CN103153932A - 回收卤素促进剂和除去高锰酸盐还原化合物的方法 - Google Patents

回收卤素促进剂和除去高锰酸盐还原化合物的方法 Download PDF

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Publication number
CN103153932A
CN103153932A CN2011800492602A CN201180049260A CN103153932A CN 103153932 A CN103153932 A CN 103153932A CN 2011800492602 A CN2011800492602 A CN 2011800492602A CN 201180049260 A CN201180049260 A CN 201180049260A CN 103153932 A CN103153932 A CN 103153932A
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CN
China
Prior art keywords
prc
stream
acetic acid
halogen
halogen promotor
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Pending
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CN2011800492602A
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English (en)
Chinese (zh)
Inventor
G·P·托伦斯
R·兹诺毕利
O·奥伊茵德
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Celanese International Corp
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Celanese International Corp
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Publication of CN103153932A publication Critical patent/CN103153932A/zh
Pending legal-status Critical Current

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    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C51/00—Preparation of carboxylic acids or their salts, halides or anhydrides
    • C07C51/10—Preparation of carboxylic acids or their salts, halides or anhydrides by reaction with carbon monoxide
    • C07C51/12—Preparation of carboxylic acids or their salts, halides or anhydrides by reaction with carbon monoxide on an oxygen-containing group in organic compounds, e.g. alcohols
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D11/00—Solvent extraction
    • B01D11/04—Solvent extraction of solutions which are liquid
    • B01D11/0488—Flow sheets
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D11/00—Solvent extraction
    • B01D11/04—Solvent extraction of solutions which are liquid
    • B01D11/0492—Applications, solvents used
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D3/00—Distillation or related exchange processes in which liquids are contacted with gaseous media, e.g. stripping
    • B01D3/14—Fractional distillation or use of a fractionation or rectification column
    • B01D3/143—Fractional distillation or use of a fractionation or rectification column by two or more of a fractionation, separation or rectification step
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C51/00—Preparation of carboxylic acids or their salts, halides or anhydrides
    • C07C51/42—Separation; Purification; Stabilisation; Use of additives
    • C07C51/43—Separation; Purification; Stabilisation; Use of additives by change of the physical state, e.g. crystallisation
    • C07C51/44—Separation; Purification; Stabilisation; Use of additives by change of the physical state, e.g. crystallisation by distillation
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C51/00—Preparation of carboxylic acids or their salts, halides or anhydrides
    • C07C51/42—Separation; Purification; Stabilisation; Use of additives
    • C07C51/48—Separation; Purification; Stabilisation; Use of additives by liquid-liquid treatment

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  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Engineering & Computer Science (AREA)
  • Oil, Petroleum & Natural Gas (AREA)
  • Crystallography & Structural Chemistry (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
CN2011800492602A 2010-10-13 2011-10-13 回收卤素促进剂和除去高锰酸盐还原化合物的方法 Pending CN103153932A (zh)

Applications Claiming Priority (3)

Application Number Priority Date Filing Date Title
US39273610P 2010-10-13 2010-10-13
US61/392,736 2010-10-13
PCT/US2011/056136 WO2012051411A2 (en) 2010-10-13 2011-10-13 Process for recovering halogen promoters and removing permanganate reducing compounds

Publications (1)

Publication Number Publication Date
CN103153932A true CN103153932A (zh) 2013-06-12

Family

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Family Applications (2)

Application Number Title Priority Date Filing Date
CN2011800492602A Pending CN103153932A (zh) 2010-10-13 2011-10-13 回收卤素促进剂和除去高锰酸盐还原化合物的方法
CN201180049274.4A Expired - Fee Related CN103153933B (zh) 2010-10-13 2011-10-13 回收卤素促进剂和除去高锰酸盐还原化合物的方法

Family Applications After (1)

Application Number Title Priority Date Filing Date
CN201180049274.4A Expired - Fee Related CN103153933B (zh) 2010-10-13 2011-10-13 回收卤素促进剂和除去高锰酸盐还原化合物的方法

Country Status (10)

Country Link
US (3) US9056825B2 (enExample)
EP (2) EP2627625B1 (enExample)
JP (2) JP5995852B2 (enExample)
CN (2) CN103153932A (enExample)
AR (2) AR083442A1 (enExample)
BR (2) BR112013008897B1 (enExample)
RS (2) RS58729B1 (enExample)
SG (2) SG189329A1 (enExample)
TW (2) TWI522344B (enExample)
WO (2) WO2012051411A2 (enExample)

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CN107108440A (zh) * 2014-11-14 2017-08-29 国际人造丝公司 在羰基化方法中减少碘化氢含量

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US8859810B2 (en) * 2012-08-21 2014-10-14 Celanese International Corporation Process for recovering permanganate reducing compounds from an acetic acid production process
WO2014143840A2 (en) 2013-03-15 2014-09-18 Celanese International Corporation Process for separating product gas using carbonylation processes
US9505691B2 (en) 2014-10-02 2016-11-29 Celanese International Corporation Process for producing acetic acid
US9458077B2 (en) 2014-11-14 2016-10-04 Celanese International Corporation Reducing hydrogen iodide content in carbonylation processes
US9302975B1 (en) 2015-07-01 2016-04-05 Celanese International Corporation Process for flashing a reaction medium
US9561994B2 (en) 2015-01-30 2017-02-07 Celanese International Corporation Processes for producing acetic acid
US9487464B2 (en) 2015-01-30 2016-11-08 Celanese International Corporation Processes for producing acetic acid
CN107207392B (zh) 2015-01-30 2021-06-08 国际人造丝公司 生产乙酸的方法
WO2016122727A1 (en) 2015-01-30 2016-08-04 Celanese International Corporation Processes for producing acetic acid
US10413840B2 (en) 2015-02-04 2019-09-17 Celanese International Coporation Process to control HI concentration in residuum stream
US9505696B2 (en) 2015-02-04 2016-11-29 Celanese International Corporation Process to control HI concentration in residuum stream
US9512056B2 (en) 2015-02-04 2016-12-06 Celanese International Corporation Process to control HI concentration in residuum stream
US9382183B1 (en) 2015-07-01 2016-07-05 Celanese International Corporation Process for flashing a reaction medium
JP5952951B1 (ja) * 2015-07-01 2016-07-13 セラニーズ・インターナショナル・コーポレーション 酢酸の製造方法
US9302974B1 (en) 2015-07-01 2016-04-05 Celanese International Corporation Process for producing acetic acid
BR112018074026A2 (pt) * 2016-07-07 2019-02-26 Daicel Corporation processos para separação ou remoção de compostos redutores de permanganato (prc?s) de uma primeira mistura e para produção de ácido acético
WO2019183549A1 (en) 2018-03-23 2019-09-26 Lyondellbasell Acetyls, Llc Removal of permanganate reducing compounds from intermediate gaa process streams
US10710953B2 (en) 2018-03-23 2020-07-14 Lyondellbasell Acetyls, Llc Method for purification of GAA
US20230127564A1 (en) * 2020-04-01 2023-04-27 Celanese International Corporation Processes for removing and/or reducing permanganate reducing compounds and alkyl iodides

Citations (4)

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US4908477A (en) * 1981-02-28 1990-03-13 Basf Aktiengesellschaft Removal of organic iodine compounds from carbonylation products of methanol methyl acetate and dimethyl ether
CN1061400A (zh) * 1990-10-01 1992-05-27 伊斯曼柯达公司 丙酮脱除方法
CN1126195A (zh) * 1994-06-15 1996-07-10 大赛璐化学工业株式会社 高纯乙酸的生产方法
CN101163658A (zh) * 2005-04-28 2008-04-16 塞拉尼斯国际公司 乙酸的制造方法

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US3769329A (en) 1970-03-12 1973-10-30 Monsanto Co Production of carboxylic acids and esters
US5001259A (en) 1984-05-03 1991-03-19 Hoechst Celanese Corporation Methanol carbonylation process
US5026908A (en) 1984-05-03 1991-06-25 Hoechst Celanese Corporation Methanol carbonylation process
US5144068A (en) 1984-05-03 1992-09-01 Hoechst Celanese Corporation Methanol carbonylation process
US4615806B1 (en) 1985-03-07 1994-05-03 Hoechst Co American Removal of iodide compounds from non-aqueous organic media
US4894477A (en) 1986-10-14 1990-01-16 Hoechst Celanese Corporation Process for regenerating a carbonylation catalyst solution to remove corrosion metals and carbonylation of methanol to acetic acid
US5672743A (en) 1993-09-10 1997-09-30 Bp Chemicals Limited Process for the production of acetic acid
BR9606725A (pt) 1995-01-06 1998-01-13 Akzo Nobel Nv Vacina para administração via mucosa eficaz para a proteção de frangos contra a queda de desempenho uso de um agente vivo atenuado de anemia de frango e processo para proteção de frangos contra a queda de desempenho
US5696284A (en) 1995-06-21 1997-12-09 Bp Chemicals Limited Process for the carbonylation of alkyl alcohols and/or reactive derivatives thereof
US6339171B1 (en) 1996-10-18 2002-01-15 Celanese International Corporation Removal or reduction of permanganate reducing compounds and alkyl iodides from a carbonylation process stream
IN192600B (enExample) 1996-10-18 2004-05-08 Hoechst Celanese Corp
GB9625335D0 (en) 1996-12-05 1997-01-22 Bp Chem Int Ltd Process
GB9626317D0 (en) 1996-12-19 1997-02-05 Bp Chem Int Ltd Process
GB9626429D0 (en) 1996-12-19 1997-02-05 Bp Chem Int Ltd Process
GB9626428D0 (en) 1996-12-19 1997-02-05 Bp Chem Int Ltd Process
US6225498B1 (en) 2000-03-24 2001-05-01 Celanese International Corporation Method of removing organic iodides from organic media
US6627770B1 (en) 2000-08-24 2003-09-30 Celanese International Corporation Method and apparatus for sequesting entrained and volatile catalyst species in a carbonylation process
US7005541B2 (en) 2002-12-23 2006-02-28 Celanese International Corporation Low water methanol carbonylation process for high acetic acid production and for water balance control
US7223886B2 (en) 2004-03-02 2007-05-29 Celanese International Corporation Removal of permanganate reducing compounds from methanol carbonylation process stream
US7271293B2 (en) * 2004-03-02 2007-09-18 Celanese International Corporation Control method for process of removing permanganate reducing compounds from methanol carbonylation process
US7223883B2 (en) 2004-03-02 2007-05-29 Celanese International Corporation Removal of permanganate reducing compounds from methanol carbonylation process stream
MX2010011850A (es) 2008-04-29 2010-11-30 Celanese Int Corp Sistema de carbonilacion de metanol que tiene un absorbedor con multiples opciones de disolvente.
US7884237B2 (en) * 2008-11-07 2011-02-08 Celanese International Corp. Methanol carbonylation with improved aldehyde removal

Patent Citations (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US4908477A (en) * 1981-02-28 1990-03-13 Basf Aktiengesellschaft Removal of organic iodine compounds from carbonylation products of methanol methyl acetate and dimethyl ether
CN1061400A (zh) * 1990-10-01 1992-05-27 伊斯曼柯达公司 丙酮脱除方法
CN1126195A (zh) * 1994-06-15 1996-07-10 大赛璐化学工业株式会社 高纯乙酸的生产方法
CN101163658A (zh) * 2005-04-28 2008-04-16 塞拉尼斯国际公司 乙酸的制造方法

Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN107108440A (zh) * 2014-11-14 2017-08-29 国际人造丝公司 在羰基化方法中减少碘化氢含量
CN117105766A (zh) * 2014-11-14 2023-11-24 国际人造丝公司 在羰基化方法中减少碘化氢含量

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Publication number Publication date
US9862669B2 (en) 2018-01-09
RS58425B1 (sr) 2019-04-30
AR083441A1 (es) 2013-02-27
SG189328A1 (en) 2013-05-31
HK1184777A1 (zh) 2014-01-30
EP2627624B1 (en) 2019-02-13
CN103153933B (zh) 2016-01-06
US9216936B2 (en) 2015-12-22
RS58729B1 (sr) 2019-06-28
US20120090981A1 (en) 2012-04-19
WO2012051411A3 (en) 2013-02-21
WO2012051412A2 (en) 2012-04-19
AR083442A1 (es) 2013-02-27
JP5995852B2 (ja) 2016-09-21
JP2014500856A (ja) 2014-01-16
JP2013543514A (ja) 2013-12-05
EP2627624A2 (en) 2013-08-21
BR112013009012A2 (pt) 2016-07-12
JP5995853B2 (ja) 2016-09-21
US9056825B2 (en) 2015-06-16
CN103153933A (zh) 2013-06-12
US20120090980A1 (en) 2012-04-19
EP2627625A2 (en) 2013-08-21
BR112013008897A2 (pt) 2016-06-28
TW201217330A (en) 2012-05-01
TWI527793B (zh) 2016-04-01
US20150274632A1 (en) 2015-10-01
EP2627625B1 (en) 2018-12-05
WO2012051411A2 (en) 2012-04-19
BR112013008897B1 (pt) 2019-01-02
SG189329A1 (en) 2013-05-31
WO2012051412A3 (en) 2013-02-21
TW201229026A (en) 2012-07-16
TWI522344B (zh) 2016-02-21

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