Lavender microcapsule 20～40%
Auxiliary agent 1%;
The Herb lavandula angustifolia powder that described matrix was 40～80 mesh sieves;
Described natural Lavender microcapsule, take natural Herba Lysimachiae foenum-graeci quintessence oil as core, the spherical natural Lavender microcapsule that the beta-schardinger dextrin-of take forms as the wall material;
Described auxiliary agent is carrageenan, Konjac glucomannan, pectin or xanthan gum.
2. a kind of natural lavandula angustifolia incense sheet as claimed in claim 1, is characterized in that, in described natural Lavender microcapsule, core and wall material are calculated by mass percentage, and its content is as follows:
Wall material 50～90%
Core 10～50%.
3. a kind of natural lavandula angustifolia incense sheet as claimed in claim 1, is characterized in that the spherical form that described natural Lavender microcapsule is particle diameter 5～10 μ m.
4. as the preparation method of claim 1,2 or 3 described a kind of natural lavandula angustifolia incense sheets, it is characterized in that specifically comprising the steps:
(1), the preparation of natural Lavender microcapsule
Natural Herba Lysimachiae foenum-graeci quintessence oil is dissolved in to ultrasonic being uniformly dispersed in dehydrated alcohol, obtains the natural Herba Lysimachiae foenum-graeci quintessence oil alcoholic solution of 200-400g/L;
Beta-schardinger dextrin-is dissolved in the distilled water of 50 ℃, obtains the beta-schardinger dextrin-aqueous solution of 40g/L;
Utilize under the mixing speed that magnetic stirring apparatus is 400～2000rpm at rotating speed, controlling drop rate is that 2-4ml/min is added drop-wise to the natural Herba Lysimachiae foenum-graeci quintessence oil alcoholic solution obtained in the beta-schardinger dextrin-aqueous solution, and standing 24h after stirring 2h, sucking filtration, and by the gained filter cake in 50 ℃ of lower forced air dryings, obtain natural Lavender microcapsule;
(2), after the natural Lavender microcapsule of step (1) gained, matrix and auxiliary agent mix homogeneously, be put in mould, carry out extrusion modling on tablet machine, obtain natural lavandula angustifolia incense sheet.
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| CN105140595A (en) * | 2015-09-06 | 2015-12-09 | 河南科技大学 | Electrolyte corrosion inhibitor, electrolyte for aluminum air cell and aluminum air cell |
| CN105596319A (en) * | 2016-01-31 | 2016-05-25 | 杭州睩客科技有限公司 | Borneol fragrant slice and preparation method thereof |
| CN105638759A (en) * | 2016-01-19 | 2016-06-08 | 深圳中纺滤材科技有限公司 | Air purification material and preparation method thereof |
| CN106860898A (en) * | 2017-02-28 | 2017-06-20 | 广西秀美壮乡能源环保有限公司 | A kind of preparation method of solid freshener |
| CN107996615A (en) * | 2017-11-24 | 2018-05-08 | 泉州永春达盛香业股份有限公司 | A kind of mosquito repellent stacte and its preparation process |
| CN108378265A (en) * | 2018-04-16 | 2018-08-10 | 齐鲁工业大学 | A method of extending the long-life noodles shelf-life |
| CN110680947A (en) * | 2019-10-24 | 2020-01-14 | 郑刚 | Lavender slow-release fragrance source body and preparation method thereof |
| CN113845977A (en) * | 2021-10-13 | 2021-12-28 | 上海应用技术大学 | Lavender essential oil microcapsule and preparation method thereof |
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Cited By (12)
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| CN105140595A (en) * | 2015-09-06 | 2015-12-09 | 河南科技大学 | Electrolyte corrosion inhibitor, electrolyte for aluminum air cell and aluminum air cell |
| CN105140595B (en) * | 2015-09-06 | 2018-01-09 | 河南科技大学 | A kind of electrolyte corrosion inhibitor, aluminium-air cell electrolyte and aluminium-air cell |
| CN105638759A (en) * | 2016-01-19 | 2016-06-08 | 深圳中纺滤材科技有限公司 | Air purification material and preparation method thereof |
| CN105638759B (en) * | 2016-01-19 | 2019-01-18 | 深圳中纺滤材科技有限公司 | A kind of material for air purification and preparation method thereof |
| CN105596319A (en) * | 2016-01-31 | 2016-05-25 | 杭州睩客科技有限公司 | Borneol fragrant slice and preparation method thereof |
| CN106860898A (en) * | 2017-02-28 | 2017-06-20 | 广西秀美壮乡能源环保有限公司 | A kind of preparation method of solid freshener |
| CN106860898B (en) * | 2017-02-28 | 2020-01-10 | 台州中知英健机械自动化有限公司 | Preparation method of solid freshener |
| CN107996615A (en) * | 2017-11-24 | 2018-05-08 | 泉州永春达盛香业股份有限公司 | A kind of mosquito repellent stacte and its preparation process |
| CN108378265A (en) * | 2018-04-16 | 2018-08-10 | 齐鲁工业大学 | A method of extending the long-life noodles shelf-life |
| CN108378265B (en) * | 2018-04-16 | 2021-05-28 | 齐鲁工业大学 | Method for prolonging shelf life of fresh wet noodles |
| CN110680947A (en) * | 2019-10-24 | 2020-01-14 | 郑刚 | Lavender slow-release fragrance source body and preparation method thereof |
| CN113845977A (en) * | 2021-10-13 | 2021-12-28 | 上海应用技术大学 | Lavender essential oil microcapsule and preparation method thereof |
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Application publication date: 20131225 |