CN103202990B - A kind of Chinese medicine granules for the treatment of female menopause symptoms - Google Patents
A kind of Chinese medicine granules for the treatment of female menopause symptoms Download PDFInfo
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- CN103202990B CN103202990B CN201310023098.8A CN201310023098A CN103202990B CN 103202990 B CN103202990 B CN 103202990B CN 201310023098 A CN201310023098 A CN 201310023098A CN 103202990 B CN103202990 B CN 103202990B
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Abstract
Treat a Chinese medicine granules for female menopause symptoms, (1) Radix Angelicae Sinensis soaks 1 hour, extracts volatile oil, then obtains volatile oil with anhydrous sodium sulfate drying, obtained clathrate, for subsequent use; (2) Fructus Ligustri Lucidi adds 50% ethanol extraction 2 times, for subsequent use; (3) get Flos Carthami 50% soak with ethanol 24 hours, collect 5 times amount percolates with percolation, for subsequent use; (4) Rhizoma Cyperi is ground into coarse powder and Radix Angelicae Sinensis medicinal residues, ethanol extraction 2 times, for subsequent use; (5) get (2), (3), supernatant obtained in (4) step, concentrated clear paste, for subsequent use; (6) Cortex Eucommiae (stir-fry), Arillus Longan, Radix Polygoni Multiflori, Semen Cuscutae, the Radix Rehmanniae, Radix Rehmanniae Preparata, Radix Codonopsis, the Radix Astragali, Poria cum Radix Pini, the Rhizoma Atractylodis Macrocephalae, Radix Salviae Miltiorrhizae, Semen Persicae, Pericarpium Citri Reticulatae Viride, Fructus Citri Sarcodactylis, the Radix Paeoniae Alba, Radix Curcumae, Radix Bupleuri, Caulis Polygoni Multiflori, Flos Albiziae and Fructus Ligustri Lucidi, Rhizoma Cyperi, Flos Carthami, Radix Angelicae Sinensis medicinal residues add water and soak 30 minutes in right amount, effective component extracting 2 times, concentrated clear paste, add clathrate obtained in (1) step again, add the lactose of its weight 10% and the mixture of dextrin, cross 100 mesh sieves, obtain extract powder with spray dryer, namely subpackage obtains granule.
Description
Technical field:
The invention belongs to technical field of Chinese medicines, particularly a kind of Chinese medicine granules for the treatment of female menopause symptoms.
Background technology:
Climacteric women kidney qi degradation, asthenia of essence and blood, causes imbalance of YIN and YANG, and showing as a series of autonomic nervous dysfunction is main symptom, paroxysmal hectic fever, with uncomfortable in chest, breathe hard, cardiopalmus, dizzy, easily tired, emotional lability, insomnia are common.Sick position is at kidney, liver, the heart, and pathogenesis is the hepatic and renal YIN deficiency, disarmony between the heart and kidney, and treatment suitable nourishing the liver and kidney, mind tranquilizing and the heart calming, help with dispersing the stagnated live-QI to relieve the stagnation of QI.
Summary of the invention:
The present invention overcomes the deficiency of the problems referred to above, there is provided a kind of Chinese medicine granules for the treatment of female menopause symptoms, this Granular formulations is: the Cortex Eucommiae 9 grams, Arillus Longan 9 grams, Radix Polygoni Multiflori 9 grams, Semen Cuscutae 12 grams, Fructus Ligustri Lucidi 12 grams, 9 grams, the Radix Rehmanniae, 12 grams, Radix Rehmanniae Preparata, Radix Codonopsis 12 grams, the Radix Astragali 12 grams, Poria cum Radix Pini 9 grams, the Rhizoma Atractylodis Macrocephalae 9 grams, the Radix Paeoniae Alba 12 grams, Radix Curcumae 9 grams, Radix Bupleuri 12 grams, Caulis Polygoni Multiflori 15 grams, Flos Albiziae 12 grams, Radix Salviae Miltiorrhizae 15 grams, Radix Angelicae Sinensis 12 grams, 9 grams, Flos Carthami, 9 grams, Semen Persicae, Rhizoma Cyperi 9 grams, 9 grams, Pericarpium Citri Reticulatae Viride and Fructus Citri Sarcodactylis 12 grams.
Manufacture method is: (1) Radix Angelicae Sinensis soaks 1 hour, extracts volatile oil, then obtains volatile oil with anhydrous sodium sulfate drying, then use beta-cyclodextrin inclusion compound with volatile oil extractor, obtained clathrate, for subsequent use;
(2) get Fructus Ligustri Lucidi and add 50% ethanol extraction 2 times, each 1 hour, merge medicinal liquid, leave standstill 24 hours, for subsequent use;
(3) get Flos Carthami 50% soak with ethanol 24 hours, collect 5 times amount percolates with percolation, leave standstill 24 hours, for subsequent use;
(4) Rhizoma Cyperi is ground into coarse powder and Radix Angelicae Sinensis medicinal residues, with appropriate 75% ethanol extraction 2 times, each 1 hour, collects extracting solution, leaves standstill 24 hours, for subsequent use;
(5) get (2), (3), supernatant obtained in (4) step, decompression recycling ethanol, is concentrated into 60 DEG C ~ 70 DEG C, and density is the clear paste of 1.03 ~ 1.09, for subsequent use;
(6) Cortex Eucommiae (stir-fry), Arillus Longan, Radix Polygoni Multiflori, Semen Cuscutae, the Radix Rehmanniae, Radix Rehmanniae Preparata, Radix Codonopsis, the Radix Astragali, Poria cum Radix Pini, the Rhizoma Atractylodis Macrocephalae, Radix Salviae Miltiorrhizae, Semen Persicae, Pericarpium Citri Reticulatae Viride, Fructus Citri Sarcodactylis, the Radix Paeoniae Alba, Radix Curcumae, Radix Bupleuri, Caulis Polygoni Multiflori, Flos Albiziae and Fructus Ligustri Lucidi, Rhizoma Cyperi, Flos Carthami, Radix Angelicae Sinensis medicinal residues add water and soak 30 minutes in right amount, put into multi-functional extractor effective component extracting 2 times, each 1 hour, merge extractive liquid, be concentrated into 60 DEG C ~ 70 DEG C, density is the clear paste of 1.03 ~ 1.09, two parts clear paste of water extraction and alcohol extraction is mixed, stir evenly, add Benexate Hydrochloride obtained in (1) step again, measure its weight, add the lactose of its weight 10% and the mixture of dextrin, in the mixture of wherein lactose and dextrin, the weight ratio of lactose and dextrin is 2: 3, stir and be heated to 80 ~ 90 DEG C, cross 100 mesh sieves, obtain extract powder with spray dryer, namely subpackage obtains granule.
Method for making illustrates:
The main component of Radix Angelicae Sinensis has volatile oil and ferulic acid, therefore first carries volatile oil, and ferulic acid is easy to propose in ethanol, rear ethanol extraction; Fructus Ligustri Lucidi contains oleanolic acid, and oleanolic acid dissolves in ethanol, and water-soluble hardly, therefore first adopts ethanol extraction; Radix Polygoni Multiflori decoction of black soybean and yellow wine are mixed stewing out of water thoroughly and are exhausted to juice, the invigorating the liver and kidney of Radix Polygoni Multiflori Preparata function, benefiting essence-blood, black beard and hair, bone and muscle strengthening; The Cortex Eucommiae is after parch, then gutta-percha is destroyed, and effective ingredient is easy to fried; Because the stickiness of Chinese medical concrete is larger, therefore the mixture adding dextrin and lactose is before spray drying to ensure spray-diredly to carry out smoothly.Red pigment and flavochrome are the effective ingredient in Flos Carthami, and the two all can be dissolved in Diluted Alcohol, and the two is more unstable, especially reddish yellow pigment less stable in hot solution, therefore with Diluted Alcohol, extract with percolation.
The mechanism of action:
The Cortex Eucommiae, the Cortex Eucommiae has invigorating the liver and kidney, bone and muscle strengthening, rubbish in purged body, strengthens human body cell substance metabolism, prevents muscle skeleton aging, balanced human's blood pressure, decomposer inner cholesterol, reduces body fat, recover blood vessel elasticity, diuresis heat clearing away, broad-spectrum antiseptic, stimulating central nervous system, improve white blood cell count, strengthen the remarkable efficacy such as body immunity; Arillus Longan, invigorating the heart and spleen, nourishing blood to tranquillize the mind, for insufficiency of vital energy and blood, severe palpitation, forgetful insomnia; Radix Polygoni Multiflori, nourishing the blood and yin, loosening bowel to relieve constipation, cure mainly the soreness of the waist and knees, early whitening of beard and hair, tinnitus, dryness of the intestine constipation etc. of blood deficiency Light-headedness, cardiopalmus, insomnia, the hepatic and renal YIN deficiency; Semen Cuscutae, invigorating the liver and kidney, beneficial marrow, improving eyesight, controls soreness of waist and knee joint, and seminal emission, quenches one's thirst, dripping urination, and order is dark; Fructus Ligustri Lucidi, liver and kidney tonifying, clearind deficient heat, improving eyesight; The Radix Rehmanniae, heat clearing away, promote the production of body fluid, moisturize, laxation, removing blood stasis with potent drugs, tissue regeneration promoting, pain relieving, regulating menstruation, removing heat from blood, hemostasis etc.; Radix Rehmanniae Preparata, yin nourishing of enriching blood, life essence-filling, marrow-benefitting; Radix Codonopsis, invigorating the spleen and replenishing QI, effect of spleen invigorating lung benefiting; The Radix Astragali, has invigorating QI to consolidate the body surface resistance, effect of diuresis poison holding, weak for the deficiency of vital energy, anorexia and loose stool, sinking of QI of middle-JIAO, exterior deficiency spontaneous perspiration, blood deficiency and yellow complexion, and interior-heat is quenched one's thirst; Poria cum Radix Pini, for palpitation with fear of having a guilty conscience, forgetful, insomnia, infantile convulsion, dysuria etc.; The Rhizoma Atractylodis Macrocephalae, invigorating the spleen and benefiting QI, dampness diuretic, hidroschesis, have loose bowels for insufficiency of the spleen lack of appetite, abdominal distention, phlegm retention vertigo and palpitation, edema, spontaneous perspiration etc.; The Radix Paeoniae Alba, nourishing blood to suppress the hyperactive liver, pain relieving in slow, yin fluid astringing receives antiperspirant; Radix Curcumae, regulating qi to disperse stagnation, the effect of heart fire-clearing upset-relieving, for amenorrhea dysmenorrhea, chest and abdomen swelling and pain, twinge, calentura coma, epilepsy is gone mad, jaundice dark coloured urine; Radix Bupleuri, clearind deficient heat Chinese medicine, comes off for stagnation of QI due to depression of the liver, sternal rib pain, uterus, menoxenia etc.; Caulis Polygoni Multiflori, cures mainly insomnia, impairment caused by overstrain, hyperhidrosis, blood deficiency general pain etc.; Flos Albiziae, has calming effects, is mainly used in the effects such as pent-up is uncomfortable in chest, insomnia forgetfulness, nourishing YIN and invigorating YANG, ophthalmic, neurasthenia; Radix Salviae Miltiorrhizae, menoxenia, amenorrhea dysmenorrhea, lump in the abdomen, breast ventral spine pain, pyretic arthralgia pain, skin infection swells and ache, dysphoria and insomnia, hepatosplenomegaly, angina pectoris etc.; Radix Angelicae Sinensis, enriches blood and invigorates blood circulation, menstruction regulating and pain relieving, loosening bowel to relieve constipation, for blood deficiency and yellow complexion, dizzy cardiopalmus, menoxenia, amenorrhea dysmenorrhea, asthenia cold abdominalgia, dryness of the intestine constipation, rheumatic arthralgia etc.; Flos Carthami, latus rectum of invigorating blood circulation, eliminating stasis to stop pain, for amenorrhea, dysmenorrhea, lochia, lump in the abdomen mass in the abdomen etc.; Semen Persicae, blood circulation promoting and blood stasis dispelling, loosening bowel to relieve constipation, relieving cough and asthma; Rhizoma Cyperi, resolving depression of regulating the flow of vital energy, menstruction regulating and pain relieving; Pericarpium Citri Reticulatae Viride, soothing the liver dispelling the stagnated QI, removing food stagnancyization are stagnant; Fructus Citri Sarcodactylis, liver-smoothing, qi-regulating, and stomach and alleviating pain.
Detailed description of the invention:
Treat a Chinese medicine granules for female menopause symptoms, this Granular formulations is: the Cortex Eucommiae 9 grams, Arillus Longan 9 grams, Radix Polygoni Multiflori 9 grams, Semen Cuscutae 12 grams, Fructus Ligustri Lucidi 12 grams, 9 grams, the Radix Rehmanniae, 12 grams, Radix Rehmanniae Preparata, Radix Codonopsis 12 grams, the Radix Astragali 12 grams, Poria cum Radix Pini 9 grams, the Rhizoma Atractylodis Macrocephalae 9 grams, the Radix Paeoniae Alba 12 grams, Radix Curcumae 9 grams, Radix Bupleuri 12 grams, Caulis Polygoni Multiflori 15 grams, Flos Albiziae 12 grams, Radix Salviae Miltiorrhizae 15 grams, Radix Angelicae Sinensis 12 grams, 9 grams, Flos Carthami, 9 grams, Semen Persicae, Rhizoma Cyperi 9 grams, 9 grams, Pericarpium Citri Reticulatae Viride and Fructus Citri Sarcodactylis 12 grams.Manufacture method is: (1) Radix Angelicae Sinensis soaks 1 hour, extracts volatile oil, then obtains volatile oil with anhydrous sodium sulfate drying, then use beta-cyclodextrin inclusion compound with volatile oil extractor, obtained clathrate, for subsequent use, (2) get Fructus Ligustri Lucidi and add 50% ethanol extraction 2 times, each 1 hour, merge medicinal liquid, leave standstill 24 hours, for subsequent use, (3) get Flos Carthami 50% soak with ethanol 24 hours, collect 5 times amount percolates with percolation, leave standstill 24 hours, for subsequent use, (4) Rhizoma Cyperi is ground into coarse powder and Radix Angelicae Sinensis medicinal residues, with appropriate 75% ethanol extraction 2 times, each 1 hour, collects extracting solution, leaves standstill 24 hours, for subsequent use, (5) get (2), (3), supernatant obtained in (4) step, decompression recycling ethanol, is concentrated into 60 DEG C ~ 70 DEG C, and density is the clear paste of 1.03 ~ 1.09, for subsequent use, (6) Cortex Eucommiae (stir-fry), Arillus Longan, Radix Polygoni Multiflori, Semen Cuscutae, the Radix Rehmanniae, Radix Rehmanniae Preparata, Radix Codonopsis, the Radix Astragali, Poria cum Radix Pini, the Rhizoma Atractylodis Macrocephalae, Radix Salviae Miltiorrhizae, Semen Persicae, Pericarpium Citri Reticulatae Viride, Fructus Citri Sarcodactylis, the Radix Paeoniae Alba, Radix Curcumae, Radix Bupleuri, Caulis Polygoni Multiflori, Flos Albiziae and Fructus Ligustri Lucidi, Rhizoma Cyperi, Flos Carthami, Radix Angelicae Sinensis medicinal residues add water and soak 30 minutes in right amount, put into multi-functional extractor effective component extracting 2 times, each 1 hour, merge extractive liquid, be concentrated into 60 DEG C ~ 70 DEG C, density is the clear paste of 1.03 ~ 1.09, two parts clear paste of water extraction and alcohol extraction is mixed, stir evenly, add Benexate Hydrochloride obtained in (1) step again, measure its weight, add the lactose of its weight 10% and the mixture of dextrin, in the mixture of wherein lactose and dextrin, the weight ratio of lactose and dextrin is 2: 3, stir and be heated to 80 ~ 90 DEG C, cross 100 mesh sieves, obtain extract powder with spray dryer, namely subpackage obtains granule.
Clinical case: by this side treatment climacteric syndrome 54 example, recovery from illness 35 example, take a turn for the better 14 examples, invalid 5 examples, total effective rate 90.7%.
Model case:
1, certain is consolidated, female, 48 years old, patient's dizziness, tinnitus, vexed, cardiopalmus, irritable, numb limbs and tense tendons, infrequent menstruation, disorder of menstrual cycle, dialectical genus kidney yin is weak, excessive rising of liver-YANG, gives and this Chinese medicine granules, every day 3 times, each 1 bag, after 6 days, symptom takes a turn for the better, and continues to strengthen 7, and all diseases are eliminated, drug withdrawal.
2, in certain, female, 53 years old, menopause 2 years, the course of disease 3 years, main manifestations is paroxysmal sweating every day, reach more than 10 times, based on above the waist, with irritability, xerostomia, cardiopalmus, insomnia and dreamful sleep, once in extramural hospital treatment, without being clearly better, taking this granule after 7 days, sweating alleviates daytime, still there are 3 ~ 4 times, sleep improvement night, continue to strengthen 14 days, vexed improvement, symptom alleviates.
3, in certain, female, 50 years old, menopause 1 year, paroxysmal sweating every day repeatedly, based on above the waist, with symptoms such as irritability, insomnia and dreamful sleeps, once in institute's treatment, without being clearly better, taking this granule after 5 days, sweating alleviates daytime, still there are 2 ~ 3 times, sleep improvement night, continue to strengthen 14 days, vexed improvement, symptom alleviates.
4, season, female, 46 years old, patient's dizziness, tinnitus, vexed, irritability, numb limbs and tense tendons, disorder of menstrual cycle, the dialectical hepatic and renal YIN deficiency, took this Chinese medicine granules, every day 3 times, and each 1 bag, after 5 days, symptom takes a turn for the better, and continues to strengthen 7, and all diseases are eliminated.
Claims (1)
1. treat a Chinese medicine granules for female menopause symptoms, the raw material composition of described Chinese medicine granules is the parch Cortex Eucommiae 9 grams, Arillus Longan 9 grams, Radix Polygoni Multiflori 9 grams, Semen Cuscutae 12 grams, Fructus Ligustri Lucidi 12 grams, 9 grams, the Radix Rehmanniae, 12 grams, Radix Rehmanniae Preparata, Radix Codonopsis 12 grams, the Radix Astragali 12 grams, Poria cum Radix Pini 9 grams, the Rhizoma Atractylodis Macrocephalae 9 grams, the Radix Paeoniae Alba 12 grams, Radix Curcumae 9 grams, Radix Bupleuri 12 grams, Caulis Polygoni Multiflori 15 grams, Flos Albiziae 12 grams, Radix Salviae Miltiorrhizae 15 grams, Radix Angelicae Sinensis 12 grams, 9 grams, Flos Carthami, 9 grams, Semen Persicae, Rhizoma Cyperi 9 grams, 9 grams, Pericarpium Citri Reticulatae Viride and Fructus Citri Sarcodactylis 12 grams, prepare by the following method: (1) Radix Angelicae Sinensis soaks 1 hour, extracts volatile oil, then obtains volatile oil with anhydrous sodium sulfate drying, then use beta-cyclodextrin inclusion compound with volatile oil extractor, obtained clathrate, for subsequent use, (2) get Fructus Ligustri Lucidi and add 50% ethanol extraction 2 times, each 1 hour, merge medicinal liquid, leave standstill 24 hours, for subsequent use, (3) get Flos Carthami 50% soak with ethanol 24 hours, collect 5 times amount percolates with percolation, leave standstill 24 hours, for subsequent use, (4) Rhizoma Cyperi is ground into coarse powder and Radix Angelicae Sinensis medicinal residues, with appropriate 75% ethanol extraction 2 times, each 1 hour, collects extracting solution, leaves standstill 24 hours, for subsequent use, (5) get (2), (3), supernatant obtained in (4) step, decompression recycling ethanol, is concentrated into 60 DEG C ~ 70 DEG C, and density is the clear paste of 1.03 ~ 1.09, for subsequent use, (6) the parch Cortex Eucommiae, Arillus Longan, Radix Polygoni Multiflori, Semen Cuscutae, the Radix Rehmanniae, Radix Rehmanniae Preparata, Radix Codonopsis, the Radix Astragali, Poria cum Radix Pini, the Rhizoma Atractylodis Macrocephalae, Radix Salviae Miltiorrhizae, Semen Persicae, Pericarpium Citri Reticulatae Viride, Fructus Citri Sarcodactylis, the Radix Paeoniae Alba, Radix Curcumae, Radix Bupleuri, Caulis Polygoni Multiflori, Flos Albiziae and Fructus Ligustri Lucidi, Rhizoma Cyperi, Flos Carthami, Radix Angelicae Sinensis medicinal residues add water and soak 30 minutes in right amount, put into multi-functional extractor effective component extracting 2 times, each 1 hour, merge extractive liquid, being concentrated into 60 DEG C ~ 70 DEG C density is the clear paste of 1.03 ~ 1.09, two parts clear paste of water extraction and alcohol extraction is mixed, stir evenly, add Benexate Hydrochloride obtained in (1) step again, measure its weight, add the lactose of its weight 10% and the mixture of dextrin, in the mixture of wherein lactose and dextrin, the weight ratio of lactose and dextrin is 2: 3, stir and be heated to 80 ~ 90 DEG C, cross 100 mesh sieves, obtain extract powder with spray dryer, namely subpackage obtains granule.
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