CN103385848B - Lotion and preparation method and application - Google Patents

Lotion and preparation method and application Download PDF

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Publication number
CN103385848B
CN103385848B CN201310264258.8A CN201310264258A CN103385848B CN 103385848 B CN103385848 B CN 103385848B CN 201310264258 A CN201310264258 A CN 201310264258A CN 103385848 B CN103385848 B CN 103385848B
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extract
skin
astringent
add
allantoin
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CN103385848A (en
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林志隆
黄妙葵
任巍
覃显丽
刘艳峰
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ANGLEE COSMETIC TECHNOLOGY Co Ltd
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ANGLEE COSMETIC TECHNOLOGY Co Ltd
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Abstract

The invention belongs to cosmetic field, and particularly relates to a lotion. The lotion provided by the invention comprises butylene glycol, polyquaternium salt-51, pansy extract, yeast extract, PCA sodium, soybean commensal matter extract, imperata rhizome extract, tremella extract, sweet orange flower extract, panthenol, Beta-glucose, EDTA disodium, vegetable amino acid, xanthan gum, hyaluronic acid, allantoin, imidiazolidinyl urea, iodopropynyl butylcarbamate and pure water. The lotion is rich in French Alps spring which injects moisture component to skin any time and releases water continuously to skin to help the moisture component permeate the bottom of the skin, and raise water content of surface layer of the skin, enhance skin natural moisture retention capacity, supplement skin nutrition, raise skin elasticity, reduce wrinkle, enhance skin defense function, prevent repeatedly occurrence of the dry skin, and recover the dry and dark skin back to smooth and moisture state.

Description

A kind of astringent and its preparation method and application
Technical field
The present invention relates to cosmetic field, be specifically related to a kind of astringent and its preparation method and application.
Background technology
The modern life and working environment cause the investigation of 2002 of skin premature aging and show: the modern life and working environment cause women's skin quality generally to decline, and occur low and deep, flavescence, lax, microgroove, decortication, coarse six large skin initial stage catabiosis." Chinese women skin investigation report " shows, 71% women has xerosis cutis symptom, the dry maximum puzzlement that has become Chinese women skin.Investigation shows, for a long time in air conditioner surroundings, for a long time in the face of radiation, poor sleeping quality, diet are irregular, the cosmetic custom of mistake, be to cause the large factor of women's skin problem most important five.
Xerodermatic major reason is that horny layer moisture reduces because playing the lipid of lock water moisture-keeping function in intercellular substance loses, and skin barrier is impaired.To resist drying, form good living habit essential.In life, select applicable skin care item, reduce number of times, the time of correctly clean skin, minimizing Exposure to Sunlight, shortening and computer intimate contact etc. of making up as far as possible, all can reduce the infringement to skin barrier.
Good skin quality is only aging crucial skin protection expert of delaying skin initial stage and points out, general synthetic nutrient is difficult to penetrate the ABB of skin, and nutrient can only rest on skin surface, and skin is nutrition for want of, cause skin quality to decline, be only improved skin quality ability delaying skin aging.
Listing in the market, research and develop or improved Anji is uncommon can just comprise more than 30 kinds such as the beautiful fair-skinned makeup removing breast of water, beautiful fair-skinned clean the glue of water, the beautiful fair-skinned 24H moisture content massage cream of water, the beautiful fair-skinned MASQUE APAISANT HYDRATANT of water, the beautiful fair-skinned 24H moisture content essence of water, the beautiful fair-skinned 24H moisturizing emulsion of water by youngster ANS water of life series of products.
Summary of the invention
In order to improve the tender moist sense of skin water, clear away the obscure colour of skin, represent smooth bright good complexion, Anji is uncommon can youngster ANS series of products on, the invention discloses a kind of astringent.
Astringent of the present invention comprises butanediol, polyquaternary ammonium salt-51, Herba Violae Hortensis extract, yeast extract, Anjidew NL50, soybean symbiosome extract, Rhizoma Imperatae extract, Tremella extract, orange blossom extract, pantothenylol, Beta-glucose, EDETATE SODIUM, plant amino acid, xanthan gum, hyaluronic acid, allantoin, imidazolidinyl urea, iodine propilolic alcohol butyl mephenesin Carbamate and pure water.
The content (mark meter by weight) that the present invention further defines the each composition of this astringent is: butanediol 0.5%~3%, polyquaternary ammonium salt-510.1%~1%, Herba Violae Hortensis extract 0.1%~0.5%, yeast extract 0.05%~0.3%, Anjidew NL50 0.05%~0.2%, soybean symbiosome extract 0.05%~0.2%, Rhizoma Imperatae extract 0.05%~0.2%, Tremella extract 0.05%~0.2%, orange blossom extract 0.05%~0.2%, pantothenylol 0.1%~0.5%, Beta-glucose 0.05%~0.3%, EDETATE SODIUM 0.05%~0.2%, plant amino acid 0.1%~0.5%, xanthan gum 0.05%~0.2%, hyaluronic acid 0.05%~0.3%, allantoin 0.05%~0.3%, imidazolidinyl urea 0.05%~0.2%, iodine propilolic alcohol butyl mephenesin Carbamate 0.05%~0.2%, surplus is pure water.
The present invention is further preferred, and the content of the each composition of this astringent (mark meter by weight :) is butanediol 1%, polyquaternary ammonium salt-510.5%, Herba Violae Hortensis extract 0.3%, yeast extract 0.2%, Anjidew NL50 0.1%, soybean symbiosome extract 0.1%, Rhizoma Imperatae extract 0.1%, Tremella extract 0.1%, orange blossom extract 0.1%, pantothenylol 0.3%, Beta-glucose 0.2%, EDETATE SODIUM 0.1%, plant amino acid 0.3%, xanthan gum 0.1%, hyaluronic acid 0.2%, allantoin 0.2%, imidazolidinyl urea 0.1%, iodine propilolic alcohol butyl mephenesin Carbamate 0.1%, surplus is pure water.
Astringent described above, preferably, the specification of above-mentioned astringent is 400mL.
Astringent described above, preferably, the specification of above-mentioned astringent is 100mL.
Astringent described above, preferably, is prepared according to the following steps:
1. in pure water, add butanediol, EDETATE SODIUM, PVC sodium, to complete swelling, add polyquaternary ammonium salt-51, be warming up to 90 DEG C and be stirred to dissolving completely, be incubated 20 minutes;
2. continue to add Beta-glucose, be stirred to after dissolving completely, then add pantothenylol, plant amino acid, xanthan gum, hyaluronic acid, allantoin to stir;
3. by step 2. solution be cooled to 50 DEG C, add Herba Violae Hortensis extract, yeast extract, soybean symbiosome extract, Rhizoma Imperatae extract, Tremella extract, orange blossom extract, be incubated 20 minutes.
4. under stirring state, 3. step is cooled to 45 DEG C and adds below imidazolidinyl urea and iodine propilolic alcohol butyl mephenesin Carbamate, stirs, and is cooled to room temperature and can obtains this product.
The application of astringent described above, preferably, this astringent is applicable to dryness, adult form skin.
The using method of astringent described above, preferably, this astringent, after clean skin of morning and evening, is got and is patted in right amount in several cervical regions of face with clean skin cotton or finger, to be absorbed.
In astringent of the present invention, concrete effect of some compositions and relative theory are:
Allantoin: be a kind of amphoteric compound, can form double salt in conjunction with many kinds of substance, there is lucifuge, sterilization and anticorrosion, pain relieving, antioxidation, can make skin keep moisture content, moisten and soft, have protective tissue, hydrophilic, absorb water and the effect such as prevent that moisture from distributing; Can make the soft high resilience of skin, and have beautiful gloss.
Hyaluronic acid: can help skin to draw a large amount of moisture, can moment deep moisturizing, increase skin elasticity and tension force, help and recover the normal oil-water balance of skin, improve dry and lax skin.
Yeast extract: contain different types of nucleic acid substances, vitamin and aminoacid, have natural nutrient component in these groups.There is obvious protection effect to resist active oxygen and lipid peroxidation, have good effect for preventing and slowing down skin aging.
Plant amino acid: commercially available or according to CN102943097A method system.Plant is the favor of the Nature, absorbs world anima and life brilliance, be rare treasured, and plant amino acid is in plant, extract high nutrient and concentrated, and its effect is powerful, effect is remarkable, can allow skin feel more silkiness soft and smooth.
Excellent moistening effect: the important element that has comprised the lasting Glycerins of 16 remainders, assist skin to recover desirable moisturizing degree.
Absorb immediately: can naturally incorporate skin, absorb completely, not waste.
Moisten immediately: salubrious as water, and be rich in calcium, manganese, zinc isoreactivity moisturizing composition, skin is infiltrated seemingly in the bosom of sweet spring water water, perfect the natural moisturizing mechanism of skin, skin will be felt instant tender with extraordinarily of moistening.
Long-acting soft skin: round-the-clock moistening effect, and strengthen skin moisturizing barrier, skin will no longer feel tight, only have comfortable tender impression.
Compared with prior art, the present invention has following beneficial effect:
The present invention can inject the powerful wet composition of mending for skin, discharge moisture continuously to skin, allow the wet composition of benefit directly ooze skin bottom, improve skin top layer water content simultaneously, strengthen skin natural moisture preserving power, supplement nutrient to skin, strengthen skin elasticity, reduce wrinkle, strengthen skin defensive enginery, stop dry skin problem repeatedly to occur, dry, the obscure skin of order is replied the tender state of soft and smooth full water; Also can releive skin, resist dry, strengthening skin, in and free radical, promotion skin cell renewal.Wherein be rich in the activity that " magnesium " element more can kinase, keep activation, equilibrium water conten function to reach.
Adjust with the collocation of various active moisturizing composition, make the effective ingredient in sweet spring water water go deep into skin deep layer cell centre, sustained release, continually for skin brings comfortable pure and fresh moistening effect, makes the lasting water profit of skin, more can be applicable to environmental change.With up-to-date nanotechnology, allow the nanometer skin moistening factor infiltrate fast skin, improve from inside to outside skin smoothness and elasticity, and the interpolation of multinomial vegetalitas moisturizing and whitening composition more can improve the tender moist sense of skin water, and clear away the obscure colour of skin, represent smooth bright good complexion!
Specific embodiment
Further explain the present invention below in conjunction with embodiment, but embodiment does not limit in any form to the present invention.
Embodiment 1,
Mark meter by weight: butanediol 1%, polyquaternary ammonium salt-510.5%, Herba Violae Hortensis extract 0.3%, yeast extract 0.2%, Anjidew NL50 0.1%, soybean symbiosome extract 0.1%, Rhizoma Imperatae extract 0.1%, Tremella extract 0.1%, orange blossom extract 0.1%, pantothenylol 0.3%, Beta-glucose 0.2%, EDETATE SODIUM 0.1%, plant amino acid 0.3%, xanthan gum 0.1%, hyaluronic acid 0.2%, allantoin 0.2%, imidazolidinyl urea 0.1%, iodine propilolic alcohol butyl mephenesin Carbamate 0.1%, surplus is pure water.Press the specification preparation of 400ml.
According to above-mentioned formula, be prepared according to following steps:
1. in pure water, add butanediol, EDETATE SODIUM, PVC sodium, to complete swelling, add polyquaternary ammonium salt-51, be warming up to 90 DEG C and be stirred to dissolving completely, be incubated 20 minutes;
2. continue to add Beta-glucose, be stirred to after dissolving completely, then add pantothenylol, plant amino acid, xanthan gum, hyaluronic acid, allantoin to stir;
3. by step 2. solution be cooled to 50 DEG C, add Herba Violae Hortensis extract, yeast extract, soybean symbiosome extract, Rhizoma Imperatae extract, Tremella extract, orange blossom extract, be incubated 20 minutes.
4. under stirring state, 3. step is cooled to 45 DEG C and adds below imidazolidinyl urea and iodine propilolic alcohol butyl mephenesin Carbamate, stirs, and is cooled to room temperature and can obtains this product.
Embodiment 2
Mark meter by weight: butanediol 0.5%, polyquaternary ammonium salt-510.1%, Herba Violae Hortensis extract 0.1%, yeast extract 0.05%, Anjidew NL50 0.05%, soybean symbiosome extract 0.05%, Rhizoma Imperatae extract 0.05%, Tremella extract 0.05%, orange blossom extract 0.05%, pantothenylol 0.1%, Beta-glucose 0.05%, EDETATE SODIUM 0.05%, plant amino acid 0.1%, xanthan gum 0.05%, hyaluronic acid 0.05%, allantoin 0.05%, imidazolidinyl urea 0.05%, iodine propilolic alcohol butyl mephenesin Carbamate 0.05%, by the specification preparation of 100ml.
Preparation method is as embodiment 1.
Embodiment 3
Mark meter by weight: butanediol 3%, polyquaternary ammonium salt-511%, Herba Violae Hortensis extract 0.5%, yeast extract 0.3%, Anjidew NL50 0.2%, soybean symbiosome extract 0.2%, Rhizoma Imperatae extract 0.2%, Tremella extract 0.2%, orange blossom extract 0.2%, pantothenylol 0.5%, Beta-glucose 0.3%, EDETATE SODIUM 0.2%, plant amino acid 0.5%, xanthan gum 0.2%, hyaluronic acid 0.3%, allantoin 0.3%, imidazolidinyl urea 0.2%, iodine propilolic alcohol butyl mephenesin Carbamate 0.2%, by the specification preparation of 400ml.
Preparation method is as embodiment 1.
Comparative example 4,
In formula, do not add hyaluronic acid, allantoin, the other the same as in Example 1.
Comparative example 5,
In formula, do not add Rhizoma Imperatae extract, Tremella extract, orange blossom extract, the other the same as in Example 1.
Comparative example 6,
In formula, do not add pantothenylol, plant amino acid, xanthan gum, the other the same as in Example 1.
Embodiment 7, Product Safety evaluation (human skin patch)
7.1 trial targets: the astringent that embodiment 1-3, comparative example 4-6 are prepared.
7.2 tested crowds
Number: 30 people
Age: between 20~50 years old
Sex: female 23 people, male 7 people
Health status: experimenter's skin health, without dermatosis allergies, meets experimenter and volunteer inclusion criteria.
7.3 patch methods: select qualified speckle examination device, with closed patch test method, by about tested material 0.020mL~0.025mL(semifluid) drip in speckle examination device, external special adhesive tape is covered on experimenter back, after 24 hours, remove tested material, within after removing respectively 0.5,6,12,24,48 hour, observe dermoreaction, record its result according to dermoreaction grade scale in " cosmetics health specification ".
7.4 result of the test
Human skin patch result shows: 30 experimenters are by astringent of the present invention (embodiment 1-3), reference substance (comparative example 4-6) patch test, observed dermoreaction at 0.5,6,12,24,48 hour, there is skin adverse reaction in 0 example wherein, illustrates that astringent of the present invention uses safety.
Embodiment 8,
8.1 trial targets: the astringent that embodiment 1-3, comparative example 4-6 are prepared
8.2 tested crowds
Sex number: female, 50 people
Age: between 20~40 years old
Health status: experimenter's skin health, without dermatosis allergies, meets experimenter and volunteer inclusion criteria.
8.3 method of testings: after experimenter face is clean, respectively astringent prepared to embodiment 1-3, comparative example 4-6 is coated on two cheek in left and right, observes and experience result of use.
8.4 testing evaluation results are as follows:
(8 days) on probation feedback conclusive table of table 1. embodiment 1 preparing product
(8 weeks) on probation feedback conclusive table of table 2. embodiment 1 preparing product
(7 days) on probation feedback conclusive table of table 3. embodiment 2-3 preparing product
(7 days) on probation feedback conclusive table of certain moisturizing emulsion of table 4. comparative example 4-6
Tester all represents, embodiment 1 preparing product is better than the prepared product of embodiment 2,3 in every respect, and is all better than the prepared product of comparative example 4-6, also not sticky after use, absorb fast, the rapid full water profit of skin.After often using, improve skin water content, strengthened skin moisturizing power and enhancing skin elasticity, more can improve the tender moist sense of skin water, cleared away the obscure colour of skin.In the questionnaire of user, there is not people to have allergic phenomena simultaneously.
Embodiment 9,
9.1 trial targets: embodiment 1-3 astringent, commercially available similar cosmetics
9.2 tested crowds
Sex number: female, 50 people
Age: between 20~40 years old
Health status: experimenter's skin health, without dermatosis allergies, meets experimenter and volunteer inclusion criteria.
9.3 method of testings: after experimenter face is clean, respectively embodiment 1-3 astringent, commercially available similar cosmetics are coated on two cheek in left and right, observe and experience result of use.
9.4 testing evaluation results are as follows:
Table 1. improves the contrast statistical table of the colour of skin
Tester all represents, in moisture-retaining capacity with improve aspect the colour of skin, embodiment 1 preparing product is better than the prepared product of embodiment 2,3 in every respect, is all better than commercially available similar cosmetics, and tester all particularly approves embodiment 1 preparing product.
The foregoing is only embodiments of the invention; not thereby limit the scope of the claims of the present invention; every equivalent structure or conversion of equivalent flow process that utilizes description of the present invention to do; or be directly or indirectly used in other relevant technical fields, within being all in like manner included in scope of patent protection of the present invention.

Claims (6)

1. an astringent, it is characterized in that, comprise following composition, according to weight fraction meter: butanediol 0.5% ~ 3%, polyquaternary ammonium salt-51 0.1% ~ 1%, Herba Violae Hortensis extract 0.1% ~ 0.5%, yeast extract 0.05% ~ 0.3%, Anjidew NL50 0.05% ~ 0.2%, soybean symbiosome extract 0.05% ~ 0.2%, Rhizoma Imperatae extract 0.05% ~ 0.2%, Tremella extract 0.05% ~ 0.2%, orange blossom extract 0.05% ~ 0.2%, pantothenylol 0.1% ~ 0.5%, Beta-glucose 0.05% ~ 0.3%, EDETATE SODIUM 0.05% ~ 0.2%, plant amino acid 0.1% ~ 0.5%, xanthan gum 0.05% ~ 0.2%, hyaluronic acid 0.05% ~ 0.3%, allantoin 0.05% ~ 0.3%, imidazolidinyl urea 0.05% ~ 0.2%, iodine propilolic alcohol butyl mephenesin Carbamate 0.05% ~ 0.2%, surplus is pure water,
It is prepared according to the following steps:
In pure water, add butanediol, EDTA disodium, PVC sodium, to complete swelling, add polyquaternary ammonium salt-51, be warming up to 90oC and be stirred to dissolving completely, be incubated 20 minutes;
Continue to add Beta-glucose, be stirred to after dissolving completely, then add pantothenylol, plant amino acid, xanthan gum, hyaluronic acid, allantoin to stir;
Step solution is cooled to 50oC, adds Herba Violae Hortensis extract, yeast extract, soybean symbiosome extract, Rhizoma Imperatae extract, Tremella extract, orange blossom extract, be incubated 20 minutes;
Under stirring state, step is cooled to 45 DEG C and adds below imidazolidinyl urea and iodine propilolic alcohol butyl mephenesin Carbamate, stirs, and is cooled to room temperature and can obtains this product.
2. astringent as claimed in claim 1, it is characterized in that, mark meter by weight: butanediol 1%, polyquaternary ammonium salt-510.5%, Herba Violae Hortensis extract 0.3%, yeast extract 0.2%, PCA sodium 0.1%, soybean symbiosome extract 0.1%, Rhizoma Imperatae extract 0.1%, Tremella extract 0.1%, orange blossom extract 0.1%, pantothenylol 0.3%, Beta-glucose 0.2%, EDTA disodium 0.1%, plant amino acid 0.3%, xanthan gum 0.1%, hyaluronic acid 0.2%, allantoin 0.2%, imidazolidinyl urea 0.1%, iodine propilolic alcohol butyl mephenesin Carbamate 0.1%, surplus is pure water.
3. astringent as claimed in claim 2, is characterized in that, the specification of this astringent is 400mL.
4. astringent as claimed in claim 2, is characterized in that, the specification of this astringent is 100mL.
5. described in claim 1-4 any one, make up as an application for moisture-keeping cosmetics, it is characterized in that, this astringent is suitable for dryness, adult form skin.
6. a using method for astringent described in claim 1-4 any one, is characterized in that, this astringent, after clean skin of morning and evening, is got and patted in right amount in several cervical regions of face with clean skin cotton or finger, to be absorbed.
CN201310264258.8A 2013-06-27 2013-06-27 Lotion and preparation method and application Active CN103385848B (en)

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CN104224644A (en) * 2014-10-14 2014-12-24 萱肌蜜(香港)生物科技有限公司 Skin care preparation
CN104434768B (en) * 2014-12-10 2017-04-12 上海新高姿化妆品有限公司 Moisturizing lotion with slow-release efficacy and preparation method of moisturizing lotion
CN105078814A (en) * 2014-12-19 2015-11-25 赵雅珺 Face cleanser
CN104644507B (en) * 2015-02-12 2016-01-20 安婕妤化妆品科技股份有限公司 A kind of nursing class cream cream composition
CN104644525B (en) * 2015-02-12 2016-03-30 安婕妤化妆品科技股份有限公司 A kind of gentle moist type cleansing milk
CN104666236B (en) * 2015-02-13 2016-02-17 安婕妤化妆品科技股份有限公司 A kind of preserving moisture and protecting skin facial film
CN105662955A (en) * 2016-01-27 2016-06-15 安婕妤化妆品科技股份有限公司 Cosmetic containing methyl-pyrimidine type substances
CN106619243A (en) * 2017-02-24 2017-05-10 韩后化妆品股份有限公司 Composition with moisture-preserving and antiallergic effects and application thereof
CN109106622B (en) * 2018-11-02 2021-05-25 广州艾蓓生物科技有限公司 Cleansing milk with moisturizing and repairing functions and preparation method thereof

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