CN103356468A - Exfoliated bletilla face mask and preparation method thereof - Google Patents
Exfoliated bletilla face mask and preparation method thereof Download PDFInfo
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- CN103356468A CN103356468A CN2013101962589A CN201310196258A CN103356468A CN 103356468 A CN103356468 A CN 103356468A CN 2013101962589 A CN2013101962589 A CN 2013101962589A CN 201310196258 A CN201310196258 A CN 201310196258A CN 103356468 A CN103356468 A CN 103356468A
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- exfoliated
- facial film
- rhizoma bletillae
- bletillae
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- 241001313855 Bletilla Species 0.000 title abstract description 6
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Landscapes
- Cosmetics (AREA)
Abstract
The invention discloses an exfoliated bletilla face mask and a preparation method thereof. The exfoliated bletilla face mask is prepared from the following raw materials in parts by weight according to a conventional method: 10-14 parts of polyvinyl alcohol, 8-12 parts of glycerinum, 0.8-1.2 parts of di ( hydroxyethyl ) lauryl amine oxide, 4-6 parts of ethyl alcohol, 6-8 parts of coco-betaine acylamino bisexual propionate, 0.8-2 parts of bletilla extracting solution, 0.03-0.08 part of compound antiseptic and 100 parts of deionized water, wherein the compound antiseptic is composed of the following components in parts by weight: 1-3 parts of carnosic acid, 3-5 parts of bamboo leaf antioxidant, 1-3 parts of nisin and 1-3 parts of iodopropynyl butylcarbamate. The exfoliated bletilla face mask has excellent moisturizing performance, effects of anti-aging anti-wrinkling and the effects of improvement of facial acne melanin and skin whitening.
Description
Technical field
The present invention relates to facial film and preparation method thereof, be specifically related to a kind of exfoliated Pseudobulbus Bletillae (Rhizoma Bletillae) facial film and preparation method thereof.
Background technology
Facial film is the important content in the skin nursing, for the regular application facial film of all kinds of skin characteristics, can make the oily skin defat, and thick pore is restrained, and the skin of withered gauffer recovers gloss, and the inflammation of skin sore skin is inhibited.After using, facial film makes skin salubrious, the smooth and pure white delicacy that seems, this is because when facial film is coated on skin, facial film and skin produce affinity, gradually drying along with facial film, the skin temperature rise, blood circulation is accelerated, skin-tightening and tension force are strengthened, and the sebum of skin secretion and moisture reverse osmosis unfold the epidermis softness in horny layer, the pore instinct is opened, effective ingredient in the facial film infiltrates skin and is absorbed, and facial film tightly links to each other with skin simultaneously, when removing facial film, the deep layer dirt makes skin pure and fresh clean also by the while leukorrhagia in aging cutin on the skin, the pore.
The principle of facial film, utilize exactly the blink that covers face, extraneous air and the pollution of temporary transient isolation improves the skin temperature, the pore expansion of skin, promote sweat gland secretion and metabolism, the oxygen content of skin is risen, be conducive to the oil substances that skin is got rid of the metabolic product of epidermis cell and accumulation, the moisture in the facial film infiltrates the horny layer of skin epidermis, it is soft that skin becomes, and skin naturally light is flexible.
Along with the raising of people's quality of the life and people to the pursuit of the beauty, the cosmetics kind is more and more various.At present, face mask of traditional Chinese medicine is one of beauty treatment educational circles effective whitening scheme, and especially some Chinese medicine extraction liquid have the preferably effect of toxin expelling, speckle dispelling, reparation, skin care, also by being applied in the facial film gradually.
But because facial film is liquid condition, Chinese medicine extraction liquid is easy to grow mycete, and a lot of face mask of traditional Chinese medicine antiseptic effects in the market are not good, and the shelf-life is short.All can add antiseptic in therefore a lot of face mask of traditional Chinese medicines.Yet a lot of antiseptic also can produce zest to skin, even cause erythema and erythra in the microorganisms such as kill bacteria, fungus, and the Long Term Contact antiseptic can increase organism material sensitization, cause the danger of anaphylactic reaction.
Iodine propilolic alcohol butyl mephenesin Carbamate (being called for short IPBC) is a kind of novel cosmetic antiseptic, has good fungistatic effect, and preferably dissolubility arranged in surfactant, emulsifying agent, polar solvent, therefore be widely used in resident class and the drip washing class cosmetic formulations, other antiseptic such as normal and diazolidinyl urea, hydantoin are used in conjunction with.Regulation IPBC limits the use of antiseptic in the components of cosmetics in China's cosmetics health standard and the European Union's regulatory affairs, and maximum permission working concentration is 0.05% in cosmetics, and can not be used for oral hygiene and lip product.But in facial film, addition is antiseptic effect and not obvious less than 0.05% the time.Therefore, there is little and antiseptic effect is poor, the shelf-life the is short problem of consumption in the antiseptic that uses in the present facial film.Iodine propilolic alcohol butyl mephenesin Carbamate or other antiseptic large usage quantities in the part facial film are also arranged, can be produced pessimal stimulation by skin, with after need to clean facial, use to bother.
The Pseudobulbus Bletillae (Rhizoma Bletillae) is a kind of of the orchid family Pseudobulbus Bletillae (Rhizoma Bletillae) genus.Perennial herb, high 20～50 centimetres, 4～5 pieces on leaf, base portion mutually cover build up the stem shape, and central authorities extract scape out.A raceme tool number flower; Flower purple or pale red, 5 centimetres of diameters are comprised of the lip of 3 pieces of sepals, 2 pieces of petals and 1 piece of specialization; Lip 3 splits, and the above has the typhloscle sheet; Stamen and style symphysis form gynostemium, and there is a flower pesticide on the gynostemium top, and there is a stigma depression front upper place.Underground have a thick thick root stock, and such as the Caput Gallus domesticus shape, rich viscosity contains Pseudobulbus Bletillae (Rhizoma Bletillae) colloid, i.e. bletilla mannan, but hyoscine have the effect of hemostasis tonifying the lung, granulation promoting pain relieving, also can be made for thickener.
Its pseudobulb is famous and precious hemostasis, anti-bacillus, fungus, treatment cough.Cough due to yin deficiency, cough due to lung-heat, pertussis, pulmonary tuberculosis cough and other intractable cough there is good antitussive action, the treatment sinusitis.
Pseudobulbus Bletillae (Rhizoma Bletillae) rich in starch, glucose, volatile oil, phlegmatic temperament etc., external is embrocated, and the vestige under can eliminating as the acne on the face makes skin smooth seamless.
Bulb contains Pseudobulbus Bletillae (Rhizoma Bletillae) colloid, starch, volatilization wet goods; Medicinal, have produce effects, the effect such as tonifying the lung hemostasis, detumescence, wound hemorrhage, carbuncle, scald, furuncle etc. are controlled in external application; Spend beauty, cultivation is for viewing and admiring.Use propagation by corm, plantation needs warm more dark and damp environment at draining good, fertile sand loam and humus loam.
Function cures mainly: astringing to arrest bleeding, detumescence and promoting granulation.Be used for hemoptysis and spit blood traumatic hemorrhage, sore swollen toxin, chapped skin; The pulmonary tuberculosis hemoptysis, ulcer haemorrhage.
The Pseudobulbus Bletillae (Rhizoma Bletillae) contains Pseudobulbus Bletillae (Rhizoma Bletillae) glucomannoglycan (bletillglucomannan), biphenyl class (bibenzyls) chemical compound, luxuriant and rich with fragrance class (dihydrophenanthrenes) chemical compound of two hydrogen, dihydro phenanthro-pyrans class (dihydrophenantropyrans) chemical compound and Pseudobulbus Bletillae (Rhizoma Bletillae) alcohol (bletilol) A, B, C.And Pseudobulbus Bletillae (Rhizoma Bletillae) glucoside polysaccharide can be directly by separation in the Pseudobulbus Bletillae (Rhizoma Bletillae), extraction, purification and get, be water-soluble glucosan, be well suited for using at cosmetics.In being 200910037451.1 invention, number of patent application mentions Pseudobulbus Bletillae (Rhizoma Bletillae) extract can improve looks speckle removing, fat-reducing, and can also Acne treatment, the dermatosiss such as tinea corporis, furuncle and phyma, cicatrix.
Summary of the invention
For above shortcomings in the prior art, one of technical problem to be solved by this invention provides a kind of exfoliated Pseudobulbus Bletillae (Rhizoma Bletillae) facial film.
Two of technical problem to be solved by this invention provides the preparation method of above-mentioned exfoliated Pseudobulbus Bletillae (Rhizoma Bletillae) facial film.
The present invention seeks to be achieved through the following technical solutions:
A kind of exfoliated Pseudobulbus Bletillae (Rhizoma Bletillae) facial film is prepared from according to a conventional method by the raw material of following weight parts:
10-14 part polyvinyl alcohol, 8-12 part glycerol, 0.8-1.2 part two (ethoxy) lauryl amine oxide, 4-6 part ethanol, 6-8 part coco betaine amide groups both sexes base propionate, 0.8-2 part Rhizoma Bletillae extraction solution, 0.03-0.08 part compound preservative, 100 parts of deionized waters.
Wherein, described compound preservative is made of by weight following component: 1-3 part carnosic acid, 3-5 part AOB, 1-3 part nisin, 1-3 part iodine propilolic alcohol butyl mephenesin Carbamate.
With carnosic acid, AOB, nisin and iodine propilolic alcohol butyl mephenesin Carbamate simple agitation mix homogeneously, can make described compound preservative.
Described exfoliated Pseudobulbus Bletillae (Rhizoma Bletillae) facial film can adopt industry conventional method to be prepared from.
Further, the present invention also provides a kind of preparation method of exfoliated Pseudobulbus Bletillae (Rhizoma Bletillae) facial film, is comprised of following step:
Polyvinyl alcohol is added in the deionized water, be heated to 70-90 ℃, dissolving, be cooled to 45-55 ℃, add glycerol, two (ethoxy) lauryl amine oxide, ethanol, the stirring of coco betaine amide groups both sexes base propionate, be cooled to 40 ℃, add Rhizoma Bletillae extraction solution and compound preservative, stir, can make described exfoliated Pseudobulbus Bletillae (Rhizoma Bletillae) facial film.
Concrete, in the present invention:
Described polyvinyl alcohol can be selected the cosmetics-stage polyvinyl alcohol, and specifically can select such as the trade mark is the polyvinyl alcohol of PVA1788, PVA1799 or PVA2488.
Glycerol has another name called: propylene glycol, English name: Glycerin, molecular formula C
3H
8O
3
Two (ethoxy) lauryl amine oxide, CAS accession number: 2530-44-1.
Coco betaine amide groups both sexes base propionate, CAS accession number: 100085-64-1.
Rhizoma Bletillae extraction solution of the present invention can pass through commercially available getting.Also can adopt the preparation of following method and get: after the Pseudobulbus Bletillae (Rhizoma Bletillae) is pulverized, add the deionized water of 6-10 times of weight, soaked 1-3 hour, ultrasonic extraction, 10-15 minute, filtration, centrifugal, discard and precipitate supernatant concentration, make Rhizoma Bletillae extraction solution.Preferably, after concentrating, control Rhizoma Bletillae extraction solution density is 1.02-1.10g/cm
3
Carnosic acid, molecular formula: C
20H
28O
4, CAS number: 3650--09-7, source: Labiatae Rosmarinus plant rosemary Rosmarinus officinalis L.
AOB, CNS number: 04.019, English name: antioxidant of bamboo leaves.That AOB extracts from the tender leaf of Phyllostachys (phyllostachys) bamboo, natural, the nutrition take flavone and phenolic compound as effective ingredient, multi-functional food antioxidant.
Nisin also claims nisin, English name: Nisin, and by the synthetic a kind of polypeptide that is formed by 34 aminoacid of streptococcus acidi lactici metabolism, molecular formula C
143H
228O
37N
42S
7Molecular weight is 3348, and nisin is made of water-wet side and hydrophobic side, is typical surfactant, be efficient, nontoxic biological antiseptic, be widely used in the anticorrosion of milk and milk products, fermented beverage, filling food, vegetable protein food, meat and its products at present.
Iodine propilolic alcohol butyl mephenesin Carbamate, English name: 3-Iodo-2-propynyl butylcarbamate, be abbreviated as IPBC, CAS number: 55406-53-6, molecular formula: C
8H
12INO
2, molecular weight is 281.10.
The present invention uses carnosic acid, AOB, nisin and iodine propilolic alcohol butyl mephenesin Carbamate composite as antiseptic, and antiseptic effect is significantly improved, the long shelf-life of facial film.And, use Compositional antiseptic agent, greatly reduce the consumption of iodine propilolic alcohol butyl mephenesin Carbamate, the consumption of iodine propilolic alcohol butyl mephenesin Carbamate is controlled at below 0.03%, meet the IPBC that stipulates in China's cosmetics health standard and the European Union's regulatory affairs and limit the use of antiseptic in the components of cosmetics, maximum permission working concentration is 0.05% in cosmetics.Carnosic acid, AOB, nisin are the nontoxic biological antiseptic, be widely used in food service industry, among the present invention it is diverted to cosmetic mask, can't brings ill effect to human body or skin, and can not produce harmful effect to the stability of facial film.
The using method of exfoliated Pseudobulbus Bletillae (Rhizoma Bletillae) facial film of the present invention is: before using facial film, deeply cleaning is facial first, again facial film is coated on face, after 15-25 minute, the facial film active substance is absorbed by the skin, the moisture evaporation, form gradually thin film at face, this thin film is peeled off from face, and the dirt on the skin of face, scurf also stick on the thin film in company with and are eliminated, and it is clean, smooth that face seems.
Exfoliated Pseudobulbus Bletillae (Rhizoma Bletillae) facial film of the present invention can the deep layer cleaning skin of face, desalinates facial microgroove, makes skin elasticity compact, and the water profit is plentiful.Continue to use, skin water profit is flexible, reproduces youthful vigor.
Exfoliated Pseudobulbus Bletillae (Rhizoma Bletillae) facial film of the present invention, performance of keeping humidity is superior, has defying age, crease-resistant effect, and facial acne melanin is improved, and whitening function is arranged.
Exfoliated Pseudobulbus Bletillae (Rhizoma Bletillae) facial film of the present invention adopts carnosic acid, AOB, nisin, the composite antiseptic of iodine propilolic alcohol butyl mephenesin Carbamate, and shelf life of products is long, and can not produce harmful effect to skin.
The specific embodiment
The invention will be further described below in conjunction with embodiment.
Embodiment 1
Take by weighing each raw material according to corresponding embodiment 1 data in the table 1, with carnosic acid, AOB, nisin and iodine propilolic alcohol butyl mephenesin Carbamate simple agitation mix homogeneously, can make described compound preservative.
Polyvinyl alcohol is added in the deionized water, be heated to 70-90 ℃, dissolving, be cooled to 45-55 ℃, add glycerol, two (ethoxy) lauryl amine oxide, ethanol, the stirring of coco betaine amide groups both sexes base propionate, be cooled to 40 ℃, add Rhizoma Bletillae extraction solution and compound preservative, stir, can make described exfoliated Pseudobulbus Bletillae (Rhizoma Bletillae) facial film.
Wherein, the Rhizoma Bletillae extraction solution among embodiment 1 and the Comparative Examples 1-5 adopts following method to be prepared from: after the Pseudobulbus Bletillae (Rhizoma Bletillae) is pulverized, add the deionized water of 8 times of weight, soaked 2 hours, ultrasonic extraction, 12 minutes, filter, centrifugal, discard precipitation with supernatant concentration, after concentrating, making density is 1.06g/cm
3Rhizoma Bletillae extraction solution.
Table 1: face pack prescription list position: kilogram
Comparative Examples 1
Take by weighing each raw material according to corresponding Comparative Examples 1 data in the table 1.Adopt embodiment 1 described method to prepare the exfoliated Pseudobulbus Bletillae (Rhizoma Bletillae) facial film of Comparative Examples 1.
Comparative Examples 2
Take by weighing each raw material according to corresponding Comparative Examples 2 data in the table 1.Adopt embodiment 1 described method to prepare the exfoliated Pseudobulbus Bletillae (Rhizoma Bletillae) facial film of Comparative Examples 2.
Comparative Examples 3
Take by weighing each raw material according to corresponding Comparative Examples 3 data in the table 1.Adopt embodiment 1 described method to prepare the exfoliated Pseudobulbus Bletillae (Rhizoma Bletillae) facial film of Comparative Examples 3.
Comparative Examples 4
Take by weighing each raw material according to corresponding Comparative Examples 4 data in the table 1.Adopt embodiment 1 described method to prepare the exfoliated Pseudobulbus Bletillae (Rhizoma Bletillae) facial film of Comparative Examples 4.
Comparative Examples 5
Take by weighing each component according to Comparative Examples 5 data corresponding in the table 1, adopt embodiment 1 described method, namely obtain the exfoliated Pseudobulbus Bletillae (Rhizoma Bletillae) facial film of Comparative Examples 5.
Test case
The exfoliated Pseudobulbus Bletillae (Rhizoma Bletillae) facial film that respectively embodiment 1 and Comparative Examples 1-5 is made carries out fill with the dark brown vial, opens wide bottle cap, places under 40 ℃ of ambient temperatures, relative humidity 85% environment, continues to observe also test, and concrete outcome sees the following form.Detect the microorganism level, concrete test item, detection method and examination criteria carry out according to QB/T2872-2007.
| ? | Observe phenomena |
| Embodiment 1 | No abnormality seen after 60 days, abnormal smells from the patient is pure |
| Comparative Examples 1 | After 50 days, mildew occurs, microorganism exceeds standard, and gives out unhappy abnormal smells from the patient |
| Comparative Examples 2 | After 40 days, mildew occurs, microorganism exceeds standard, and gives out unhappy abnormal smells from the patient |
| Comparative Examples 3 | After 40 days, mildew occurs, microorganism exceeds standard, and gives out unhappy abnormal smells from the patient |
| Comparative Examples 4 | After 40 days, mildew occurs, microorganism exceeds standard, and gives out unhappy abnormal smells from the patient |
| Comparative Examples 5 | After 5 days, mildew occurs, microorganism exceeds standard, and gives out unhappy abnormal smells from the patient |
The antiseptic methyl parahydroxybenzoate that uses in the Comparative Examples 4 is one of the most frequently used cosmetics preservative in this area.Belong to antiseptic phenols, generally effective to mycete, yeast, antibacterial, the effect that suppresses growth of microorganism is arranged, effectively prolong the shelf-life (40 days lower shelf-lifves of test condition of the present invention) of cosmetics after adding, but long-term this antiseptic of excessive use, the Diazolidinyl Urea epidermis cell causes the epidermis transition aging.
Can significantly be drawn by test data, the embodiment of the invention 1 is used carnosic acid, AOB, nisin and the composite Synergistic of iodine propilolic alcohol butyl mephenesin Carbamate, and antiseptic effect (60 days lower shelf-lifves of test condition of the present invention) obviously is better than Comparative Examples 1-3 and only adopts AOB, nisin and iodine propilolic alcohol butyl mephenesin Carbamate three composite (in lower shelf-life of test condition of the present invention below 50 days).
The facial film of the embodiment of the invention 1 places accelerated test under 40 ℃ of ambient temperatures, relative humidity 85% environment at opening, can reach 60 days antiseptic effects, the long shelf-life of facial film, and conversion shady and cool dry its shelf-life of place under sealing state far surpasses 3 years.
The above; it only is the specific embodiment of the present invention; but protection scope of the present invention is not limited to this; any those of ordinary skill in the art are in the disclosed technical scope of the present invention; variation or the replacement that can expect without creative work all should be encompassed within protection scope of the present invention.Therefore, protection scope of the present invention should be as the criterion with the protection domain that claims were limited.
Claims (3)
1. exfoliated Pseudobulbus Bletillae (Rhizoma Bletillae) facial film, it is characterized in that, raw material by following weight parts is prepared from according to a conventional method: 10-14 part polyvinyl alcohol, 8-12 part glycerol, 0.8-1.2 part two (ethoxy) lauryl amine oxide, 4-6 part ethanol, 6-8 part coco betaine amide groups both sexes base propionate, 0.8-2 part Rhizoma Bletillae extraction solution, 0.03-0.08 part compound preservative, 100 parts of deionized waters.
2. exfoliated Pseudobulbus Bletillae (Rhizoma Bletillae) facial film as claimed in claim 1, it is characterized in that, described compound preservative is made of by weight following component: 1-3 part carnosic acid, 3-5 part AOB, 1-3 part nisin, 1-3 part iodine propilolic alcohol butyl mephenesin Carbamate.
3. the preparation method of exfoliated Pseudobulbus Bletillae (Rhizoma Bletillae) facial film as claimed in claim 2, it is characterized in that, formed by following step: polyvinyl alcohol is added in the deionized water, be heated to 70-90 ℃, dissolving is cooled to 45-55 ℃, add glycerol, two (ethoxy) lauryl amine oxide, ethanol, the stirring of coco betaine amide groups both sexes base propionate, be cooled to 40 ℃, add Rhizoma Bletillae extraction solution and compound preservative, stir.
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Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
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| CN105055263A (en) * | 2015-10-02 | 2015-11-18 | 王学建 | Traditional Chinese medicine mask with whitening and spot reducing effects and preparation method of traditional Chinese medicine mask |
| CN109498529A (en) * | 2017-09-15 | 2019-03-22 | 伽蓝（集团）股份有限公司 | The application of bletilla striata extract |
| CN109846720A (en) * | 2019-01-22 | 2019-06-07 | 湖北中医药大学 | A kind of tear-pull bletilla whitening mask and preparation method thereof |
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2013
- 2013-05-23 CN CN201310196258.9A patent/CN103356468B/en not_active Expired - Fee Related
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Cited By (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN105055263A (en) * | 2015-10-02 | 2015-11-18 | 王学建 | Traditional Chinese medicine mask with whitening and spot reducing effects and preparation method of traditional Chinese medicine mask |
| CN109498529A (en) * | 2017-09-15 | 2019-03-22 | 伽蓝（集团）股份有限公司 | The application of bletilla striata extract |
| CN109846720A (en) * | 2019-01-22 | 2019-06-07 | 湖北中医药大学 | A kind of tear-pull bletilla whitening mask and preparation method thereof |
| CN109846720B (en) * | 2019-01-22 | 2021-11-16 | 湖北中医药大学 | Tear-type bletilla striata whitening mask and preparation method thereof |
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