CN103931896A - Feed composite antioxidant and preparing method thereof - Google Patents
Feed composite antioxidant and preparing method thereof Download PDFInfo
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- CN103931896A CN103931896A CN201310024406.9A CN201310024406A CN103931896A CN 103931896 A CN103931896 A CN 103931896A CN 201310024406 A CN201310024406 A CN 201310024406A CN 103931896 A CN103931896 A CN 103931896A
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Abstract
The invention discloses a feed composite antioxidant. The feed composite antioxidant comprises following compounds by weight: 20-35% of an antioxidant, 1-5% of an emulsifier, 1-10% of a synergist and 50-70% of a carrier. The feed composite antioxidant has advantages of significant antioxidation effects, strong efficacy, high performance cost ratio, simple production process, high benefit, low equipment investment, no "three-waste" pollution, and the like.
Description
Technical field
The present invention relates to a kind of composite oxidation preventive for fodder and preparation method thereof.
Background technology
The competition of feed product quality and selling price, the proportion that feed antioxidant accounts in feed is very little, and the cost accounting in raw material is also very low, but larger on quality of the fodder impact.At present, the oxidation in production, storage and transportation of feed and feedstuff is fully subject to everybody attention.The fat-soluble antioxidant of use has di-t-butyl to hydroxy-methylbenzene (BHT), butylhydroxy anisole (BHA), TBHQ (TBHQ), n-propyl gallate (PG) and ethoxyquin (EMQ) etc. both at home and abroad at present.Directly result of use is poor in feed for BHT, uses hell to pay, therefore really not too welcome at feedstuff industry after dissolving.BHA and PG effect are better, but expensive, and the reason due to price when feedstuff industry is used is forbidding.
The effect of composite antioxidant is generally better than single antioxidant kind at present.Juice is being pursued equally by domestic a large amount of enterprises, and What is more is that production firm selects inferior raw material to be processed into composite antioxidant to sell pin.The investigation that recent two decades comes shows, the imported product of some old brand, fresh (ENDOX) of for example Jian Ming company, the guarantor of Ao Teqi company are happy fresh, the cost performance using in feed still can, domestic Shang You feed a part enterprise continues to use.In recent years, the antioxygen peace that Mei Nong company produces enters China's feed antioxidant market, and effect is bad, in fact in antioxygen eutocia product EMQ only 2.65%, BHT only 1.45%, mixed feed at least per ton adds 1kg antioxygen peace, and antioxidant concentration just reaches 41mg/kg, still can have antioxygen preservation.Composite antioxidant in the market, its active constituent content is low, and major part is carrier, but price is not low.Low and the significant feed antioxidant of antioxidant effect of preparation cost seems very necessary as can be seen here.
Summary of the invention
The object of the invention is high in order to solve existing composite oxidation preventive for fodder cost, and weak effect and the problem such as unreasonable of filling a prescription provide low and significant composite antioxidant of antioxidant effect of a kind of cost and preparation method thereof.
The invention provides a kind of composite oxidation preventive for fodder, it comprises the material of following percentage by weight: antioxidant 20% ~ 35%, emulsifying agent 1% ~ 5%, synergist 1% ~ 10%, carrier 50% ~ 70%.
Antioxidant of the present invention is made up of ethoxyquin (EMQ) and TBHQ (TBHQ) and the a-lipoic acid that can be dissolved in ethoxyquin, and the percentage by weight of the each component of antioxidant in composite oxidation preventive for fodder is as follows: ethoxyquin (EMQ) 15% ~ 25%, TBHQ (TBHQ) 3% ~ 12%, a-lipoic acid 1% ~ 5%.
Emulsifying agent of the present invention is glycerin monostearate.
Synergist of the present invention is citric acid.
Carrier of the present invention is 40-60 object zeolite powder and 80-120 object white carbon.The percentage by weight of the each component of carrier in composite oxidation preventive for fodder is as follows: 40-60 object zeolite powder: 15% ~ 30%, 80-120 object white carbon: 35% ~ 55%.
The preparation method of composite oxidation preventive for fodder of the present invention, it is characterized in that: comprise the following steps: step 1: the preparation of antioxidant: get the each component of antioxidant by proportioning and mix, be heated to 60-70 DEG C, other various antioxidants are all dissolved in ethoxyquin, after stirring, obtain oily liquids stand-by; Step 2: the preparation of synergist: get citric acid water by proportioning and dissolve, stand-by after stirring; Step 3: the material of step 1 and step 2 gained is mixed in described ratio, then add emulsifying agent by proportioning, the oily liquids after stirring pressurizes and sprays in the carrier taking by proportioning.
Compared with prior art, composite oxidation preventive for fodder of the present invention possesses following advantage:
1, antioxidant effect is remarkable.Various antioxidant proportionings play the effect of Synergistic, without antagonism, the antioxidant adopting in the present invention all can be dissolved in Main Components EMQ, and there is very strong " stream of wriggling, diffusion, infiltration " performance, can be fully after various antioxidants are mixed with feed in each component fully mix, therefore its antioxidant effect can be given full play to.
2, synergist of the present invention is selected and is referred to as " green feed additive "---citric acid, and it has added effectively the effect that improves antioxidant.
3, emulsifying agent of the present invention is also selected and is referred to as " green feed additive "---glycerin monostearate, and it adds can be distributed in antioxidant synergist to go, improved antioxidant effect.
4, antioxidant Main Components of the present invention is EMQ, and it is cheap and antioxygenic property is good, makes this kind of composite oxidation preventive for fodder cost performance very high.
5, composite antioxidant production technology of the present invention is simple, high efficiency, and equipment investment is few, and pollutes without " three wastes ".
Detailed description of the invention
The object of the invention is high in order to solve existing composite oxidation preventive for fodder cost, and weak effect and the problem such as unreasonable of filling a prescription provide low and significant composite antioxidant of antioxidant effect of a kind of cost and preparation method thereof.
The invention provides a kind of composite oxidation preventive for fodder, it comprises the material of following percentage by weight: antioxidant 20% ~ 35%, emulsifying agent 1% ~ 5%, synergist 1% ~ 10%, carrier 50% ~ 70%.
Antioxidant of the present invention is made up of ethoxyquin (EMQ) and TBHQ (TBHQ) and the a-lipoic acid that can be dissolved in ethoxyquin, and the percentage by weight of the each component of antioxidant in composite oxidation preventive for fodder is as follows: ethoxyquin (EMQ) 15% ~ 25%, TBHQ (TBHQ) 3% ~ 12%, a-lipoic acid 1% ~ 5%.
Emulsifying agent of the present invention is glycerin monostearate.
Synergist of the present invention is citric acid.
Carrier of the present invention is 40-60 object zeolite powder and 80-120 object white carbon.The percentage by weight of the each component of carrier in composite oxidation preventive for fodder is as follows: 40-60 object zeolite powder: 15% ~ 30%, 80-120 object white carbon: 35% ~ 55%.
The preparation method of composite oxidation preventive for fodder of the present invention, it is characterized in that: comprise the following steps: step 1: the preparation of antioxidant: get the each component of antioxidant by proportioning and mix, be heated to 60-70 DEG C, other various antioxidants are all dissolved in ethoxyquin, after stirring, obtain oily liquids stand-by; Step 2: the preparation of synergist: get citric acid water by proportioning and dissolve, stand-by after stirring; Step 3: the material of step 1 and step 2 gained is mixed in described ratio, then add emulsifying agent by proportioning, the oily liquids after stirring pressurizes and sprays in the carrier taking by proportioning.
Wherein, in step 2 for the water that dissolves citric acid for appropriate, it is advisable to dissolve citric acid of being got, water volatilizees being sprayed into after carrier, therefore its consumption can not produce any impact to the cooperation of product compositions of the present invention and character.
Further illustrate the present invention below in conjunction with embodiment:
embodiment 1:
Formula 1:
The preparation method of this composite oxidation preventive for fodder is as follows, step 1: the preparation of antioxidant: get the each component of antioxidant by said ratio and mix, be heated to 60-70 DEG C, other various antioxidants are all dissolved in ethoxyquin, after stirring, obtain oily liquids stand-by; Step 2: the preparation of synergist: get citric acid water by said ratio and dissolve, stand-by after stirring; Step 3: the material of step 1 and step 2 gained is mixed in described ratio, then add emulsifying agent by said ratio, the oily liquids after stirring pressurizes and sprays in the carrier taking by said ratio.
embodiment 2:
Formula 2:
The preparation method of this composite oxidation preventive for fodder is as follows, step 1: the preparation of antioxidant: get the each component of antioxidant by said ratio and mix, be heated to 60-70 DEG C, other various antioxidants are all dissolved in ethoxyquin, after stirring, obtain oily liquids stand-by; Step 2: the preparation of synergist: get citric acid water by said ratio and dissolve, stand-by after stirring; Step 3: the material of step 1 and step 2 gained is mixed in described ratio, then add emulsifying agent by said ratio, the oily liquids after stirring pressurizes and sprays in the carrier taking by said ratio.
embodiment 3:
Formula 3:
The preparation method of this composite oxidation preventive for fodder is as follows, step 1: the preparation of antioxidant: get the each component of antioxidant by said ratio and mix, be heated to 60-70 DEG C, other various antioxidants are all dissolved in ethoxyquin, after stirring, obtain oily liquids stand-by; Step 2: the preparation of synergist: get citric acid water by said ratio and dissolve, stand-by after stirring; Step 3: the material of step 1 and step 2 gained is mixed in described ratio, then add emulsifying agent by said ratio, the oily liquids after stirring pressurizes and sprays in the carrier taking by said ratio.
embodiment 4:
Formula 4:
The preparation method of this composite oxidation preventive for fodder is as follows, step 1: the preparation of antioxidant: get the each component of antioxidant by said ratio and mix, be heated to 60-70 DEG C, other various antioxidants are all dissolved in ethoxyquin, after stirring, obtain oily liquids stand-by; Step 2: the preparation of synergist: get citric acid water by said ratio and dissolve, stand-by after stirring; Step 3: the material of step 1 and step 2 gained is mixed in described ratio, then add emulsifying agent by said ratio, the oily liquids after stirring pressurizes and sprays in the carrier taking by said ratio.
embodiment 5:
Formula 5:
The preparation method of this composite oxidation preventive for fodder is as follows, step 1: the preparation of antioxidant: get the each component of antioxidant by said ratio and mix, be heated to 60-70 DEG C, other various antioxidants are all dissolved in ethoxyquin, after stirring, obtain oily liquids stand-by; Step 2: the preparation of synergist: get citric acid water by said ratio and dissolve, stand-by after stirring; Step 3: the material of step 1 and step 2 gained is mixed in described ratio, then add emulsifying agent by said ratio, the oily liquids after stirring pressurizes and sprays in the carrier taking by said ratio.
embodiment 6:
Formula 6:
The preparation method of this composite oxidation preventive for fodder is as follows, step 1: the preparation of antioxidant: get the each component of antioxidant by said ratio and mix, be heated to 60-70 DEG C, other various antioxidants are all dissolved in ethoxyquin, after stirring, obtain oily liquids stand-by; Step 2: the preparation of synergist: get citric acid water by said ratio and dissolve, stand-by after stirring; Step 3: the material of step 1 and step 2 gained is mixed in described ratio, then add emulsifying agent by said ratio, the oily liquids after stirring pressurizes and sprays in the carrier taking by said ratio.
embodiment 7:
Formula 7:
The preparation method of this composite oxidation preventive for fodder is as follows, step 1: the preparation of antioxidant: get the each component of antioxidant by said ratio and mix, be heated to 60-70 DEG C, other various antioxidants are all dissolved in ethoxyquin, after stirring, obtain oily liquids stand-by; Step 2: the preparation of synergist: get citric acid water by said ratio and dissolve, stand-by after stirring; Step 3: the material of step 1 and step 2 gained is mixed in described ratio, then add emulsifying agent by said ratio, the oily liquids after stirring pressurizes and sprays in the carrier taking by said ratio.
embodiment 8:
Formula 8:
The preparation method of this composite oxidation preventive for fodder is as follows, step 1: the preparation of antioxidant: get the each component of antioxidant by said ratio and mix, be heated to 60-70 DEG C, other various antioxidants are all dissolved in ethoxyquin, after stirring, obtain oily liquids stand-by; Step 2: the preparation of synergist: get citric acid water by said ratio and dissolve, stand-by after stirring; Step 3: the material of step 1 and step 2 gained is mixed in described ratio, then add emulsifying agent by said ratio, the oily liquids after stirring pressurizes and sprays in the carrier taking by said ratio.
embodiment 9:
Formula 9:
The preparation method of this composite oxidation preventive for fodder is as follows, step 1: the preparation of antioxidant: get the each component of antioxidant by said ratio and mix, be heated to 60-70 DEG C, other various antioxidants are all dissolved in ethoxyquin, after stirring, obtain oily liquids stand-by; Step 2: the preparation of synergist: get citric acid water by said ratio and dissolve, stand-by after stirring; Step 3: the material of step 1 and step 2 gained is mixed in described ratio, then add emulsifying agent by said ratio, the oily liquids after stirring pressurizes and sprays in the carrier taking by said ratio.
embodiment 10:
Formula 10:
The preparation method of this composite oxidation preventive for fodder is as follows, step 1: the preparation of antioxidant: get the each component of antioxidant by said ratio and mix, be heated to 60-70 DEG C, other various antioxidants are all dissolved in ethoxyquin, after stirring, obtain oily liquids stand-by; Step 2: the preparation of synergist: get citric acid water by said ratio and dissolve, stand-by after stirring; Step 3: the material of step 1 and step 2 gained is mixed in described ratio, then add emulsifying agent by said ratio, the oily liquids after stirring pressurizes and sprays in the carrier taking by said ratio.
embodiment 11:
Formula 11:
The preparation method of this composite oxidation preventive for fodder is as follows, step 1: the preparation of antioxidant: get the each component of antioxidant by said ratio and mix, be heated to 60-70 DEG C, other various antioxidants are all dissolved in ethoxyquin, after stirring, obtain oily liquids stand-by; Step 2: the preparation of synergist: get citric acid water by said ratio and dissolve, stand-by after stirring; Step 3: the material of step 1 and step 2 gained is mixed in described ratio, then add emulsifying agent by said ratio, the oily liquids after stirring pressurizes and sprays in the carrier taking by said ratio.
Claims (6)
1. a composite oxidation preventive for fodder, is characterized in that: it comprises the material of following percentage by weight: antioxidant 20% ~ 35%, emulsifying agent 1% ~ 5%, synergist 1% ~ 10%, carrier 50% ~ 70%.
2. composite oxidation preventive for fodder according to claim 1, it is characterized in that: described antioxidant is made up of ethoxyquin and TBHQ and the a-lipoic acid that can be dissolved in ethoxyquin, and the percentage by weight of the each component of antioxidant in composite oxidation preventive for fodder is as follows: ethoxyquin: 15% ~ 25%, TBHQ: 3% ~ 12%, a-lipoic acid: 1% ~ 5%.
3. composite oxidation preventive for fodder according to claim 1, is characterized in that: described emulsifying agent is glycerin monostearate.
4. composite oxidation preventive for fodder according to claim 1, is characterized in that: described synergist is citric acid.
5. composite oxidation preventive for fodder according to claim 1, it is characterized in that: described carrier is 40-60 object zeolite powder and 80-120 object white carbon, and the percentage by weight of the each component of carrier in composite oxidation preventive for fodder is as follows: 40-60 object zeolite powder: 15% ~ 30%, 80-120 object white carbon: 35% ~ 55%.
6. the preparation method of the composite oxidation preventive for fodder described in the arbitrary claim of claim 1-5, is characterized in that: comprise the following steps:
Step 1: the preparation of antioxidant: get the each component of antioxidant by proportioning and mix, be heated to 60-70 DEG C, other various antioxidants are all dissolved in ethoxyquin, obtain oily liquids after stirring stand-by;
Step 2: the preparation of synergist: get citric acid water by proportioning and dissolve, stand-by after stirring;
Step 3: the material of step 1 and step 2 gained is mixed in described ratio, then add emulsifying agent by proportioning, the oily liquids after stirring pressurizes and sprays in the carrier taking by proportioning.
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| Application Number | Priority Date | Filing Date | Title |
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| CN201310024406.9A CN103931896B (en) | 2013-01-23 | 2013-01-23 | A kind of composite oxidation preventive for fodder and preparation method thereof |
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| CN201310024406.9A CN103931896B (en) | 2013-01-23 | 2013-01-23 | A kind of composite oxidation preventive for fodder and preparation method thereof |
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| CN103931896A true CN103931896A (en) | 2014-07-23 |
| CN103931896B CN103931896B (en) | 2016-07-06 |
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Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
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| CN105053640A (en) * | 2015-08-06 | 2015-11-18 | 张剑逸 | Antioxidation broiler chicken feed additive and application thereof |
| CN106173188A (en) * | 2015-05-07 | 2016-12-07 | 上海邦成生物工程有限公司 | A kind of composite oxidation preventive for fodder and preparation method thereof |
| CN112155132A (en) * | 2020-09-26 | 2021-01-01 | 北京华阜康生物科技股份有限公司 | High-reproduction feed for laboratory mice and production process thereof |
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| CN112155132A (en) * | 2020-09-26 | 2021-01-01 | 北京华阜康生物科技股份有限公司 | High-reproduction feed for laboratory mice and production process thereof |
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| CN103931896B (en) | 2016-07-06 |
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Effective date of registration: 20200525 Address after: 362000 building 7, phase 1, Siming Industrial Park, Guanqiao Town, Anxi County, Quanzhou City, Fujian Province Patentee after: Quanzhou Mudan Biotechnology Co., Ltd Address before: The Lake District of Xiamen City, Fujian province 361000 Fang Lake Industrial Zone No. 33 CuO she. Patentee before: XIAMEN PEONY FEED SCIENCE AND TECHNOLOGY DEVELOPMENT Co.,Ltd. |