CN103403929A - 锂电池的两相正极材料及其合成方法 - Google Patents
锂电池的两相正极材料及其合成方法 Download PDFInfo
- Publication number
- CN103403929A CN103403929A CN2012800120661A CN201280012066A CN103403929A CN 103403929 A CN103403929 A CN 103403929A CN 2012800120661 A CN2012800120661 A CN 2012800120661A CN 201280012066 A CN201280012066 A CN 201280012066A CN 103403929 A CN103403929 A CN 103403929A
- Authority
- CN
- China
- Prior art keywords
- lithium
- type
- oxide
- metal
- metal oxide
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Granted
Links
- 229910052744 lithium Inorganic materials 0.000 title claims abstract description 53
- WHXSMMKQMYFTQS-UHFFFAOYSA-N Lithium Chemical compound [Li] WHXSMMKQMYFTQS-UHFFFAOYSA-N 0.000 title claims abstract description 52
- 239000007774 positive electrode material Substances 0.000 title claims abstract description 9
- 238000000034 method Methods 0.000 title claims description 11
- 230000015572 biosynthetic process Effects 0.000 title claims description 5
- 238000003786 synthesis reaction Methods 0.000 title claims description 5
- 239000000463 material Substances 0.000 claims abstract description 26
- 229910044991 metal oxide Inorganic materials 0.000 claims abstract description 25
- 150000004706 metal oxides Chemical class 0.000 claims abstract description 25
- 239000002245 particle Substances 0.000 claims abstract description 18
- 229910052751 metal Inorganic materials 0.000 claims abstract description 9
- 239000002184 metal Substances 0.000 claims abstract description 9
- 238000010438 heat treatment Methods 0.000 claims abstract description 8
- 239000007864 aqueous solution Substances 0.000 claims abstract description 7
- 238000002156 mixing Methods 0.000 claims abstract description 7
- 229910052782 aluminium Inorganic materials 0.000 claims abstract description 6
- 239000002243 precursor Substances 0.000 claims abstract description 6
- 229910052725 zinc Inorganic materials 0.000 claims abstract description 5
- 239000011572 manganese Substances 0.000 claims description 32
- PXHVJJICTQNCMI-UHFFFAOYSA-N nickel Substances [Ni] PXHVJJICTQNCMI-UHFFFAOYSA-N 0.000 claims description 32
- 239000010406 cathode material Substances 0.000 claims description 13
- 150000001875 compounds Chemical class 0.000 claims description 11
- 239000000203 mixture Substances 0.000 claims description 10
- WMFOQBRAJBCJND-UHFFFAOYSA-M Lithium hydroxide Chemical compound [Li+].[OH-] WMFOQBRAJBCJND-UHFFFAOYSA-M 0.000 claims description 6
- 229910012985 LiVO3 Inorganic materials 0.000 claims description 3
- 229910003206 NH4VO3 Inorganic materials 0.000 claims description 3
- 239000011248 coating agent Substances 0.000 claims description 3
- 238000000576 coating method Methods 0.000 claims description 3
- 238000001816 cooling Methods 0.000 claims description 3
- 238000010791 quenching Methods 0.000 claims description 3
- 230000000171 quenching effect Effects 0.000 claims description 3
- 239000012080 ambient air Substances 0.000 claims description 2
- 150000004649 carbonic acid derivatives Chemical class 0.000 claims description 2
- XGZVUEUWXADBQD-UHFFFAOYSA-L lithium carbonate Chemical compound [Li+].[Li+].[O-]C([O-])=O XGZVUEUWXADBQD-UHFFFAOYSA-L 0.000 claims description 2
- 229910052808 lithium carbonate Inorganic materials 0.000 claims description 2
- 229940093474 manganese carbonate Drugs 0.000 claims description 2
- 235000006748 manganese carbonate Nutrition 0.000 claims description 2
- 239000011656 manganese carbonate Substances 0.000 claims description 2
- 229910000016 manganese(II) carbonate Inorganic materials 0.000 claims description 2
- 229910000008 nickel(II) carbonate Inorganic materials 0.000 claims description 2
- 150000002823 nitrates Chemical class 0.000 claims description 2
- 150000003467 sulfuric acid derivatives Chemical class 0.000 claims description 2
- 229910019501 NaVO3 Inorganic materials 0.000 claims 1
- CMZUMMUJMWNLFH-UHFFFAOYSA-N sodium metavanadate Chemical compound [Na+].[O-][V](=O)=O CMZUMMUJMWNLFH-UHFFFAOYSA-N 0.000 claims 1
- 230000002194 synthesizing effect Effects 0.000 claims 1
- 239000000126 substance Substances 0.000 abstract description 5
- 230000002427 irreversible effect Effects 0.000 description 14
- 238000002441 X-ray diffraction Methods 0.000 description 6
- 239000002131 composite material Substances 0.000 description 5
- 238000001308 synthesis method Methods 0.000 description 5
- 238000005516 engineering process Methods 0.000 description 4
- 239000000843 powder Substances 0.000 description 4
- 238000004458 analytical method Methods 0.000 description 3
- 238000001228 spectrum Methods 0.000 description 3
- 238000003860 storage Methods 0.000 description 3
- 238000010189 synthetic method Methods 0.000 description 3
- 229910018072 Al 2 O 3 Inorganic materials 0.000 description 2
- IJGRMHOSHXDMSA-UHFFFAOYSA-N Atomic nitrogen Chemical compound N#N IJGRMHOSHXDMSA-UHFFFAOYSA-N 0.000 description 2
- HBBGRARXTFLTSG-UHFFFAOYSA-N Lithium ion Chemical compound [Li+] HBBGRARXTFLTSG-UHFFFAOYSA-N 0.000 description 2
- XLOMVQKBTHCTTD-UHFFFAOYSA-N Zinc monoxide Chemical compound [Zn]=O XLOMVQKBTHCTTD-UHFFFAOYSA-N 0.000 description 2
- 239000011149 active material Substances 0.000 description 2
- 239000003570 air Substances 0.000 description 2
- 230000001351 cycling effect Effects 0.000 description 2
- 229910001416 lithium ion Inorganic materials 0.000 description 2
- 239000000243 solution Substances 0.000 description 2
- 229910052723 transition metal Inorganic materials 0.000 description 2
- 150000003624 transition metals Chemical class 0.000 description 2
- KMTRUDSVKNLOMY-UHFFFAOYSA-N Ethylene carbonate Chemical compound O=C1OCCO1 KMTRUDSVKNLOMY-UHFFFAOYSA-N 0.000 description 1
- 229910013870 LiPF 6 Inorganic materials 0.000 description 1
- 101100513612 Microdochium nivale MnCO gene Proteins 0.000 description 1
- 229910016485 Mn1/3Ni1/3Co1/3 Inorganic materials 0.000 description 1
- 239000002033 PVDF binder Substances 0.000 description 1
- 238000003991 Rietveld refinement Methods 0.000 description 1
- 229910004298 SiO 2 Inorganic materials 0.000 description 1
- 229910006404 SnO 2 Inorganic materials 0.000 description 1
- 229910010413 TiO 2 Inorganic materials 0.000 description 1
- -1 V 2 O 5 or VO x Chemical class 0.000 description 1
- 239000002253 acid Substances 0.000 description 1
- XAGFODPZIPBFFR-UHFFFAOYSA-N aluminium Chemical compound [Al] XAGFODPZIPBFFR-UHFFFAOYSA-N 0.000 description 1
- QVGXLLKOCUKJST-UHFFFAOYSA-N atomic oxygen Chemical compound [O] QVGXLLKOCUKJST-UHFFFAOYSA-N 0.000 description 1
- 230000005540 biological transmission Effects 0.000 description 1
- 239000006229 carbon black Substances 0.000 description 1
- 238000012512 characterization method Methods 0.000 description 1
- 238000006243 chemical reaction Methods 0.000 description 1
- 239000013078 crystal Substances 0.000 description 1
- IEJIGPNLZYLLBP-UHFFFAOYSA-N dimethyl carbonate Chemical compound COC(=O)OC IEJIGPNLZYLLBP-UHFFFAOYSA-N 0.000 description 1
- 238000001035 drying Methods 0.000 description 1
- 239000007772 electrode material Substances 0.000 description 1
- 239000003792 electrolyte Substances 0.000 description 1
- 238000001704 evaporation Methods 0.000 description 1
- 230000008020 evaporation Effects 0.000 description 1
- 238000000227 grinding Methods 0.000 description 1
- 238000009830 intercalation Methods 0.000 description 1
- 230000002687 intercalation Effects 0.000 description 1
- 239000007788 liquid Substances 0.000 description 1
- 239000011244 liquid electrolyte Substances 0.000 description 1
- 238000004519 manufacturing process Methods 0.000 description 1
- 239000000320 mechanical mixture Substances 0.000 description 1
- 229910052987 metal hydride Inorganic materials 0.000 description 1
- 150000004681 metal hydrides Chemical class 0.000 description 1
- 229910000652 nickel hydride Inorganic materials 0.000 description 1
- 229910052757 nitrogen Inorganic materials 0.000 description 1
- 229910052760 oxygen Inorganic materials 0.000 description 1
- 239000001301 oxygen Substances 0.000 description 1
- 229920002981 polyvinylidene fluoride Polymers 0.000 description 1
- 238000001878 scanning electron micrograph Methods 0.000 description 1
- 238000004626 scanning electron microscopy Methods 0.000 description 1
- 239000006104 solid solution Substances 0.000 description 1
- 238000003756 stirring Methods 0.000 description 1
- 239000000725 suspension Substances 0.000 description 1
- 238000007669 thermal treatment Methods 0.000 description 1
- 238000004627 transmission electron microscopy Methods 0.000 description 1
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 1
Images
Classifications
-
- H—ELECTRICITY
- H01—ELECTRIC ELEMENTS
- H01M—PROCESSES OR MEANS, e.g. BATTERIES, FOR THE DIRECT CONVERSION OF CHEMICAL ENERGY INTO ELECTRICAL ENERGY
- H01M4/00—Electrodes
- H01M4/02—Electrodes composed of, or comprising, active material
- H01M4/36—Selection of substances as active materials, active masses, active liquids
- H01M4/48—Selection of substances as active materials, active masses, active liquids of inorganic oxides or hydroxides
- H01M4/485—Selection of substances as active materials, active masses, active liquids of inorganic oxides or hydroxides of mixed oxides or hydroxides for inserting or intercalating light metals, e.g. LiTi2O4 or LiTi2OxFy
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01D—COMPOUNDS OF ALKALI METALS, i.e. LITHIUM, SODIUM, POTASSIUM, RUBIDIUM, CAESIUM, OR FRANCIUM
- C01D15/00—Lithium compounds
- C01D15/02—Oxides; Hydroxides
-
- H—ELECTRICITY
- H01—ELECTRIC ELEMENTS
- H01M—PROCESSES OR MEANS, e.g. BATTERIES, FOR THE DIRECT CONVERSION OF CHEMICAL ENERGY INTO ELECTRICAL ENERGY
- H01M4/00—Electrodes
- H01M4/02—Electrodes composed of, or comprising, active material
- H01M4/13—Electrodes for accumulators with non-aqueous electrolyte, e.g. for lithium-accumulators; Processes of manufacture thereof
- H01M4/131—Electrodes based on mixed oxides or hydroxides, or on mixtures of oxides or hydroxides, e.g. LiCoOx
-
- H—ELECTRICITY
- H01—ELECTRIC ELEMENTS
- H01M—PROCESSES OR MEANS, e.g. BATTERIES, FOR THE DIRECT CONVERSION OF CHEMICAL ENERGY INTO ELECTRICAL ENERGY
- H01M4/00—Electrodes
- H01M4/02—Electrodes composed of, or comprising, active material
- H01M4/36—Selection of substances as active materials, active masses, active liquids
- H01M4/362—Composites
- H01M4/366—Composites as layered products
-
- H—ELECTRICITY
- H01—ELECTRIC ELEMENTS
- H01M—PROCESSES OR MEANS, e.g. BATTERIES, FOR THE DIRECT CONVERSION OF CHEMICAL ENERGY INTO ELECTRICAL ENERGY
- H01M4/00—Electrodes
- H01M4/02—Electrodes composed of, or comprising, active material
- H01M4/36—Selection of substances as active materials, active masses, active liquids
- H01M4/48—Selection of substances as active materials, active masses, active liquids of inorganic oxides or hydroxides
- H01M4/50—Selection of substances as active materials, active masses, active liquids of inorganic oxides or hydroxides of manganese
- H01M4/505—Selection of substances as active materials, active masses, active liquids of inorganic oxides or hydroxides of manganese of mixed oxides or hydroxides containing manganese for inserting or intercalating light metals, e.g. LiMn2O4 or LiMn2OxFy
-
- H—ELECTRICITY
- H01—ELECTRIC ELEMENTS
- H01M—PROCESSES OR MEANS, e.g. BATTERIES, FOR THE DIRECT CONVERSION OF CHEMICAL ENERGY INTO ELECTRICAL ENERGY
- H01M4/00—Electrodes
- H01M4/02—Electrodes composed of, or comprising, active material
- H01M4/36—Selection of substances as active materials, active masses, active liquids
- H01M4/48—Selection of substances as active materials, active masses, active liquids of inorganic oxides or hydroxides
- H01M4/52—Selection of substances as active materials, active masses, active liquids of inorganic oxides or hydroxides of nickel, cobalt or iron
- H01M4/525—Selection of substances as active materials, active masses, active liquids of inorganic oxides or hydroxides of nickel, cobalt or iron of mixed oxides or hydroxides containing iron, cobalt or nickel for inserting or intercalating light metals, e.g. LiNiO2, LiCoO2 or LiCoOxFy
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02E—REDUCTION OF GREENHOUSE GAS [GHG] EMISSIONS, RELATED TO ENERGY GENERATION, TRANSMISSION OR DISTRIBUTION
- Y02E60/00—Enabling technologies; Technologies with a potential or indirect contribution to GHG emissions mitigation
- Y02E60/10—Energy storage using batteries
Landscapes
- Chemical & Material Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Electrochemistry (AREA)
- General Chemical & Material Sciences (AREA)
- Inorganic Chemistry (AREA)
- Engineering & Computer Science (AREA)
- Materials Engineering (AREA)
- Composite Materials (AREA)
- Organic Chemistry (AREA)
- Battery Electrode And Active Subsutance (AREA)
- Inorganic Compounds Of Heavy Metals (AREA)
Abstract
Description
Claims (12)
Applications Claiming Priority (3)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
FR1100057A FR2970376B1 (fr) | 2011-01-07 | 2011-01-07 | Materiau d'electrode positive biphase pour accumulateur au lithium et son procede de synthese |
FR1100057 | 2011-01-07 | ||
PCT/FR2012/050045 WO2012093239A1 (fr) | 2011-01-07 | 2012-01-06 | Matériau d'électrode positive biphase pour accumulateur au lithium et son procédé de synthèse |
Publications (2)
Publication Number | Publication Date |
---|---|
CN103403929A true CN103403929A (zh) | 2013-11-20 |
CN103403929B CN103403929B (zh) | 2016-02-17 |
Family
ID=44461982
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
CN201280012066.1A Active CN103403929B (zh) | 2011-01-07 | 2012-01-06 | 锂电池的两相正极材料及其合成方法 |
Country Status (7)
Country | Link |
---|---|
US (1) | US9359220B2 (zh) |
EP (1) | EP2661780B1 (zh) |
JP (1) | JP5968339B2 (zh) |
KR (1) | KR101760114B1 (zh) |
CN (1) | CN103403929B (zh) |
FR (1) | FR2970376B1 (zh) |
WO (1) | WO2012093239A1 (zh) |
Cited By (2)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN105813981A (zh) * | 2013-12-17 | 2016-07-27 | 陶氏环球技术有限责任公司 | 改进的锂金属氧化物阴极材料及其制备方法 |
CN115863571A (zh) * | 2022-12-01 | 2023-03-28 | 宁德时代新能源科技股份有限公司 | 正极活性材料及其制备方法、二次电池和用电装置 |
Families Citing this family (6)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
FR2996838B1 (fr) * | 2012-10-17 | 2014-11-21 | Commissariat Energie Atomique | Procede de preparation d'un oxyde mixte de titane et de niobium par traitement solvothermal ; electrode et accumulateur au lithium comprenant ledit oxyde mixte |
JP6251042B2 (ja) * | 2014-01-06 | 2017-12-20 | 株式会社東芝 | 電極及び非水電解質電池 |
US20190020057A1 (en) * | 2016-03-03 | 2019-01-17 | Nec Energy Devices, Ltd. | Positive electrode for lithium-ion secondary battery and lithium-ion secondary battery |
FR3061992B1 (fr) * | 2017-01-19 | 2021-12-17 | Commissariat Energie Atomique | Materiau d'electrode positive a base d'un oxyde lamellaire lithie recouvert, en tout ou partie, par un autre oxyde a base de manganese et procede de preparation de ce materiau |
KR102116005B1 (ko) * | 2017-12-29 | 2020-05-28 | 포항공과대학교 산학협력단 | 리튬 이차 전지용 양극 활물질의 제조방법 및 리튬 이차 전지용 양극 활물질 |
US20240262709A1 (en) * | 2023-02-01 | 2024-08-08 | Stratus Materials Inc. | Substituted lithium-rich cathode materials |
Citations (4)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN1667865A (zh) * | 2004-03-12 | 2005-09-14 | 三星Sdi株式会社 | 锂二次电池 |
US20060093871A1 (en) * | 2004-10-29 | 2006-05-04 | Medtronic, Inc. | Lithium-ion battery |
CN1898824A (zh) * | 2003-12-23 | 2007-01-17 | 特诺有限公司 | 用于锂充电电池的高压薄片阴极材料,以及其制造方法 |
US20090081529A1 (en) * | 2007-09-21 | 2009-03-26 | Uchicago Argonne, Llc | Positive electrodes for lithium batteries |
Family Cites Families (13)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
GB8916568D0 (en) * | 1989-07-20 | 1989-09-06 | Dowty Electronic Components | A battery |
US6017654A (en) * | 1997-08-04 | 2000-01-25 | Carnegie Mellon University | Cathode materials for lithium-ion secondary cells |
WO2002086993A1 (fr) * | 2001-04-20 | 2002-10-31 | Yuasa Corporation | Matiere active anodique et son procede de production, anode pour pile secondaire a electrolyte non aqueux et pile secondaire a electrolyte non aqueux |
KR100420034B1 (ko) * | 2001-10-17 | 2004-02-25 | 삼성에스디아이 주식회사 | 리튬 이차 전지용 양극 활물질의 제조방법 |
JP2007123251A (ja) * | 2005-09-28 | 2007-05-17 | Sanyo Electric Co Ltd | 非水電解質二次電池 |
JP5076332B2 (ja) * | 2006-03-06 | 2012-11-21 | ソニー株式会社 | 正極活物質の製造方法、および非水電解質二次電池の製造方法 |
KR101264332B1 (ko) | 2006-09-20 | 2013-05-14 | 삼성에스디아이 주식회사 | 캐소드 활물질 및 이를 채용한 리튬 전지 |
CN101542788A (zh) * | 2006-09-25 | 2009-09-23 | 德克萨斯州立大学董事会 | 具有低不可逆容量损失的经表面和整体改性的高容量层状氧化物阴极 |
KR100814885B1 (ko) * | 2006-11-17 | 2008-03-20 | 삼성에스디아이 주식회사 | 리튬 이차 전지 |
US7981545B2 (en) * | 2006-12-28 | 2011-07-19 | Samsung Sdi Co., Ltd. | Negative active material for rechargeable lithium battery and rechargeable lithium battery including the same |
KR101430615B1 (ko) * | 2007-09-19 | 2014-08-14 | 삼성에스디아이 주식회사 | 캐소드 및 이를 채용한 리튬 전지 |
FR2932175B1 (fr) * | 2008-06-05 | 2011-06-03 | Commissariat Energie Atomique | Materiau d'electrode positive forme d'un oxyde de type lamellaire pour accumulateur au lithium. |
JP2010027482A (ja) * | 2008-07-23 | 2010-02-04 | Sony Corp | 正極活物質の製造方法および正極活物質 |
-
2011
- 2011-01-07 FR FR1100057A patent/FR2970376B1/fr not_active Expired - Fee Related
-
2012
- 2012-01-06 CN CN201280012066.1A patent/CN103403929B/zh active Active
- 2012-01-06 EP EP12702593.0A patent/EP2661780B1/fr not_active Not-in-force
- 2012-01-06 JP JP2013547899A patent/JP5968339B2/ja active Active
- 2012-01-06 WO PCT/FR2012/050045 patent/WO2012093239A1/fr active Application Filing
- 2012-01-06 US US13/978,556 patent/US9359220B2/en not_active Expired - Fee Related
- 2012-01-06 KR KR1020137020664A patent/KR101760114B1/ko active Active
Patent Citations (4)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN1898824A (zh) * | 2003-12-23 | 2007-01-17 | 特诺有限公司 | 用于锂充电电池的高压薄片阴极材料,以及其制造方法 |
CN1667865A (zh) * | 2004-03-12 | 2005-09-14 | 三星Sdi株式会社 | 锂二次电池 |
US20060093871A1 (en) * | 2004-10-29 | 2006-05-04 | Medtronic, Inc. | Lithium-ion battery |
US20090081529A1 (en) * | 2007-09-21 | 2009-03-26 | Uchicago Argonne, Llc | Positive electrodes for lithium batteries |
Cited By (3)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN105813981A (zh) * | 2013-12-17 | 2016-07-27 | 陶氏环球技术有限责任公司 | 改进的锂金属氧化物阴极材料及其制备方法 |
CN115863571A (zh) * | 2022-12-01 | 2023-03-28 | 宁德时代新能源科技股份有限公司 | 正极活性材料及其制备方法、二次电池和用电装置 |
CN115863571B (zh) * | 2022-12-01 | 2025-02-18 | 宁德时代新能源科技股份有限公司 | 正极活性材料及其制备方法、二次电池和用电装置 |
Also Published As
Publication number | Publication date |
---|---|
JP2014506387A (ja) | 2014-03-13 |
FR2970376A1 (fr) | 2012-07-13 |
KR101760114B1 (ko) | 2017-07-31 |
WO2012093239A1 (fr) | 2012-07-12 |
CN103403929B (zh) | 2016-02-17 |
JP5968339B2 (ja) | 2016-08-10 |
KR20140043320A (ko) | 2014-04-09 |
US20130344388A1 (en) | 2013-12-26 |
EP2661780A1 (fr) | 2013-11-13 |
US9359220B2 (en) | 2016-06-07 |
EP2661780B1 (fr) | 2015-05-20 |
FR2970376B1 (fr) | 2013-01-25 |
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