CN102125299A - Additive for cigarettes as well as preparation and application thereof - Google Patents
Additive for cigarettes as well as preparation and application thereof Download PDFInfo
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- CN102125299A CN102125299A CN2010106194996A CN201010619499A CN102125299A CN 102125299 A CN102125299 A CN 102125299A CN 2010106194996 A CN2010106194996 A CN 2010106194996A CN 201010619499 A CN201010619499 A CN 201010619499A CN 102125299 A CN102125299 A CN 102125299A
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- eucommia
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Abstract
The invention relates to an additive for cigarettes as well as preparation and application thereof. The additive for cigarettes, provided by the invention, is an effective component extract of a Chinese medicinal material called eucommia. The invention also provides the preparation of the additive for cigarettes and the application of the additive for cigarettes to cigarette preparation. By means of the additive for cigarettes, provided by the invention, the aroma of the cigarettes is markedly enhanced and the cigarette tar and the content of the harmful components are reduced.
Description
Technical field
The present invention relates to the Chinese medicine bark of eucommia is a kind of cigarette additive and preparation and application that promotes cigarette fragrance, reduces coke tar in cigarette and harmful components content of raw material invention.
Background technology
Assorted gas in the cigarette, astringent taste, bitter taste and flue gas are to human oral cavity, the excitements of throat etc. all have very big relation with the sucking quality of cigarette, how to reduce or cover assorted gas in the flue gas, astringent taste and bitter taste etc., reduce excitement, the characteristic perfume that the increase cigarette is difficult to copy has been the difficult problem that the tobacco scientific worker faces, simultaneously, how to reduce the content of tar and harmful components in the cigarette, reduce and suck the harm of cigarette smoker's health, be again the difficult problem of one pendulum in face of the tobacco scientific worker, present many correlative study work are all launching around these two difficult problems.
Chinese medicine also can be used for producing health care of food product, coloring agent, food additives, bio-fuel or the like except that can be used for treating disease.Select suitable Chinese medicine extract to can be used for tobacco flavouring, removal of impurities, lowering harm and decreasing coking, promotion tobacco leaf biofermentation etc. as additive, this is the emerging hot research in tobacco field.Advantage and the characteristic of giving full play to Chinese medicine improved the cigarette quality, reduced the harm of cigarette harmful components, promotes the tobacco leaf biofermentation, will play huge impetus to the development of tobacco industry.
The Guizhou authentic medicinal herbs bark of eucommia is the dry bark of the Eucommiaceae plant bark of eucommia (Eucommia ulmoides Oliver), is Chinese famous and precious tonic herb, tool filling liver kidney, strengthening the bones and muscles, many effects such as hypotensive, antiabortive.Shennong's Herbal is classified as top grade, and the bark of eucommia has filling liver kidney, strengthening the bones and muscles, remove rubbish in the body, strengthen the human body cell metabolism, prevent that muscle skeleton is aging, the balance human blood-pressure, the decomposer inner cholesterol reduces body fat, recover blood vessel elasticity, the diuresis heat-clearing, broad-spectrum antiseptic, stimulating central nervous system, improve white blood cell count, strengthen remarkable efficacy such as body immunity.This patent is a raw material with the bark of eucommia, finds that it has the effect that promotes cigarette fragrance, reduces harmful components content in coke tar in cigarette and the cigarette mainstream flue gas.
Summary of the invention
The objective of the invention is to overcome defective of the prior art, a kind of cigarette additive and application thereof that promotes cigarette fragrance, reduces harmful components content in coke tar in cigarette and the cigarette mainstream flue gas is provided.
The present invention at first provides a kind of cigarette additive that promotes cigarette fragrance, reduces harmful components content in coke tar in cigarette and the cigarette mainstream flue gas, is the effective component extracts of the Chinese medicine bark of eucommia.
The described Chinese medicine bark of eucommia is the dry bark of the Eucommiaceae plant bark of eucommia (Eucommia ulmoides Oliver).
Cigarette additive of the present invention can adopt following method to obtain:
With the Chinese medicine bark of eucommia is raw material, adopts organic solvent or water-containing organic solvent to extract repeatedly, filters and merging filtrate, and filtrate obtains additive after concentrating.
Described organic solvent is selected from absolute ethyl alcohol, acetoneand ethyl acetate; Described water-containing organic solvent is that percent by volume is 30～95% ethanol water; Extracting method be 40～75 ℃ add that hot reflux, temperature are soaked, cold soaking, Microwave Extraction or ultrasonic extraction.
Preferably, adopt the following step to prepare described additive:
1) be raw material with the Chinese medicine bark of eucommia, broken back is that 30～95% ethanol water is as the extraction solvent with absolute ethyl alcohol, acetone, ethyl acetate or the volume ratio of 2～5 times of amounts of crude drug weight, with 40～75 ℃ add that hot reflux, temperature are soaked, cold soaking, Microwave Extraction or the ultrasonic extracting method that is extracted as, extract and filter (extraction time was conventional, as 0.5～148 hour); Repeat to extract merging filtrate 2～4 times;
2) at 40-70 ℃ of reduce pressure down concentrated make medicinal extract shape or solution.Generally be concentrated into 1～20 times of crude drug weight.
The natural additive that cigarette additive of the present invention can be used as and promote cigarette fragrance, reduced harmful components content in coke tar in cigarette and/or the reduction cigarette mainstream flue gas is used to prepare cigarette, pipe tobacco, stem or reconstituted tobacoo.
Harmful components in the described cigarette mainstream flue gas include but not limited to that aldehydes matter such as phenol, benzo [a] pyrene and carbonyls class material such as crotonaldehyde etc. are harmful to the material of health.
Further, when preparation pipe tobacco, stem or reconstituted tobacoo, the addition of described cigarette additive in pipe tobacco, stem or reconstituted tobacoo is the 0.05-3.0% of pipe tobacco, stem or reconstituted tobacoo weight, when the preparation cigarette, the addition of described cigarette additive in cigarette is the 0.05-3.0% of pipe tobacco in the cigarette, stem and reconstituted tobacoo gross weight, or is the 0.15-8.0% of the filter stick weight of cigarette.Can only contain pipe tobacco in the described cigarette and not contain stem and reconstituted tobacoo, also can promptly contain pipe tobacco and also contain in stem and the reconstituted tobacoo one or both.
The present invention also provides a kind of and promoted cigarette fragrance, reduce coke tar in cigarette and/or reduce the method for harmful components content in the cigarette mainstream flue gas: for on additive stoste of the present invention or the after-applied pipe tobacco in cigarettes plus of stoste dilution, stem, reconstituted tobacoo and/or the filter stick, and balance was not less than 48 hours under the condition of constant temperature and humidity.Applying method can be to spray before rolling or roll the back to inject.For example before rolling, roll into cigarette on cigarette shreds, stem and/or the reconstituted tobacoo again and prop up evenly being sprayed at after the stoste of additive of the present invention or the stoste dilution, perhaps test also can be by being injected into cigarette with cigarette pipe tobacco and/or the mode in the filter stick additive is added cigarette.
Further, the additive dilution is organic solvent or water-containing organic solvent with solvent, is 30～95% ethanol water as ethanol, acetone, ethyl acetate or volume ratio.The balance temperature is 22 ± 1 ℃, and balance humidity is relative humidity 60 ± 2%.
The present invention also provides a kind of cigarette, for cigarette is obtained after cigarette additive of the present invention is handled.
Beneficial effect of the present invention:
The present invention will have the natural plants bark of eucommia of special effect, extract wherein active ingredient through multiple mode, add in sample pipe tobacco or the filter stick, can reduce harmful substance in the cigarette mainstream flue gas, alleviate harm of smoking,, can promote the fragrance of cigarette again especially to the tangible reduction effect that has of aldehydes matters such as phenol in the cigarette mainstream flue gas, the assorted gas and the flue gas that significantly reduce in the flue gas stimulate oral cavity, throat, make cigarette smoke exquisiteness, soft.Cigarette of the present invention is based on local resource with natural additive, and preparation technology is simple, cost is low, has important market prospects.
The specific embodiment
Below enumerate specific embodiment with further elaboration the present invention, should understand example is not to be used to limit protection scope of the present invention.
Embodiment 1
(1) preparation natural tobacco additive extract: get the bark of eucommia 50 grams, be crushed to a certain size, after alcohol immersion 10-15 minute of usefulness 200ml 95%, ultrasonic extraction is 30-60 minute under the room temperature, uses the qualitative filter paper suction filtration, collects filtrate.Repeat to extract twice again, merging filtrate.
(2) preparation natural tobacco additive: bark of eucommia extract rotary evaporation under 40-70 ℃ of water bath condition that step 1 is obtained is evaporated to 30ml, obtains natural tobacco additive solution.
Above prepared natural tobacco additive solution is injected the sample cigarette, injects the 20ul amount in the pipe tobacco of every sample cigarette and the filter stick respectively, and under constant temperature (22 ± 1 ℃) constant humidity (relative humidity 60 ± 2%) condition balance 48 hours.
The result of the test that additive reduces harmful substances such as phenols in the main flume see the following form (wherein, aldehydes matter is representative with phenol):
Experimental result shows: this cigarette can reduce harmful substance in the cigarette mainstream flue gas, alleviates harm of smoking, and especially the reduction effect to aldehydes matters such as phenol in the cigarette mainstream flue gas is the most obvious.
Sensory evaluating smoking result shows: this cigarette has can promote cigarette fragrance, and the assorted gas and the flue gas that can significantly reduce again in the flue gas stimulate oral cavity, throat, make cigarette smoke exquisiteness, soft.
Embodiment 2
(1) preparation natural tobacco additive extract: get the bark of eucommia 50 grams, be crushed to a certain size, use the ethyl acetate of 200ml to soak after 10-15 minute, ultrasonic extraction is 45-75 minute under the room temperature, uses the qualitative filter paper suction filtration, collects filtrate.Repeat to extract twice again, merging filtrate.
(2) preparation natural tobacco additive: bark of eucommia extract rotary evaporation under 40-70 ℃ of water bath condition is evaporated to 30ml, obtains natural tobacco additive solution.
Prepared natural tobacco additive solution is injected the sample cigarette, inject the 20ul amount in the pipe tobacco of every sample cigarette and the filter stick respectively, and balance was not less than 48 hours under constant temperature (22 ± 1 ℃) constant humidity (relative humidity 60 ± 2%) condition.Effect is with embodiment 1.
Embodiment 3
(1) preparation natural tobacco additive extract: get the bark of eucommia 50 grams, be crushed to a certain size, add the absolute ethyl alcohol of 300ml, in 40～75 ℃ of water-baths heating and refluxing extraction 4-6 hour, use the qualitative filter paper suction filtration, collection filtrate.Repeat to extract twice again, merging filtrate.
(2) preparation natural tobacco additive: bark of eucommia extract rotary evaporation under 40-70 ℃ of water bath condition is evaporated to 30ml, obtains natural tobacco additive solution.
With the ratio of prepared natural tobacco additive solution in pipe tobacco weight 2%, the process of perfuming evenly is sprayed on the sample cigarette shreds routinely, sealing was preserved 24 hours, make cigarette, and cigarette balance under constant temperature (22 ± 1 ℃) constant humidity (relative humidity 60 ± 2%) condition was not less than 48 hours.Effect is with embodiment 1.
Claims (13)
1. a cigarette additive is the effective component extracts of the Chinese medicine bark of eucommia.
2. cigarette additive according to claim 1 is characterized in that the described Chinese medicine bark of eucommia is the dry bark of the Eucommiaceae plant bark of eucommia.
3. the preparation method of cigarette additive as claimed in claim 1 or 2 comprises the following steps: that with the Chinese medicine bark of eucommia be raw material, adopts organic solvent or water-containing organic solvent to extract repeatedly, filters and merging filtrate, and filtrate obtains additive after concentrating.
4. as the preparation method of cigarette additive as described in the claim 3, it is characterized in that described organic solvent is selected from ethanol, acetoneand ethyl acetate; Described water-containing organic solvent is that volume ratio is 30～95% ethanol water; The method of described extraction be 40～75 ℃ add that hot reflux, temperature are soaked, cold soaking, Microwave Extraction or ultrasonic extraction.
5. as the preparation method of cigarette additive as described in the claim 3, it is characterized in that, specifically adopt the following step to prepare described additive:
1) be raw material with the Chinese medicine bark of eucommia, broken back is that 30～95% ethanol water is as the extraction solvent with absolute ethyl alcohol, acetone, ethyl acetate or the volume ratio of 2～5 times of amounts of crude drug weight, with 40～75 ℃ add that hot reflux, temperature are soaked, cold soaking, Microwave Extraction or the ultrasonic extracting method that is extracted as, extract also and filter; Repeat to extract merging filtrate 2～4 times;
2) at 40-70 ℃ of reduce pressure down concentrated make medicinal extract shape or solution.
6. cigarette additive is used to prepare the purposes of cigarette, pipe tobacco, stem or reconstituted tobacoo as the natural additive that promotes cigarette fragrance, reduces coke tar in cigarette and/or reduce harmful components content in the cigarette mainstream flue gas as claimed in claim 1 or 2.
7. as the purposes of cigarette additive as described in the claim 6, it is characterized in that, when preparation pipe tobacco, stem or reconstituted tobacoo, the addition of described cigarette additive in pipe tobacco, stem or reconstituted tobacoo is the 0.05-3.0% of pipe tobacco, stem or reconstituted tobacoo weight, when the preparation cigarette, the addition of described cigarette additive in cigarette is the 0.05-3.0% of pipe tobacco in the cigarette, stem and reconstituted tobacoo gross weight, or is the 0.15-8.0% of the filter stick weight of cigarette.
8. one kind promotes cigarette fragrance, reduces coke tar in cigarette and/or reduces the method for harmful components content in the cigarette mainstream flue gas, for with on claim 1 or 2 described cigarette additive stostes or the after-applied pipe tobacco in cigarettes plus of stoste dilution, stem, reconstituted tobacoo and/or the filter stick, and balance was not less than 48 hours under the condition of constant temperature and humidity.
9. method as claimed in claim 8 is characterized in that, the addition of described cigarette additive in cigarette is the 0.05-3.0% of pipe tobacco in the cigarette, stem and reconstituted tobacoo gross weight, or is the 0.15-8.0% of the filter stick weight of cigarette.
10. method as claimed in claim 8 is characterized in that, the method that applies cigarette additive is injected for spraying before rolling or rolling the back.
11. method as claimed in claim 8 is characterized in that, the dilution of additive stoste is that absolute ethyl alcohol, ethyl acetate, acetone or volume ratio are the ethanol water of 30-95% with solvent.
12., it is characterized in that described balance temperature is 21-23 ℃ as the described method of the arbitrary claim of claim 8-11, balance humidity is relative humidity 58-62%.
13. a cigarette is for obtaining cigarette after the described method of the arbitrary claim of claim 8-12 is handled.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN 201010619499 CN102125299B (en) | 2010-12-31 | 2010-12-31 | Additive for cigarettes and application thereof |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN 201010619499 CN102125299B (en) | 2010-12-31 | 2010-12-31 | Additive for cigarettes and application thereof |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| CN102125299A true CN102125299A (en) | 2011-07-20 |
| CN102125299B CN102125299B (en) | 2013-10-16 |
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| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN 201010619499 Active CN102125299B (en) | 2010-12-31 | 2010-12-31 | Additive for cigarettes and application thereof |
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| CN (1) | CN102125299B (en) |
Cited By (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN107361398A (en) * | 2017-06-26 | 2017-11-21 | 河南中烟工业有限责任公司 | A kind of tea extraction in May and preparation method thereof and the application in cigarette |
| CN109619642A (en) * | 2018-11-14 | 2019-04-16 | 河南中烟工业有限责任公司 | A kind of fragrance-enhancing tobacco tobacco extract and preparation method thereof |
| CN110237292A (en) * | 2019-07-31 | 2019-09-17 | 国家能源大规模物理储能技术（毕节）研发中心 | A kind of preparation method of Chinese medicine slag charcoal base no-smoke incense |
| CN115067541A (en) * | 2022-01-11 | 2022-09-20 | 常德集智生物科技有限公司 | Cigarette additive and preparation method and application thereof |
Citations (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1356153A (en) * | 2000-12-06 | 2002-07-03 | 陕西安康志朗生物资源应用研究所 | Process for preparing eucommia bark gelatin and extract powder of eucommia leaf |
-
2010
- 2010-12-31 CN CN 201010619499 patent/CN102125299B/en active Active
Patent Citations (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1356153A (en) * | 2000-12-06 | 2002-07-03 | 陕西安康志朗生物资源应用研究所 | Process for preparing eucommia bark gelatin and extract powder of eucommia leaf |
Non-Patent Citations (1)
| Title |
|---|
| 杨玉琼等: "丙酮－乙醇－水三组分体系提取杜仲叶中总黄酮", 《微量元素与健康研究》 * |
Cited By (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN107361398A (en) * | 2017-06-26 | 2017-11-21 | 河南中烟工业有限责任公司 | A kind of tea extraction in May and preparation method thereof and the application in cigarette |
| CN109619642A (en) * | 2018-11-14 | 2019-04-16 | 河南中烟工业有限责任公司 | A kind of fragrance-enhancing tobacco tobacco extract and preparation method thereof |
| CN110237292A (en) * | 2019-07-31 | 2019-09-17 | 国家能源大规模物理储能技术（毕节）研发中心 | A kind of preparation method of Chinese medicine slag charcoal base no-smoke incense |
| CN115067541A (en) * | 2022-01-11 | 2022-09-20 | 常德集智生物科技有限公司 | Cigarette additive and preparation method and application thereof |
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| Publication number | Publication date |
|---|---|
| CN102125299B (en) | 2013-10-16 |
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