CN103125635B - Preparation method of Syringa pubescens scented tea having liver protection efficacy - Google Patents

Preparation method of Syringa pubescens scented tea having liver protection efficacy Download PDF

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Publication number
CN103125635B
CN103125635B CN201310060752.2A CN201310060752A CN103125635B CN 103125635 B CN103125635 B CN 103125635B CN 201310060752 A CN201310060752 A CN 201310060752A CN 103125635 B CN103125635 B CN 103125635B
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syringa pubescens
flower
subsequent use
syringa
tea
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CN103125635A (en
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邓瑞雪
刘普
尹卫平
高嘉屿
李明
段文录
柴元武
时清亮
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Henan University of Science and Technology
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Abstract

The invention relates to a preparation method of a scented tea, and concretely relates to a preparation method of a Syringa pubescens scented tea having a liver protection efficacy. The Syringa pubescens scented tea is prepared through adding a tea base to Syringa pubescens which is adopted as a raw material, and carrying out material choosing, airing, pretreatment, mixed fumigating, rolling, drying and the like. The prepared Syringa pubescens scented tea provided by the invention has a golden color and a rich fragrance after immersion, and has liver protection and liver fibrosis treatment effects.

Description

A kind of preparation method of the Syringa pubescens jasmine tea with liver-protecting efficacy
Technical field
The present invention relates to a kind of jasmine tea and preparation method thereof, specifically a kind of preparation method of the Syringa pubescens jasmine tea with liver-protecting efficacy.
Background technology
Syringa pubescens ( syringa pubescensturca) be Oleaceae genus syringa, shrub, has another name called daphne lilac, and hair (leaf) cloves, Littleleat Lilac, originate from the ground such as Henan, Hebei, Shaanxi.Find after deliberation, in Syringa pubescens, contain triterpenes, flavonoids and glucoside compound, the content of its glucosides is relatively high, and activity is stronger, has larger research and development to be worth.In Syringa pubescens, be rich in multiple glucoside compound, these compounds have multiple biologically active, and research shows, the glucoside compound obtaining from the extraction of Syringa pubescens has the effect of stronger treatment liver fibrosis.The patent No. is that the patent of invention of ZL201010126938.X has illustrated that the glucoside compound in Syringa pubescens has stronger anti-hepatic fibrosis and hepatoprotective effect; Master's thesis [Li Liying, Weiping YIN, Liu Pu. daphne lilac anti-hepatic fibrosis active ingredient and technical study [D], University Of Science and Technology Of He'nan's master thesis, 2009; Shandong Ford, Li Yuehua. the impact [D] of daphne lilac extract on fibrosis Liver Function and cell factor. Zhengzhou University's master thesis, 2004] also illustrate that the larger position of skilful tinkling of pieces of jade Semi-polarity has stronger anti-hepatic fibrosis and hepatoprotective effect.About the medical treatment of Syringa pubescens and extract thereof, the day by day maturation of research of health-care efficacy, and the product that is the anti-hepatic fibrosis prepared of direct material and hepatoprotective effect about Syringa pubescens never occurs, this has the new herb resource of better treatment and health care how to develop Syringa pubescens, its good medical treatment, health-care efficacy can be applied, significant.Syringa pubescens petal after conventional drying among the people is made tea, but the tea that the petal after this direct airing bubbles out is comparatively dry and astringent, bitter, be difficult to adapt to modern's taste, and because Syringa pubescens corolla part is longer, use traditional tea-manufacturing technology to be difficult to improve and drink mouthfeel and give full play to colored medical value.
Summary of the invention
Technical problem to be solved by this invention is for drinking dry and astringent, bitter after the direct airing of Syringa pubescens petal in prior art, existing tea-manufacturing technology is difficult to be applied on Syringa pubescens, a kind of preparation method of the Syringa pubescens jasmine tea with liver-protecting efficacy is provided, prepared Syringa pubescens jasmine tea makes petal fully mix with tea, and drink conveniently, the tea golden yellow color bubbling out, give off a strong fragrance, drink taste superior, there is the effect that protects the liver preferably and treat liver fibrosis, given full play to the medical value of Syringa pubescens.
The present invention for solving the problems of the technologies described above adopted technical scheme is: a kind of preparation method of the Syringa pubescens jasmine tea with liver-protecting efficacy, and each constituent mass percentage is: Syringa pubescens 90%-95%, tea base 5%-10%, making step is as follows:
(1) select materials: the flower of choosing Syringa pubescens is raw material, impurity elimination, for subsequent use after removal branches and leaves;
(2) airing: step (1) gained Syringa pubescens flower is spread to airing on platform, and while spreading, flower layer thickness is not more than 8cm, airing time 6-8 hour, packs up for subsequent use when, moisture soft to flower qualitative change reaches 60-70%;
(3) pretreatment: will scratch a seam from petal top to bottom through step (2) Syringa pubescens flower after treatment, and the petal after scratching will be paved to slabbing, for subsequent use afterwards;
(4) mixed fumigation: fumigate processing with steam after the step of learning from else's experience (3) Syringa pubescens flower after treatment mixes according to the above ratio with tea base, after stifling 1.5-2.5min, stop passing into steam, leave standstill 0.5-1h, then carry out processed 1.5-2min with the hot blast that temperature is 70-100 ℃, after naturally cooling mixture is for subsequent use;
(5) knead: the step of learning from else's experience (4) mixture after treatment is put into kneading machine and kneaded 15-40min, the Syringa pubescens flower of sheet can curlingly be mixed with tea base, obtain after compound for subsequent use;
(6) dry: the compound that step (5) is obtained is placed in drying plant dries, bake out temperature is 150-180 ℃, after being 10-15%, bake out temperature being adjusted to 80-100 ℃ and continuing to dry to mixture moisture content, to mixture moisture content be 3-4%, afterwards take out get product.
Flower when the Syringa pubescens flower that described step (1) is chosen in selecting materials is Syringa pubescens full-bloom stage.
Beneficial effect:
1. the preparation method of a kind of Syringa pubescens jasmine tea with liver-protecting efficacy provided by the invention, in manufacturing process, the corolla of long tubular is scratched, and be launched into sheet, can avoid tubular corolla to knead time, Hua Yucha is difficult to mix, make the flower of sheet can be good at mixing with tea base is curling, well promote the overall mouthfeel of jasmine tea, and can also avoid tubular corolla low problem of long cylinder tapetum cell destructive rate in the process of kneading, while making to drink, active ingredient and the fragrance of flower can fully be discharged in water;
2. a kind of Syringa pubescens jasmine tea with liver-protecting efficacy provided by the invention and preparation method thereof, after Syringa pubescens being mixed with tea in preparation process, fumigate processing with steam, make the fragrance in Syringa pubescens fully distribute and merge with the fragrance of tea, make the tea golden yellow color bubbling out, give off a strong fragrance, and can make its active ingredient well be dissolved in water, be beneficial to absorption of human body;
3. Syringa pubescens jasmine tea provided by the invention utilizes and in Syringa pubescens, contains triterpenes, flavonoids and glucoside compound, its glucosides has relatively high, the active stronger characteristic of content, after brewing, drink and can improve body immunity, and can treat to a certain extent, repair hepatic injury, prevent human liver's fibrillatable, there is stronger medical care effect, make this plant with very strong herbal function of Syringa pubescens be able to effective exploitation.
The specific embodiment
Illustrate the specific embodiment of the present invention below:
Embodiment mono-
Have a preparation method for the Syringa pubescens jasmine tea of liver-protecting efficacy, each constituent mass percentage is: Syringa pubescens 90%, and tea base 10%, making step is as follows:
(1) select materials: the flower of choosing Syringa pubescens is raw material, impurity elimination, for subsequent use after removal branches and leaves;
(2) airing: step (1) gained Syringa pubescens flower is spread to airing on platform, and while spreading, flower layer thickness is not more than 8cm, 6 hours airing time, packs up for subsequent use when, moisture soft to flower qualitative change reaches 60%;
(3) pretreatment: will scratch a seam from petal top to bottom through step (2) Syringa pubescens flower after treatment, and the petal after scratching will be paved to slabbing, for subsequent use afterwards;
(4) mixed fumigation: fumigate processing with steam after the step of learning from else's experience (3) Syringa pubescens flower after treatment mixes according to the above ratio with tea base, after stifling 1.5min, stop passing into steam, leave standstill 0.5h, then carry out processed 1.5min with the hot blast that temperature is 70-100 ℃, after naturally cooling mixture is for subsequent use;
(5) knead: the step of learning from else's experience (4) mixture after treatment is put into kneading machine and kneaded 15min, the Syringa pubescens flower of sheet can curlingly be mixed with tea base, obtain after compound for subsequent use;
(6) dry: the compound that step (5) is obtained is placed in drying plant dries, bake out temperature is 150-180 ℃, after being 10%, bake out temperature being adjusted to 80-100 ℃ and continuing to dry to mixture moisture content, to mixture moisture content be 3-4%, afterwards take out get product.
Flower when the Syringa pubescens flower that described step (1) is chosen in selecting materials is Syringa pubescens full-bloom stage.
Embodiment bis-
Have a preparation method for the Syringa pubescens jasmine tea of liver-protecting efficacy, each constituent mass percentage is: Syringa pubescens 92%, and tea base 8%, making step is as follows:
(1) select materials: the flower of choosing Syringa pubescens is raw material, impurity elimination, for subsequent use after removal branches and leaves;
(2) airing: step (1) gained Syringa pubescens flower is spread to airing on platform, and while spreading, flower layer thickness is not more than 8cm, 6.5 hours airing time, packs up for subsequent use when, moisture soft to flower qualitative change reaches 62%;
(3) pretreatment: will scratch a seam from petal top to bottom through step (2) Syringa pubescens flower after treatment, and the petal after scratching will be paved to slabbing, for subsequent use afterwards;
(4) mixed fumigation: fumigate processing with steam after the step of learning from else's experience (3) Syringa pubescens flower after treatment mixes according to the above ratio with tea base, after stifling 1.7min, stop passing into steam, leave standstill 0.6h, then carry out processed 1.6min with the hot blast that temperature is 70-100 ℃, after naturally cooling mixture is for subsequent use;
(5) knead: the step of learning from else's experience (4) mixture after treatment is put into kneading machine and kneaded 20 min, the Syringa pubescens flower of sheet can curlingly be mixed with tea base, obtain after compound for subsequent use;
(6) dry: the compound that step (5) is obtained is placed in drying plant dries, bake out temperature is 150-180 ℃, after being 12%, bake out temperature being adjusted to 80-100 ℃ and continuing to dry to mixture moisture content, to mixture moisture content be 3-4%, afterwards take out get product.
Flower when the Syringa pubescens flower that described step (1) is chosen in selecting materials is Syringa pubescens full-bloom stage.
Embodiment tri-
Have a preparation method for the Syringa pubescens jasmine tea of liver-protecting efficacy, each constituent mass percentage is: Syringa pubescens 93%, and tea base 7%, making step is as follows:
(1) select materials: the flower of choosing Syringa pubescens is raw material, impurity elimination, for subsequent use after removal branches and leaves;
(2) airing: step (1) gained Syringa pubescens flower is spread to airing on platform, and while spreading, flower layer thickness is not more than 8cm, 6.8 hours airing time, packs up for subsequent use when, moisture soft to flower qualitative change reaches 60-70%;
(3) pretreatment: will scratch a seam from petal top to bottom through step (2) Syringa pubescens flower after treatment, and the petal after scratching will be paved to slabbing, for subsequent use afterwards;
(4) mixed fumigation: fumigate processing with steam after the step of learning from else's experience (3) Syringa pubescens flower after treatment mixes according to the above ratio with tea base, after stifling 2min, stop passing into steam, leave standstill 0.7h, then carry out processed 1.8min with the hot blast that temperature is 70-100 ℃, after naturally cooling mixture is for subsequent use;
(5) knead: the step of learning from else's experience (4) mixture after treatment is put into kneading machine and kneaded 30min, the Syringa pubescens flower of sheet can curlingly be mixed with tea base, obtain after compound for subsequent use;
(6) dry: the compound that step (5) is obtained is placed in drying plant dries, bake out temperature is 150-180 ℃, after being 13%, bake out temperature being adjusted to 80-100 ℃ and continuing to dry to mixture moisture content, to mixture moisture content be 3-4%, afterwards take out get product.
Flower when the Syringa pubescens flower that described step (1) is chosen in selecting materials is Syringa pubescens full-bloom stage.
Embodiment tetra-
Have a preparation method for the Syringa pubescens jasmine tea of liver-protecting efficacy, each constituent mass percentage is: Syringa pubescens 94%, and tea base 6%, making step is as follows:
(1) select materials: the flower of choosing Syringa pubescens is raw material, impurity elimination, for subsequent use after removal branches and leaves;
(2) airing: step (1) gained Syringa pubescens flower is spread to airing on platform, and while spreading, flower layer thickness is not more than 8cm, 6.9 hours airing time, packs up for subsequent use when, moisture soft to flower qualitative change reaches 60-70%;
(3) pretreatment: will scratch a seam from petal top to bottom through step (2) Syringa pubescens flower after treatment, and the petal after scratching will be paved to slabbing, for subsequent use afterwards;
(4) mixed fumigation: fumigate processing with steam after the step of learning from else's experience (3) Syringa pubescens flower after treatment mixes according to the above ratio with tea base, after stifling 2.2min, stop passing into steam, leave standstill 0.9h, then carry out processed 1.9min with the hot blast that temperature is 70-100 ℃, after naturally cooling mixture is for subsequent use;
(5) knead: the step of learning from else's experience (4) mixture after treatment is put into kneading machine and kneaded 35min, the Syringa pubescens flower of sheet can curlingly be mixed with tea base, obtain after compound for subsequent use;
(6) dry: the compound that step (5) is obtained is placed in drying plant dries, bake out temperature is 150-180 ℃, after being 14%, bake out temperature being adjusted to 80-100 ℃ and continuing to dry to mixture moisture content, to mixture moisture content be 3-4%, afterwards take out get product.
Flower when the Syringa pubescens flower that described step (1) is chosen in selecting materials is Syringa pubescens full-bloom stage.
Embodiment five
Have a preparation method for the Syringa pubescens jasmine tea of liver-protecting efficacy, each constituent mass percentage is: Syringa pubescens 95%, and tea base 5%, making step is as follows:
(1) select materials: the flower of choosing Syringa pubescens is raw material, impurity elimination, for subsequent use after removal branches and leaves;
(2) airing: step (1) gained Syringa pubescens flower is spread to airing on platform, and while spreading, flower layer thickness is not more than 8cm, 8 hours airing time, packs up for subsequent use when, moisture soft to flower qualitative change reaches 60-70%;
(3) pretreatment: will scratch a seam from petal top to bottom through step (2) Syringa pubescens flower after treatment, and the petal after scratching will be paved to slabbing, for subsequent use afterwards;
(4) mixed fumigation: fumigate processing with steam after the step of learning from else's experience (3) Syringa pubescens flower after treatment mixes according to the above ratio with tea base, after stifling 2.5min, stop passing into steam, leave standstill 1h, then carry out processed 2min with the hot blast that temperature is 70-100 ℃, after naturally cooling mixture is for subsequent use;
(5) knead: the step of learning from else's experience (4) mixture after treatment is put into kneading machine and kneaded 40min, the Syringa pubescens flower of sheet can curlingly be mixed with tea base, obtain after compound for subsequent use;
(6) dry: the compound that step (5) is obtained is placed in drying plant dries, bake out temperature is 150-180 ℃, after being 15%, bake out temperature being adjusted to 80-100 ℃ and continuing to dry to mixture moisture content, to mixture moisture content be 3-4%, afterwards take out get product.
Flower when the Syringa pubescens flower that described step (1) is chosen in selecting materials is Syringa pubescens full-bloom stage.
pharmacological evaluation
one, Syringa pubescens jasmine tea anti-hepatic fibrosis experiment
1. experiment material
Adopt according to 1000 grams of the prepared Syringa pubescens jasmine tea of embodiment, steep respectively 3 times with boiling water, each 30 minutes, mix 3 times and soak gained tea, concentrated as test sample under vacuum condition, carbon tetrachloride (is analyzed pure, Tianjin good fortune chemical reagent factory in morning) modeling, adopt silymarin (being produced by German doctor Ma pharmaceutical factory) as positive control, SD level Wistar rat, male and female half and half, body weight 190-250g, random packet, standard feed is fed, freely intake (University Of Science and Technology Of He'nan's Experimental Animal Center provides).
Serum alanine aminotransferase (ALT) kit, serum winter propylhomoserin aminopherase (AST) kit, seralbumin (ALB) kit and serum globulins (GLB) kits (Zhongsheng Beikong Biological Science & Technology Co., Ltd.).
2. test method
By rat random packet, be divided into: (1) normal group: with hypodermic injection vegetable oil, 2 times/week, continue 6 weeks; (2) model group: hypodermic injection CCL 4with vegetable oil 1:1 mixture, 2 times/week, continue 6 weeks; (3) positive controls: hypodermic injection CCL 4with vegetable oil 1:1 mixture, 2 times/week, give silymarin every day, continue 6 weeks; (4) dosage group: use CCL 4with vegetable oil 1:1 mixture, 2 times/week, divide high, medium and low dosage group simultaneously, and give test sample by the amount of 800mg/kg/ days, 400mg/kg/ days, 200mg/kg/ days to high, medium and low dosage group respectively, continue 6 weeks.
3. experimental data and interpretation of result
Figure 2013100607522100002DEST_PATH_IMAGE002
Table
Figure 165456DEST_PATH_IMAGE003
the impact of the concentrated sample of Syringa pubescens jasmine tea on Serum Indexes ALT, AST, Alb, TP, TNF-, IFN-
The effect of anti hepatic fibrosis analysis of sample: * P<0.05 vs Normal group; #p<0.05 vs model control group, experimental result is effective, and result shows: successive administration is after 4 weeks, and known by Serum Indexes between each group is analyzed, Syringa pubescens jasmine tea has the effect of certain inhibition liver fibrosis.
two, Syringa pubescens jasmine tea Chronic Alcohol liver damage reparative experiment
1. experiment material
Adopt according to 1000 grams of the prepared Syringa pubescens jasmine tea of embodiment, steep respectively 3 times with boiling water, each 30 minutes, mix 3 times and soak gained tea, concentrated as test sample under vacuum condition, alcohol (is analyzed pure, Tianjin good fortune chemical reagent factory in morning) modeling, adopt silymarin (being produced by German doctor Ma pharmaceutical factory) as positive control, SD level Wistar rat, male and female half and half, body weight 190-250g, random packet, standard feed is fed, freely intake (University Of Science and Technology Of He'nan's Experimental Animal Center provides).
Serum alanine aminotransferase (ALT) kit, serum winter propylhomoserin aminopherase (AST) kit, seralbumin (ALB) kit and serum globulins (GLB) kits (Zhongsheng Beikong Biological Science & Technology Co., Ltd.).
2. test method
By rat random packet, be divided into: (1) Normal group: with distilled water gavage, 1 times/day, hypodermic injection vegetable oil, 2 times/week, and continue 6 weeks; (2) model group: 10% alcohol+distilled water gavage,, continues 6 weeks by 1 times/day; (3) positive controls: 10% alcohol+distilled water gavage,, in ratio hypodermic injection silymarin+vegetable oil of 1:1,2 times/week, continues 6 weeks by 1 times/day; (4) dosage group: 10% alcohol, gavage is divided high, medium and low dosage group simultaneously, and gives test sample by the amount of 800mg/kg/ days, 400mg/kg/ days, 200mg/kg/ days to high, medium and low dosage group respectively, continues 6 weeks.
3. experimental data and interpretation of result
Figure 2013100607522100002DEST_PATH_IMAGE004
The impact of the concentrated sample of table 2 Syringa pubescens jasmine tea on alcohol induced mice chronic liver injury serum TG, ALT, AST
The protective effect analysis of sample to mouse Chronic Alcohol liver damage: with Normal group comparison, #p<0.05; With relatively * p<0.05 of model control group.Experimental result shows: with the comparison of blank group, model control group mice serum ALT, AST, TG content significantly raise (p<0.05), and in hepatic tissue, TG, MDA content significantly raise; The high, medium and low dosage group of sample can significantly reduce MDA content in mice serum ALT, AST, TG content and hepatic tissue, is dose dependent, proves that Syringa pubescens jasmine tea has certain hepatic injury repair.

Claims (1)

1. have a preparation method for the Syringa pubescens jasmine tea of liver-protecting efficacy, each constituent mass percentage is: Syringa pubescens 90%-95%, tea base 5%-10%, is characterized in that: making step is as follows
(1) select materials: the flower of choosing Syringa pubescens full-bloom stage is raw material, impurity elimination, for subsequent use after removal branches and leaves;
(2) airing: step (1) gained Syringa pubescens flower is spread to airing on platform, and while spreading, flower layer thickness is not more than 8cm, airing time 6-8 hour, packs up for subsequent use when, moisture soft to flower qualitative change reaches 60-70%;
(3) pretreatment: will scratch a seam from petal top to bottom through step (2) Syringa pubescens flower after treatment, and the petal after scratching will be paved to slabbing, for subsequent use afterwards;
(4) mixed fumigation: fumigate processing with steam after the step of learning from else's experience (3) Syringa pubescens flower after treatment mixes according to the above ratio with tea base, after stifling 1.5-2.5min, stop passing into steam, leave standstill 0.5-1h, then carry out processed 1.5-2min with the hot blast that temperature is 70-100 ℃, after naturally cooling mixture is for subsequent use;
(5) knead: the step of learning from else's experience (4) mixture after treatment is put into kneading machine and kneaded 15-40min, the Syringa pubescens flower of sheet can curlingly be mixed with tea base, obtain after compound for subsequent use;
(6) dry: the compound that step (5) is obtained is placed in drying plant dries, bake out temperature is 150-180 ℃, after being 10-15%, bake out temperature being adjusted to 80-100 ℃ and continuing to dry to mixture moisture content, to mixture moisture content be 3-4%, afterwards take out get product.
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CN103636827B (en) * 2013-12-13 2016-05-11 四川省峨眉红茶业有限公司 Rose scent fruity black tea processing method
CN104222434B (en) * 2014-09-30 2016-08-17 河南科技大学 A kind of Syringa pubescens bagged tea with hypotensive effect and preparation method thereof
CN104472804A (en) * 2014-12-12 2015-04-01 河北润升农业科技有限公司 Xanthoceras sorbifolia flower bud tea and preparation method thereof
CN104705452A (en) * 2015-01-19 2015-06-17 蒲绪萍 Method for preparing scented tea by using peony petals

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CN1245089C (en) * 2003-09-09 2006-03-15 江西省蚕桑茶叶研究所 Mulberry leaf deodorization and astringency removal process and mulberry cold tea preparation method
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