CN103254350B - 纺织粘合衬布用共聚苯乙烯丙烯酸酯乳液及其制备方法 - Google Patents
纺织粘合衬布用共聚苯乙烯丙烯酸酯乳液及其制备方法 Download PDFInfo
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- CN103254350B CN103254350B CN201210036476.1A CN201210036476A CN103254350B CN 103254350 B CN103254350 B CN 103254350B CN 201210036476 A CN201210036476 A CN 201210036476A CN 103254350 B CN103254350 B CN 103254350B
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- 239000000839 emulsion Substances 0.000 title claims abstract description 24
- 239000004744 fabric Substances 0.000 title claims abstract description 16
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- 229920002223 polystyrene Polymers 0.000 title claims abstract description 13
- 238000002360 preparation method Methods 0.000 title claims abstract description 11
- 238000004945 emulsification Methods 0.000 title abstract description 5
- 239000004970 Chain extender Substances 0.000 claims abstract description 18
- 239000003995 emulsifying agent Substances 0.000 claims abstract description 15
- 239000003999 initiator Substances 0.000 claims abstract description 15
- PPBRXRYQALVLMV-UHFFFAOYSA-N Styrene Chemical compound C=CC1=CC=CC=C1 PPBRXRYQALVLMV-UHFFFAOYSA-N 0.000 claims abstract description 13
- 150000002148 esters Chemical class 0.000 claims abstract description 13
- 239000000463 material Substances 0.000 claims abstract description 12
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims abstract description 12
- NIXOWILDQLNWCW-UHFFFAOYSA-M Acrylate Chemical compound [O-]C(=O)C=C NIXOWILDQLNWCW-UHFFFAOYSA-M 0.000 claims abstract description 9
- 230000001681 protective effect Effects 0.000 claims abstract description 7
- VLKZOEOYAKHREP-UHFFFAOYSA-N n-Hexane Chemical group CCCCCC VLKZOEOYAKHREP-UHFFFAOYSA-N 0.000 claims description 11
- 239000002904 solvent Substances 0.000 claims description 8
- RTZKZFJDLAIYFH-UHFFFAOYSA-N Diethyl ether Chemical compound CCOCC RTZKZFJDLAIYFH-UHFFFAOYSA-N 0.000 claims description 6
- NIMLQBUJDJZYEJ-UHFFFAOYSA-N isophorone diisocyanate Chemical group CC1(C)CC(N=C=O)CC(C)(CN=C=O)C1 NIMLQBUJDJZYEJ-UHFFFAOYSA-N 0.000 claims description 6
- 239000005058 Isophorone diisocyanate Substances 0.000 claims description 5
- 238000000034 method Methods 0.000 claims description 5
- 150000002917 oxazolidines Chemical class 0.000 claims description 5
- JYJFNDQBESEHJQ-UHFFFAOYSA-N 5,5-dimethyloxazolidine-2,4-dione Chemical class CC1(C)OC(=O)NC1=O JYJFNDQBESEHJQ-UHFFFAOYSA-N 0.000 claims description 4
- LYCAIKOWRPUZTN-UHFFFAOYSA-N Ethylene glycol Chemical compound OCCO LYCAIKOWRPUZTN-UHFFFAOYSA-N 0.000 claims description 4
- 150000001412 amines Chemical class 0.000 claims description 4
- 238000010792 warming Methods 0.000 claims description 4
- XMNIXWIUMCBBBL-UHFFFAOYSA-N 2-(2-phenylpropan-2-ylperoxy)propan-2-ylbenzene Chemical compound C=1C=CC=CC=1C(C)(C)OOC(C)(C)C1=CC=CC=C1 XMNIXWIUMCBBBL-UHFFFAOYSA-N 0.000 claims description 3
- WROUWQQRXUBECT-UHFFFAOYSA-N 2-ethylacrylic acid Chemical compound CCC(=C)C(O)=O WROUWQQRXUBECT-UHFFFAOYSA-N 0.000 claims description 3
- 239000004159 Potassium persulphate Substances 0.000 claims description 3
- NWGKJDSIEKMTRX-AAZCQSIUSA-N Sorbitan monooleate Chemical compound CCCCCCCC\C=C/CCCCCCCC(=O)OC[C@@H](O)[C@H]1OC[C@H](O)[C@H]1O NWGKJDSIEKMTRX-AAZCQSIUSA-N 0.000 claims description 3
- USHAGKDGDHPEEY-UHFFFAOYSA-L potassium persulfate Chemical compound [K+].[K+].[O-]S(=O)(=O)OOS([O-])(=O)=O USHAGKDGDHPEEY-UHFFFAOYSA-L 0.000 claims description 3
- 235000019394 potassium persulphate Nutrition 0.000 claims description 3
- 229950004959 sorbitan oleate Drugs 0.000 claims description 3
- LCPVQAHEFVXVKT-UHFFFAOYSA-N 2-(2,4-difluorophenoxy)pyridin-3-amine Chemical group NC1=CC=CN=C1OC1=CC=C(F)C=C1F LCPVQAHEFVXVKT-UHFFFAOYSA-N 0.000 claims description 2
- CERQOIWHTDAKMF-UHFFFAOYSA-N Methacrylic acid Chemical compound CC(=C)C(O)=O CERQOIWHTDAKMF-UHFFFAOYSA-N 0.000 claims description 2
- 229920003171 Poly (ethylene oxide) Polymers 0.000 claims description 2
- 125000000217 alkyl group Chemical group 0.000 claims description 2
- XXMIOPMDWAUFGU-UHFFFAOYSA-N hexane-1,6-diol Chemical compound OCCCCCCO XXMIOPMDWAUFGU-UHFFFAOYSA-N 0.000 claims description 2
- WGCNASOHLSPBMP-UHFFFAOYSA-N hydroxyacetaldehyde Natural products OCC=O WGCNASOHLSPBMP-UHFFFAOYSA-N 0.000 claims description 2
- VZCYOOQTPOCHFL-UPHRSURJSA-N maleic acid Chemical compound OC(=O)\C=C/C(O)=O VZCYOOQTPOCHFL-UPHRSURJSA-N 0.000 claims description 2
- IPMWIVQWGGRTLD-UHFFFAOYSA-N n'-[2-(propylamino)ethyl]ethane-1,2-diamine Chemical class CCCNCCNCCN IPMWIVQWGGRTLD-UHFFFAOYSA-N 0.000 claims description 2
- 125000004123 n-propyl group Chemical group [H]C([H])([H])C([H])([H])C([H])([H])* 0.000 claims description 2
- 229940051841 polyoxyethylene ether Drugs 0.000 claims description 2
- 229920000056 polyoxyethylene ether Polymers 0.000 claims description 2
- CHQMHPLRPQMAMX-UHFFFAOYSA-L sodium persulfate Substances [Na+].[Na+].[O-]S(=O)(=O)OOS([O-])(=O)=O CHQMHPLRPQMAMX-UHFFFAOYSA-L 0.000 claims description 2
- AIDLAEPHWROGFI-UHFFFAOYSA-N 2-methylbenzene-1,3-dicarboxylic acid Chemical compound CC1=C(C(O)=O)C=CC=C1C(O)=O AIDLAEPHWROGFI-UHFFFAOYSA-N 0.000 claims 1
- JZUHIOJYCPIVLQ-UHFFFAOYSA-N 2-methylpentane-1,5-diamine Chemical group NCC(C)CCCN JZUHIOJYCPIVLQ-UHFFFAOYSA-N 0.000 claims 1
- RKQHHPKZOBFSRR-UHFFFAOYSA-N 6-methylhept-2-enoic acid Chemical compound CC(C)CCC=CC(O)=O RKQHHPKZOBFSRR-UHFFFAOYSA-N 0.000 claims 1
- WERYXYBDKMZEQL-UHFFFAOYSA-N butane-1,4-diol Chemical group OCCCCO WERYXYBDKMZEQL-UHFFFAOYSA-N 0.000 claims 1
- 229920005553 polystyrene-acrylate Polymers 0.000 abstract description 4
- 150000001408 amides Chemical class 0.000 abstract description 3
- 229920000728 polyester Polymers 0.000 abstract description 3
- 239000000126 substance Substances 0.000 abstract description 2
- CQEYYJKEWSMYFG-UHFFFAOYSA-N butyl acrylate Chemical compound CCCCOC(=O)C=C CQEYYJKEWSMYFG-UHFFFAOYSA-N 0.000 description 5
- 239000000843 powder Substances 0.000 description 4
- 238000004132 cross linking Methods 0.000 description 3
- 229920001909 styrene-acrylic polymer Polymers 0.000 description 3
- PUPZLCDOIYMWBV-UHFFFAOYSA-N (+/-)-1,3-Butanediol Chemical compound CC(O)CCO PUPZLCDOIYMWBV-UHFFFAOYSA-N 0.000 description 2
- QCPKTLDULZJCLB-UHFFFAOYSA-N 2-(1,3-oxazolidin-2-yl)ethanol Chemical class OCCC1NCCO1 QCPKTLDULZJCLB-UHFFFAOYSA-N 0.000 description 2
- 239000007795 chemical reaction product Substances 0.000 description 2
- 239000000470 constituent Substances 0.000 description 2
- 238000001816 cooling Methods 0.000 description 2
- 229920001577 copolymer Polymers 0.000 description 2
- 238000005108 dry cleaning Methods 0.000 description 2
- 238000007701 flash-distillation Methods 0.000 description 2
- 239000003292 glue Substances 0.000 description 2
- 238000010438 heat treatment Methods 0.000 description 2
- 125000002496 methyl group Chemical group [H]C([H])([H])* 0.000 description 2
- RGSFGYAAUTVSQA-UHFFFAOYSA-N pentamethylene Natural products C1CCCC1 RGSFGYAAUTVSQA-UHFFFAOYSA-N 0.000 description 2
- 229910001220 stainless steel Inorganic materials 0.000 description 2
- 239000010935 stainless steel Substances 0.000 description 2
- 238000003756 stirring Methods 0.000 description 2
- 238000005406 washing Methods 0.000 description 2
- DUIOKRXOKLLURE-UHFFFAOYSA-N 2-octylphenol Chemical group CCCCCCCCC1=CC=CC=C1O DUIOKRXOKLLURE-UHFFFAOYSA-N 0.000 description 1
- RDRURTGSFBSIKX-UHFFFAOYSA-N 3-ethyl-1,3-oxazolidine Chemical compound CCN1CCOC1 RDRURTGSFBSIKX-UHFFFAOYSA-N 0.000 description 1
- MBRVKEJIEFZNST-UHFFFAOYSA-N 3-methyl-2-methylidenebutanoic acid Chemical compound CC(C)C(=C)C(O)=O MBRVKEJIEFZNST-UHFFFAOYSA-N 0.000 description 1
- XDTMQSROBMDMFD-UHFFFAOYSA-N Cyclohexane Chemical compound C1CCCCC1 XDTMQSROBMDMFD-UHFFFAOYSA-N 0.000 description 1
- 239000004908 Emulsion polymer Substances 0.000 description 1
- 239000003945 anionic surfactant Substances 0.000 description 1
- 230000015556 catabolic process Effects 0.000 description 1
- 238000006243 chemical reaction Methods 0.000 description 1
- 239000011248 coating agent Substances 0.000 description 1
- 238000000576 coating method Methods 0.000 description 1
- 239000000498 cooling water Substances 0.000 description 1
- 230000007547 defect Effects 0.000 description 1
- 230000007812 deficiency Effects 0.000 description 1
- 238000006731 degradation reaction Methods 0.000 description 1
- 230000009977 dual effect Effects 0.000 description 1
- 125000004494 ethyl ester group Chemical group 0.000 description 1
- 239000000446 fuel Substances 0.000 description 1
- 238000004519 manufacturing process Methods 0.000 description 1
- 150000004702 methyl esters Chemical class 0.000 description 1
- 239000011347 resin Substances 0.000 description 1
- 229920005989 resin Polymers 0.000 description 1
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- Treatments For Attaching Organic Compounds To Fibrous Goods (AREA)
- Polymerisation Methods In General (AREA)
Abstract
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CN201210036476.1A CN103254350B (zh) | 2012-02-17 | 2012-02-17 | 纺织粘合衬布用共聚苯乙烯丙烯酸酯乳液及其制备方法 |
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CN201210036476.1A CN103254350B (zh) | 2012-02-17 | 2012-02-17 | 纺织粘合衬布用共聚苯乙烯丙烯酸酯乳液及其制备方法 |
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CN103254350A CN103254350A (zh) | 2013-08-21 |
CN103254350B true CN103254350B (zh) | 2016-03-16 |
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Citations (4)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN1817981A (zh) * | 2005-12-31 | 2006-08-16 | 浙江大学 | 一种纳米级颜料型喷墨印花油墨及其制备方法 |
CN101165264A (zh) * | 2006-10-16 | 2008-04-23 | 恒源祥(集团)有限公司 | 一种纳米型纺织物多功能整理剂及其整理方法 |
CN101768895A (zh) * | 2009-01-07 | 2010-07-07 | 湖北大学 | 一种苯丙乳液型高效表面施胶剂及其制备方法 |
CN101784573A (zh) * | 2007-08-30 | 2010-07-21 | 大赛璐化学工业株式会社 | 共聚物 |
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JPS59115365A (ja) * | 1982-12-22 | 1984-07-03 | Mitsui Toatsu Chem Inc | 被覆用組成物 |
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Patent Citations (4)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN1817981A (zh) * | 2005-12-31 | 2006-08-16 | 浙江大学 | 一种纳米级颜料型喷墨印花油墨及其制备方法 |
CN101165264A (zh) * | 2006-10-16 | 2008-04-23 | 恒源祥(集团)有限公司 | 一种纳米型纺织物多功能整理剂及其整理方法 |
CN101784573A (zh) * | 2007-08-30 | 2010-07-21 | 大赛璐化学工业株式会社 | 共聚物 |
CN101768895A (zh) * | 2009-01-07 | 2010-07-07 | 湖北大学 | 一种苯丙乳液型高效表面施胶剂及其制备方法 |
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Effective date of registration: 20171214 Address after: 201512 Shanghai city Jinshan District No. 639 Sheng Lu Xia Patentee after: SHANGHAI DONGRUI CHEMICAL Co.,Ltd. Address before: No. 601, No. six, Bao Yuan, Shanghai, Jiading District, Jiangqiao town Patentee before: SHANGHAI DONGRUI PLASTIC PRODUCTS Co.,Ltd. |
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Denomination of invention: Co polystyrene acrylate lotion for textile adhesive interlining and its preparation method Effective date of registration: 20220721 Granted publication date: 20160316 Pledgee: Industrial Bank Co.,Ltd. Shanghai Branch Pledgor: SHANGHAI DONGRUI CHEMICAL Co.,Ltd. Registration number: Y2022310000135 |
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Denomination of invention: Co polystyrene acrylate lotion for textile adhesive interlining and its preparation method Effective date of registration: 20230726 Granted publication date: 20160316 Pledgee: Industrial Bank Co.,Ltd. Shanghai Jinshan Branch Pledgor: SHANGHAI DONGRUI CHEMICAL Co.,Ltd. Registration number: Y2023310000400 |
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Address after: 639 Xiasheng Road, Jinshan District, Shanghai, May 12, 2015 Patentee after: Shanghai Dongrui New Materials Co.,Ltd. Country or region after: China Address before: 639 Xiasheng Road, Jinshan District, Shanghai, May 12, 2015 Patentee before: SHANGHAI DONGRUI CHEMICAL Co.,Ltd. Country or region before: China |
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