CN1044035A - Feed for fish and shrimp containing stale-proof and anti-oxygenic agent - Google Patents

Feed for fish and shrimp containing stale-proof and anti-oxygenic agent Download PDF

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Publication number
CN1044035A
CN1044035A CN90100533A CN90100533A CN1044035A CN 1044035 A CN1044035 A CN 1044035A CN 90100533 A CN90100533 A CN 90100533A CN 90100533 A CN90100533 A CN 90100533A CN 1044035 A CN1044035 A CN 1044035A
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China
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antioxidant
feed
fish
proof
bait
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CN90100533A
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CN1018144B (en
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汪锦邦
高学敏
马金城
付晴鸥
李平
靳莉
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Beijing Nutrient Source Research Institute
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Beijing Nutrient Source Research Institute
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Priority to CN90100533A priority Critical patent/CN1018144B/en
Publication of CN1044035A publication Critical patent/CN1044035A/en
Publication of CN1018144B publication Critical patent/CN1018144B/en
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Abstract

The present invention is a kind of fishes and shrimps bait preservation antioxidation additive, and it is the compound preservative by 44.4-49.4%, the composite antioxidant of 0.5-1.5%, and the citric acid synergist of 0.1-0.3%, one-tenth such as the white bole carrier of 50-55% are grouped into.That this prescription has is anticorrosion, anti-oxidant, keep feed nutrient, prolong the bait effect of storage period.In use nontoxic, the nonirritant stink does not influence the quality and the palatability of feed, does not pollute bait and operating environment, and antibacterial antioxidant effect is remarkable, and is with low cost.

Description

Feed for fish and shrimp containing stale-proof and anti-oxygenic agent
What the present invention relates to is a kind of additive of bait feed for fish and shrimp containing stale-proof and anti-oxygenic agent blended together with bait that can make fishes and shrimps bait prevent fat oxidation and nutriment corruption in transportation, storage, preservation process.
Contain abundant nutrition in the fishes and shrimps bait, a lot of prescriptions adopt fresh trash fish, shrimp chaff, scallop etc. to do raw material, allocate soya-bean cake powder, bean dregs, whey, vitamin, trace element, adhesive etc. simultaneously into.These raw materials all contain a large amount of microorganisms again, after being combined together, bait itself has just become the good breeding base of harmful microorganism, and fishes and shrimps are higher to nutritional requirement, very sensitive again to various chemical compositions, so how the preservation of fishes and shrimps bait and manufacture the influence that will consider the each side composite factor keeps feed, prevent that wherein fat oxidation and nutriment corruption are the binomial critical problems.Domestic bigger fishes and shrimps bait processing factory adopts the prescription and the various unicity additive of import mostly at present.These single anticorrisive agents, antioxidant all be not really desirable on antibacterial and antioxidant effect, and cost are than higher.
Purpose of the present invention be exactly to existing can be used for fishes and shrimps bait various anticorrosion, antioxidant is collected, screen.And experiments such as to the two be used, that various accrete selections are carried out is anticorrosion, anti-oxidant, raising, toxicity, thereby select the new mix type preservation antioxidation agent prescription of one group of best collocation.Add in the fishes and shrimps bait, make it can reach best antibacterial anticorrosion and antioxidant effect, and don't influence food quality and palatability, and with low cost.
Fishes and shrimps bait feed anticorrosion antioxidant of the present invention is to be 40-100 purpose white powder comprising Sodium Benzoate by particle
Figure 901005339_IMG1
, sorbic acid (CH 3CH=CHCH=CHCOOH), calcium propionate ((CH 3CH 2CHOO) 2Ca) dehydroacetic acid
Figure 901005339_IMG2
Compound preservative Deng composition; White, the yellow powder shape.Comprising dibutyl hydroxy toluene
Figure 901005339_IMG3
The Chinese dihydropyridine of dwelling
Figure 901005339_IMG4
N-propyl gallate Different-vitamin C Composite antioxidant Deng composition; The white powder citric acid
Figure 901005339_IMG7
, pale powder shape white bole (H 2Al 2Si 2O 8H 2O, Al 2O 32SiO 2H 2O) etc. become to be grouped into.
Each constituent content scope wherein: (percentage by weight)
Compound preservative 44.4-49.4%
Composite antioxidant 0.5-1.5%
Citric acid 0.1-0.3%
White bole 50-55%
Each component summation is 100%.
Wherein each component content of compound preservative is: (percentage by weight)
Sorbic acid 25-30%
Dehydroacetic acid 0-19%
Calcium propionate 23-69%
Sodium Benzoate 0-30%
The summation of each component is 100%
Wherein each component content of composite antioxidant is: dibutyl hydroxy toluene, the Chinese dwell dihydropyridine, n-propyl gallate, different-vitamin C, any two kinds match, respectively account for the 40-60%(percentage by weight).
Each component summation is 100%.
The preparation method of feed for fish and shrimp containing stale-proof and anti-oxygenic agent of the present invention is, earlier above-mentioned various anticorrisive agents, antioxidant, citric acid synergist, white bole carrier are ground into the 40-100 order with pulverizer, then with their respectively in proportion with the premixed of white bole carrier, to evenly mix each other with the anticorrisive agent of carrier again after mixing, and make anticorrisive agent total amount and carrier total amount ratio reach ratio requirement, in the polypropylene plastics pocket of packing into.Antioxidant behind the various premixs is evenly mixed each other with the synergist citric acid, and make antioxidant and synergist total amount and carrier total amount ratio reach ratio requirement, be loaded in the band look polybag.
That this prescription has is anticorrosion, anti-oxidant, keep the feed nutrition composition, prolong the bait effect of storage period.In use nontoxic (1), the nonirritant stink does not influence bait quality and palatability, does not pollute bait and operating environment, and antibacterial antioxidant effect is good, keeps feed to never degenerate in storage period.With low cost.This preparation adds in the fishes and shrimps bait, and is remarkable in duration of storage preservation antioxidation effect to the bait finished product.
Table 1. fungistatic effect
Bacterial classification MIC value
(ppm)
Bacillus subtilis BacSubtilis 500
Bacillus coagulans Baccoaglans 500
Aerogenesis brevibacterium Brevibacterium ammoniagenes 500
Sarcina lutea Sarcina lutea 500
Staphylococcus aureus StaphAureus 500
Excrement produces gives alkali bacterium Alcaligenes faecalis 250
Escherichia coli Ecoli 250
Proteus vulgaris PrVulgaris 1000
Pseudomonas aeruginosa PsAeraginosa 600
Fluorescent pseudomonas PsFluorescens 600
Aspergillus niger (AspNiger) 1000
Aspergillus flavus (AspFlavus) 900
Cluster mould (Penclaviforme) 900
Penicillium expansum (PenExpansum) 900
Penicillium roqueforti (PenRoqueforti) 800
Penicillium urticae (PenUrticae) 900
Penicillium digitatum (PenDigitatum) 800
Penicillium notatum (PenNotatum) 600
Trichoderma viride (Trichoderma Viride) 900
Paecilomyces varioti (PenVarioti) 800
Aspergillus fumigatus (AspFumigatus) 800
Aspergillus oryzae (AspOryzae) 900
Aspergillus parasiticus (AspParasiticus) 800
Aspergillus versicolor (AspVersicolor) 1000
Sickle-like bacteria (FuGraminerarum) 1000
Alternaria (AltiAlternate) 600
MIC value: be illustrated in the various mushrooms of growing in the defined medium and suppressed the least concentration of growing by a certain anticorrisive agent fully.
Table 2. antioxidant effect
Peroxide value The TBA value Carbonyl value Acid value
CK is sample after 1 month 0.145 0.145 2.64 2.64 3431.44 2949.00 53.36 47.01
CK is sample after 50 days 0.579 0.311 3.85 2.67 6603 4706 108 113
Embodiment 1:
(1) with water content at 400 below 0.15% gram calcium propionate, water content is at the gram of 300 1.5% below sorbic acid, water content is at the gram of 288 1.5% below Sodium Benzoate, respectively with after the pulverizing of SF type high speed disintegrator, 40 mesh sieves.
(2) foregoing preservatives after will sieving is evenly mixed in mixer with the white bole carrier that accounts for the weight 50% of anticorrisive agent own respectively.
(3) will evenly mix with the even mixed various anticorrisive agents of white bole again, and add a certain amount of white bole, and make last gross weight reach 1950 grams, packing is put into the polypropylene plastics pocket.
(4) water content is restrained and pulverized 40 mesh sieves respectively in SF type high speed disintegrator at the antioxidant dibutyl hydroxy toluene below 1.0% 5 gram and the antioxidant Chinese dihydropyridine 5 of dwelling.
(5) antioxidant after will sieving carries out premixed with the white bole that accounts for weight 50% own respectively.
(6) 2 gram citric acids are pulverized the back with SF type high speed disintegrator and cross 40 mesh sieves, the citric acid after will sieving again with carry out premixed for the white bole of citric acid weight 50% with mixer.
(7) citric acid behind the antioxidant behind the premix and the premix is evenly mixed in mixer, add a certain amount of white bole, making final weight is 50 grams, in the band look polybag of packing into.
The preservation antioxidation agent of filling a prescription and obtaining thus, proterties is a pale powder, and tart flavour is arranged, and granularity is the 40-100 order, and volume density is 0.74g/ml, moisture<9%, arsenic content<0.60ppm; Lead content is less than 10ppm, and the pH value is 5.5.
Embodiment 2:
Get water content at 238 grams of the calcium propionate below 0.15%, water content is at 289 grams of the sorbic acid below 1.5%, water content is at 300 grams of the Sodium Benzoate below 1.5%, water content is at 150 grams of the dehydroacetic acid below 1.0%, water content is at 10 grams of the n-propyl gallate below 1.0%, different-vitamin C 10 grams, citric acid 3 grams, white bole with above-mentioned each material equivalent, make compound preservative 1950 grams that have the white bole carrier with the compounding method identical, have composite antioxidant 50 grams of carrier and synergist with embodiment 1.Pack packing respectively.
Embodiment 3:
Get water content at 616 grams of the calcium propionate below 0.15%, water content is at 200 grams of the sorbic acid below 1.5%, water content is at 150 grams of the dehydroacetic acid below 1.5%, water content is at 15 grams of the n-propyl gallate below 1.0%, dibutyl hydroxy toluene 15 grams, citric acid 4 grams, white bole with above-mentioned each material gross weight equivalent, make compound preservative 1950 grams that have the white bole carrier with the compounding method identical with embodiment 1, composite antioxidant 50 grams that have carrier and synergist, pack packing respectively.
Appendix:
(1) acute toxicological experiment report.

Claims (6)

1, a kind of feed for fish and shrimp containing stale-proof and anti-oxygenic agent that is grouped into by one-tenth such as anticorrisive agent, antioxidant, synergist, carriers is characterized in that containing: (percentage by weight)
Compound preservative 44.4-49.4%
Composite antioxidant 0.5-1.5%
Citric acid 0.1-0.3%
White bole 50-55%
Each component summation is 100%;
2, feed for fish and shrimp containing stale-proof and anti-oxygenic agent according to claim 1 is characterized in that compound preservative is:
Sorbic acid, dehydroacetic acid, calcium propionate, Sodium Benzoate;
3, compound preservative according to claim 2 is characterized in that: (percentage by weight) sorbic acid 25-30%
Dehydroacetic acid 0-19%
Calcium propionate 23-69%
Sodium Benzoate 0-30%
The summation of each component is 100%;
4, feed for fish and shrimp containing stale-proof and anti-oxygenic agent according to claim 1 is characterized in that composite antioxidant is:
Dibutyl hydroxy toluene, the Chinese dwell dihydropyridine, n-propyl gallate, different-vitamin C;
5, composite antioxidant according to claim 4 is characterized in that: (percentage by weight) dibutyl hydroxy toluene, the Chinese dwell dihydropyridine, n-propyl gallate, different-vitamin C; Any two kinds match, respectively account for 40-60%
Each component summation is 100%;
6, a kind of preparation method of feed for fish and shrimp containing stale-proof and anti-oxygenic agent is characterized in that:
(1) various anticorrisive agents, antioxidant, citric acid synergist, the white bole carrier in will filling a prescription is ground into the 40-100 order with pulverizer, sieves;
(2) material of each after will pulverizing is even with the white bole premixed in proportion respectively;
(3) anticorrisive agent after the premixed is evenly mixed each other pack;
(4) antioxidant after the premixed is evenly mixed each other pack with synergist.
CN90100533A 1990-02-06 1990-02-06 Feed for fish and shrimp containing stale-proof and anti-oxygenic agent Expired CN1018144B (en)

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CN90100533A CN1018144B (en) 1990-02-06 1990-02-06 Feed for fish and shrimp containing stale-proof and anti-oxygenic agent

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Application Number Priority Date Filing Date Title
CN90100533A CN1018144B (en) 1990-02-06 1990-02-06 Feed for fish and shrimp containing stale-proof and anti-oxygenic agent

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CN1044035A true CN1044035A (en) 1990-07-25
CN1018144B CN1018144B (en) 1992-09-09

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Cited By (7)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
FR2748635A1 (en) * 1996-05-20 1997-11-21 Guildali Sa DELAY EFFECT ACIDIFYING ADDITIVES FOR ANIMAL FEEDING AND METHODS OF IMPLEMENTATION
CN1044551C (en) * 1995-04-25 1999-08-11 李侯根 Composite oxidation preventive for fodder and its production method
CN1057197C (en) * 1997-05-21 2000-10-11 李侯根 Compound feed antifermenting and antioxidizing agent and its production process
CN1062422C (en) * 1996-10-21 2001-02-28 浙江德清东立实业总公司 Compound fodder acidulant and its preparation method
CN103168974A (en) * 2013-03-25 2013-06-26 重庆民泰香料化工有限责任公司 Liquid mildewproof agent for feed and method for avoiding mildew of feed
CN108094822A (en) * 2017-12-15 2018-06-01 柳州飞升鹏科技有限公司 A kind of preparation method of feed anticorrosion agent
CN111938028A (en) * 2020-07-27 2020-11-17 惠州市康维健生物科技有限公司 Antioxidant formula for animal feed

Cited By (8)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN1044551C (en) * 1995-04-25 1999-08-11 李侯根 Composite oxidation preventive for fodder and its production method
FR2748635A1 (en) * 1996-05-20 1997-11-21 Guildali Sa DELAY EFFECT ACIDIFYING ADDITIVES FOR ANIMAL FEEDING AND METHODS OF IMPLEMENTATION
CN1062422C (en) * 1996-10-21 2001-02-28 浙江德清东立实业总公司 Compound fodder acidulant and its preparation method
CN1057197C (en) * 1997-05-21 2000-10-11 李侯根 Compound feed antifermenting and antioxidizing agent and its production process
CN103168974A (en) * 2013-03-25 2013-06-26 重庆民泰香料化工有限责任公司 Liquid mildewproof agent for feed and method for avoiding mildew of feed
CN103168974B (en) * 2013-03-25 2014-06-11 重庆民泰香料化工有限责任公司 Liquid mildewproof agent for feed and method for avoiding mildew of feed
CN108094822A (en) * 2017-12-15 2018-06-01 柳州飞升鹏科技有限公司 A kind of preparation method of feed anticorrosion agent
CN111938028A (en) * 2020-07-27 2020-11-17 惠州市康维健生物科技有限公司 Antioxidant formula for animal feed

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