CN103250731A - Insecticide sterilization compound agent containing hymexazol - Google Patents
Insecticide sterilization compound agent containing hymexazol Download PDFInfo
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- CN103250731A CN103250731A CN2013102101159A CN201310210115A CN103250731A CN 103250731 A CN103250731 A CN 103250731A CN 2013102101159 A CN2013102101159 A CN 2013102101159A CN 201310210115 A CN201310210115 A CN 201310210115A CN 103250731 A CN103250731 A CN 103250731A
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Abstract
The invention discloses an insecticide sterilization compound agent containing hymexazol. The insecticide sterilization compound agent comprises the following components in percentage by weight: 0.01-10 percent of hymexazol, 0.05-50 percent of an insecticide component, 1-40 percent of humic acid, 1-25 percent of assistants, and the balance of a carrier, wherein the insecticide component is any one of dinotefuran, clothianidin or thiamethoxam. The insecticide sterilization compound agent is remarkable in synergistic effect, is capable of simultaneously controlling pests and diseases, and is remarkable in control effect, so that the applying frequency and the applying dosage of the compound agent are effectively reduced, and the pesticide applying cost is lowered; and the disease and pest resisting capability of crops can be remarkably improved by the compound agent, so that the rhizome development and plant growth of the crops are promoted, and the yield and quality of the crops are improved.
Description
Technical field
The present invention relates to the pesticidal preparations field, specifically is a kind of composite dose of pesticide-germicide of disliking mould spirit that contains.
Background technology
At present, the mode of domestic cultural control damage by disease and insect takes insecticide and bactericide to use separately more, has following three aspect problems:
(1) use is incomplete to crop pest, pest integrative control separately for insecticide, bactericide, cause a certain disease or insect pest to control easily, and another insect pest or disease is not controlled, and influence crop production.
(2) China peasant household drug level is not very high at present, many times the medicament at control different times generation disease, insect pest can be mixed and use, and this makes a certain composition medicament cause waste, causes the loss of labour's financial resources.
(3) the long-term single use of desinsection, bactericide causes crop disease and insect to can not get comprehensive treatment, and peasant household blindly strengthens dosage or the medication that is mixed for output, has further increased the weight of the agricultural residual risk that exceeds standard and poison, and has increased the drug cost of peasant household.
In recent years, agrotechnique consultant much is deep into the field and instructs peasant household's medication, promoted peasant household's drug level to a certain extent, but on the market separately desinsection, bactericide agricultural chemicals product many, mix, scientific and reasonable pesticide-germicide mixed agent is considerably less, this is selecting medicinal medicine to bring very big inconvenience for peasant household, prevents and treats at crop disease and insect comprehensively and does not satisfy the demand of peasant household.
Summary of the invention
The purpose of this invention is to provide a kind of composite dose of pesticide-germicide of disliking mould spirit that contains, solve the narrow problem of present single insecticide or bactericidal agent for preventing and treating spectrum, in insect protected, solve the crop pest problem, can improve crop growing state after the medication, strengthen resistance against diseases, increase output.
The present invention solves the problems of the technologies described above the technical scheme of taking: a kind of composite dose of pesticide-germicide of disliking mould spirit that contains, formed by following component by mass percent: dislike mould clever 0.01～10%, insecticide component 0.05～50%, humus 1～40%, auxiliary agent 1～25%, carrier supplies 100%; Wherein, insecticide component is any one in MTI-446, thiophene worm amine or the thiophene worm piperazine.
Described auxiliary agent is at least a in lauryl sodium sulfate, calcium lignosulfonate, sodium lignin sulfonate, sodium butylnaphthalenesulfonate, fatty alcohol-polyoxyethylene ether, dioctyl sodium sulfosuccinate, naphthalenesulfonate formaldehyde condensation compound, starch, sucrose, polyvinyl alcohol or the carboxymethyl cellulose.
Described carrier is at least a in White Carbon black, kaolin, bentonite, diatomite, calcium carbonate, ammonium chloride, ammonium sulfate, potassium sulphate, potassium dihydrogen phosphate, ammonium dihydrogen phosphate (ADP), calcium dihydrogen phosphate or the flyash.
Described composite dose of the pesticide-germicide of disliking mould spirit that contains is prepared into wetting powder, granule or seed dressing.
The present invention can be used in soil insect, ground insect, nematode, fusarium wilt and the damping off that control comprises the various crop of sugarcane, peanut, corn, banana, wild cabbage and paddy rice.Compared with prior art, have following beneficial effect:
(1) active ingredient of the present invention is disliked mould spirit by any and bactericide in insecticide thiophene worm amine, MTI-446 or the thiophene worm piperazine and is mixed and forms, it is obvious to mix collaborative preventive effect effect, but not only pest control but also can prevent and treat disease, and preventive effect is obvious, reduce spraying times and formulation rate, reduce drug cost.
(2) the present invention not only can realize the generation of prevention and control damage by disease and insect effectively, and can significantly improve the pest-resistant power of crop disease-resistant, promotes crop root development and plant strain growth simultaneously, improves the yield and quality of crop.
Embodiment
Except specified otherwise was arranged, constituent content of the present invention was mass percentage content.
EXAMPLE l
0.06% thiophene worm amine is disliked mould clever granule
Prescription: thiophene worm amine 0.05kg, dislike mould clever 0.0lkg, humus 1kg, calcium lignosulfonate 0.4kg, lauryl sodium sulfate 0.6kg, polyvinyl alcohol lkg, ammonium chloride l0kg, ammonium dihydrogen phosphate (ADP) 25kg, kaolin complements to 100kg.
Above-mentioned recipe ingredient is mixed, pulverize, stir after adding water-wet, use the screw extruder pelletizer granulation again, sieving after the drying namely gets 0.06% thiophene worm amine and dislikes mould clever granule.
Embodiment 2
6% thiophene worm amine is disliked mould clever granule
Prescription: thiophene worm amine 5kg, dislike mould clever 1kg, humus 40kg, fatty alcohol-polyoxyethylene ether lkg, lauryl sodium sulfate 0.5kg, starch lkg, kaolin 20kg, diatomite complements to l00kg.
Above-mentioned recipe ingredient is mixed, pulverize, stir after adding water-wet, use the screw extruder pelletizer granulation again, sieving after the drying namely gets 6% thiophene worm amine and dislikes mould clever granule.
Embodiment 3
12% thiophene worm amine is disliked mould clever granule
Prescription: thiophene worm amine 2kg, dislike mould clever l0kg, humus 20kg, dioctyl sodium sulfosuccinate lkg, naphthalenesulfonate formaldehyde condensation compound 3kg, sucrose 7kg, carboxymethyl cellulose 3kg, ammonium sulfate 15kg, calcium carbonate 10kg, kaolin complements to l00kg.
Above-mentioned recipe ingredient is mixed, pulverize, stir after adding water-wet, use the screw extruder pelletizer granulation again, sieving after the drying namely gets 12% thiophene worm amine and dislikes mould clever granule.
Embodiment 4
60% thiophene worm amine is disliked mould clever wetting powder
Prescription: thiophene worm amine 50kg, dislike mould clever 10kg, humus 5kg, calcium lignosulfonate 15kg, lauryl sodium sulfate 5kg, White Carbon black 3kg, bentonite complements to l00kg.
Above-mentioned recipe ingredient double helix is fully mixed, after air-flow is pulverized, stir, namely get 60% thiophene worm amine and dislike mould clever wetting powder.
Embodiment 5
5% thiophene worm amine is disliked mould clever wetting powder
Prescription: thiophene worm amine 1kg, dislike mould clever 4kg, humus 20kg, sodium butylnaphthalenesulfonate 1kg, lauryl sodium sulfate 3kg, 15 kilograms of White Carbon blacks, kaolin complements to l00kg.
Above-mentioned recipe ingredient double helix is fully mixed, after air-flow is pulverized, stir, namely get 5% thiophene worm amine and dislike mould clever wetting powder.
Embodiment 6
0.5% thiophene worm amine is disliked mould clever wetting powder
Prescription: thiophene worm amine 0.05kg, dislike mould clever 0.45kg, humus 10kg, lauryl sodium sulfate 3kg, potassium dihydrogen phosphate 15kg, ammonium chloride 20kg, 10 kilograms of White Carbon blacks, kaolin complements to l00kg.
Above-mentioned recipe ingredient double helix is fully mixed, after air-flow is pulverized, namely get 0.5% thiophene worm amine and dislike mould clever wetting powder.
Embodiment 7
55% thiophene worm amine is disliked mould clever seed dressing
Prescription: thiophene worm amine 50kg, dislike mould clever 5kg, humus 15kg, calcium lignosulfonate 2kg, lauryl sodium sulfate 3kg, kaolin complements to l00kg.
Above-mentioned recipe ingredient double helix is fully mixed, after air-flow is pulverized, namely get 55% thiophene worm amine and dislike mould clever seed dressing.
Embodiment 8
15% thiophene worm amine is disliked mould clever seed dressing
Prescription: thiophene worm amine 5kg, dislike mould clever 10kg, humus 5kg, sodium butylnaphthalenesulfonate 5kg, lauryl sodium sulfate 3kg, potassium sulphate 10kg, calcium sulphate 5kg, ammonium sulfate 20kg, flyash complements to l00kg.
Above-mentioned recipe ingredient double helix is fully mixed, after air-flow is pulverized, namely get 15% thiophene worm amine and dislike mould clever seed dressing.
Embodiment 9
5% thiophene worm amine is disliked mould clever seed dressing
Prescription: thiophene worm amine 1kg, dislike mould clever 4kg, humus 40kg, sodium butylnaphthalenesulfonate 3kg, lauryl sodium sulfate 3kg, potassium sulphate 5kg, calcium sulphate 5kg, ammonium sulfate 15kg, flyash complements to l00kg.
Above-mentioned recipe ingredient double helix is fully mixed, after air-flow is pulverized, namely get 5% thiophene worm amine and dislike mould clever seed dressing.
EXAMPLE l 0
0.06% MTI-446 is disliked mould clever granule
Prescription: MTI-446 0.05kg dislikes mould clever 0.0lkg, humus 1kg, and sodium lignin sulfonate 0.4kg, lauryl sodium sulfate 0.6kg, polyvinyl alcohol lkg, ammonium chloride l0kg, ammonium dihydrogen phosphate (ADP) 25kg, kaolin complements to 100kg.
Above-mentioned recipe ingredient is mixed, pulverize, stir after adding water-wet, use the screw extruder pelletizer granulation again, sieving after the drying namely gets 0.06% MTI-446 and dislikes mould clever granule.
Embodiment 11
6% MTI-446 is disliked mould clever granule
Prescription: MTI-446 5kg dislikes mould clever 1kg, humus 40kg, and fatty alcohol-polyoxyethylene ether lkg, lauryl sodium sulfate 0.5kg, starch lkg, kaolin 20kg, diatomite complements to l00kg.
Above-mentioned recipe ingredient is mixed, pulverize, stir after adding water-wet, use the screw extruder pelletizer granulation again, sieving after the drying namely gets 6% MTI-446 and dislikes mould clever granule.
Embodiment 12
12% MTI-446 is disliked mould clever granule
Prescription: MTI-446 2kg dislikes mould clever l0kg, humus 20kg, and dioctyl sodium sulfosuccinate lkg, naphthalenesulfonate formaldehyde condensation compound 3kg, sucrose 7kg, carboxymethyl cellulose 3kg, ammonium sulfate 15kg, calcium carbonate 10kg, kaolin complements to l00kg.
Above-mentioned recipe ingredient is mixed, pulverize, stir after adding water-wet, use the screw extruder pelletizer granulation again, sieving after the drying namely gets 12% MTI-446 and dislikes mould clever granule.
Embodiment 13
40% MTI-446 is disliked mould clever wetting powder
Prescription: MTI-446 30kg dislikes mould clever 10kg, humus 5kg, and calcium lignosulfonate 12kg, lauryl sodium sulfate 3kg, White Carbon black 3kg, bentonite complements to l00kg.
Above-mentioned recipe ingredient double helix is fully mixed, after air-flow is pulverized, stir, namely get 40% MTI-446 and dislike mould clever wetting powder.
Embodiment 14
5% MTI-446 is disliked mould clever wetting powder
Prescription: MTI-446 1kg dislikes mould clever 4kg, humus 20kg, and sodium butylnaphthalenesulfonate 1kg, lauryl sodium sulfate 3kg, 15 kilograms of White Carbon blacks, kaolin complements to l00kg.
Above-mentioned recipe ingredient double helix is fully mixed, after air-flow is pulverized, stir, namely get 5% MTI-446 and dislike mould clever wetting powder.
Embodiment 15
0.5% MTI-446 is disliked mould clever wetting powder
Prescription: MTI-446 0.05kg dislikes mould clever 0.45kg, humus 10kg, and lauryl sodium sulfate 3kg, potassium dihydrogen phosphate 15kg, calcium dihydrogen phosphate 2kg, ammonium chloride 20kg, 10 kilograms of White Carbon blacks, kaolin complements to l00kg.
Above-mentioned recipe ingredient double helix is fully mixed, after air-flow is pulverized, namely get 0.5% MTI-446 and dislike mould clever wetting powder.
Embodiment 16
25% MTI-446 is disliked mould clever seed dressing
Prescription: MTI-446 20kg dislikes mould clever 5kg, humus 15kg, and calcium lignosulfonate 2kg, lauryl sodium sulfate 3kg, kaolin complements to l00kg.
Above-mentioned recipe ingredient double helix is fully mixed, after air-flow is pulverized, namely get 25% MTI-446 and dislike mould clever seed dressing.
Embodiment 17
15% MTI-446 is disliked mould clever seed dressing
Prescription: MTI-446 5kg dislikes mould clever 10kg, humus 5kg, and sodium butylnaphthalenesulfonate 5kg, lauryl sodium sulfate 3kg, potassium sulphate 10kg, calcium sulphate 5kg, ammonium sulfate 20kg, flyash complements to l00kg.
Above-mentioned recipe ingredient double helix is fully mixed, after air-flow is pulverized, namely get 15% MTI-446 and dislike mould clever seed dressing.
Embodiment 18
5% MTI-446 is disliked mould clever seed dressing
Prescription: MTI-446 1kg dislikes mould clever 4kg, humus 40kg, and sodium butylnaphthalenesulfonate 3kg, lauryl sodium sulfate 3kg, potassium sulphate 5kg, calcium sulphate 5kg, ammonium sulfate 15kg, flyash complements to l00kg.
Above-mentioned recipe ingredient double helix is fully mixed, after air-flow is pulverized, namely get 5% MTI-446 and dislike mould clever seed dressing.
EXAMPLE l 9
0.06% thiophene worm piperazine is disliked mould clever granule
Prescription: thiophene worm piperazine 0.05kg, dislike mould clever 0.0lkg, humus 1kg, calcium lignosulfonate 0.4kg, lauryl sodium sulfate 0.6kg, polyvinyl alcohol lkg, ammonium chloride l0kg, ammonium dihydrogen phosphate (ADP) 25kg, kaolin complements to 100kg.
Above-mentioned recipe ingredient is mixed, pulverize, stir after adding water-wet, use the screw extruder pelletizer granulation again, sieving after the drying namely gets 0.06% thiophene worm piperazine and dislikes mould clever granule.
Embodiment 20
6% thiophene worm piperazine is disliked mould clever granule
Prescription: thiophene worm piperazine 5kg, dislike mould clever 1kg, humus 40kg, fatty alcohol-polyoxyethylene ether lkg, lauryl sodium sulfate 0.5kg, starch lkg, kaolin 20kg, diatomite complements to l00kg.
Above-mentioned recipe ingredient is mixed, pulverize, stir after adding water-wet, use the screw extruder pelletizer granulation again, sieving after the drying namely gets 6% thiophene worm piperazine and dislikes mould clever granule.
Embodiment 21
12% thiophene worm piperazine is disliked mould clever granule
Prescription: thiophene worm piperazine 2kg, dislike mould clever l0kg, humus 20kg, dioctyl sodium sulfosuccinate lkg, naphthalenesulfonate formaldehyde condensation compound 3kg, sucrose 7kg, carboxymethyl cellulose 3kg, ammonium sulfate 15kg, calcium carbonate 10kg, kaolin complements to l00kg.
Above-mentioned recipe ingredient is mixed, pulverize, stir after adding water-wet, use the screw extruder pelletizer granulation again, sieving after the drying namely gets 12% thiophene worm piperazine and dislikes mould clever granule.
Embodiment 22
60% thiophene worm piperazine is disliked mould clever wetting powder
Prescription: thiophene worm piperazine 50kg, dislike mould clever 10kg, humus 5kg, calcium lignosulfonate 12kg, lauryl sodium sulfate 3kg, White Carbon black 3kg, bentonite complements to l00kg.
Above-mentioned recipe ingredient double helix is fully mixed, after air-flow is pulverized, stir, namely get 60% thiophene worm piperazine and dislike mould clever wetting powder.
Embodiment 23
5% thiophene worm piperazine is disliked mould clever wetting powder
Prescription: thiophene worm piperazine 1kg, dislike mould clever 4kg, humus 20kg, sodium butylnaphthalenesulfonate 1kg, lauryl sodium sulfate 3kg, 15 kilograms of White Carbon blacks, kaolin complements to l00kg.
Above-mentioned recipe ingredient double helix is fully mixed, after air-flow is pulverized, stir, namely get 5% thiophene worm piperazine and dislike mould clever wetting powder.
Embodiment 24
0.5% thiophene worm piperazine is disliked mould clever wetting powder
Prescription: thiophene worm piperazine 0.05kg, dislike mould clever 0.45kg, humus 10kg, lauryl sodium sulfate 3kg, potassium dihydrogen phosphate 15kg, ammonium chloride 20kg, 10 kilograms of White Carbon blacks, kaolin complements to l00kg.
Above-mentioned recipe ingredient double helix is fully mixed, after air-flow is pulverized, namely get 0.5% thiophene worm piperazine and dislike mould clever wetting powder.
Embodiment 25
55% thiophene worm piperazine is disliked mould clever seed dressing
Prescription: thiophene worm piperazine 50kg, dislike mould clever 5kg, humus 15kg, calcium lignosulfonate 2kg, lauryl sodium sulfate 3kg, kaolin complements to l00kg.
Above-mentioned recipe ingredient double helix is fully mixed, after air-flow is pulverized, namely get 55% thiophene worm piperazine and dislike mould clever seed dressing.
Embodiment 26
15% thiophene worm piperazine is disliked mould clever seed dressing
Prescription: thiophene worm piperazine 5kg, dislike mould clever 10kg, humus 5kg, sodium butylnaphthalenesulfonate 5kg, lauryl sodium sulfate 3kg, potassium sulphate 10kg, calcium sulphate 5kg, ammonium sulfate 20kg, flyash complements to l00kg.
Above-mentioned recipe ingredient double helix is fully mixed, after air-flow is pulverized, namely get 15% thiophene worm piperazine and dislike mould clever seed dressing.
Embodiment 27
5% thiophene worm piperazine is disliked mould clever seed dressing
Prescription: thiophene worm piperazine 1kg, dislike mould clever 4kg, humus 40kg, sodium butylnaphthalenesulfonate 3kg, lauryl sodium sulfate 3kg, potassium sulphate 5kg, calcium sulphate 5kg, ammonium sulfate 15kg, flyash complements to l00kg.
Above-mentioned recipe ingredient double helix is fully mixed, after air-flow is pulverized, namely get 5% thiophene worm piperazine and dislike mould clever seed dressing.
Application example l
Carry out the control of banana root-knot nematode and fusarium wilt with embodiment 1-3 products obtained therefrom, according to the product estimated cost, will test processing and arrange as follows:
Handle l:0.06% thiophene worm amine and dislike mould clever granule 100kg/ mu;
Handle 2:6% thiophene worm amine and dislike mould clever granule 1.5kg/ mu;
Handle 3:12% thiophene worm amine and dislike mould clever granule 3kg/ mu;
Handle 4:1% thiophene worm amine granule 5kg/ mu;
Handle 5:2% and dislike mould clever granule 2.5kg/ mu;
Handle 6: blank.
Above-mentioned processing is used when the banana field planting, carries out root-knot nematode and fusarium wilt investigation in 45 days behind the medicine, carries out determination of yield during results, and final statistics is as shown in the table:
| Test is handled | To root-knot nematode preventive effect (%) | To fusarium wilt preventive effect (%) | Rate of growth (%) |
| Handle 1 | 83.3 | 80.6 | 21.4 |
| Handle 2 | 85.6 | 81.4 | 23.6 |
| Handle 3 | 79.3 | 75.6 | 20.5 |
| Handle 4 | 54.3 | / | 8.5 |
| Handle 5 | / | 50.7 | 5.8 |
| Handle 6 | / | / | / |
As seen, under the prerequisite that use cost approaches, embodiment 1-3 products obtained therefrom obviously than disliking mould spirit, the preventive effect height of thiophene worm amine list time spent, and can make banana production increase more than 20% to the preventive effect of banana root-knot nematode and fusarium wilt.
Application example 2
Carry out the control of peanut grub and slijmziekte with embodiment 10-12 products obtained therefrom, according to the product estimated cost, will test processing and arrange as follows:
Handle the 7:0.06% MTI-446 and dislike mould clever granule 100kg/ mu;
Handle the 8:6% MTI-446 and dislike mould clever granule 1.5kg/ mu;
Handle the 9:12% MTI-446 and dislike mould clever granule 3kg/ mu;
Handle 10:1% MTI-446 granule 5kg/ mu;
Handle 11:2% and dislike mould clever granule 2.5kg/ mu
Handle 12: blank.
Above-mentioned processing is used when peanut seeding, and a situation arises for 30 days " Invest, Then Investigate " slijmziektes and peanut grub, gathers in the crops after 100 days and carries out peanut grub insect population number, fusarium wilt investigation and peanut yield and measure, and final statistics is as shown in the table:
| Test is handled | To slijmziekte preventive effect (%) | To peanut grub preventive effect (%) | Rate of growth (%) |
| Handle 7 | 86.4 | 93.6 | 25.4 |
| Handle 8 | 88.3 | 92.5 | 22.6 |
| Handle 9 | 80.9 | 88.6 | 21.8 |
| Handle 10 | / | 68.7 | 9.3 |
| Handle 11 | 60.5 | / | 5.6 |
| Handle 12 | / | / | / |
As seen, under the prerequisite that use cost approaches, embodiment 10-12 products obtained therefrom is being prevented and treated aspect slijmziekte and the peanut grub, and preventive effect is all obviously than disliking mould spirit, the preventive effect height of single time spent of MTI-446, and can make peanut yield increase more than 20%.
Application example 3
Carry out the control of sugarcane moth borer, fusarium wilt with embodiment 19-21 products obtained therefrom, according to the product estimated cost, will test processing and arrange as follows:
Handle 13:0.06% thiophene worm piperazine and dislike mould clever granule 100kg/ mu;
Handle 14:6% thiophene worm piperazine and dislike mould clever granule 1.5kg/ mu;
Handle 15:12% thiophene worm piperazine and dislike mould clever granule 3kg/ mu;
Handle 16:1% thiophene worm piperazine granule 5kg/ mu;
Handle 17:2% and dislike mould clever granule 2.5kg/ mu
Handle 18: blank.
Above-mentioned processing is used when sugarcane is sowed, and carries out behind the medicine that sugarcane moth borer is caused harm in 60 days and fusarium wilt a situation arises investigation, carries out determination of yield during the sugarcane harvesting, and final statistics is as shown in the table:
| Test is handled | To sugarcane fusarium wilt preventive effect (%) | To sugarcane moth borer preventive effect (%) | Rate of growth (%) |
| Handle 13 | 82.1 | 78.6 | 21.4 |
| Handle 14 | 84.0 | 80.5 | 24.1 |
| Handle 15 | 77.7 | 82.6 | 20.6 |
| Handle 16 | / | 46.8 | 8.8 |
| Handle 17 | 47.5 | / | 6.4 |
| Handle 18 | / | / | / |
As seen, under the prerequisite that use cost approaches, embodiment 19-21 products obtained therefrom obviously than disliking mould spirit, the preventive effect height of thiophene worm piperazine list time spent, and can make sugarcane yield increase more than 20% to the preventive effect of sugarcane moth borer and fusarium wilt.
Application example 4
Mix fertilizer with embodiment 4-6, embodiment 13-15 and embodiment 22-24 products obtained therefrom and spread fertilizer over the fields the control of carrying out peanut grub and fusarium wilt, according to the product estimated cost, will test processing and arrange as follows:
Handle 19:60% thiophene worm amine and dislike mould clever wetting powder 40g/ mu;
Handle 20:5% thiophene worm amine and dislike mould clever wetting powder 500g/ mu;
Handle 21:0.5% thiophene worm amine and dislike mould clever wetting powder 8kg/ mu;
Handle the 22:40% MTI-446 and dislike mould clever wetting powder 60g/ mu;
Handle the 23:5% MTI-446 and dislike mould clever wetting powder 500g/ mu;
Handle the 24:0.5% MTI-446 and dislike mould clever wetting powder 8kg/ mu;
Handle 25:60% thiophene worm piperazine and dislike mould clever wetting powder 40g/ mu;
Handle 26:5% thiophene worm piperazine and dislike mould clever wetting powder 500g/ mu;
Handle 27:0.5% thiophene worm piperazine and dislike mould clever wetting powder 8kg/ mu;
Handle 28:5% thiophene worm amine wetting powder 400g/ mu;
Handle 29:5% MTI-446 wetting powder 400g/ mu;
Handle 30:5% thiophene worm piperazine wetting powder 400g/ mu;
Handle 31:5% and dislike mould clever wetting powder 200g/ mu;
Handle 32: blank.
Above-mentioned processing is used when peanut seeding applies fertilizer, and carries out behind the medicine that peanut grub is caused harm in 30 days and fusarium wilt a situation arises investigation, carries out determination of yield during harvesting peanut, and final statistics is as shown in the table:
| Test is handled | To slijmziekte preventive effect (%) | To peanut grub preventive effect (%) | Rate of growth (%) |
| Handle 19 | 83.9 | 91.3 | 25.8 |
| Handle 20 | 86.4 | 88.6 | 22.5 |
| Handle 21 | 80.2 | 87.3 | 21.6 |
| Handle 22 | 85.6 | 89.5 | 25.3 |
| Handle 23 | 84.5 | 86.5 | 24.7 |
| Handle 24 | 88.3 | 87.3 | 25.6 |
| Handle 25 | 82.5 | 86.5 | 27.9 |
| Handle 26 | 88.2 | 85.4 | 25.5 |
| Handle 27 | 85.4 | 86.5 | 23.6 |
| Handle 28 | / | 52.3 | 10.2 |
| Handle 29 | / | 54.7 | 5.6 |
| Handle 30 | / | 58.9 | 9.6 |
| Handle 31 | 42.8 | / | 8.5 |
| Handle 32 | / | / | / |
As seen, under the prerequisite that use cost approaches, embodiment 4-6, embodiment 13-15 and embodiment 22-24 products obtained therefrom obviously than disliking mould spirit, the preventive effect height of thiophene worm amine list time spent, and can make peanut yield increase more than 20% to the preventive effect of peanut grub and fusarium wilt.
Application example 5
Carry out the control of the snout moth's larva of rice, damping off with embodiment 7-9, embodiment 16-18, the seed dressing of embodiment 25-27 products obtained therefrom, according to the product estimated cost, will test processing and arrange as follows:
Processing 33:55% thiophene worm amine is disliked mould clever seed dressing 20g and is mixed 5kg paddy rice kind;
Processing 34:15% thiophene worm amine is disliked mould clever seed dressing 100g and is mixed 5kg paddy rice kind;
Processing 35:5% thiophene worm amine is disliked mould clever seed dressing 200g and is mixed 5kg paddy rice kind;
Processing 36:25% MTI-446 is disliked mould clever seed dressing 30g and is mixed 5kg paddy rice kind;
Processing 37:15% MTI-446 is disliked mould clever seed dressing 100g and is mixed 5kg paddy rice kind;
Processing 38:5% MTI-446 is disliked mould clever seed dressing 200g and is mixed 5kg paddy rice kind;
Processing 39:55% thiophene worm piperazine is disliked mould clever seed dressing 20g and is mixed 5kg paddy rice kind;
Processing 40:15% thiophene worm piperazine is disliked mould clever seed dressing 100g and is mixed 5kg paddy rice kind;
Processing 41:5% thiophene worm piperazine is disliked mould clever seed dressing 200g and is mixed 5kg paddy rice kind;
Handle 42:5% thiophene worm amine seed dressing 20g and mix 5kg paddy rice kind;
Handle 43:5% MTI-446 seed dressing 20g and mix 5kg paddy rice kind;
Handle 44:5% thiophene worm piperazine seed dressing 20g and mix 5kg paddy rice kind;
Processing 45:5% dislikes mould clever seed dressing 20g and mixes 5kg paddy rice kind.
Handle 46: blank.
Above-mentioned processing is used after the seed dressing in 1-2 days before rice growing, carries out behind the medicine that the snout moth's larva of rice is caused harm in 30 days and damping off a situation arises investigation, carries out determination of yield during rice harves, and final statistics is as shown in the table:
| Test is handled | To paddy rice damping off preventive effect (%) | To snout moth's larva of rice preventive effect (%) | Rate of growth (%) |
| Handle 33 | 86.4 | 83.5 | 22.7 |
| Handle 34 | 85.3 | 87.2 | 24.3 |
| Handle 35 | 81.6 | 89.5 | 23.8 |
| Handle 36 | 85.3 | 88.5 | 22.5 |
| Handle 37 | 82.4 | 80.9 | 23.6 |
| Handle 38 | 88.6 | 83.5 | 28.4 |
| Handle 39 | 87.5 | 86.4 | 25.6 |
| Handle 40 | 85.6 | 82.5 | 24.3 |
| Handle 41 | 84.4 | 81.3 | 21.7 |
| Handle 42 | / | 49.6 | 7.7 |
| Handle 43 | / | 52.4 | 8.6 |
| Handle 44 | / | 50.3 | 10.3 |
| Handle 45 | 54.2 | / | 9.7 |
| Handle 46 | / | / | / |
As seen, under the prerequisite that use cost approaches, embodiment 7-9, embodiment 16-18, embodiment 25-27 products obtained therefrom obviously than disliking mould spirit, the preventive effect height of thiophene worm amine list time spent, and can make rice yield increase more than 20% to the preventive effect of the snout moth's larva of rice and damping off.
Indoor joint toxicity measuring test l
Thiophene worm amine, dislike mould spirit and be mixed to the indoor joint toxicity measuring of corn borer, test with thiophene worm amine, dislike mould clever two kinds of single agent medicament in contrast, and according to following ratio preparation mixture l number to No. 5, mixture:
Mixture l thiophene worm amine: dislike mould spirit=1:5
No. 2 thiophene worms of mixture amine: dislike mould spirit=5:1
No. 3 thiophene worms of mixture amine: dislike mould spirit=1:200
No. 4 thiophene worms of mixture amine: dislike mould spirit=200:1
No. 5 thiophene worms of mixture amine: dislike mould spirit=1:1
Test is the examination worm with the corn borer, and blank is set, and adopts dip method to carry out toxicity test and do statistical analysis thiophene worm amine and above-mentioned 5 mixtures, and final statistics is as shown in the table:
| Medicament | Virulence regression equation | Correlation coefficient | LC 50(mg/L) | Co-toxicity coefficient |
| The former medicine of thiophene worm amine | Y=4.1383+1.7699X | 0.9843 | 3.10 | / |
| No. 1, mixture | Y=4.3894+1.5584X | 0.9962 | 2.47 | 124.3 |
| No. 2, mixture | Y=4.2103+2.0811X | 0.9719 | 2.40 | 127.9 |
| No. 3, mixture | Y=4.4272+1.7189X | 0.9827 | 2.15 | 142.8 |
| No. 4, mixture | Y=4.4169+1.5712X | 0.9954 | 2.35 | 130.6 |
| No. 5, mixture | Y=4.2923+1.8519X | 0.9949 | 2.41 | 127.4 |
Toxicity Determination result shows, the mixed agent of above-mentioned 5 different proportions all greater than 120, namely shows synergistic effect to the co-toxicity coefficient of corn borer.
Indoor joint toxicity measuring test 2
MTI-446, dislike mould spirit and be mixed to the indoor joint toxicity measuring of watermelon blight, test to be disliking the single agent of mould spirit medicament in contrast, and according to No. 6, following ratio preparation mixture to No. 10, mixture:
No. 6 MTI-446 of mixture: dislike mould spirit=1:10
No. 7 MTI-446 of mixture: dislike mould spirit=10:1
No. 8 MTI-446 of mixture: dislike mould spirit=1:300
No. 9 MTI-446 of mixture: dislike mould spirit=300:1
No. 10 MTI-446 of mixture: dislike mould spirit=1:2
Test was pathogeny with watermelon blight originally, and blank is set, and will dislike the single agent of mould spirit and above-mentioned 5 mixtures and adopt the colony diameter method to carry out toxicity test and do statistical analysis, and final statistics is as shown in the table:
| Medicament | Virulence regression equation | Correlation coefficient | EC 50(mg/L) | Co-toxicity coefficient |
| The former medicine of MTI-446 | Y=2.8883+1.4014X | 0.9985 | 32.13 | / |
| No. 6, mixture | Y=2.2750+1.9450X | 0.9868 | 25.18 | 124.0 |
| No. 7, mixture | Y=1.9097+2.1974X | 0.9933 | 25.49 | 122.5 |
| No. 8, mixture | Y=2.4686+1.7932X | 0.9788 | 25.80 | 121.0 |
| No. 9, mixture | Y=2.6732+1.6478X | 0.9977 | 25.83 | 120.9 |
| No. 10, mixture | Y=2.4578+1.8519X | 0.9978 | 23.59 | 132.4 |
Toxicity Determination result shows, above-mentioned 5 different ratios are mixed co-toxicity coefficient to watermelon blight all greater than 120, namely show synergistic effect.
Indoor joint toxicity measuring test 3
Thiophene worm piperazine, dislike mould spirit and be mixed to the indoor joint toxicity measuring of rice-stem borer, test is with thiophene worm piperazine list agent medicament in contrast, and according to No. 11, following ratio preparation mixture to No. 15, mixture:
No. 11 thiophene worms of mixture piperazine: dislike mould spirit=1:30
No. 12 thiophene worms of mixture piperazine: dislike mould spirit=30:1
No. 13 thiophene worms of mixture piperazine: dislike mould spirit=1:500
No. 14 thiophene worms of mixture piperazine: dislike mould spirit=500:1
No. 15 thiophene worms of mixture piperazine: dislike mould spirit=1:100
Test is the examination worm with the rice-stem borer, and blank is set, and adopts dip method to carry out toxicity test and do statistical analysis the list agent of thiophene worm piperazine and above-mentioned 5 mixtures, and final statistics is as shown in the table:
| Medicament | Virulence regression equation | Correlation coefficient | LC 50(mg/L) | Co-toxicity coefficient |
| The former medicine of thiophene worm piperazine | Y=2.6447+1.8015X | 0.9927 | 20.30 | / |
| No. 11, mixture | Y=2.4524+2.1409X | 0.9871 | 15.49 | 131.1 |
| No. 12, mixture | Y=2.6624+1.9512X | 0.9958 | 15.78 | 128.6 |
| No. 13, mixture | Y=2.5067+1.8985X | 0.9958 | 20.57 | 98.7 |
| No. 14, mixture | Y=2.8498+1.6478X | 0.9977 | 20.18 | 100.6 |
| No. 15, mixture | Y=2.8131+1.8519X | 0.9978 | 15.17 | 133.8 |
Toxicity Determination result shows, except the co-toxicity coefficient of No. 14, No. 13, mixture and mixture showed summation action, the co-toxicity coefficient of mixture No. 11, No. 12 and No. 15 namely showed obvious synergistic effect all greater than 120.
Claims (4)
1. one kind contains composite dose of the pesticide-germicide of disliking mould spirit, it is characterized in that, is made up of following component by mass percent: dislike mould clever 0.01～10%, insecticide component 0.05～50%, humus 1～40%, auxiliary agent 1～25%, carrier supplies 100%; Wherein, insecticide component is any one in MTI-446, thiophene worm amine or the thiophene worm piperazine.
2. composite dose of the pesticide-germicide of disliking mould spirit that contains according to claim 1, it is characterized in that auxiliary agent is at least a in lauryl sodium sulfate, calcium lignosulfonate, sodium lignin sulfonate, sodium butylnaphthalenesulfonate, fatty alcohol-polyoxyethylene ether, dioctyl sodium sulfosuccinate, naphthalenesulfonate formaldehyde condensation compound, starch, sucrose, polyvinyl alcohol or the carboxymethyl cellulose.
3. composite dose of the pesticide-germicide of disliking mould spirit that contains according to claim 1 and 2, it is characterized in that carrier is at least a in White Carbon black, kaolin, bentonite, diatomite, calcium carbonate, ammonium chloride, ammonium sulfate, potassium sulphate, potassium dihydrogen phosphate, ammonium dihydrogen phosphate (ADP), calcium dihydrogen phosphate or the flyash.
4. composite dose of the pesticide-germicide of disliking mould spirit that contains according to claim 1 and 2 is characterized in that, is prepared into wetting powder, granule or seed dressing.
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Cited By (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN104145965A (en) * | 2014-07-28 | 2014-11-19 | 浙江省化工研究院有限公司 | Insecticidal and fungicidal composition containing hymexazol |
| CN104604921A (en) * | 2014-12-24 | 2015-05-13 | 陈燕婷 | Azole seed treatment agent composition |
| CN104817407A (en) * | 2014-05-09 | 2015-08-05 | 青岛中达农业科技有限公司 | Paddy field pesticide-fertilizer granule containing silicon and zinc elements and chitosan and preparation method of same |
| CN105211106A (en) * | 2015-10-26 | 2016-01-06 | 广西南宁益土生物科技有限责任公司 | A kind of granule containing trichoderma harzianum and humus |
| CN107593750A (en) * | 2017-09-15 | 2018-01-19 | 河南中威高科技化工有限公司 | Kill sustained-release granular formulation of the anti-root disease of nematode and preparation method thereof |
| CN109287642A (en) * | 2018-11-16 | 2019-02-01 | 山东省花生研究所 | One cultivates peanut antibacterial insect prevention seed coat agent |
Citations (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101541179A (en) * | 2006-11-29 | 2009-09-23 | 三井化学株式会社 | Pest control composition and method of preventing pest damage |
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Patent Citations (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101541179A (en) * | 2006-11-29 | 2009-09-23 | 三井化学株式会社 | Pest control composition and method of preventing pest damage |
Cited By (8)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN104817407A (en) * | 2014-05-09 | 2015-08-05 | 青岛中达农业科技有限公司 | Paddy field pesticide-fertilizer granule containing silicon and zinc elements and chitosan and preparation method of same |
| CN104145965A (en) * | 2014-07-28 | 2014-11-19 | 浙江省化工研究院有限公司 | Insecticidal and fungicidal composition containing hymexazol |
| CN104145965B (en) * | 2014-07-28 | 2016-08-24 | 浙江省化工研究院有限公司 | A kind of insecticidal and bactericidal composition containing mould spirit |
| CN104604921A (en) * | 2014-12-24 | 2015-05-13 | 陈燕婷 | Azole seed treatment agent composition |
| CN105211106A (en) * | 2015-10-26 | 2016-01-06 | 广西南宁益土生物科技有限责任公司 | A kind of granule containing trichoderma harzianum and humus |
| CN105211106B (en) * | 2015-10-26 | 2018-04-24 | 广西南宁益土生物科技有限责任公司 | A kind of granule containing trichoderma harzianum and humic acid |
| CN107593750A (en) * | 2017-09-15 | 2018-01-19 | 河南中威高科技化工有限公司 | Kill sustained-release granular formulation of the anti-root disease of nematode and preparation method thereof |
| CN109287642A (en) * | 2018-11-16 | 2019-02-01 | 山东省花生研究所 | One cultivates peanut antibacterial insect prevention seed coat agent |
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