CN103168974A - Liquid mildewproof agent for feed and method for avoiding mildew of feed - Google Patents
Liquid mildewproof agent for feed and method for avoiding mildew of feed Download PDFInfo
- Publication number
- CN103168974A CN103168974A CN2013100968094A CN201310096809A CN103168974A CN 103168974 A CN103168974 A CN 103168974A CN 2013100968094 A CN2013100968094 A CN 2013100968094A CN 201310096809 A CN201310096809 A CN 201310096809A CN 103168974 A CN103168974 A CN 103168974A
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- China
- Prior art keywords
- feed
- liquid
- acid
- mildewproof
- water
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
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Links
- 239000007788 liquid Substances 0.000 title claims abstract description 39
- 238000000034 method Methods 0.000 title claims abstract description 9
- XBDQKXXYIPTUBI-UHFFFAOYSA-N dimethylselenoniopropionate Natural products CCC(O)=O XBDQKXXYIPTUBI-UHFFFAOYSA-N 0.000 claims abstract description 28
- WPYMKLBDIGXBTP-UHFFFAOYSA-N benzoic acid Chemical compound OC(=O)C1=CC=CC=C1 WPYMKLBDIGXBTP-UHFFFAOYSA-N 0.000 claims abstract description 24
- BGNXCDMCOKJUMV-UHFFFAOYSA-N Tert-Butylhydroquinone Chemical compound CC(C)(C)C1=CC(O)=CC=C1O BGNXCDMCOKJUMV-UHFFFAOYSA-N 0.000 claims abstract description 23
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims abstract description 19
- 235000019260 propionic acid Nutrition 0.000 claims abstract description 14
- IUVKMZGDUIUOCP-BTNSXGMBSA-N quinbolone Chemical compound O([C@H]1CC[C@H]2[C@H]3[C@@H]([C@]4(C=CC(=O)C=C4CC3)C)CC[C@@]21C)C1=CCCC1 IUVKMZGDUIUOCP-BTNSXGMBSA-N 0.000 claims abstract description 14
- 235000010199 sorbic acid Nutrition 0.000 claims abstract description 13
- 239000005711 Benzoic acid Substances 0.000 claims abstract description 12
- 239000004287 Dehydroacetic acid Substances 0.000 claims abstract description 12
- 235000010233 benzoic acid Nutrition 0.000 claims abstract description 12
- 235000019258 dehydroacetic acid Nutrition 0.000 claims abstract description 12
- JEQRBTDTEKWZBW-UHFFFAOYSA-N dehydroacetic acid Chemical compound CC(=O)C1=C(O)OC(C)=CC1=O JEQRBTDTEKWZBW-UHFFFAOYSA-N 0.000 claims abstract description 12
- 229940061632 dehydroacetic acid Drugs 0.000 claims abstract description 12
- PGRHXDWITVMQBC-UHFFFAOYSA-N dehydroacetic acid Natural products CC(=O)C1C(=O)OC(C)=CC1=O PGRHXDWITVMQBC-UHFFFAOYSA-N 0.000 claims abstract description 12
- BEFDCLMNVWHSGT-UHFFFAOYSA-N ethenylcyclopentane Chemical compound C=CC1CCCC1 BEFDCLMNVWHSGT-UHFFFAOYSA-N 0.000 claims abstract description 12
- 235000010482 polyoxyethylene sorbitan monooleate Nutrition 0.000 claims abstract description 12
- 229920000053 polysorbate 80 Polymers 0.000 claims abstract description 12
- JXKPEJDQGNYQSM-UHFFFAOYSA-M sodium propionate Chemical compound [Na+].CCC([O-])=O JXKPEJDQGNYQSM-UHFFFAOYSA-M 0.000 claims abstract description 12
- 235000010334 sodium propionate Nutrition 0.000 claims abstract description 12
- 239000004324 sodium propionate Substances 0.000 claims abstract description 12
- 229960003212 sodium propionate Drugs 0.000 claims abstract description 12
- 239000004334 sorbic acid Substances 0.000 claims abstract description 12
- 229940075582 sorbic acid Drugs 0.000 claims abstract description 12
- 239000004250 tert-Butylhydroquinone Substances 0.000 claims abstract description 12
- 235000019281 tert-butylhydroquinone Nutrition 0.000 claims abstract description 12
- 239000003112 inhibitor Substances 0.000 claims description 34
- XJMWHXZUIGHOBA-UHFFFAOYSA-N azane;propanoic acid Chemical compound N.CCC(O)=O XJMWHXZUIGHOBA-UHFFFAOYSA-N 0.000 claims description 12
- 238000007865 diluting Methods 0.000 claims description 3
- 238000010790 dilution Methods 0.000 claims description 3
- 239000012895 dilution Substances 0.000 claims description 3
- 230000000694 effects Effects 0.000 abstract description 10
- 239000003795 chemical substances by application Substances 0.000 abstract 12
- KRKNYBCHXYNGOX-UHFFFAOYSA-N citric acid Chemical compound OC(=O)CC(O)(C(O)=O)CC(O)=O KRKNYBCHXYNGOX-UHFFFAOYSA-N 0.000 description 3
- 241000233866 Fungi Species 0.000 description 2
- JVTAAEKCZFNVCJ-UHFFFAOYSA-N lactic acid Chemical compound CC(O)C(O)=O JVTAAEKCZFNVCJ-UHFFFAOYSA-N 0.000 description 2
- 244000144972 livestock Species 0.000 description 2
- 238000004519 manufacturing process Methods 0.000 description 2
- 244000144977 poultry Species 0.000 description 2
- 230000003449 preventive effect Effects 0.000 description 2
- 239000007787 solid Substances 0.000 description 2
- 239000000243 solution Substances 0.000 description 2
- 231100000678 Mycotoxin Toxicity 0.000 description 1
- 235000015165 citric acid Nutrition 0.000 description 1
- 235000019621 digestibility Nutrition 0.000 description 1
- 239000004459 forage Substances 0.000 description 1
- 238000002372 labelling Methods 0.000 description 1
- 239000004310 lactic acid Substances 0.000 description 1
- 235000014655 lactic acid Nutrition 0.000 description 1
- 239000002636 mycotoxin Substances 0.000 description 1
- 235000016709 nutrition Nutrition 0.000 description 1
- 150000007524 organic acids Chemical class 0.000 description 1
- 235000005985 organic acids Nutrition 0.000 description 1
- 230000003647 oxidation Effects 0.000 description 1
- 238000007254 oxidation reaction Methods 0.000 description 1
- 235000019629 palatability Nutrition 0.000 description 1
- 231100000572 poisoning Toxicity 0.000 description 1
- 230000000607 poisoning effect Effects 0.000 description 1
- 239000002994 raw material Substances 0.000 description 1
- 150000003398 sorbic acids Chemical class 0.000 description 1
- 238000003860 storage Methods 0.000 description 1
- 239000004094 surface-active agent Substances 0.000 description 1
- 239000002699 waste material Substances 0.000 description 1
- 238000003809 water extraction Methods 0.000 description 1
- 238000005303 weighing Methods 0.000 description 1
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- Fodder In General (AREA)
Abstract
The invention discloses a liquid mildewproof agent for a feed and a method for avoiding mildew of the feed. The liquid mildewproof agent for the feed comprises the following components: 10-15 of propionic acid, 5-10 of sodium propionate, 8-10 of benzoic acid, 3-5 of sorbic acid, 1-5 of dehydroacetic acid, 30-50 of propionic acid, 1-2 of tween-80, 5-10 of water and 0.5-1 of tert-butyl hydroquinone. When the agent is used, the mildewproof agent and water are mixed according to a mass ratio of 1:(15-20) and diluted to be added into the feed, and 800-850g of the liquid mildewproof agent is correspondingly added in each ton of feed. The liquid mildewproof agent has good distribution consistency in the feed, the water content of a feed finished product can be obviously increased, the liquid mildewproof agent cannot easily cause mildew, and the addition of the liquid mildewproof agent is reduced; the addition of the liquid mildewproof agent is reduced, but a mildewproof effect is improved; and tests on the water and mold number variations of the feed in which the mildewproof agent is added show that the liquid mildewproof agent has mildewproof effect better than that of other liquid mildewproof agents at present.
Description
Technical field
The present invention relates to the improvement of feedstuff mildew technology, specifically refer to a kind of Midew preventive for feed that is in a liquid state and prevent the method for feed mold, belong to the feedstuff mildew technical field.
Background technology
Going mouldy is the phenomenon that the most often faces in feed storage, has a strong impact on product quality, has caused the waste of resource.The harm of feed mold has: the feed caking, and produce peculiar smell and cause the livestock and poultry food refusal, the nutritional labeling loss, digestibility reduces, and mycotoxin causes that livestock and poultry are poisoning even dead.China is vast in territory, and longitude and latitude is crossed over larger, and forage crop plantation skewness weighing apparatus has caused the fluctuation of enterprise production process Raw and finished product feedstuff moisture to change.Therefore, usually face finished product feedstuff moisture in the Feed Enterprise production process and can't reach setting value, directly adding water extraction high-moisture value increases again the risk of going mouldy.
The liquid mould inhibitor is generally added surfactant by wherein one or more such as propionic acid, propionic acid ammonium, lactic acid, citric acid, sorbic acids and is formed as a kind of novel Midew preventive for feed, and generation on the one hand can effectively prevent from going mouldy; Can replenish moisture too low in raw material again on the other hand, thereby make finished product feedstuff moisture reach setting value, more have advantage with respect to traditional solid mould inhibitor.The easy oxidation of existing liquid mould inhibitor and going bad, thus anti-mold effect affected; Although anti-mold effect is good than the solid mould inhibitor, add by mensuration that the variation of Moisture in Feed and fungi count shows after mould inhibitor, its anti-mold effect still needs further raising.Simultaneously, existing liquid mould inhibitor addition is larger, greatly about 1200g left and right/ton, causes feed cost to increase, and also affects the palatability of feed simultaneously.
Summary of the invention
For existing feedstuff mildew technology above shortcomings, the object of the present invention is to provide a kind of feed liquid mould inhibitor that reduces consumption when anti-mold effect improves.
The present invention also provides a kind of method that prevents feed mold simultaneously.
To achieve these goals, the technical solution used in the present invention is such:
Feed liquid mould inhibitor of the present invention is made of each component of following mass parts, propionic acid ammonium 10-15; Sodium propionate 5-10; Benzoic acid 8-10; Sorbic acid 3-5; Dehydroacetic acid 1-5; Propionic acid 30-50; Tween-80 1-2; Water 5-10; TBHQ 0.5-1.
A kind of method that prevents feed mold, with described liquid mould inhibitor and water with 1: the quality of 15-20 is than mixed diluting, then dilution is added in feed with Sprayable, and the liquid mould inhibitor that feed per ton is corresponding is 800-850g.
This liquid mould inhibitor is as a kind of novel mould inhibitor, mainly reach anti-mold effect by the synergy between different organic acids, need be diluted with water when using and be finite concentration, therefore the uniformity that makes the liquid mould inhibitor distribute in feed is better, and anti-mold effect also is better than other existing various mould inhibitors.Simultaneously, this liquid mould inhibitor can significantly improve the moisture of finished feed and be difficult for causing going mouldy.The present invention compares with present other liquid mould inhibitor, and addition reduces, and existing other liquid mould inhibitor addition is approximately the 1200g/ ton, and the present invention only needs the 800-850g/ ton.When consumption reduced, anti-mold effect improved, and added by mensurations that the variation of Moisture in Feed and fungi count shows after mould inhibitor, and this liquid mould inhibitor anti-mold effect is better than present other liquid mould inhibitor.
The specific embodiment
The invention will be further described below in conjunction with the specific embodiment.
Feed liquid mould inhibitor of the present invention is made of each component of following mass parts, propionic acid ammonium 10-15; Sodium propionate 5-10; Benzoic acid 8-10; Sorbic acid 3-5; Dehydroacetic acid 1-5; Propionic acid 30-50; Tween-80 1-2; Water 5-10; TBHQ 0.5-1.
Below provide several liquid mould inhibitor formula (being mass parts) preferred embodiments.
Propionic acid ammonium 13; Sodium propionate 8; Benzoic acid 10; Sorbic acid 3.5; Dehydroacetic acid 2.7; Propionic acid 45; Tween-80 1.8; Water 6; TBHQ 0.6.
Propionic acid ammonium 11; Sodium propionate 5; Benzoic acid 8.5; Sorbic acid 3; Dehydroacetic acid 1.8; Propionic acid 33; Tween-80 1.2; Water 8; TBHQ 0.5.
Propionic acid ammonium 14.5; Sodium propionate 8.8; Benzoic acid 10; Sorbic acid 4.5; Dehydroacetic acid 4.5; Propionic acid 50; Tween-80 2; Water 9.5; TBHQ 0.9.
Propionic acid ammonium 15; Sodium propionate 9.5; Benzoic acid 8; Sorbic acid 5; Dehydroacetic acid 1; Propionic acid 40; Tween-80 1.2; Water 6.8; TBHQ 0.8.
This liquid mould inhibitor using method: with described liquid mould inhibitor and water with 1: 15-20(preferred 1: quality 16-18) is than mixed diluting, then dilution is added in feed with Sprayable, and the liquid mould inhibitor that feed per ton needs is 800-850g.Use by this method, both replenished the moisture in the feed and do not cause going mouldy, the uniformity that makes again the liquid mould inhibitor distribute in feed is better.
Explanation is at last, above embodiment is only unrestricted in order to technical scheme of the present invention to be described, although with reference to preferred embodiment, the present invention is had been described in detail, those of ordinary skill in the art is to be understood that, can modify or be equal to replacement technical scheme of the present invention, and not breaking away from aim and the scope of technical solution of the present invention, it all should be encompassed in the middle of claim scope of the present invention.
Claims (6)
1. feed liquid mould inhibitor, it is characterized in that: each component by following mass parts consists of, propionic acid ammonium 10-15; Sodium propionate 5-10; Benzoic acid 8-10; Sorbic acid 3-5; Dehydroacetic acid 1-5; Propionic acid 30-50; Tween-80 1-2; Water 5-10; TBHQ 0.5-1.
2. feed liquid mould inhibitor according to claim 1, it is characterized in that: each component by following mass parts consists of, propionic acid ammonium 13; Sodium propionate 8; Benzoic acid 10; Sorbic acid 3.5; Dehydroacetic acid 2.7; Propionic acid 45; Tween-80 1.8; Water 6; TBHQ 0.6.
3. feed liquid mould inhibitor according to claim 1, it is characterized in that: each component by following mass parts consists of, propionic acid ammonium 11; Sodium propionate 5; Benzoic acid 8.5; Sorbic acid 3; Dehydroacetic acid 1.8; Propionic acid 33; Tween-80 1.2; Water 8; TBHQ 0.5.
4. feed liquid mould inhibitor according to claim 1, it is characterized in that: each component by following mass parts consists of, propionic acid ammonium 14.5; Sodium propionate 8.8; Benzoic acid 10; Sorbic acid 4.5; Dehydroacetic acid 4.5; Propionic acid 50; Tween-80 2; Water 9.5; TBHQ 0.9.
5. feed liquid mould inhibitor according to claim 1, it is characterized in that: each component by following mass parts consists of, propionic acid ammonium 15; Sodium propionate 9.5; Benzoic acid 8; Sorbic acid 5; Dehydroacetic acid 1; Propionic acid 40; Tween-80 1.2; Water 6.8; TBHQ 0.8.
6. method that prevents feed mold, it is characterized in that: with the arbitrary described liquid mould inhibitor of claim 1-5 and water with 1: the quality of 15-20 compares mixed diluting, dilution is added in feed with Sprayable, the liquid mould inhibitor that feed per ton is corresponding is 800-850g again.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201310096809.4A CN103168974B (en) | 2013-03-25 | 2013-03-25 | Liquid mildewproof agent for feed and method for avoiding mildew of feed |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201310096809.4A CN103168974B (en) | 2013-03-25 | 2013-03-25 | Liquid mildewproof agent for feed and method for avoiding mildew of feed |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| CN103168974A true CN103168974A (en) | 2013-06-26 |
| CN103168974B CN103168974B (en) | 2014-06-11 |
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| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201310096809.4A Active CN103168974B (en) | 2013-03-25 | 2013-03-25 | Liquid mildewproof agent for feed and method for avoiding mildew of feed |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN103168974B (en) |
Cited By (7)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN103988989A (en) * | 2014-04-17 | 2014-08-20 | 上海邦成生物科技有限公司 | Feed liquid mildew inhibitor with mildew inhibition and water retention efficacies |
| CN105341360A (en) * | 2015-12-07 | 2016-02-24 | 重庆华睿隆生物科技有限公司 | Carrier-free propionic acid solid feed mildew preventive and preparation and use thereof |
| CN106819764A (en) * | 2016-12-27 | 2017-06-13 | 新昌县拜瑞珂生物技术有限公司 | It is a kind of with mould proof, water conservation effect feed liquid mildew preventive |
| CN107198084A (en) * | 2017-07-07 | 2017-09-26 | 太仓市荣德生物技术研究所 | A kind of harmless biological mildew inhibitor |
| CN108056357A (en) * | 2017-11-30 | 2018-05-22 | 南宁学院 | A kind of method for preventing feed mold |
| CN109497390A (en) * | 2018-12-28 | 2019-03-22 | 上海邦成生物工程有限公司 | A kind of feed molasses special mildewproof agent and its preparation method and application |
| CN112971001A (en) * | 2019-12-18 | 2021-06-18 | 无锡金杰中盛生物科技有限公司 | Efficient composite mildew inhibitor for feed and preparation method thereof |
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Cited By (8)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN103988989A (en) * | 2014-04-17 | 2014-08-20 | 上海邦成生物科技有限公司 | Feed liquid mildew inhibitor with mildew inhibition and water retention efficacies |
| CN103988989B (en) * | 2014-04-17 | 2016-08-24 | 上海邦成生物工程有限公司 | A kind of feedstuff liquid mildew preventive with mildew-resistant, water conservation effect |
| CN105341360A (en) * | 2015-12-07 | 2016-02-24 | 重庆华睿隆生物科技有限公司 | Carrier-free propionic acid solid feed mildew preventive and preparation and use thereof |
| CN106819764A (en) * | 2016-12-27 | 2017-06-13 | 新昌县拜瑞珂生物技术有限公司 | It is a kind of with mould proof, water conservation effect feed liquid mildew preventive |
| CN107198084A (en) * | 2017-07-07 | 2017-09-26 | 太仓市荣德生物技术研究所 | A kind of harmless biological mildew inhibitor |
| CN108056357A (en) * | 2017-11-30 | 2018-05-22 | 南宁学院 | A kind of method for preventing feed mold |
| CN109497390A (en) * | 2018-12-28 | 2019-03-22 | 上海邦成生物工程有限公司 | A kind of feed molasses special mildewproof agent and its preparation method and application |
| CN112971001A (en) * | 2019-12-18 | 2021-06-18 | 无锡金杰中盛生物科技有限公司 | Efficient composite mildew inhibitor for feed and preparation method thereof |
Also Published As
| Publication number | Publication date |
|---|---|
| CN103168974B (en) | 2014-06-11 |
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Address after: 400063 Mintai Road, Jiguan Shilong Industrial Park, Nanan District, Chongqing Patentee after: CHONGQING MINTAI NEW AGROTECH DEVELOPMENT GROUP Co.,Ltd. Address before: 400063 Mintai Road, Jiguan Shilong Industrial Park, Nanan District, Chongqing Patentee before: CHONGQING MINTAI FLAVOR CHEMICAL CO.,LTD. |
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Denomination of invention: Feed liquid mould inhibitor and method of preventing feed mould Effective date of registration: 20210219 Granted publication date: 20140611 Pledgee: Chongqing Branch of China Everbright Bank Co.,Ltd. Pledgor: CHONGQING MINTAI NEW AGROTECH DEVELOPMENT GROUP Co.,Ltd. Registration number: Y2021500000005 |
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Date of cancellation: 20220307 Granted publication date: 20140611 Pledgee: Chongqing Branch of China Everbright Bank Co.,Ltd. Pledgor: CHONGQING MINTAI NEW AGROTECH DEVELOPMENT GROUP Co.,Ltd. Registration number: Y2021500000005 |
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Denomination of invention: Feed liquid mildew inhibitor and method for preventing feed mildew Effective date of registration: 20220329 Granted publication date: 20140611 Pledgee: Chongqing Branch of China Everbright Bank Co.,Ltd. Pledgor: CHONGQING MINTAI NEW AGROTECH DEVELOPMENT GROUP Co.,Ltd. Registration number: Y2022500000014 |
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Date of cancellation: 20230406 Granted publication date: 20140611 Pledgee: Chongqing Branch of China Everbright Bank Co.,Ltd. Pledgor: CHONGQING MINTAI NEW AGROTECH DEVELOPMENT GROUP Co.,Ltd. Registration number: Y2022500000014 |
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Denomination of invention: Liquid antifungal agents for feed and methods for preventing feed mold Effective date of registration: 20230411 Granted publication date: 20140611 Pledgee: Chongqing Branch of China Everbright Bank Co.,Ltd. Pledgor: CHONGQING MINTAI NEW AGROTECH DEVELOPMENT GROUP Co.,Ltd. Registration number: Y2023500000025 |
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Denomination of invention: Liquid antifungal agents for feed and methods for preventing feed mold Granted publication date: 20140611 Pledgee: Chongqing Branch of China Everbright Bank Co.,Ltd. Pledgor: CHONGQING MINTAI NEW AGROTECH DEVELOPMENT GROUP Co.,Ltd. Registration number: Y2024500000032 |