CN103242955A - Method for preparing orange juice extract for cigarettes - Google Patents
Method for preparing orange juice extract for cigarettes Download PDFInfo
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- CN103242955A CN103242955A CN2013101732360A CN201310173236A CN103242955A CN 103242955 A CN103242955 A CN 103242955A CN 2013101732360 A CN2013101732360 A CN 2013101732360A CN 201310173236 A CN201310173236 A CN 201310173236A CN 103242955 A CN103242955 A CN 103242955A
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- Prior art keywords
- orange juice
- enriched material
- extract
- orange
- cigarette
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Granted
Links
- 235000015205 orange juice Nutrition 0.000 title claims abstract description 161
- 239000000284 extract Substances 0.000 title claims abstract description 61
- 235000019504 cigarettes Nutrition 0.000 title claims abstract description 57
- 238000000034 method Methods 0.000 title abstract description 4
- XEKOWRVHYACXOJ-UHFFFAOYSA-N Ethyl acetate Chemical compound CCOC(C)=O XEKOWRVHYACXOJ-UHFFFAOYSA-N 0.000 claims abstract description 48
- DNIAPMSPPWPWGF-UHFFFAOYSA-N Propylene glycol Chemical compound CC(O)CO DNIAPMSPPWPWGF-UHFFFAOYSA-N 0.000 claims abstract description 45
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 claims abstract description 34
- JVTAAEKCZFNVCJ-UHFFFAOYSA-N lactic acid Chemical compound CC(O)C(O)=O JVTAAEKCZFNVCJ-UHFFFAOYSA-N 0.000 claims abstract description 32
- 239000004310 lactic acid Substances 0.000 claims abstract description 16
- 235000014655 lactic acid Nutrition 0.000 claims abstract description 16
- 238000004062 sedimentation Methods 0.000 claims abstract description 3
- 239000000463 material Substances 0.000 claims description 92
- 239000000706 filtrate Substances 0.000 claims description 26
- 235000011389 fruit/vegetable juice Nutrition 0.000 claims description 22
- 238000002360 preparation method Methods 0.000 claims description 18
- NOPLRNXKHZRXHT-YFVJMOTDSA-N beta-Sinensal Chemical compound O=CC(/C)=C/CCC(/C)=C/CCC(=C)C=C NOPLRNXKHZRXHT-YFVJMOTDSA-N 0.000 claims description 15
- 229930000308 sinensal Natural products 0.000 claims description 15
- 238000003756 stirring Methods 0.000 claims description 13
- 230000000694 effects Effects 0.000 abstract description 5
- 240000002319 Citrus sinensis Species 0.000 abstract description 3
- 235000005976 Citrus sinensis Nutrition 0.000 abstract description 3
- 239000002253 acid Substances 0.000 abstract description 2
- 235000009508 confectionery Nutrition 0.000 abstract description 2
- 239000000796 flavoring agent Substances 0.000 abstract description 2
- 235000019634 flavors Nutrition 0.000 abstract description 2
- 238000002156 mixing Methods 0.000 abstract description 2
- 239000000779 smoke Substances 0.000 abstract description 2
- 239000012141 concentrate Substances 0.000 abstract 6
- 238000001914 filtration Methods 0.000 abstract 2
- 235000016623 Fragaria vesca Nutrition 0.000 abstract 1
- 240000009088 Fragaria x ananassa Species 0.000 abstract 1
- 235000011363 Fragaria x ananassa Nutrition 0.000 abstract 1
- 235000015197 apple juice Nutrition 0.000 abstract 1
- 125000002485 formyl group Chemical class [H]C(*)=O 0.000 abstract 1
- 230000007794 irritation Effects 0.000 abstract 1
- 238000007670 refining Methods 0.000 abstract 1
- 241000208125 Nicotiana Species 0.000 description 13
- 235000002637 Nicotiana tabacum Nutrition 0.000 description 13
- 239000002994 raw material Substances 0.000 description 9
- 238000012360 testing method Methods 0.000 description 6
- 235000013399 edible fruits Nutrition 0.000 description 4
- UGFAIRIUMAVXCW-UHFFFAOYSA-N Carbon monoxide Chemical compound [O+]#[C-] UGFAIRIUMAVXCW-UHFFFAOYSA-N 0.000 description 3
- -1 ange Species 0.000 description 3
- KRKNYBCHXYNGOX-UHFFFAOYSA-N citric acid Chemical compound OC(=O)CC(O)(C(O)=O)CC(O)=O KRKNYBCHXYNGOX-UHFFFAOYSA-N 0.000 description 3
- 239000003546 flue gas Substances 0.000 description 3
- 238000004519 manufacturing process Methods 0.000 description 3
- KBPLFHHGFOOTCA-UHFFFAOYSA-N 1-Octanol Chemical compound CCCCCCCCO KBPLFHHGFOOTCA-UHFFFAOYSA-N 0.000 description 2
- 241000196324 Embryophyta Species 0.000 description 2
- 238000011161 development Methods 0.000 description 2
- 239000012153 distilled water Substances 0.000 description 2
- 238000011156 evaluation Methods 0.000 description 2
- 235000013305 food Nutrition 0.000 description 2
- XMGQYMWWDOXHJM-UHFFFAOYSA-N limonene Chemical compound CC(=C)C1CCC(C)=CC1 XMGQYMWWDOXHJM-UHFFFAOYSA-N 0.000 description 2
- 239000002304 perfume Substances 0.000 description 2
- 230000001953 sensory effect Effects 0.000 description 2
- 239000007921 spray Substances 0.000 description 2
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Chemical compound O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 2
- AKNNEGZIBPJZJG-MSOLQXFVSA-N (-)-noscapine Chemical compound CN1CCC2=CC=3OCOC=3C(OC)=C2[C@@H]1[C@@H]1C2=CC=C(OC)C(OC)=C2C(=O)O1 AKNNEGZIBPJZJG-MSOLQXFVSA-N 0.000 description 1
- 239000001606 7-[(2S,3R,4S,5S,6R)-4,5-dihydroxy-6-(hydroxymethyl)-3-[(2S,3R,4R,5R,6S)-3,4,5-trihydroxy-6-methyloxan-2-yl]oxyoxan-2-yl]oxy-5-hydroxy-2-(4-hydroxyphenyl)chroman-4-one Substances 0.000 description 1
- WTEVQBCEXWBHNA-UHFFFAOYSA-N Citral Natural products CC(C)=CCCC(C)=CC=O WTEVQBCEXWBHNA-UHFFFAOYSA-N 0.000 description 1
- 241000207199 Citrus Species 0.000 description 1
- 244000183685 Citrus aurantium Species 0.000 description 1
- 235000007716 Citrus aurantium Nutrition 0.000 description 1
- QUQPHWDTPGMPEX-UHFFFAOYSA-N Hesperidine Natural products C1=C(O)C(OC)=CC=C1C1OC2=CC(OC3C(C(O)C(O)C(COC4C(C(O)C(O)C(C)O4)O)O3)O)=CC(O)=C2C(=O)C1 QUQPHWDTPGMPEX-UHFFFAOYSA-N 0.000 description 1
- 239000011149 active material Substances 0.000 description 1
- 239000000654 additive Substances 0.000 description 1
- 230000000996 additive effect Effects 0.000 description 1
- 230000002411 adverse Effects 0.000 description 1
- 238000004458 analytical method Methods 0.000 description 1
- 230000036528 appetite Effects 0.000 description 1
- 235000019789 appetite Nutrition 0.000 description 1
- 235000013361 beverage Nutrition 0.000 description 1
- 210000001124 body fluid Anatomy 0.000 description 1
- 239000010839 body fluid Substances 0.000 description 1
- 229940043350 citral Drugs 0.000 description 1
- 239000002537 cosmetic Substances 0.000 description 1
- 238000005516 engineering process Methods 0.000 description 1
- WTEVQBCEXWBHNA-JXMROGBWSA-N geranial Chemical compound CC(C)=CCC\C(C)=C\C=O WTEVQBCEXWBHNA-JXMROGBWSA-N 0.000 description 1
- QUQPHWDTPGMPEX-QJBIFVCTSA-N hesperidin Chemical compound C1=C(O)C(OC)=CC=C1[C@H]1OC2=CC(O[C@H]3[C@@H]([C@@H](O)[C@H](O)[C@@H](CO[C@H]4[C@@H]([C@H](O)[C@@H](O)[C@H](C)O4)O)O3)O)=CC(O)=C2C(=O)C1 QUQPHWDTPGMPEX-QJBIFVCTSA-N 0.000 description 1
- 229940087305 limonene Drugs 0.000 description 1
- 235000001510 limonene Nutrition 0.000 description 1
- 239000000178 monomer Substances 0.000 description 1
- 229930019673 naringin Natural products 0.000 description 1
- DFPMSGMNTNDNHN-ZPHOTFPESA-N naringin Chemical compound O[C@@H]1[C@H](O)[C@@H](O)[C@H](C)O[C@H]1O[C@H]1[C@H](OC=2C=C3O[C@@H](CC(=O)C3=C(O)C=2)C=2C=CC(O)=CC=2)O[C@H](CO)[C@@H](O)[C@@H]1O DFPMSGMNTNDNHN-ZPHOTFPESA-N 0.000 description 1
- 229940052490 naringin Drugs 0.000 description 1
- HXTFHSYLYXVTHC-UHFFFAOYSA-N narirutin Chemical compound OC1C(O)C(O)C(C)OC1OCC1C(O)C(O)C(O)C(OC=2C=C3OC(CC(=O)C3=C(O)C=2)C=2C=CC(O)=CC=2)O1 HXTFHSYLYXVTHC-UHFFFAOYSA-N 0.000 description 1
- HXTFHSYLYXVTHC-ZPHOTFPESA-N narirutin Natural products C[C@@H]1O[C@H](OC[C@H]2O[C@@H](Oc3cc(O)c4C(=O)C[C@H](Oc4c3)c5ccc(O)cc5)[C@H](O)[C@@H](O)[C@@H]2O)[C@H](O)[C@H](O)[C@H]1O HXTFHSYLYXVTHC-ZPHOTFPESA-N 0.000 description 1
- 238000001556 precipitation Methods 0.000 description 1
- 238000012545 processing Methods 0.000 description 1
- 230000001737 promoting effect Effects 0.000 description 1
- 238000010791 quenching Methods 0.000 description 1
- 238000005096 rolling process Methods 0.000 description 1
- 238000007789 sealing Methods 0.000 description 1
- 230000001932 seasonal effect Effects 0.000 description 1
- 210000000697 sensory organ Anatomy 0.000 description 1
- 230000000391 smoking effect Effects 0.000 description 1
- 241000894007 species Species 0.000 description 1
- 239000000126 substance Substances 0.000 description 1
- 238000002560 therapeutic procedure Methods 0.000 description 1
- 230000035922 thirst Effects 0.000 description 1
- 239000000341 volatile oil Substances 0.000 description 1
- 238000005303 weighing Methods 0.000 description 1
Landscapes
- Preparation Of Fruits And Vegetables (AREA)
Abstract
The invention relates to a method for preparing an orange juice extract for cigarettes. The method comprises the following steps of: juicing oranges, filtering the obtained orange juice, and then, concentrating the orange juice until the density of the orange juice is 1.202-1.218 g/cm<3> so as to obtain an orange juice concentrate A; adding ethanol which is 1.5-2.5 times the orange juice concentrate A by weight and has the mass percentage of 85-90% into the orange juice concentrate A, carrying out sedimentation, filtering, and concentrating until the density is 0.944-0.956 g/cm<3> so as to obtain an orange juice concentrate B; and blending the orange juice concentrate B according to the following mass percentage: 40-60% of orange juice concentrate B, 0.1-0.3% of lactic acid, 0.2-0.4% of strawberry acid, 0.1-0.2% of ethyl acetate, 0.2-0.5% of sweet orange aldehyde, 5-10% of apple juice, 2-3% of plum extract and the balance of propylene glycol, thereby obtaining the orange juice extract for cigarettes. The orange juice extract has the effects of reducing irritation, returning sweet, refining smoke and increasing fruity flavor on the cigarettes.
Description
Technical field
The invention belongs to preparation and the applied technical field of tobacco aromatics using, refer to a kind of cigarette orange juice preparation method of extract particularly.
Background technology
Orange is the fruit of Rutaceae citrus plant orange tree, also is called orange, sweet orange, yellow fruit, Jin Huan etc., belongs to aiphyllium, comprises two elementary species of sweet orange and bitter orange, is one of the world four your name fruit, and all there is cultivation each provinces and regions on the south China Yangtze valley.Orange is distinguished the flavor of sweet cool in nature, has promoting the production of body fluid to quench thirst, an effect of the therapeutic method to keep the adverse qi flowing downward of whetting the appetite, and is to have very usury with the plant resources that is worth.Pulp is direct-edible or make orange juice, mainly contains chemical ingredientss such as hesperidine, Naringenin 7-rutinoside, naringin, obacalactone, opianine, citric acid, oxysuccinic acid; The volatile oil that extracts from full pericarp has typical characteristic perfume, and 70 various active materials are arranged, and is mainly n-capric aldehyde, citral, limonene and octanol etc., is widely used in food, tobacco, cosmetic industry.
Be the orange extract of feedstock production with the orange, be mainly used in beverage, medical treatment and field of food, and be that the orange juice extract of feedstock production is not seen application as yet with the orange juice in tobacco industry, and orange belongs to seasonal fruit, can not deposit for a long time, this just uses for the large-scale popularization of orange in cigarette and has brought difficulty, is the novel cigarette additive of development of raw materials development with the orange juice, can effectively improve the aesthetic quality of cigarette, also be conducive to the deeper processing and utilization of this resource.
Summary of the invention
The purpose of this invention is to provide a kind of cigarette orange juice preparation method of extract, add the gained cigarette to be used for improving cigarette in the cigarette organoleptic quality with the orange juice extract.
Technical scheme of the present invention: a kind of cigarette orange juice preparation method of extract may further comprise the steps:
(1) gets that to be concentrated into density after after orange is squeezed the juice the gained orange juice being filtered be 1.202～1.218g/cm
3, obtain orange juice enriched material A.
(2) massfraction that adds 1.5～2.5 times of amounts of its weight in described orange juice enriched material A is that to carry out sedimentation, filter, be concentrated into density behind 85%～90% the ethanol be 0.944～0.956g/cm
3, obtain orange juice enriched material B.
(3) by following mass percent described orange juice enriched material B is allocated: orange juice enriched material B 40～60%, lactic acid 0.1～0.3%, strawberriff 0.2～0.4%, ethyl acetate 0.1～0.2%, sinensal 0.2～0.5%, Sucus Mali pumilae 5～10%, plum extract 2～3%, surplus is propylene glycol, and described orange juice enriched material B namely gets cigarette orange juice extract after allocating.
The present invention is technical scheme more specifically: a kind of cigarette orange juice preparation method of extract may further comprise the steps:
(1) get and will filter under the gained orange juice normal temperature after orange is squeezed the juice, gained filtrate at pressure is-0.08MPa～0.1MPa, and temperature is that to be evaporated to density under 40～50 ℃ of conditions be 1.202～1.218g/cm
3, obtain orange juice enriched material A.
(2) massfraction that adds 1.5～2.5 times of amounts of its weight in described orange juice enriched material A is 85%～90% ethanol, stir and be placed under-10 ℃～5 ℃ environment, natural subsidence 24h～36h, normal temperature filters, gained filtrate at pressure is-0.08MPa～0.1MPa, and temperature is that to be evaporated to density under 30～45 ℃ of conditions be 0.944～0.956g/cm
3, obtain orange juice enriched material B.
(3) by following mass percent described orange juice enriched material B is allocated: orange juice enriched material B 40～60%, lactic acid 0.1～0.3%, strawberriff 0.2～0.4%, ethyl acetate 0.1～0.2%, sinensal 0.2～0.5%, Sucus Mali pumilae 5～10%, plum extract 2～3%, surplus is propylene glycol, and described orange juice enriched material B namely gets cigarette orange juice extract after allocating.
The better technical scheme of the present invention: a kind of cigarette orange juice preparation method of extract may further comprise the steps:
(1) get and will filter under the gained orange juice normal temperature after orange is squeezed the juice, gained filtrate at pressure is-0.08MPa～0.1MPa, and temperature is that to be evaporated to density under 40～50 ℃ of conditions be 1.202～1.218g/cm
3, obtain orange juice enriched material A.
(2) massfraction that adds 2～2.5 times of amounts of its weight in described orange juice enriched material A is 85%～90% ethanol, stir and be placed under-10 ℃～5 ℃ environment, natural subsidence 30h～36h, normal temperature filters, gained filtrate at pressure is-0.08MPa～0.1MPa, and temperature is that to be evaporated to density under 40～45 ℃ of conditions be 0.944～0.950g/cm
3, obtain orange juice enriched material B.
(3) by following mass percent described orange juice enriched material B is allocated: orange juice enriched material B 50～60%, lactic acid 0.1～0.25%, strawberriff 0.25～0.3%, ethyl acetate 0.1～0.15%, sinensal 0.35～0.4%, Sucus Mali pumilae 8～10%, plum extract 2～3%, surplus is propylene glycol, and described orange juice enriched material B namely gets cigarette orange juice extract after allocating.
In the such scheme, Sucus Mali pumilae is to get fresh apple to squeeze the juice and obtain, and all the other raw materials are buied by market.
The gained cigarette is added in the cigarette with the orange juice extract, and the cigarette that adds accounts for 0.6～0.9% of tobacco leaf weight with the weight of orange juice extract.
The present invention is that raw material can not exist safety issue with the orange juice, and lactic acid, strawberriff, ethyl acetate, sinensal, Sucus Mali pumilae and plum extract are the common monomer perfume of tobacco, can coordinate preferably with cigarette.Simultaneously, the present invention is simple and practical, and operation and enforcement are easy, and resulting cigarette can well be coordinated with cigarette with the orange juice extract, improves the aesthetic quality of cigarette, has the effect of falling thorn, Hui Tian, fine and smooth flue gas and increase fruital note in cigarette.
Embodiment:
The present invention is described in further detail below in conjunction with specific embodiment.
Embodiment 1:
A kind of cigarette orange juice preparation method of extract may further comprise the steps:
(1) get and will filter under the gained orange juice normal temperature after orange is squeezed the juice, gained filtrate at pressure is-0.08MPa, and temperature is that to be evaporated to density under 45 ℃ of conditions be 1.202g/cm
3, obtain orange juice enriched material A.
(2) massfraction of 2.5 times of amounts of its weight of adding is 85% ethanol in described orange juice enriched material A, stirring is placed under 5 ℃ of environment, natural subsidence 36h, and normal temperature filters, gained filtrate at pressure is-0.08MPa, and temperature is that to be evaporated to density under 40 ℃ of conditions be 0.944g/cm
3, obtain orange juice enriched material B.
(3) by following mass percent described orange juice enriched material B is allocated: orange juice enriched material B50%, lactic acid 0.1%, strawberriff 0.3%, ethyl acetate 0.15%, sinensal 0.35%, Sucus Mali pumilae 10%, plum extract 2%, propylene glycol 37.1% namely gets cigarette orange juice extract after described orange juice enriched material B allocates.Wherein, Sucus Mali pumilae is to get fresh apple to squeeze the juice and obtain, and all the other raw materials are buied by market.
Embodiment 2:
A kind of cigarette orange juice preparation method of extract may further comprise the steps:
(1) get and will filter under the gained orange juice normal temperature after orange is squeezed the juice, gained filtrate is 0.01MPa at pressure, and temperature is that to be evaporated to density under 40 ℃ of conditions be 1.210g/cm
3, obtain orange juice enriched material A.
(2) massfraction of 2 times of amounts of its weight of adding is 90% ethanol in described orange juice enriched material A, stirring is placed under-10 ℃ of environment, natural subsidence 30h, and normal temperature filters, gained filtrate is 0.01MPa at pressure, and temperature is that to be evaporated to density under 45 ℃ of conditions be 0.950g/cm
3, obtain orange juice enriched material B.
(3) by following mass percent described orange juice enriched material B is allocated: orange juice enriched material B60%, lactic acid 0.25%, strawberriff 0.25%, ethyl acetate 0.1%, sinensal 0.4%, Sucus Mali pumilae 8%, plum extract 3%, propylene glycol 28% namely gets cigarette orange juice extract after described orange juice enriched material B allocates.Wherein, Sucus Mali pumilae is to get fresh apple to squeeze the juice and obtain, and all the other raw materials are buied by market.
Embodiment 3:
A kind of cigarette orange juice preparation method of extract may further comprise the steps:
(1) get and will filter under the gained orange juice normal temperature after orange is squeezed the juice, gained filtrate is 0.1MPa at pressure, and temperature is that to be evaporated to density under 50 ℃ of conditions be 1.218g/cm
3, obtain orange juice enriched material A.
(2) massfraction that adds 1.5 times of amounts of its weight in described orange juice enriched material A is 87% ethanol, stirring is placed under 5 ℃ of environment, natural subsidence 24h, and normal temperature filters, gained filtrate is 0.1MPa at pressure, and temperature is that to be evaporated to density under 30 ℃ of conditions be 0.956g/cm
3, obtain orange juice enriched material B.
(3) by following mass percent described orange juice enriched material B is allocated: orange juice enriched material B 60%, lactic acid 0.1%, strawberriff 0.2%, ethyl acetate 0.2%, sinensal 0.5%, Sucus Mali pumilae 5%, plum extract 2%, propylene glycol 32%.After allocating, described orange juice enriched material B namely gets cigarette orange juice extract.Wherein, Sucus Mali pumilae is to get fresh apple to squeeze the juice and obtain, and all the other raw materials are buied by market.
Embodiment 4:
A kind of cigarette orange juice preparation method of extract may further comprise the steps:
(1) get and will filter under the gained orange juice normal temperature after orange is squeezed the juice, gained filtrate is 0.1MPa at pressure, and temperature is that to be evaporated to density under 45 ℃ of conditions be 1.210g/cm
3, obtain orange juice enriched material A.
(2) massfraction that adds 2.5 times of amounts of its weight in described orange juice enriched material A is 90% ethanol, stirring is placed under 0 ℃ of environment, natural subsidence 36h, and normal temperature filters, gained filtrate is 0.1MPa at pressure, and temperature is that to be evaporated to density under 35 ℃ of conditions be 0.950g/cm
3, obtain orange juice enriched material B.
(3) by following mass percent described orange juice enriched material B is allocated: orange juice enriched material B 40%, lactic acid 0.2%, strawberriff 0.4%, ethyl acetate 0.2%, sinensal 0.2%, Sucus Mali pumilae 7.5%, plum extract 3%, propylene glycol 48.5%.After allocating, described orange juice enriched material B namely gets cigarette orange juice extract.Wherein, Sucus Mali pumilae is to get fresh apple to squeeze the juice and obtain, and all the other raw materials are buied by market.
Embodiment 5:
A kind of cigarette orange juice preparation method of extract may further comprise the steps:
(1) get and will filter under the gained orange juice normal temperature after orange is squeezed the juice, gained filtrate at pressure is-0.08MPa, and temperature is that to be evaporated to density under 40 ℃ of conditions be 1.218g/cm
3, obtain orange juice enriched material A.
(2) massfraction that adds 2.5 times of amounts of its weight in described orange juice enriched material A is 90% ethanol, stir and be placed under-10 ℃ of environment, natural subsidence 24h, normal temperature filters, gained filtrate at pressure is-0.08MPa, and temperature is that to be evaporated to density under 45 ℃ of conditions be 0.956g/cm
3, obtain orange juice enriched material B.
(3) by following mass percent described orange juice enriched material B is allocated: orange juice enriched material B 60%, lactic acid 0.1%, strawberriff 0.2%, ethyl acetate 0.2%, sinensal 0.5%, Sucus Mali pumilae 5%, plum extract 2%, propylene glycol 32%.After allocating, described orange juice enriched material B namely gets cigarette orange juice extract.Wherein, Sucus Mali pumilae is to get fresh apple to squeeze the juice and obtain, and all the other raw materials are buied by market.
Embodiment 6:
A kind of cigarette orange juice preparation method of extract may further comprise the steps:
(1) get and will filter under the gained orange juice normal temperature after orange is squeezed the juice, gained filtrate is 0.01MPa at pressure, and temperature is that to be evaporated to density under 45 ℃ of conditions be 1.210g/cm
3, obtain orange juice enriched material A.
(2) massfraction that adds 2 times of amounts of its weight in described orange juice enriched material A is 86% ethanol, stirring is placed under 5 ℃ of environment, natural subsidence 30h, and normal temperature filters, gained filtrate at pressure is-0.08MPa, and temperature is that to be evaporated to density under 30 ℃ of conditions be 0.950g/cm
3, obtain orange juice enriched material B.
(3) by following mass percent described orange juice enriched material B is allocated: orange juice enriched material B50%, lactic acid 0.3%, strawberriff 0.3%, ethyl acetate 0.1%, sinensal 0.35%, Sucus Mali pumilae 10%, plum extract 2.5%.Propylene glycol 36.45%.After allocating, described orange juice enriched material B namely gets cigarette orange juice extract.Wherein, Sucus Mali pumilae is to get fresh apple to squeeze the juice and obtain, and all the other raw materials are buied by market.
Take by weighing 0.4g cigarette orange juice extract, add distilled water to 2.6g, behind the mixing, spray equably with micro sprayer and to be added on the blank pipe tobacco of 50g, feeding quantity is 0.8%.Pipe tobacco is packed in the sealing bag, place 60 ℃ of constant temperature 30min in the baking oven, shake pipe tobacco then rapidly, moisture in cut tobacco should be about 12.5%, rolling into cigarette props up, the climatic chamber inner equilibrium 48h that put into temperature and be 22 ℃ ± 1, relative humidity is 60 % ± 2 % is above as sample 1 of the present invention, please the group of smokeing panel test smoke panel test.Under similarity condition, add identical deal distilled water with same pipe tobacco spray, roll into the sample 2 of cigarette Zhi Zuowei blank.Smoking result is asked for an interview following table 1.
The contrast of smokeing panel test of table 1 sample 1 and sample 2
Table 1 result shows that gained cigarette of the present invention adds in the cigarette with the orange juice extract makes the effect of falling thorn, Hui Tian, fine and smooth flue gas and increase fruital note.
It is as follows below the orange juice extract of different methods preparation to be carried out sensory evaluation:
Get and will filter under the gained orange juice normal temperature after orange is squeezed the juice, gained filtrate at pressure is-0.08MPa～0.1MPa, and temperature is that to be evaporated to density under 40～50 ℃ of conditions be 1.210 ± 0.008g/cm
3, obtain orange juice enriched material A.The massfraction that adds 2 times of amounts of its weight in described orange juice enriched material A is 95% ethanol, stir and be placed under-10 ℃～5 ℃ environment, natural subsidence 24h～36h, normal temperature filters, gained filtrate at pressure is-0.08MPa～0.1MPa, and temperature is that to be evaporated to density under 30～45 ℃ of conditions be 0.950 ± 0.006g/cm
3, obtain orange juice enriched material B.Described orange juice enriched material joins in the tobacco leaf by 0.6%, makes cigarette Zhi Zuowei sample a and smokes panel test.
Get and will filter under the gained orange juice normal temperature after orange is squeezed the juice, gained filtrate at pressure is-0.08MPa～0.1MPa, and temperature is that to be evaporated to density under 40～50 ℃ of conditions be 1.210 ± 0.008g/cm
3, obtain orange juice enriched material A.The massfraction that adds 2 times of amounts of its weight in described orange juice enriched material A is 95% ethanol, stir and be placed under-10 ℃～5 ℃ environment, natural subsidence 24h～36h, normal temperature filters, gained filtrate at pressure is-0.08MPa～0.1MPa, and temperature is that to be evaporated to density under 30～45 ℃ of conditions be 0.950 ± 0.006g/cm
3, obtain orange juice enriched material B.Described orange juice enriched material B is carried out suitable allotment modify, allocate by following mass percent: orange juice enriched material B60%; Lactic acid 0.20%; Strawberriff 0.20%, ethyl acetate 0.15%; Sinensal 0.35%; Sucus Mali pumilae 6%; Plum extract 2.5%; Propylene glycol 30.6%, the enriched material B after the allotment is cigarette orange juice extract.Described orange juice enriched material joins in the tobacco leaf by 0.6%, makes cigarette Zhi Zuowei sample b and smokes panel test.
Get and will filter under the gained orange juice normal temperature after orange is squeezed the juice, gained filtrate at pressure is-0.08MPa～0.1MPa, and temperature is that to be evaporated to density under 40～50 ℃ of conditions be 1.210 ± 0.008g/cm
3, obtain orange juice enriched material A.The massfraction that adds 2 times of amounts of its weight in described orange juice enriched material A is 90% ethanol, stir and be placed under-10 ℃～5 ℃ environment, natural subsidence 24h～36h, normal temperature filters, gained filtrate at pressure is-0.08MPa～0.1MPa, and temperature is that to be evaporated to density under 30～45 ℃ of conditions be 0.950 ± 0.006g/cm
3, obtain orange juice enriched material B.Described orange juice enriched material B is carried out suitable allotment modify, allocate by following mass percent: orange juice enriched material B60%; Lactic acid 0.20%; Strawberriff 0.20%, ethyl acetate 0.15%; Sinensal 0.35%; Sucus Mali pumilae 6%; Plum extract 2.5%; Propylene glycol 30.6%, the enriched material B after the allotment is cigarette orange juice extract.Described orange juice enriched material joins in the tobacco leaf by 0.6%, makes cigarette Zhi Zuowei sample c and smokes panel test.
The sense organ evaluating meter of table 2 orange juice extract
By the sensory evaluation of table 2 as can be known, the ethanol concn of precipitation orange juice enriched material A and organoleptic quality that the allotment that orange juice enriched material B carries out is modified cigarette have a significant impact.Comprehensive above the analysis as can be known, the orange juice extract that adopts the present invention's preparation can improve the cigarette aesthetic quality significantly in that to fall aspect effects such as thorn, Hui Tian, fine and smooth flue gas more obvious.
Claims (3)
1. cigarette orange juice preparation method of extract may further comprise the steps:
(1) gets that to be concentrated into density after after orange is squeezed the juice the gained orange juice being filtered be 1.202～1.218g/cm
3, obtain orange juice enriched material A;
(2) massfraction that adds 1.5～2.5 times of amounts of its weight in described orange juice enriched material A is that to carry out sedimentation, filter, be concentrated into density behind 85%～90% the ethanol be 0.944～0.956g/cm
3, obtain orange juice enriched material B;
(3) by following mass percent described orange juice enriched material B is allocated: orange juice enriched material B 40～60%, lactic acid 0.1～0.3%, strawberriff 0.2～0.4%, ethyl acetate 0.1～0.2%, sinensal 0.2～0.5%, Sucus Mali pumilae 5～10%, plum extract 2～3%, surplus is propylene glycol, and described orange juice enriched material B namely gets cigarette orange juice extract after allocating.
2. a kind of cigarette orange juice preparation method of extract according to claim 1, it is characterized in that: it may further comprise the steps:
(1) get and will filter under the gained orange juice normal temperature after orange is squeezed the juice, gained filtrate at pressure is-0.08MPa～0.1MPa, and temperature is that to be evaporated to density under 40～50 ℃ of conditions be 1.202～1.218g/cm
3, obtain orange juice enriched material A;
(2) massfraction that adds 1.5～2.5 times of amounts of its weight in described orange juice enriched material A is 85%～90% ethanol, stir and be placed under-10 ℃～5 ℃ environment, natural subsidence 24h～36h, normal temperature filters, gained filtrate at pressure is-0.08MPa～0.1MPa, and temperature is that to be evaporated to density under 30～45 ℃ of conditions be 0.944～0.956g/cm
3, obtain orange juice enriched material B;
(3) by following mass percent described orange juice enriched material B is allocated: orange juice enriched material B 40～60%, lactic acid 0.1～0.3%, strawberriff 0.2～0.4%, ethyl acetate 0.1～0.2%, sinensal 0.2～0.5%, Sucus Mali pumilae 5～10%, plum extract 2～3%, surplus is propylene glycol, and described orange juice enriched material B namely gets cigarette orange juice extract after allocating.
3. a kind of cigarette orange juice preparation method of extract according to claim 1 and 2, it is characterized in that: it may further comprise the steps:
(1) get and will filter under the gained orange juice normal temperature after orange is squeezed the juice, gained filtrate at pressure is-0.08MPa～0.1MPa, and temperature is that to be evaporated to density under 40～50 ℃ of conditions be 1.202～1.218g/cm
3, obtain orange juice enriched material A;
(2) massfraction that adds 2～2.5 times of amounts of its weight in described orange juice enriched material A is 85%～90% ethanol, stir and be placed under-10 ℃～5 ℃ environment, natural subsidence 30h～36h, normal temperature filters, gained filtrate at pressure is-0.08MPa～0.1MPa, and temperature is that to be evaporated to density under 40～45 ℃ of conditions be 0.944～0.950g/cm
3, obtain orange juice enriched material B;
(3) by following mass percent described orange juice enriched material B is allocated: orange juice enriched material B 50～60%, lactic acid 0.1～0.25%, strawberriff 0.25～0.3%, ethyl acetate 0.1～0.15%, sinensal 0.35～0.4%, Sucus Mali pumilae 8～10%, plum extract 2～3%, surplus is propylene glycol, and described orange juice enriched material B namely gets cigarette orange juice extract after allocating.
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Cited By (4)
| Publication number | Priority date | Publication date | Assignee | Title |
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| CN104130864A (en) * | 2014-07-16 | 2014-11-05 | 湖北中烟工业有限责任公司 | Preparation method of sweet orange flavor for cigarettes |
| CN107674762A (en) * | 2017-05-24 | 2018-02-09 | 湖北中烟工业有限责任公司 | A kind of preparation method of cigarette Red wine extract and its application in cigarette |
| CN111184256A (en) * | 2020-03-20 | 2020-05-22 | 云南中烟工业有限责任公司 | Sugar candy orange essence bead for cigarettes and preparation method thereof |
| CN115644490A (en) * | 2022-11-07 | 2023-01-31 | 广西中烟工业有限责任公司 | Sugarcane concentrated juice and application thereof in tobacco and novel tobacco products |
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| CN101608144A (en) * | 2008-06-16 | 2009-12-23 | 湖北中烟工业有限责任公司 | A kind of preparation method of strawberry tobacco aromatics using |
| CN102687901A (en) * | 2011-03-22 | 2012-09-26 | 湖北中烟工业有限责任公司 | A faint scent-type special cigarette flavor and application thereof in cigarettes |
| CN102697167A (en) * | 2012-06-25 | 2012-10-03 | 湖北中烟工业有限责任公司 | Preparation method for cabo extractive with assistance of steam explosion |
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Patent Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
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| CN101608144A (en) * | 2008-06-16 | 2009-12-23 | 湖北中烟工业有限责任公司 | A kind of preparation method of strawberry tobacco aromatics using |
| CN102687901A (en) * | 2011-03-22 | 2012-09-26 | 湖北中烟工业有限责任公司 | A faint scent-type special cigarette flavor and application thereof in cigarettes |
| CN102697167A (en) * | 2012-06-25 | 2012-10-03 | 湖北中烟工业有限责任公司 | Preparation method for cabo extractive with assistance of steam explosion |
Cited By (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN104130864A (en) * | 2014-07-16 | 2014-11-05 | 湖北中烟工业有限责任公司 | Preparation method of sweet orange flavor for cigarettes |
| CN107674762A (en) * | 2017-05-24 | 2018-02-09 | 湖北中烟工业有限责任公司 | A kind of preparation method of cigarette Red wine extract and its application in cigarette |
| CN111184256A (en) * | 2020-03-20 | 2020-05-22 | 云南中烟工业有限责任公司 | Sugar candy orange essence bead for cigarettes and preparation method thereof |
| CN115644490A (en) * | 2022-11-07 | 2023-01-31 | 广西中烟工业有限责任公司 | Sugarcane concentrated juice and application thereof in tobacco and novel tobacco products |
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