CN103124718A - 合成2-取代的-1,4-二苯胺的方法 - Google Patents

合成2-取代的-1,4-二苯胺的方法 Download PDF

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Publication number
CN103124718A
CN103124718A CN201080069340XA CN201080069340A CN103124718A CN 103124718 A CN103124718 A CN 103124718A CN 201080069340X A CN201080069340X A CN 201080069340XA CN 201080069340 A CN201080069340 A CN 201080069340A CN 103124718 A CN103124718 A CN 103124718A
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CN
China
Prior art keywords
alkyl
mixture
nitro
replaces
hydrogenation
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Pending
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CN201080069340XA
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English (en)
Chinese (zh)
Inventor
J·M·加德里克
G·S·加瑞特
B·P·墨菲
G·张
R·E·舒梅特
J·S·安德森
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Procter and Gamble Co
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Procter and Gamble Co
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Application filed by Procter and Gamble Co filed Critical Procter and Gamble Co
Priority to CN201610493921.5A priority Critical patent/CN106117068A/zh
Publication of CN103124718A publication Critical patent/CN103124718A/zh
Pending legal-status Critical Current

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    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C217/00—Compounds containing amino and etherified hydroxy groups bound to the same carbon skeleton
    • C07C217/78—Compounds containing amino and etherified hydroxy groups bound to the same carbon skeleton having amino groups and etherified hydroxy groups bound to carbon atoms of six-membered aromatic rings of the same carbon skeleton
    • C07C217/80—Compounds containing amino and etherified hydroxy groups bound to the same carbon skeleton having amino groups and etherified hydroxy groups bound to carbon atoms of six-membered aromatic rings of the same carbon skeleton having amino groups and etherified hydroxy groups bound to carbon atoms of non-condensed six-membered aromatic rings
    • C07C217/82—Compounds containing amino and etherified hydroxy groups bound to the same carbon skeleton having amino groups and etherified hydroxy groups bound to carbon atoms of six-membered aromatic rings of the same carbon skeleton having amino groups and etherified hydroxy groups bound to carbon atoms of non-condensed six-membered aromatic rings of the same non-condensed six-membered aromatic ring
    • C07C217/84—Compounds containing amino and etherified hydroxy groups bound to the same carbon skeleton having amino groups and etherified hydroxy groups bound to carbon atoms of six-membered aromatic rings of the same carbon skeleton having amino groups and etherified hydroxy groups bound to carbon atoms of non-condensed six-membered aromatic rings of the same non-condensed six-membered aromatic ring the oxygen atom of at least one of the etherified hydroxy groups being further bound to an acyclic carbon atom
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C213/00—Preparation of compounds containing amino and hydroxy, amino and etherified hydroxy or amino and esterified hydroxy groups bound to the same carbon skeleton
    • C07C213/02—Preparation of compounds containing amino and hydroxy, amino and etherified hydroxy or amino and esterified hydroxy groups bound to the same carbon skeleton by reactions involving the formation of amino groups from compounds containing hydroxy groups or etherified or esterified hydroxy groups
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C209/00—Preparation of compounds containing amino groups bound to a carbon skeleton
    • C07C209/04—Preparation of compounds containing amino groups bound to a carbon skeleton by substitution of functional groups by amino groups
    • C07C209/06—Preparation of compounds containing amino groups bound to a carbon skeleton by substitution of functional groups by amino groups by substitution of halogen atoms
    • C07C209/10—Preparation of compounds containing amino groups bound to a carbon skeleton by substitution of functional groups by amino groups by substitution of halogen atoms with formation of amino groups bound to carbon atoms of six-membered aromatic rings or from amines having nitrogen atoms bound to carbon atoms of six-membered aromatic rings
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C209/00—Preparation of compounds containing amino groups bound to a carbon skeleton
    • C07C209/30—Preparation of compounds containing amino groups bound to a carbon skeleton by reduction of nitrogen-to-oxygen or nitrogen-to-nitrogen bonds
    • C07C209/32—Preparation of compounds containing amino groups bound to a carbon skeleton by reduction of nitrogen-to-oxygen or nitrogen-to-nitrogen bonds by reduction of nitro groups

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  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
  • Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)
  • Heterocyclic Carbon Compounds Containing A Hetero Ring Having Oxygen Or Sulfur (AREA)
CN201080069340XA 2010-09-29 2010-12-14 合成2-取代的-1,4-二苯胺的方法 Pending CN103124718A (zh)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN201610493921.5A CN106117068A (zh) 2010-09-29 2010-12-14 合成2‑取代的‑1,4‑二苯胺的方法

Applications Claiming Priority (5)

Application Number Priority Date Filing Date Title
US38772710P 2010-09-29 2010-09-29
US61/387,727 2010-09-29
US41953010P 2010-12-03 2010-12-03
US61/419,530 2010-12-03
PCT/US2010/060241 WO2012050593A1 (en) 2010-09-29 2010-12-14 Methods of synthesizing 2- substituted-1,4-benzenediamine

Related Child Applications (1)

Application Number Title Priority Date Filing Date
CN201610493921.5A Division CN106117068A (zh) 2010-09-29 2010-12-14 合成2‑取代的‑1,4‑二苯胺的方法

Publications (1)

Publication Number Publication Date
CN103124718A true CN103124718A (zh) 2013-05-29

Family

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Family Applications (2)

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CN201080069340XA Pending CN103124718A (zh) 2010-09-29 2010-12-14 合成2-取代的-1,4-二苯胺的方法
CN201610493921.5A Pending CN106117068A (zh) 2010-09-29 2010-12-14 合成2‑取代的‑1,4‑二苯胺的方法

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CN201610493921.5A Pending CN106117068A (zh) 2010-09-29 2010-12-14 合成2‑取代的‑1,4‑二苯胺的方法

Country Status (6)

Country Link
US (2) US8618326B2 (enExample)
EP (1) EP2621888B1 (enExample)
JP (1) JP5654686B2 (enExample)
CN (2) CN103124718A (enExample)
MX (1) MX2013003692A (enExample)
WO (1) WO2012050593A1 (enExample)

Families Citing this family (11)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
EP2621885B1 (en) * 2010-09-29 2014-10-29 The Procter and Gamble Company Methods of synthesizing 2-methoxymethyl-1,4-benzenediamine
US8529637B2 (en) 2011-09-30 2013-09-10 The Procter & Gamble Company Foam oxidative hair colorant composition with the free-base of 1,4-diamino-2-methoxymethyl benzene
US8663340B2 (en) 2012-06-25 2014-03-04 The Procter & Gamble Company Hair colorant compositions comprising 2-methoxymethyl-1,4-diaminobenzene and 2,6-dihydroxyethylaminotoluene, methods, and kits comprising the compositions
EP2912009A1 (en) * 2012-10-26 2015-09-02 The Procter & Gamble Company Process for preparing 2-methoxymethyl-1,4-benzenediamine and salts thereof
EP2912008B1 (en) * 2012-10-26 2020-08-05 Noxell Corporation Process for preparing 2-methoxymethyl-1,4-benzenediamine and salts thereof
EP2926802B1 (en) 2014-04-02 2017-09-27 Noxell Corporation Hair colouring compositions, kits, method, and use thereof
MX366192B (es) 2014-11-04 2019-07-01 Noxell Corp Nueva sintesis telescopica de 2-metoximetil-p-fenilenediamina.
WO2016073274A1 (en) 2014-11-04 2016-05-12 The Procter & Gamble Company Telescoping synthesis of 2-methoxymethyl-p-phenylenediamine
MX374017B (es) 2014-11-04 2020-03-25 Wella Operations Us Llc Procedimiento para la preparacion de 1,4-bencenodiaminas 2-sustituidas y sales de las mismas.
US9587116B2 (en) 2014-11-04 2017-03-07 Noxell Corporation Azo direct dyes and method for dyeing hair using these dyes
US20240390244A1 (en) * 2021-09-30 2024-11-28 Kao Corporation Composition comprising an oxidative dye salt

Citations (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JPS60202847A (ja) * 1984-03-27 1985-10-14 Kao Corp ２，５−ジアミノアルキルベンゼンの製造方法
US4997451A (en) * 1989-04-29 1991-03-05 Wella Aktiengesellschaft Oxidative hair dyeing compositions based on 4-aminophenol derivatives and new 4-aminophenol derivatives
US20030041392A1 (en) * 1999-11-29 2003-03-06 Otto Goettel Process for making 1,4-diamino-2-methoxymethylbenzene and salts thereof and compositions and methods for dyeing keratin fibers containing same
CN101343231A (zh) * 2008-08-21 2009-01-14 苏州市罗森助剂有限公司 一种对硝基苯胺的生产方法
WO2010042834A1 (en) * 2008-10-09 2010-04-15 Anadys Pharmaceuticals, Inc. A method of inhibiting hepatitis c virus by combination of a 5,6-dihydro-1h-pyridin-2-one and one or more additional antiviral compounds
US20100160685A1 (en) * 2008-12-18 2010-06-24 E. I. Du Pont De Nemours And Company Integrated process for the preparation of polybenzimidazole precursors

Family Cites Families (9)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US2048790A (en) * 1933-06-02 1936-07-28 Du Pont Process of producing arylamines of the benzene series
US2273564A (en) 1939-04-21 1942-02-17 Eastman Kodak Co Diamino benzyl alcohols and process for making same
JPS57134449A (en) * 1981-02-13 1982-08-19 Sumitomo Chem Co Ltd Production of nitroaniline
DE3731202A1 (de) 1987-09-17 1989-07-13 Basf Ag Doppelankerreaktivfarbstoffe und benzylsulfonylverbindungen als deren zwischenprodukte
JPH0537420A (ja) 1991-07-31 1993-02-12 Fuji Tec Kk 医療情報無線伝送方法
JPH1112239A (ja) * 1997-06-23 1999-01-19 Kao Corp １−（β−ヒドロキシエチル）−２，５−ジアミノベンゼン又はその塩の製造法
FR2769910B1 (fr) * 1997-10-22 2001-06-15 Oreal Procede de synthese de 2-hydroxyalkyl paraphenylenediamines, nouvelles 2-hydroxyalkyl paraphenylenediamines, leur utilisation pour la teinture d'oxydation, compositions tinctoriales et procedes de teinture
US7445645B2 (en) 2004-02-27 2008-11-04 L'oreal S.A. Ortho-and/or meta-substituted N-alkylhydroxylated secondary para-phenylenediamine compounds, compositions for dyeing keratin fibers comprising such compounds, and processes of dyeing therewith
DE102004031590A1 (de) 2004-06-30 2006-02-16 Henkel Kgaa Phenylpropandiol-Farbstoffprodukte

Patent Citations (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JPS60202847A (ja) * 1984-03-27 1985-10-14 Kao Corp ２，５−ジアミノアルキルベンゼンの製造方法
US4997451A (en) * 1989-04-29 1991-03-05 Wella Aktiengesellschaft Oxidative hair dyeing compositions based on 4-aminophenol derivatives and new 4-aminophenol derivatives
US20030041392A1 (en) * 1999-11-29 2003-03-06 Otto Goettel Process for making 1,4-diamino-2-methoxymethylbenzene and salts thereof and compositions and methods for dyeing keratin fibers containing same
CN101343231A (zh) * 2008-08-21 2009-01-14 苏州市罗森助剂有限公司 一种对硝基苯胺的生产方法
WO2010042834A1 (en) * 2008-10-09 2010-04-15 Anadys Pharmaceuticals, Inc. A method of inhibiting hepatitis c virus by combination of a 5,6-dihydro-1h-pyridin-2-one and one or more additional antiviral compounds
US20100160685A1 (en) * 2008-12-18 2010-06-24 E. I. Du Pont De Nemours And Company Integrated process for the preparation of polybenzimidazole precursors

Non-Patent Citations (1)

* Cited by examiner, † Cited by third party
Title
HANHUI XU，CHRISTIAN WOLF: "Efficient copper-catalyzed coupling of aryl chlorides, bromides and iodides with aqueous ammonia", 《CHEM.COMMUN.》 *

Also Published As

Publication number Publication date
US20140081049A1 (en) 2014-03-20
US20120078016A1 (en) 2012-03-29
JP2013544769A (ja) 2013-12-19
WO2012050593A1 (en) 2012-04-19
MX2013003692A (es) 2013-05-09
JP5654686B2 (ja) 2015-01-14
CN106117068A (zh) 2016-11-16
US8618326B2 (en) 2013-12-31
EP2621888A1 (en) 2013-08-07
US9216945B2 (en) 2015-12-22
EP2621888B1 (en) 2018-09-12

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Application publication date: 20130529