CN103385848A - Lotion and preparation method and application - Google Patents

Lotion and preparation method and application Download PDF

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Publication number
CN103385848A
CN103385848A CN2013102642588A CN201310264258A CN103385848A CN 103385848 A CN103385848 A CN 103385848A CN 2013102642588 A CN2013102642588 A CN 2013102642588A CN 201310264258 A CN201310264258 A CN 201310264258A CN 103385848 A CN103385848 A CN 103385848A
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extract
skin
astringent
add
allantoin
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CN103385848B (en
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林志隆
黄妙葵
任巍
覃显丽
刘艳峰
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ANGLEE COSMETIC TECHNOLOGY Co Ltd
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ANGLEE COSMETIC TECHNOLOGY Co Ltd
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Abstract

The invention belongs to cosmetic field, and particularly relates to a lotion. The lotion provided by the invention comprises butylene glycol, polyquaternium salt-51, pansy extract, yeast extract, PCA sodium, soybean commensal matter extract, imperata rhizome extract, tremella extract, sweet orange flower extract, panthenol, Beta-glucose, EDTA disodium, vegetable amino acid, xanthan gum, hyaluronic acid, allantoin, imidiazolidinyl urea, iodopropynyl butylcarbamate and pure water. The lotion is rich in French Alps spring which injects moisture component to skin any time and releases water continuously to skin to help the moisture component permeate the bottom of the skin, and raise water content of surface layer of the skin, enhance skin natural moisture retention capacity, supplement skin nutrition, raise skin elasticity, reduce wrinkle, enhance skin defense function, prevent repeatedly occurrence of the dry skin, and recover the dry and dark skin back to smooth and moisture state.

Description

A kind of astringent and its preparation method and application
Technical field
The present invention relates to cosmetic field, be specifically related to a kind of astringent and its preparation method and application.
Background technology
The modern life and working environment cause the investigation of 2002 of skin premature aging and show: the modern life and working environment cause women's skin quality generally to descend, and occur low and deep, flavescence, relax, microgroove, decortication, coarse six large skin initial stage catabiosis." Chinese women skin investigation report " shows, 71% women has the xerosis cutis symptom, the dry maximum puzzlement that has become the Chinese women skin.Investigation shows, is in for a long time air conditioner surroundings, is accustomed in the face of radiation, poor sleeping quality, diet cosmetic irregular, mistake for a long time, and be to cause the large factor of women's skin problem most important five.
Xerodermatic major reason is that horny layer moisture reduces because playing the lipid of lock water moisture-keeping function in intercellular substance loses, and skin barrier is impaired., to resist drying, form good living habit essential.The skin care item that select to be fit in life, as far as possible reduce the number of times of making up, correctly clean skin, reduce the time of Exposure to Sunlight, shortening and computer intimate contact etc., all can reduce the infringement to skin barrier.
Good skin quality is only aging crucial skin protection expert of delaying skin initial stage and points out, general synthetic nutrient is difficult to penetrate the ABB of skin, and nutrient can only rest on skin surface, and skin is nutrition for want of, cause skin quality to descend, only be improved skin quality ability delaying skin aging.
Listing in the market, research and develop or but the uncommon youngster ANS water of life series of products in improved Anji have just comprised more than 30 kinds such as the beautiful fair-skinned makeup removing breast of water, beautiful fair-skinned clean the glue of water, the beautiful fair-skinned 24H moisture content massage cream of water, the beautiful fair-skinned MASQUE APAISANT HYDRATANT of water, the beautiful fair-skinned 24H moisture content essence of water, the beautiful fair-skinned 24H moisturizing emulsion of water.
Summary of the invention
In order to improve the tender moist sense of skin water, clear away the obscure colour of skin, represent smooth bright good complexion, but on the uncommon youngster ANS series of products in Anji, the invention discloses a kind of astringent.
Astringent of the present invention comprises butanediol, polyquaternary ammonium salt-51, Herba Violae Hortensis extract, yeast extract, Anjidew NL50, Semen sojae atricolor Symbiont extract, Rhizoma Imperatae extract, Tremella extract, orange blossom extract, pantothenylol, Beta-glucose, EDETATE SODIUM, plant amino acid, xanthan gum, hyaluronic acid, allantoin, imidazolidinyl urea, iodine propilolic alcohol butyl mephenesin Carbamate and pure water.
the content (mark meter by weight) that the present invention further defines this each composition of astringent is: butanediol 0.5%~3%, polyquaternary ammonium salt-510.1%~1%, Herba Violae Hortensis extract 0.1%~0.5%, yeast extract 0.05%~0.3%, Anjidew NL50 0.05%~0.2%, Semen sojae atricolor Symbiont extract 0.05%~0.2%, Rhizoma Imperatae extract 0.05%~0.2%, Tremella extract 0.05%~0.2%, orange blossom extract 0.05%~0.2%, pantothenylol 0.1%~0.5%, Beta-glucose 0.05%~0.3%, EDETATE SODIUM 0.05%~0.2%, plant amino acid 0.1%~0.5%, xanthan gum 0.05%~0.2%, hyaluronic acid 0.05%~0.3%, allantoin 0.05%~0.3%, imidazolidinyl urea 0.05%~0.2%, iodine propilolic alcohol butyl mephenesin Carbamate 0.05%~0.2%, surplus is pure water.
the present invention is the further preferred content of this each composition of astringent (mark meter :) by weight is butanediol 1%, polyquaternary ammonium salt-510.5%, Herba Violae Hortensis extract 0.3%, yeast extract 0.2%, Anjidew NL50 0.1%, Semen sojae atricolor Symbiont extract 0.1%, Rhizoma Imperatae extract 0.1%, Tremella extract 0.1%, orange blossom extract 0.1%, pantothenylol 0.3%, Beta-glucose 0.2%, EDETATE SODIUM 0.1%, plant amino acid 0.3%, xanthan gum 0.1%, hyaluronic acid 0.2%, allantoin 0.2%, imidazolidinyl urea 0.1%, iodine propilolic alcohol butyl mephenesin Carbamate 0.1%, surplus is pure water.
Astringent described above, preferably, the specification of above-mentioned astringent is 400mL.
Astringent described above, preferably, the specification of above-mentioned astringent is 100mL.
Astringent described above preferably, is prepared according to the following steps:
1. add butanediol, EDETATE SODIUM, PVC sodium in pure water,, to complete swelling, add polyquaternary ammonium salt-51, be warming up to 90 ℃ and be stirred to dissolving fully, be incubated 20 minutes;
2. continue to add the Beta-glucose, after being stirred to dissolving fully, then add pantothenylol, plant amino acid, xanthan gum, hyaluronic acid, allantoin to stir;
3. with step 2. solution be cooled to 50 ℃, add Herba Violae Hortensis extract, yeast extract, Semen sojae atricolor Symbiont extract, Rhizoma Imperatae extract, Tremella extract, orange blossom extract, be incubated 20 minutes.
4. under stirring state, 3. step is cooled to below 45 ℃ and adds imidazolidinyl urea and iodine propilolic alcohol butyl mephenesin Carbamate, stirs, and is cooled to room temperature and can obtains this product.
The application of astringent described above, preferably, this astringent is fit to dryness, adult form skin.
The using method of astringent described above, preferably, this astringent after clean skin of morning and evening, is got and is patted in right amount in several cervical regions of face with clean skin cotton or finger, waits to absorb to get final product.
In astringent of the present invention, the concrete effect of some compositions and relative theory are:
Allantoin: be a kind of amphoteric compound, can form double salt in conjunction with many kinds of substance, have lucifuge, sterilization and anticorrosion, pain relieving, antioxidation, can make skin keep moisture content, moisten and soft, have protective tissue, hydrophilic, absorb water and the effect such as prevent that moisture from distributing; Can make the soft high resilience of skin, and beautiful gloss is arranged.
Hyaluronic acid: can help skin to draw a large amount of moisture, but moment deep moisturizing, increase skin elasticity and tension force, help and recover the normal oil-water balance of skin, improve dry and lax skin.
Yeast extract: contain different types of nucleic acid substances, vitamin and aminoacid, have natural nutrient component in these groups.There is obvious protection effect to resist active oxygen and lipid peroxidation, for preventing and slowing down skin aging, good effect is arranged.
Plant amino acid: commercially available or according to CN102943097A method system.Plant is the favor of the Nature, absorbs world anima and life brilliance, is rare treasured, and plant amino acid is to extract high nutrient and it is concentrated in plant, and its effect is powerful, effect is remarkable, can allow skin feel more silkiness soft and smooth.
Excellent moistening effect: comprised the important element of the lasting Glycerins of 16 remainders, assisted skin to recover desirable moisturizing degree.
Absorb immediately: can nature incorporate skin, absorb completely, do not waste.
Moisten immediately: salubrious as water, and be rich in calcium, manganese, zinc isoreactivity moisturizing composition, skin is infiltrated seemingly in the bosom of sweet spring water water, perfect the natural moisturizing mechanism of skin, skin will be felt instant tender with extraordinarily of moistening.
Long-acting gentle skin: round-the-clock moistening effect, and strengthen skin moisturizing barrier, skin will no longer feel tight, only have comfortable tender impression.
Compared with prior art, the present invention has following beneficial effect:
The present invention can inject the powerful wet composition of mending for skin, to skin release moisture continuously, allow the wet composition of benefit directly ooze skin bottom, improve simultaneously skin top layer water content, strengthen skin natural moisture preserving power, to skin, supplement nutrient, strengthen skin elasticity, reduce wrinkle, strengthen the skin defensive enginery, stop the dry skin problem repeatedly to occur, dry, the obscure skin of order is replied the tender state of soft and smooth full water; Also can releive skin, resist dry, strengthen skin, in and free radical, promotion skin cell renewal.Wherein be rich in " magnesium " but the element activity of kinase more keeps activation, equilibrium water conten function to reach.
Adjust with the collocation of various active moisturizing composition, make the effective ingredient in sweet spring water water go deep into skin deep layer cell centre, sustained release,, continually for skin brings comfortable pure and fresh moistening effect, make the lasting water profit of skin, more can be fit to environmental change.With up-to-date nanotechnology, allow the nanometer skin moistening factor infiltrate fast skin, improve from inside to outside skin smoothness and elasticity, and the interpolation of multinomial vegetalitas moisturizing and whitening composition more can improve the tender moist sense of skin water, and clear away the obscure colour of skin, represent smooth bright good complexion!
Specific embodiment
Further explain the present invention below in conjunction with embodiment, but embodiment does not limit in any form to the present invention.
Embodiment 1,
Mark meter by weight: butanediol 1%, polyquaternary ammonium salt-510.5%, Herba Violae Hortensis extract 0.3%, yeast extract 0.2%, Anjidew NL50 0.1%, Semen sojae atricolor Symbiont extract 0.1%, Rhizoma Imperatae extract 0.1%, Tremella extract 0.1%, orange blossom extract 0.1%, pantothenylol 0.3%, Beta-glucose 0.2%, EDETATE SODIUM 0.1%, plant amino acid 0.3%, xanthan gum 0.1%, hyaluronic acid 0.2%, allantoin 0.2%, imidazolidinyl urea 0.1%, iodine propilolic alcohol butyl mephenesin Carbamate 0.1%, surplus is pure water.Press the specification preparation of 400ml.
, according to above-mentioned formula, according to following steps, be prepared:
1. add butanediol, EDETATE SODIUM, PVC sodium in pure water,, to complete swelling, add polyquaternary ammonium salt-51, be warming up to 90 ℃ and be stirred to dissolving fully, be incubated 20 minutes;
2. continue to add the Beta-glucose, after being stirred to dissolving fully, then add pantothenylol, plant amino acid, xanthan gum, hyaluronic acid, allantoin to stir;
3. with step 2. solution be cooled to 50 ℃, add Herba Violae Hortensis extract, yeast extract, Semen sojae atricolor Symbiont extract, Rhizoma Imperatae extract, Tremella extract, orange blossom extract, be incubated 20 minutes.
4. under stirring state, 3. step is cooled to below 45 ℃ and adds imidazolidinyl urea and iodine propilolic alcohol butyl mephenesin Carbamate, stirs, and is cooled to room temperature and can obtains this product.
Embodiment 2
Mark meter by weight: butanediol 0.5%, polyquaternary ammonium salt-510.1%, Herba Violae Hortensis extract 0.1%, yeast extract 0.05%, Anjidew NL50 0.05%, Semen sojae atricolor Symbiont extract 0.05%, Rhizoma Imperatae extract 0.05%, Tremella extract 0.05%, orange blossom extract 0.05%, pantothenylol 0.1%, Beta-glucose 0.05%, EDETATE SODIUM 0.05%, plant amino acid 0.1%, xanthan gum 0.05%, hyaluronic acid 0.05%, allantoin 0.05%, imidazolidinyl urea 0.05%, iodine propilolic alcohol butyl mephenesin Carbamate 0.05%, the specification preparation of pressing 100ml.
Preparation method such as embodiment 1.
Embodiment 3
Mark meter by weight: butanediol 3%, polyquaternary ammonium salt-511%, Herba Violae Hortensis extract 0.5%, yeast extract 0.3%, Anjidew NL50 0.2%, Semen sojae atricolor Symbiont extract 0.2%, Rhizoma Imperatae extract 0.2%, Tremella extract 0.2%, orange blossom extract 0.2%, pantothenylol 0.5%, Beta-glucose 0.3%, EDETATE SODIUM 0.2%, plant amino acid 0.5%, xanthan gum 0.2%, hyaluronic acid 0.3%, allantoin 0.3%, imidazolidinyl urea 0.2%, iodine propilolic alcohol butyl mephenesin Carbamate 0.2%, the specification preparation of pressing 400ml.
Preparation method such as embodiment 1.
Comparative Examples 4,
Do not add hyaluronic acid, allantoin, the other the same as in Example 1 in formula.
Comparative Examples 5,
Do not add Rhizoma Imperatae extract, Tremella extract, orange blossom extract in formula, the other the same as in Example 1.
Comparative Examples 6,
Do not add pantothenylol, plant amino acid, xanthan gum, the other the same as in Example 1 in formula.
Embodiment 7, Product Safety evaluation (human skin patch)
7.1 trial target: the astringent that embodiment 1-3, Comparative Examples 4-6 are prepared.
7.2 tested crowd
Number: 30 people
Age: between 20~50 years old
Sex: female 23 people, male 7 people
Health status: experimenter's skin health, without the dermatosis allergies, meets the experimenter and volunteers inclusion criteria.
7.3 patch method: select qualified speckle examination device, with closed patch test method, with the about 0.020mL~0.025mL(semifluid of tested material) drip in speckle examination device, the external special adhesive tape is covered on the experimenter back, remove tested material after 24 hours, observe dermoreaction in 0.5,6,12,24,48 hour after removing respectively, according to dermoreaction grade scale in " cosmetics health standard ", record its result.
7.4 result of the test
The human skin patch result shows: 30 experimenters are by astringent of the present invention (embodiment 1-3), reference substance (Comparative Examples 4-6) patch test, observed dermoreaction at 0.5,6,12,24,48 hour, wherein skin adverse reaction appears in 0 example, illustrates that astringent of the present invention uses safety.
Embodiment 8,
8.1 trial target: the astringent that embodiment 1-3, Comparative Examples 4-6 are prepared
8.2 tested crowd
Sex number: female, 50 people
Age: between 20~40 years old
Health status: experimenter's skin health, without the dermatosis allergies, meets the experimenter and volunteers inclusion criteria.
8.3 method of testing: after experimenter face cleaning, the astringent that embodiment 1-3, Comparative Examples 4-6 is prepared is coated on the cheek of two of left and right respectively, observes and experiences result of use.
8.4 the testing evaluation result is as follows:
(8 days) on probation feedback conclusive table of table 1. embodiment 1 preparing product
Figure BDA00003421072900051
Figure BDA00003421072900061
(8 week) on probation feedback conclusive table of table 2. embodiment 1 preparing product
(7 days) on probation feedback conclusive table of table 3. embodiment 2-3 preparing product
Figure BDA00003421072900063
(7 days) on probation feedback conclusive table of certain moisturizing emulsion of table 4. Comparative Examples 4-6
Figure BDA00003421072900064
Figure BDA00003421072900071
The tester all represents, embodiment 1 preparing product is better than embodiment 2,3 prepared products in every respect, and all is better than the prepared product of Comparative Examples 4-6, and is also not sticky after use, absorb fast, the rapid full water profit of skin.After often using, improve the skin water content, strengthened skin moisturizing power and enhancing skin elasticity, more can improve the tender moist sense of skin water, cleared away the obscure colour of skin.There do not is the people that allergic phenomena is arranged in the questionnaire of user simultaneously.
Embodiment 9,
9.1 trial target: embodiment 1-3 astringent, commercially available similar cosmetics
9.2 tested crowd
Sex number: female, 50 people
Age: between 20~40 years old
Health status: experimenter's skin health, without the dermatosis allergies, meets the experimenter and volunteers inclusion criteria.
9.3 method of testing: after experimenter face cleaning, respectively embodiment 1-3 astringent, commercially available similar cosmetics are coated on the cheek of two of left and right, observe and experience result of use.
9.4 the testing evaluation result is as follows:
Table 1. improves the contrast statistical table of the colour of skin
Figure BDA00003421072900072
The tester all represents, in moisture-retaining capacity with improve aspect the colour of skin, embodiment 1 preparing product is better than embodiment 2,3 prepared products in every respect, all is better than commercially available similar cosmetics, and the tester all particularly approves embodiment 1 preparing product.
The foregoing is only embodiments of the invention; not thereby limit the scope of the claims of the present invention; every equivalent structure or equivalent flow process conversion that utilizes description of the present invention to do; or directly or indirectly be used in other relevant technical fields, within all in like manner being included in scope of patent protection of the present invention.

Claims (2)

1. astringent, it is characterized in that, comprise butanediol, polyquaternary ammonium salt-51, Herba Violae Hortensis extract, yeast extract, Anjidew NL50, Semen sojae atricolor Symbiont extract, Rhizoma Imperatae extract, Tremella extract, orange blossom extract, pantothenylol, Beta-glucose, EDETATE SODIUM, plant amino acid, xanthan gum, hyaluronic acid, allantoin, imidazolidinyl urea, iodine propilolic alcohol butyl mephenesin Carbamate and pure water.
2. astringent as claimed in claim 1, it is characterized in that, following composition is according to the weight fraction meter: butanediol 0.5% ~ 3%, polyquaternary ammonium salt-51 0.1% ~ 1%, Herba Violae Hortensis extract 0.1% ~ 0.5%, yeast extract 0.05% ~ 0.3%, Anjidew NL50 0.05% ~ 0.2%, Semen sojae atricolor Symbiont extract 0.05% ~ 0.2%, Rhizoma Imperatae extract 0.05% ~ 0.2%, Tremella extract 0.05% ~ 0.2%, orange blossom extract 0.05% ~ 0.2%, pantothenylol 0.1% ~ 0.5%, Beta-glucose 0.05% ~ 0.3%, EDETATE SODIUM 0.05% ~ 0.2%, plant amino acid 0.1% ~ 0.5%, xanthan gum 0.05% ~ 0.2%, hyaluronic acid 0.05% ~ 0.3%, allantoin 0.05% ~ 0.3%, imidazolidinyl urea 0.05% ~ 0.2%, iodine propilolic alcohol butyl mephenesin Carbamate 0.05% ~ 0.2%, surplus is pure water.
3, astringent as claimed in claim 2, it is characterized in that, mark meter by weight: butanediol 1%, polyquaternary ammonium salt-51 0.5%, Herba Violae Hortensis extract 0.3%, yeast extract 0.2%, Anjidew NL50 0.1%, Semen sojae atricolor Symbiont extract 0.1%, Rhizoma Imperatae extract 0.1%, Tremella extract 0.1%, orange blossom extract 0.1%, pantothenylol 0.3%, Beta-glucose 0.2%, EDETATE SODIUM 0.1%, plant amino acid 0.3%, xanthan gum 0.1%, hyaluronic acid 0.2%, allantoin 0.2%, imidazolidinyl urea 0.1%, iodine propilolic alcohol butyl mephenesin Carbamate 0.1%, surplus is pure water.
4, astringent as claimed in claim 3, is characterized in that, the specification of this astringent is 400mL.
5, astringent as claimed in claim 3, is characterized in that, the specification of this astringent is 100mL.
6, the described astringent of a kind of claim 1-5, is characterized in that, is prepared according to the following steps:
Figure DEST_PATH_934840DEST_PATH_IMAGE001
Add butanediol, EDETATE SODIUM, PVC sodium in pure water,, to complete swelling, add polyquaternary ammonium salt-51, be warming up to 90oC and be stirred to dissolving fully, be incubated 20 minutes;
Figure DEST_PATH_946789DEST_PATH_IMAGE002
Continue to add the Beta-glucose, after being stirred to dissolving fully, then add pantothenylol, plant amino acid, xanthan gum, hyaluronic acid, allantoin to stir;
Figure DEST_PATH_615668DEST_PATH_IMAGE003
With step
Figure DEST_PATH_671349DEST_PATH_IMAGE002
Solution is cooled to 50oC, adds Herba Violae Hortensis extract, yeast extract, Semen sojae atricolor Symbiont extract, Rhizoma Imperatae extract, Tremella extract, orange blossom extract, is incubated 20 minutes.
Figure DEST_PATH_425678DEST_PATH_IMAGE004
Under stirring state, step
Figure DEST_PATH_162690DEST_PATH_IMAGE003
Be cooled to below 45 ℃ and add imidazolidinyl urea and iodine propilolic alcohol butyl mephenesin Carbamate, stir, be cooled to room temperature and can obtain this product.
7, the application of the described astringent of a kind of claim 1-6, is characterized in that, this astringent is suitable for dryness, adult form skin.
8, the using method of the described astringent of a kind of claim 1-6, is characterized in that, this astringent after clean skin of morning and evening, is got and patted in right amount in several cervical regions of face with clean skin cotton or finger, waits to absorb to get final product.
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CN104666236A (en) * 2015-02-13 2015-06-03 安婕妤化妆品科技股份有限公司 Moisturizing skincare mask
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CN106619243A (en) * 2017-02-24 2017-05-10 韩后化妆品股份有限公司 Composition with moisture-preserving and antiallergic effects and application thereof
CN109106622A (en) * 2018-11-02 2019-01-01 广州艾蓓生物科技有限公司 There is one kind moisturizing to repair makeup removing breast and preparation method thereof

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CN104224644A (en) * 2014-10-14 2014-12-24 萱肌蜜(香港)生物科技有限公司 Skin care preparation
CN104434768A (en) * 2014-12-10 2015-03-25 上海新高姿化妆品有限公司 Moisturizing lotion with slow-release efficacy and preparation method of moisturizing lotion
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CN104644507B (en) * 2015-02-12 2016-01-20 安婕妤化妆品科技股份有限公司 A kind of nursing class cream cream composition
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CN105662955A (en) * 2016-01-27 2016-06-15 安婕妤化妆品科技股份有限公司 Cosmetic containing methyl-pyrimidine type substances
CN106619243A (en) * 2017-02-24 2017-05-10 韩后化妆品股份有限公司 Composition with moisture-preserving and antiallergic effects and application thereof
CN109106622A (en) * 2018-11-02 2019-01-01 广州艾蓓生物科技有限公司 There is one kind moisturizing to repair makeup removing breast and preparation method thereof

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