CN103214313B - Composition for removing residual phytotoxicity of herbicide, and preparation method thereof - Google Patents
Composition for removing residual phytotoxicity of herbicide, and preparation method thereof Download PDFInfo
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Abstract
The invention relates to a composition for removing residual phytotoxicity of herbicide, and a preparation method thereof; the composition comprises the components in parts by weight: 30-60 parts of soybean extract liquid, 5-20 parts of liquorice extract liquid and 8-20 parts of barley malt extract liquid. The composition for removing the residual phytotoxicity of the herbicide can rapidly remove the drifting phytotoxicity of the herbicide and the phytotoxicity caused by excessive pesticide applications, takes effect in two days later after being sprayed, enables grasses to get right after a week, and is simple in using method and low in cost.
Description
Technical field
The present invention relates to remove the technical field of pesticide residue, be specifically related to a kind of composition and method of making the same of removing herbicide residue poisoning.
Background technology
Weedicide, claims again weedkiller, in order to eliminate or to suppress a class material of plant-growth.Effect is subject to the impact of weedicide, plant and envrionment conditions three factors.Be divided into by effect go out natural disposition and selective herbicide, conventional kind is organic compound.Can be widely used in ground weeds, the assorted noxious plants such as tree of filling with, mix such as control farmland, orchard, floral nursery, grassland and bare place, railway and Highways ', river course, reservoir, warehouse.
The introducing of weedicide has alleviated peasant's work burden, but weedicide residual shortest time in soil is half a year, what have reaches 2-3, herbicide residue poisoning is difficult to solve, not only place restrictions on the plantation of second stubble crop, and make the herbicide residue poisoning severe overweights of farm crop itself, and carry out problem seriously to food securing band, also can cause serious impact to HUMAN HEALTH.
Herbicide residue and pesticide injury are removed in tool understanding in the market, be mainly by hormone and chemical classes agricultural chemicals (chemical classes agricultural chemicals is called again toxinicide and comprises: use the seed dressing of naphthalene acid anhydride, Plant hormones regulators,gibberellins, the agent of OM(cauline leaf spraying seedling-protection), allyl dichloride amine, R-28725, the spirit of evil seedling, carboxin, choline dichloride, brassinolide, DA-6, think carefully the medicines such as spirit of enlarging afforested area, be mostly agricultural chemicals) reconcile the herbicide residue of plant and pesticide injury.The agricultural chemicals that use contains hormone and chemical classes, to the residue problem of field crop and the hormone of gourd, fruit and vegetable generation own and chemical classes agricultural chemicals, is to be to eat at short notice as gourd, fruit and vegetable.Itself just has the residual of hormone and agricultural chemicals, after eating, can bring very large impact to HUMAN HEALTH.The present invention just can effectively solve use hormone and chemical pesticide.Be used for pesticide residue and the drug injury problem that degrading plant produces.
At present, do not adopt Chinese medicinal materials and plant to remove the relevant report of herbicide residue.
Summary of the invention
The object of this invention is to provide the preparation of a kind of nontoxic, harmless, free of contamination a kind of herbal medicine solution herbicide residue poisoning.Itself there is the function of medicine, fertile effect, reach the fertile economic benefits and social benefits of medicine, in order to solve above-mentioned existing technological deficiency.
In order to achieve the above object, a kind of composition of separating herbicide residue poisoning provided by the present invention, said composition contains following composition: soybean extract, licorice extract, Fructus Hordei Germinatus extracting solution.
Concrete, the composition that described composition contains following weight part: soybean extract 30-60 part, licorice extract 5-20 part, Fructus Hordei Germinatus extracting solution 8-20 part.
Preferably, the composition that described composition contains following weight part: soybean extract 40-60 part, licorice extract 8-15 part, Fructus Hordei Germinatus extracting solution 10-18 part.
Further preferably, the composition that described composition contains following weight part: soybean extract 40-50 part, licorice extract 8-10 part, Fructus Hordei Germinatus extracting solution 10-15 part.
Composition of the present invention also contains following composition: extract solution from aloe, its consumption is 5-15 part, is preferably 6-13 part, more preferably 8-12 part.
Further, composition of the present invention also contains following composition: reed rhizome, Tree Peony Bark, Japanese Honeysuckle.
Concrete, described composition also contains the extracting solution that the Chinese medicine of following weight part is made: reed rhizome 6-9 part, Tree Peony Bark 4-9 part, Japanese Honeysuckle 3-6 part.
In above-mentioned composition:
Described soybean extract is prepared by following methods: soybean is put into the warm water soaking 18-20 hour of 20-45 ℃, then pull soybean out and add water to drop in slurry slag separator and extract Semen sojae atricolor pulp, obtain soybean extract; Wherein the weight ratio of soybean and warm water is 1:2-6, is preferably 1:3-4, more preferably 1:4; The temperature of warm water is preferably 30-40 ℃, more preferably 35 ℃; When described extraction the consumption of water be dry soybean weight 5-8 doubly; The ratio of soybean and soybean extract is: 1 portion of soybean obtains soybean liquid 4-8 part, is preferably 1 portion of soybean and obtains soybean liquid 6-8.
Described licorice extract is to extract by Radix Glycyrrhizae the licorice extract that contains glycyrrhizin 50-60% obtaining, and concrete extracting method is: directly squeeze the juice, obtain by ammoniacal liquor lixiviate, dilute sulphuric acid precipitation or direct water extraction; The method of described ammoniacal liquor lixiviate, dilute sulphuric acid precipitation comprises the following steps: 1) ammoniacal liquor and warm water mix, wherein 1 part of ammoniacal liquor, and 3 parts, water, ammonia soln, water temperature is 27-30 ℃; 2) with above-mentioned ammonia soln lixiviate Radix Glycyrrhizae, then add dilute sulphuric acid precipitation 16-18 hour of Radix Glycyrrhizae weight 4-8%, collect supernatant liquor, the licorice extract that to obtain containing glycyrrhizin be 50-60%; Wherein the weight ratio of ammoniacal liquor and water, Radix Glycyrrhizae is 1:3:2, extraction time 12-16 hour; The concentration of dilute sulphuric acid is 30-60%.
Described licorice extract also can be prepared by another method: when Radix Glycyrrhizae branch grows to 50-70cm, cut off, then squeeze the juice with juice extractor, to obtain final product.
Described Fructus Hordei Germinatus extracting solution, is prepared by following methods: barley warm water is invaded to bubble and after 12-16 hour, pull out, vernalization, in the time that barley grows 5-6cm bud, pulverizes its entirety, then Fructus Hordei Germinatus is mixed with water, drops in slurry slag separator and extracts barley liquid; The temperature of warm water is 30-40 ℃, is preferably 35-38 ℃; Soak time is preferably 12-14 hour, more preferably 12 hours; When extraction, the weight ratio of Fructus Hordei Germinatus and water is 1:0.5-5.5, is preferably 1:1-3, more preferably 1:2;
Described extract solution from aloe, is prepared by following methods: fresh aloe is pulverized, squeeze the juice, add monoammonium phosphate, stir, to obtain final product; Wherein the weight ratio of asparagus juice and monoammonium phosphate is 8-12:2, is preferably 10:2;
The preparation method of described reed rhizome, Tree Peony Bark, Japanese Honeysuckle: take reed rhizome, Tree Peony Bark, Japanese Honeysuckle according to proportioning, then the 40-60 ℃ of warm water soaking 5-6 hour doubly measuring with three taste Chinese medicine gross weight 2-5, the decocting that adds again three taste Chinese medicine gross weight 1-2 doubly to measure boils 40-50 minute, temperature is controlled at 100-110 ℃, obtains the extracting solution of three taste Chinese medicines; The temperature of described warm water is preferably 45-55 ℃.
The present invention also provides the preparation method of above-mentioned composition, and the method comprises the following steps: take each composition according to proportioning, then directly mix, to obtain final product.
The present invention also provides the compound of above-mentioned composition and agricultural chemicals, and described compound contains following composition: 100 parts of compositions, potassium primary phosphate 25-50 part, zinc sulfate 10-20 part.
The present invention also provides the preparation method of above-mentioned compound, directly mixes, and to obtain final product.
The application that also provides above-mentioned composition or compound to remove herbicide damage in preparation is provided.Described weedicide is preferably except acetochlor, G-30027 2.4D butyl ester, methoxone or formamido group sulfometuron-methyl.
The using method of composition provided by the invention or compound is: by spraying crop leaf, spread manuer in holes, drip irrigation etc.
The usage quantity of composition provided by the invention or compound is: 20-500g/ mu, is preferably 100-300g/ mu, more preferably 200-250g/ mu.
A kind of composition of removing herbicide residue poisoning provided by the invention has the following advantages:
1, the composition of solution herbicide residue provided by the invention poisoning contains removing toxic substances licorice extract, soybean extract, Fructus Hordei Germinatus extracting solution, Flos Lonicerae extractive solution, wherein: from soybean extract, Fructus Hordei Germinatus extracting solution, extract amino acid, a large amount of protein, Methionin, lipid acid and multivitamin, there is extraordinary detoxification and fertilizer effect simultaneously.
In order further to strengthen effect of fertilizer, can also in above-mentioned composition, add the liquid of various trace elements.By spraying farm crop blade, spread manuer in holes, drip irrigation, rely on itself absorbing of soil and crop, very effective this difficult problem of herbicide residue poisoning that solved.
2, the composition of solution herbicide residue provided by the invention poisoning, play the effect of nutrient-reinforced and removing toxic substances, can meet the demand of plant growth and nutrition comprehensively, improve the quality of crop, effectively improvement soil, the regenerative power of raising soil, promotes the absorption of crop to fertilizer, improve the second stage employ rate of solid chemical fertilizer, be a kind of green, environmental protection, nontoxic, harmless, pollution-free, do not contain any hormone and chemicals composition.Be applicable to crop extensive, as cash crop such as corn, soybean, paddy rice, peanut, various vegetables, Chinese medicinal materials, tea trees.Having the effect of the fertile economic benefits and social benefits of medicine, is the first-selected product of current development green, nuisanceless, the ecological agriculture.
3, the composition of solution herbicide residue provided by the invention poisoning has nutrient-reinforced, strengthens farm crop photosynthesis, promotes the strong seedling of plant establishment, the effect in strong sprout, improves crop yield 15-20%.
4, the composition of solution herbicide residue provided by the invention poisoning has the resistance ability such as disease-resistant, cold-resistant, drought resisting that strengthens crop, protects flower, fruit retention, prevents the various plants physiological diseases such as fallen leaves, yellow.
5, the composition of solution herbicide residue provided by the invention poisoning can be removed weedicide drift poisoning and excessive the produced poisoning of agricultural chemicals use fast, sprays and takes effect for latter two days, within one week, recovers normal, and using method is simple, and cost is low.
Embodiment
Following examples are used for illustrating the present invention, but are not used for limiting the scope of the invention.
Embodiment 1: a kind of composition of separating herbicide residue poisoning
1, composition: soybean extract 45g, licorice extract 10g, Fructus Hordei Germinatus extracting solution 12g.
2, preparation method:
1) preparation of soybean extract: soybean is placed in to 35 ℃ of warm water soaking 18 hours, the weight ratio of soybean and warm water is 1:4, then pull out soybean after immersion add water (6 times that the consumption of water is dry soybean) drop in slurry slag separator and extract Semen sojae atricolor pulp, obtain soybean extract, 1 portion of soybean obtains 6 parts of soybean extracts, for subsequent use;
2) preparation of Fructus Hordei Germinatus extracting solution: barley is invaded to bubble 12 hours with the warm water of 35-38 ℃, pull out, put into temperature control germinating box and carry out vernalization, in the time that Fructus Hordei Germinatus grows 5-6 centimetre, barley and Fructus Hordei Germinatus are pulverized, pulverize, then drop in slurry slag separator with together with the water of 2 times of its weight, extract Fructus Hordei Germinatus extracting solution liquid, for subsequent use;
3) preparation of licorice extract: ammoniacal liquor and warm water mix, wherein 1 part of ammoniacal liquor, 3 parts, water, water temperature is controlled at 27-30 ℃, obtains ammonia soln, for subsequent use; With above-mentioned ammonia soln lixiviate Radix Glycyrrhizae, the weight ratio of ammoniacal liquor and Radix Glycyrrhizae is 4:2, and extraction time is 16 hours, then adds the dilute sulphuric acid precipitation 18 hours of 0.48g, collects supernatant liquor, and the licorice extract that to obtain containing glycyrrhizin be 56% is for subsequent use;
4) take each composition according to proportioning, mix, obtain composition.
Embodiment 2: a kind of composition of separating herbicide residue poisoning
1, composition: soybean extract 40g, licorice extract 8g, Fructus Hordei Germinatus extracting solution 15g, extract solution from aloe 10g.
2, preparation method:
1) preparation of soybean extract: soybean is placed in to 35 ℃ of warm water soaking 18 hours, the weight ratio of soybean and warm water is 1:4, then pull out soybean after immersion add water (8 times that the consumption of water is dry soybean) drop in slurry slag separator and extract Semen sojae atricolor pulp, obtain soybean extract, 1 portion of soybean obtains 6 parts of soybean extracts, for subsequent use;
2) preparation of Fructus Hordei Germinatus extracting solution: barley is invaded to bubble 12 hours with the warm water of 35-38 ℃, pull out, put into temperature control germinating box and carry out vernalization, in the time that Fructus Hordei Germinatus grows 5-6 centimetre, barley and Fructus Hordei Germinatus are pulverized, then drop in slurry slag separator with together with the water of 2 times of its weight, extract Fructus Hordei Germinatus extracting solution liquid, for subsequent use;
3) preparation of licorice extract: ammoniacal liquor and warm water mix, wherein 1 part of ammoniacal liquor, 3 parts, water, water temperature is controlled at 27-30 ℃, obtains ammonia soln, for subsequent use; With above-mentioned ammonia soln lixiviate Radix Glycyrrhizae, the weight ratio of ammoniacal liquor and Radix Glycyrrhizae is 4:2, and extraction time is 16 hours, then adds the dilute sulphuric acid precipitation 16 hours of 0.40g, collects supernatant liquor, and the licorice extract that to obtain containing glycyrrhizin be 60% is for subsequent use;
4) preparation of extract solution from aloe: fresh aloe is pulverized, squeeze the juice, add monoammonium phosphate, stir, the weight ratio of asparagus juice and monoammonium phosphate is 10:2, obtains extract solution from aloe, for subsequent use;
5) take each composition according to proportioning, mix, obtain composition.
Embodiment 3: a kind of composition of separating herbicide residue poisoning
1, raw material: soybean extract 50g, licorice extract 10g, Fructus Hordei Germinatus extracting solution 15g, extract solution from aloe 10g, Japanese Honeysuckle 6g, reed rhizome 9g and Tree Peony Bark 8g.
2, preparation method:
1) preparation of soybean extract: soybean is placed in to 35 ℃ of warm water soaking 18 hours, the weight ratio of soybean and warm water is 1:4, then pull out soybean after immersion add water (6 times that the consumption of water is dry soybean) drop in slurry slag separator and extract Semen sojae atricolor pulp, obtain soybean extract, 1 portion of soybean obtains 6 parts of soybean extracts, for subsequent use;
2) preparation of Fructus Hordei Germinatus extracting solution: barley is invaded to bubble 12 hours with the warm water of 35-38 ℃, pull out, put into temperature control germinating box and carry out vernalization, in the time that Fructus Hordei Germinatus grows 5-6 centimetre, barley and Fructus Hordei Germinatus are pulverized, then drop in slurry slag separator with together with the water of 2 times of its weight, extract Fructus Hordei Germinatus extracting solution liquid, for subsequent use;
3) preparation of licorice extract: ammoniacal liquor and warm water mix, wherein 1 part of ammoniacal liquor, 3 parts, water, water temperature is controlled at 27-30 ℃, obtains ammonia soln, for subsequent use; With above-mentioned ammonia soln lixiviate Radix Glycyrrhizae, the weight ratio of ammoniacal liquor and Radix Glycyrrhizae is 4:2, and extraction time is 15 hours, then adds the dilute sulphuric acid precipitation 18 hours of 0.48g, collects supernatant liquor, and the licorice extract that to obtain containing glycyrrhizin be 58% is for subsequent use;
4) preparation of extract solution from aloe: fresh aloe is pulverized, squeeze the juice, add monoammonium phosphate, stir, the weight ratio of asparagus juice and monoammonium phosphate is 8:2, obtains extract solution from aloe, for subsequent use;
5) take reed rhizome, Tree Peony Bark, Japanese Honeysuckle according to proportioning, be then equivalent to 2.6 times of three taste Chinese medicines with 60g() 50 ℃ of warm water soaking 5 hours, then add 30g decocting to boil 50 minutes, temperature is controlled at 100-110 ℃, obtains the extracting solution of three taste Chinese medicines, for subsequent use;
6) according to proportioning 1)-4) extracting solution that obtains, then add the extracting solution of the three taste Chinese medicines that step 5) obtains, mix, obtain composition.
Embodiment 4: a kind of composition of separating herbicide residue poisoning
1, raw material: soybean extract 60g, licorice extract 15g, Fructus Hordei Germinatus extracting solution 18g, extract solution from aloe 15g, Japanese Honeysuckle 4g, reed rhizome 8g and Tree Peony Bark 6g.
2, preparation method:
1) preparation of soybean extract: soybean is placed in to 40 ℃ of warm water soaking 20 hours, the weight ratio of soybean and warm water is 1:3, then pull out soybean after immersion add water (7 times that the consumption of water is dry soybean) drop in slurry slag separator and extract Semen sojae atricolor pulp, obtain soybean extract, 1 portion of soybean obtains 8 parts of soybean extracts, for subsequent use;
2) preparation of Fructus Hordei Germinatus extracting solution: barley is invaded to bubble 12 hours with the warm water of 35-38 ℃, pull out, put into temperature control germinating box and carry out vernalization, in the time that Fructus Hordei Germinatus grows 5-6 centimetre, pluck Fructus Hordei Germinatus, pulverize, then drop in slurry slag separator with together with the water of 2 times of its weight, extract Fructus Hordei Germinatus extracting solution liquid, for subsequent use;
3) preparation of licorice extract: ammoniacal liquor and warm water mix, wherein 1 part of ammoniacal liquor, 3 parts, water, water temperature is controlled at 27-30 ℃, obtains ammonia soln, for subsequent use; With above-mentioned ammonia soln lixiviate Radix Glycyrrhizae, the weight ratio of ammoniacal liquor and Radix Glycyrrhizae is 4:2, and extraction time is 13 hours, then adds the dilute sulphuric acid precipitation 16 hours of 0.50g, collects supernatant liquor, and the licorice extract that to obtain containing glycyrrhizin be 57% is for subsequent use;
4) preparation of extract solution from aloe: fresh aloe is pulverized, squeeze the juice, add monoammonium phosphate, stir, the weight ratio of asparagus juice and monoammonium phosphate is 12:2, obtains extract solution from aloe, for subsequent use;
5) take reed rhizome, Tree Peony Bark, Japanese Honeysuckle according to proportioning, be then equivalent to 2.5 times of three taste Chinese medicines with 45g() 50 ℃ of warm water soaking 5 hours, then add 20g decocting to boil 40 minutes, temperature is controlled at 100-110 ℃, obtains the extracting solution of three taste Chinese medicines, for subsequent use;
6) according to proportioning 1)-4) extracting solution that obtains, then add the extracting solution of the three taste Chinese medicines that step 5) obtains, mix, obtain composition.
Embodiment 5: a kind of compound of separating herbicide residue poisoning
1, composition: soybean extract 60g, licorice extract 20g, Fructus Hordei Germinatus extracting solution 20g, Japanese Honeysuckle 6g, extract solution from aloe 10g, reed rhizome 9g, Tree Peony Bark 8g, potassium primary phosphate 40g, zinc sulfate 20g.
2, prepare composition according to the method for embodiment 3, directly mix, to obtain final product.
Experimental example 1: remove the experiment of herbicide for paddy field poisoning
Services have been opened in triumph village in Baoxing township, Fangzheng County, Heilongjiang Province in 2011 ten mu of rice terraces, rice varieties is longdao No.3, April 20 grew seedlings, May 28 rice transplanting rice seedling, grow fine, start for 6 the end of month with herbicides for use in paddy, due to excessive use, after 7 days, produce herbicide damage, rice seedling jaundice root is brown, does not send new root, has stopped growth, test as basis take this field, experimental technique and result are as follows:
1, experiment grouping and method: be divided into 6 groups, be specially 1,2 group of contrast, experiment 1-4 group, wherein: by 10 mu of rice fields, contrast 1 group, 1 mu, 100 grams of melon dish toxinicides, are watered 15 kilograms and squirt half mu; Contrast 2 groups, 1 mu, 15 grams of plant solution evil spirits are watered 15 kilograms and squirt paddy rice footpath leaf; Experiment 1-4 group,, gives respectively the product of embodiment 1-4 by 2 mu every group, simultaneously, on the basis of Example formulations, add potassium primary phosphate and zinc sulfate, (each group of embodiment 1-4 is 100:32:15 with the weight ratio of potassium primary phosphate and zinc sulfate, be watered 30 kilograms), usage quantity is 250g/ mu.
2, experimental result:
Contrast 1 group, the rice seedling that sprays poisoning in latter 3 days does not significantly take a turn for the better, and the not more new root of poor growth occurs, contrast 2 groups, use the spirit of plant solution evil to spray the rice seedlings phenomenon that do not note abnormalities, paddy growth is slow, there is no the core that makes new advances of growing, root does not grow new white root, and poisoning slightly alleviates; And the herbal medicine that uses embodiment of the present invention 1-4 group to provide was removed the residual poisoning preparation of medicament after 7 days, send new core, root bears white simultaneously, has sprayed altogether whole vegetative period 3 times, to autumn, produces through surveying, and per mu yield reaches 680 kilograms.With contrast 1,2 group and compare, embodiment 1-4 respectively organizes paddy rice and increases production respectively 10-12%, 15-18%.Effect comparison between embodiment 1-4 group, incremental order is embodiment 1, embodiment 2, embodiment 3, embodiment 4.
Result shows: composition provided by the invention can significantly be removed the residual poisoning of herbicides for use in paddy, is equipped with potassium primary phosphate and zinc sulfate, obviously practise midwifery, and effect is better than prior art.
Experimental example 2: remove corn stubble and replant the residual experiment of soybean field herbicide poisoning
Poplar forest township Yang Jia depression village, Nongan County, Jilin Province in 2011 2 Li Junzhe of society in the corn field kind of last year 20 mu of order soybean, sowing on May 15, start by the end of May to emerge, after emerging, find leaflet jaundice, the seedling also having does not encircle unearthed next, extracting seedling root is brown, does not grow new root, and there is seedling death phenomenon in serious plot, in the time that seedling grows to 4-5 sheet leaf, common deep green of color, blade thickness, has shrinkage phenomenon, root does not continue the phenomenon of lower bundle, white root is little, tests as basis take this field, and experimental technique and result are as follows:
1, experiment grouping and method: be divided into 6 groups, be specially 1,2 group of contrast, experiment 1-4 group, wherein: 20 mu of Soybean Fields, contrast 1 group, 2 mu, 100 grams of melon dish toxinicides, are watered 30 grams; Contrast 2 groups, 2 mu, brassinolide (6 grams)+DN-6(4 gram) be watered 15 kilograms and carry out foliage-spray; Experiment 1-4 group,, gives respectively the product of embodiment 1-4 by 4 mu every group, simultaneously, on the basis of Example formulations, add potassium primary phosphate and zinc sulfate, (each group of embodiment 1-4 is 100:32:15 with the weight ratio of potassium primary phosphate and zinc sulfate, be watered 30 kilograms), usage quantity is 250g/ mu.
2, experimental result:
Contrast 1 group, some soybean seedling leafs stretch not open, and also have the phenomenon of yellow leaf, and only some soybean seedling sends new core, and seedling also has stiffness, poor growth.Contrast 2 groups, herbicide residue poisoning slightly alleviates, and recovers slowly.And the composition that uses embodiment 1-4 provided by the invention to provide used after three days, young leaves greening, within one week, rear blade growing way is normal, grown a lot of little Bai roots, sprayed week about once, sprayed altogether whole seedling stage three times, growing way is fine, blade hypertrophy, root system is strong, has obtained good harvest after autumn.With contrast 1,2 group and compare, embodiment 1-4 respectively organizes soybean and increases production respectively 11-15%, 15-18%.Effect comparison between embodiment 1-4 group, incremental order is embodiment 1, embodiment 2, embodiment 3, embodiment 4.
Result shows: composition provided by the invention can significantly be removed the residual poisoning of Soybean herbicides, is equipped with potassium primary phosphate and zinc sulfate, obviously practise midwifery, and effect is better than prior art.
Experimental example 3: remove the experiment of muskmelon booth weedicide drift poisoning
The managining director Zhao Wenchuan of Operation in Dandong Area, Liaoning Province in 2012 Dong Xiang Muskmelon Planting cooperative society has 60 booths, it is all the muskmelon of plantation, February 20 seeding and seedling raising, at the beginning of 4 months, move on to booth field planting, all listings at the beginning of annual late June to 7 month, mail to Beijing, Tianjin, sell in Ge great market, northeast, because a lot of booth periphery major parts are corn fields, mid or late May connects the rainfall in several days that continues, what the peasant household of periphery relatively concentrated has sprayed corn field herbicide, spring breeze season just at that time, melon temperature of shed is between 33-40 ℃, melon canopy must ventilate in time, so just weedicide is floated in canopy by the ventilation opening of booth, in whole air, all contain weedicide composition, there is more than 70 booth to occur weedicide drift poisoning, leaf color becomes deep green, blade thickness young sprout upwarps, vegetative point is not long, ventilation opening place is even more serious, some blades are withered and yellow, blade edge is burnt shape, test as basis take this field, experimental technique and result are as follows:
1, experiment grouping and method: be divided into 6 groups, be specially 1,2 group of contrast, experiment 1-4 group, wherein: 60 booths, every group of 10 booths, contrast 1 group, (potassium primary phosphate and zinc sulfate are according to 32g, 15g proportioning to give potassium primary phosphate and zinc sulfate, dosage is 57g/ mu, is watered 30 kilograms) 5 booths, DA-6(8 gram)+brassinolide (12 grams) is watered 30 kilograms booth melon seedling carried out to foliage-spray; Experiment 1-4 group,, gives respectively the product of embodiment 1-4 by 4 mu every group, simultaneously, on the basis of Example formulations, add potassium primary phosphate and zinc sulfate, (each group of embodiment 1-4 is 100:32:15 with the weight ratio of potassium primary phosphate and zinc sulfate, be watered 30 kilograms), usage quantity is 250g/ mu.
2, experimental result:
Contrast 1 group, spray rear melon seedling and be not clearly better, slightly alleviate phenomenon; Contrast 2 groups, use the drift poisoning of brassinolide+DA-6 product melon and fruit to alleviate to some extent, recover slower.And each group of embodiment 1-4 provided by the invention sprays latter two days with regard to appearance effect, within four days, just there is afterwards the effect of highly significant, after one week, recover normal completely, in time of listing and output, be not affected.With contrast 1,2 group and compare, embodiment 1-4 respectively organizes muskmelon and increases production respectively 13-15%, 20-30%.Effect comparison between embodiment 1-4 group, incremental order is embodiment 1, embodiment 2, embodiment 3, embodiment 4.
Result shows: composition provided by the invention can significantly be removed melon patch weedicide drift poisoning, is equipped with potassium primary phosphate and zinc sulfate, obviously practise midwifery, and effect is better than prior art.
Although, above use general explanation, embodiment and test, the present invention is described in detail, on basis of the present invention, can make some modifications or improvements it, and this will be apparent to those skilled in the art.Therefore, these modifications or improvements without departing from theon the basis of the spirit of the present invention, all belong to the scope of protection of present invention.
Claims (27)
1. separate the composition of herbicide residue poisoning for one kind, it is characterized in that, the composition that described composition contains following weight part: soybean extract 30-60 part, licorice extract 5-20 part, Fructus Hordei Germinatus extracting solution 8-20 part, described soybean extract is prepared by following methods: soybean is put into the warm water soaking 18-20 hour of 20-45 ℃, then pull soybean out and add water to drop in slurry slag separator and extract Semen sojae atricolor pulp, obtain soybean extract; Described licorice extract is to be extracted by Radix Glycyrrhizae, the licorice extract that contains glycyrrhizin 50-60% obtaining; Described Fructus Hordei Germinatus extracting solution, is prepared by following methods: barley warm water soaking was pulled out after 12-16 hour, and vernalization, in the time that barley grows 5-6cm bud, pulverizes its entirety, then Fructus Hordei Germinatus is mixed with water, drops in slurry slag separator and extracts barley liquid.
2. composition according to claim 1, is characterized in that, the composition that described composition contains following weight part: soybean extract 40-60 part, licorice extract 8-15 part, Fructus Hordei Germinatus extracting solution 10-18 part.
3. composition according to claim 1, is characterized in that, the composition that described composition contains following weight part: soybean extract 40-50 part, licorice extract 8-10 part, Fructus Hordei Germinatus extracting solution 10-15 part.
4. composition according to claim 1, is characterized in that, described composition also contains following composition: extract solution from aloe, and its consumption is 5-15 part; Described extract solution from aloe, is prepared by following methods: fresh aloe is pulverized, squeeze the juice, add monoammonium phosphate, stir, to obtain final product.
5. composition according to claim 4, is characterized in that, the consumption of described extract solution from aloe is 6-13 part.
6. composition according to claim 4, is characterized in that, the consumption of described extract solution from aloe is 8-12 part.
7. composition according to claim 4, it is characterized in that, described composition also contains the extracting solution that the Chinese medicine of following weight part is made: reed rhizome 6-9 part, Tree Peony Bark 4-9 part, Japanese Honeysuckle 3-6 part, the preparation method of described reed rhizome, Tree Peony Bark, Japanese Honeysuckle: take reed rhizome, Tree Peony Bark, Japanese Honeysuckle according to proportioning, then the 40-60 ℃ of warm water soaking 5-6 hour doubly measuring with three taste Chinese medicine gross weight 2-5, the decocting that adds again three taste Chinese medicine gross weight 1-2 doubly to measure boils 40-50 minute, temperature is controlled at 100-110 ℃, obtains the extracting solution of three taste Chinese medicines.
8. according to the composition described in claim 1-7 any one, it is characterized in that, in the preparation method of described soybean extract, wherein the weight ratio of soybean and warm water is 1:2-6.
9. composition according to claim 8, is characterized in that, in the preparation method of described soybean extract, the weight ratio of soybean and warm water is 1:3-4.
10. composition according to claim 9, is characterized in that, in the preparation method of described soybean extract, the weight ratio of soybean and warm water is 1:4.
11. according to the composition described in claim 1-7 any one, it is characterized in that, in the preparation method of described soybean extract, the temperature of warm water is 30-40 ℃.
12. compositions according to claim 11, is characterized in that, in the preparation method of described soybean extract, the temperature of warm water is 35 ℃.
13. according to the composition described in claim 1-7 any one, it is characterized in that, in the preparation method of described soybean extract, when described extraction the consumption of water be dry soybean weight 5-8 doubly; The ratio of soybean and soybean extract is: 1 portion of soybean obtains soybean liquid 4-8 part.
14. compositions according to claim 13, is characterized in that, in the preparation method of described soybean extract, the ratio of soybean and soybean extract is that 1 portion of soybean obtains soybean liquid 6-8 part.
15. according to the composition described in claim 1-7 any one, it is characterized in that, the concrete extracting method of described licorice extract is: directly squeeze the juice, by ammoniacal liquor lixiviate, dilute sulphuric acid precipitation or directly water extraction obtains.
16. according to the composition described in claim 1-7 any one, it is characterized in that, in the preparation method of described Fructus Hordei Germinatus extracting solution, the temperature of warm water is 30-40 ℃.
17. compositions according to claim 16, is characterized in that, in the preparation method of described Fructus Hordei Germinatus extracting solution, the temperature of warm water is 35-38 ℃.
18. according to the composition described in claim 1-7 any one, it is characterized in that, in the preparation method of described Fructus Hordei Germinatus extracting solution, soak time is 12-14 hour.
19. compositions according to claim 18, is characterized in that, in the preparation method of described Fructus Hordei Germinatus extracting solution, soak time is 12 hours.
20. according to the composition described in claim 1-7 any one, it is characterized in that, in the preparation method of described Fructus Hordei Germinatus extracting solution, the weight ratio of Fructus Hordei Germinatus and water is 1:0.5-5.5.
21. compositions according to claim 20, is characterized in that, in the preparation method of described Fructus Hordei Germinatus extracting solution, the weight ratio of Fructus Hordei Germinatus and water is 1:1-3.
22. compositions according to claim 21, is characterized in that, in the preparation method of described Fructus Hordei Germinatus extracting solution, the weight ratio of Fructus Hordei Germinatus and water is 1:2.
23. according to the composition described in claim 4-7 any one, it is characterized in that, in the preparation method of described extract solution from aloe, the weight ratio of asparagus juice and monoammonium phosphate is 8-12:2.
24. compositions according to claim 23, is characterized in that, in the preparation method of described extract solution from aloe, the weight ratio of asparagus juice and monoammonium phosphate is 10:2.
25. compositions according to claim 7, is characterized in that, the temperature of warm water described in the preparation method of described reed rhizome, Tree Peony Bark, Japanese Honeysuckle is 45-55 ℃.
26. compounds containing composition described in claim 1-25 any one, is characterized in that, described compound contains following composition: 100 parts of compositions, potassium primary phosphate 25-50 part, zinc sulfate 10-20 part.
Compound described in 27. claim 1-25 any one described in composition or claim 26 is being removed the application of herbicide residue poisoning.
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| CN104082291B (en) * | 2014-07-02 | 2016-05-18 | 谭丕和 | A kind of organic plant antidote |
| CN105368462A (en) * | 2015-12-16 | 2016-03-02 | 梁宗贵 | Crop soil purifying agent and production technology thereof |
| CN105368463A (en) * | 2015-12-16 | 2016-03-02 | 梁宗贵 | Crop soil purifying agent and preparing method thereof |
| CN106396877A (en) * | 2016-08-30 | 2017-02-15 | 漯河市科汇生物工程有限公司 | Herbicide injury removal agent with nourishing and sterilizing functions |
| CN107987836A (en) * | 2017-10-12 | 2018-05-04 | 山东礽健生物科技有限公司 | A kind of pesticide contaminated soil renovation agent and its production method |
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| CN1413963A (en) * | 2002-09-19 | 2003-04-30 | 上海九康农业科技发展有限公司 | Compound application technology for nano-biological fertilizer and soil conditioner |
| CN1833496A (en) * | 2006-04-18 | 2006-09-20 | 郭红甫 | Harm remedial agent of weedicide |
| CN101322491A (en) * | 2008-07-29 | 2008-12-17 | 董长江 | Agent for eliminating chemical injury of crops |
| CN102746066A (en) * | 2012-07-19 | 2012-10-24 | 谭赫 | Plant nutrient solution |
| CN103044159B (en) * | 2013-01-28 | 2014-08-13 | 大庆农心农业科技开发有限公司 | Pesticide residue degradation agent |
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