MX366192B - Nueva sintesis telescopica de 2-metoximetil-p-fenilenediamina. - Google Patents
Nueva sintesis telescopica de 2-metoximetil-p-fenilenediamina.Info
- Publication number
- MX366192B MX366192B MX2017005810A MX2017005810A MX366192B MX 366192 B MX366192 B MX 366192B MX 2017005810 A MX2017005810 A MX 2017005810A MX 2017005810 A MX2017005810 A MX 2017005810A MX 366192 B MX366192 B MX 366192B
- Authority
- MX
- Mexico
- Prior art keywords
- methoxymethyl
- phenylenediamine
- telescoping
- telescoping synthesis
- synthesis
- Prior art date
Links
- AVKBLCWBDLLVRL-UHFFFAOYSA-N 2-(methoxymethyl)benzene-1,4-diamine Chemical compound COCC1=CC(N)=CC=C1N AVKBLCWBDLLVRL-UHFFFAOYSA-N 0.000 title abstract 2
- 230000015572 biosynthetic process Effects 0.000 title 1
- 238000003786 synthesis reaction Methods 0.000 title 1
- 238000000034 method Methods 0.000 abstract 3
- 239000003054 catalyst Substances 0.000 abstract 1
- VYFOAVADNIHPTR-UHFFFAOYSA-N isatoic anhydride Chemical compound NC1=CC=CC=C1CO VYFOAVADNIHPTR-UHFFFAOYSA-N 0.000 abstract 1
- 239000000203 mixture Substances 0.000 abstract 1
- 238000004064 recycling Methods 0.000 abstract 1
- 150000003839 salts Chemical class 0.000 abstract 1
- 239000007858 starting material Substances 0.000 abstract 1
- 239000000126 substance Substances 0.000 abstract 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C213/00—Preparation of compounds containing amino and hydroxy, amino and etherified hydroxy or amino and esterified hydroxy groups bound to the same carbon skeleton
- C07C213/02—Preparation of compounds containing amino and hydroxy, amino and etherified hydroxy or amino and esterified hydroxy groups bound to the same carbon skeleton by reactions involving the formation of amino groups from compounds containing hydroxy groups or etherified or esterified hydroxy groups
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C213/00—Preparation of compounds containing amino and hydroxy, amino and etherified hydroxy or amino and esterified hydroxy groups bound to the same carbon skeleton
- C07C213/06—Preparation of compounds containing amino and hydroxy, amino and etherified hydroxy or amino and esterified hydroxy groups bound to the same carbon skeleton from hydroxy amines by reactions involving the etherification or esterification of hydroxy groups
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C245/00—Compounds containing chains of at least two nitrogen atoms with at least one nitrogen-to-nitrogen multiple bond
- C07C245/02—Azo compounds, i.e. compounds having the free valencies of —N=N— groups attached to different atoms, e.g. diazohydroxides
- C07C245/06—Azo compounds, i.e. compounds having the free valencies of —N=N— groups attached to different atoms, e.g. diazohydroxides with nitrogen atoms of azo groups bound to carbon atoms of six-membered aromatic rings
- C07C245/08—Azo compounds, i.e. compounds having the free valencies of —N=N— groups attached to different atoms, e.g. diazohydroxides with nitrogen atoms of azo groups bound to carbon atoms of six-membered aromatic rings with the two nitrogen atoms of azo groups bound to carbon atoms of six-membered aromatic rings, e.g. azobenzene
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C245/00—Compounds containing chains of at least two nitrogen atoms with at least one nitrogen-to-nitrogen multiple bond
- C07C245/02—Azo compounds, i.e. compounds having the free valencies of —N=N— groups attached to different atoms, e.g. diazohydroxides
- C07C245/06—Azo compounds, i.e. compounds having the free valencies of —N=N— groups attached to different atoms, e.g. diazohydroxides with nitrogen atoms of azo groups bound to carbon atoms of six-membered aromatic rings
- C07C245/10—Azo compounds, i.e. compounds having the free valencies of —N=N— groups attached to different atoms, e.g. diazohydroxides with nitrogen atoms of azo groups bound to carbon atoms of six-membered aromatic rings with nitrogen atoms of azo groups bound to carbon atoms of six-membered aromatic rings being part of condensed ring systems
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C245/00—Compounds containing chains of at least two nitrogen atoms with at least one nitrogen-to-nitrogen multiple bond
- C07C245/20—Diazonium compounds
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C245/00—Compounds containing chains of at least two nitrogen atoms with at least one nitrogen-to-nitrogen multiple bond
- C07C245/22—Compounds containing chains of at least two nitrogen atoms with at least one nitrogen-to-nitrogen multiple bond containing chains of three or more nitrogen atoms with one or more nitrogen-to-nitrogen double bonds
- C07C245/24—Chains of only three nitrogen atoms, e.g. diazoamines
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02P—CLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
- Y02P20/00—Technologies relating to chemical industry
- Y02P20/50—Improvements relating to the production of bulk chemicals
- Y02P20/582—Recycling of unreacted starting or intermediate materials
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
- Cosmetics (AREA)
- Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)
Abstract
Un procedimiento telescópico para la preparación de 2-metoximetil-p-fenilendiamina, una de sus sales cosméticamente aceptables, o una mezcla de la misma. El procedimiento de acuerdo con la presente invención es un procedimiento particularmente rentable en el sentido de que evita etapas químicas sofisticadas que requieren equipo especial o catalizadores costosos y porque comprende una etapa de reciclaje de uno de los materiales de partida, a saber 2-hidroximetilanilina.
Applications Claiming Priority (2)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| US201462074952P | 2014-11-04 | 2014-11-04 | |
| PCT/US2015/058046 WO2016073276A1 (en) | 2014-11-04 | 2015-10-29 | Telescoping synthesis of 2-methoxymethyl-p-phenylenediamine |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| MX2017005810A MX2017005810A (es) | 2017-08-02 |
| MX366192B true MX366192B (es) | 2019-07-01 |
Family
ID=54479011
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| MX2017005810A MX366192B (es) | 2014-11-04 | 2015-10-29 | Nueva sintesis telescopica de 2-metoximetil-p-fenilenediamina. |
Country Status (6)
| Country | Link |
|---|---|
| US (1) | US9688609B2 (es) |
| EP (1) | EP3215484B1 (es) |
| JP (1) | JP6383492B2 (es) |
| CN (1) | CN107074739B (es) |
| MX (1) | MX366192B (es) |
| WO (1) | WO2016073276A1 (es) |
Families Citing this family (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| MX366190B (es) | 2014-11-04 | 2019-07-01 | Noxell Corp | Nueva sintesis telescopica de 2-metoximetil-p-fenilenediamina. |
| MX374017B (es) | 2014-11-04 | 2020-03-25 | Wella Operations Us Llc | Procedimiento para la preparacion de 1,4-bencenodiaminas 2-sustituidas y sales de las mismas. |
| WO2023052512A1 (en) * | 2021-09-30 | 2023-04-06 | Kao Corporation | Composition comprising an oxidative dye salt |
| US12396938B2 (en) | 2022-08-31 | 2025-08-26 | L'oreal | Compositions and methods for coloring hair |
| CN117209383B (zh) * | 2023-11-07 | 2024-01-23 | 天津深蓝化工技术有限公司 | 一种苯二胺的制备方法 |
| WO2025099119A1 (en) | 2023-11-10 | 2025-05-15 | Wella Germany Gmbh | A novel and highly cost-efficient telescoping synthesis of 2-methoxymethyl-p-phenylenediamine |
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| US2273564A (en) | 1939-04-21 | 1942-02-17 | Eastman Kodak Co | Diamino benzyl alcohols and process for making same |
| US2528378A (en) | 1947-09-20 | 1950-10-31 | John J Mccabe Jr | Metal salts of substituted quaternary hydroxy cycloimidinic acid metal alcoholates and process for preparation of same |
| US2781354A (en) | 1956-03-26 | 1957-02-12 | John J Mccabe Jr | Imidazoline derivatives and process |
| US4279815A (en) | 1979-01-09 | 1981-07-21 | Herkes Frank E | Production of high-quality aromatic amino azo compounds by the rearrangement of 1,3-diaryl triazenes |
| JPS5936974B2 (ja) * | 1980-11-17 | 1984-09-06 | イ−・アイ・デユ・ポン・ドウ・ヌム−ル・アンド・カンパニ− | p−フエニレンジアミンの製造法 |
| DE3162533D1 (en) * | 1980-11-17 | 1984-04-12 | Du Pont | Production of p-phenylenediamine |
| DE3524329A1 (de) | 1985-07-08 | 1987-01-08 | Henkel Kgaa | Neue aminophenole und deren verwendung in oxidationshaarfaerbemitteln |
| DE3914253A1 (de) | 1989-04-29 | 1990-10-31 | Wella Ag | Oxidationshaarfaerbemittel auf der basis von 4-aminophenol-derivaten sowie neue 4-aminophenol-derivate |
| AU684483B2 (en) | 1992-11-23 | 1997-12-18 | Estee Lauder Inc. | Self-tanning cosmetic compositions and methods of using the same |
| DE19957282C1 (de) | 1999-11-29 | 2001-05-17 | Wella Ag | Verfahren zur Herstellung von 1,4-Diamino-2-methoxymethyl-benzol und dessen Salzen |
| DE10000460B4 (de) | 2000-01-07 | 2004-05-06 | Wella Aktiengesellschaft | Mittel und Verfahren zur Färbung von Haaren |
| DE10032135B4 (de) | 2000-07-01 | 2004-06-03 | Wella Ag | 2,4-Diamino-1-(2-methoxyethoxy)-benzol enthaltendes Mittel und Verfahren zur Färbung von menschlichen Haaren |
| DE20107481U1 (de) | 2001-05-02 | 2001-07-12 | Wella Ag | Mittel zur Färbung keratinischer Fasern |
| US20040018163A1 (en) | 2002-04-29 | 2004-01-29 | Wei Yu | Cosmetic compositions comprising at least one dimethicone, at least one linear hydrocarbon wax and at least one compatibilizing agent |
| JP4156625B2 (ja) | 2003-03-07 | 2008-09-24 | 株式会社マンダム | 中性フェノールオキシダーゼ |
| US7591860B2 (en) | 2004-02-27 | 2009-09-22 | L'oreal, S.A. | N-alkylpolyhydroxylated secondary para-phenylenediamines, dye compositions comprising them, processes, and uses thereof |
| DE102004031590A1 (de) | 2004-06-30 | 2006-02-16 | Henkel Kgaa | Phenylpropandiol-Farbstoffprodukte |
| FR2901794A1 (fr) | 2006-06-01 | 2007-12-07 | Oreal | Composition pour la coloration des fibres keratiniques comprenant un colorant direct diazoique a motif 2-imidazolium |
| FR2909868B1 (fr) | 2006-12-14 | 2009-03-06 | Oreal | Article cosmetique pour la coloration capillaire a sec, son utilisation, procede de mise en oeuvre dudit article |
| US20080160620A1 (en) | 2006-12-28 | 2008-07-03 | United Technologies Corporation | Method for quantitatively determining the dye content in dyed oils |
| CA2576189A1 (en) | 2007-01-29 | 2007-06-11 | The Procter & Gamble Company | Hair dyes comprising 1,4-diamino-2-methoxymethylbenzene |
| WO2008124178A1 (en) | 2007-04-10 | 2008-10-16 | Sun Chemical Corporation | Method and apparatus for determination of pigment color properties in situ |
| US7862822B2 (en) | 2007-09-25 | 2011-01-04 | Elc Management Llc | Extracts from black yeast for whitening skin |
| DE102008061864A1 (de) | 2008-12-15 | 2010-10-21 | Henkel Ag & Co. Kgaa | Neue Entwicklerkomponenten |
| AU2010239437A1 (en) | 2009-04-20 | 2011-11-17 | The Procter & Gamble Company | Keratin dyeing compositions comprising a radical scavenger and use thereof |
| AU2010239440A1 (en) | 2009-04-20 | 2011-11-10 | The Procter & Gamble Company | Keratin dyeing compositions comprising a radical scavenger and a chelant and use thereof |
| FR2945734B1 (fr) | 2009-05-19 | 2011-06-17 | Oreal | Compositon tinctoriale comprenant uine base d'oxydation para-phenylene diamine secondaire et un agent nacrant. |
| FR2945739B1 (fr) | 2009-05-19 | 2011-07-29 | Oreal | Composition tinctoriale comprenant une base d'oxydation para-phenylene diamine secondaire et une base d'oxydation aminopyrazolopyridine |
| FR2945730B1 (fr) | 2009-05-19 | 2012-10-19 | Oreal | Composition tinctoriale comprenant une base d'oxydation para-phenylene diamine secondaire et un corps gras liquide non silicone. |
| FR2945737B1 (fr) | 2009-05-19 | 2011-06-10 | Oreal | Composition tinctoriale comprenant une base d'oxydation para-phenylene diamine secondaire et une base d'oxydation para-amino phenol particuliere |
| WO2010133575A2 (en) | 2009-05-19 | 2010-11-25 | L'oreal | Dyeing composition comprising a secondary para-phenylenediamine oxidation base and a silicone fatty substance or a non-silicone liquid fatty substance |
| WO2010133573A2 (en) | 2009-05-19 | 2010-11-25 | L'oreal | Dyeing composition comprising a secondary para-phenylenediamine oxidation base and a thickening polymer |
| FR2945727B1 (fr) | 2009-05-19 | 2012-08-24 | Oreal | Composition tinctoriale comprenant une base d'oxydation para-phenylene diamine secondaire et un polymere cationique. |
| FR2945726B1 (fr) | 2009-05-19 | 2011-06-10 | Oreal | Composition tinctoriale comprenant une base d'oxydation para-phenylene diamine secondaire et un polymere associatif non ionique, anionique ou cationique. |
| FR2945731B1 (fr) | 2009-05-19 | 2011-06-10 | Oreal | Composition tinctoriale comprenant une base d'oxydation para-phenylene diamine secondaire et une silicone. |
| FR2945742B1 (fr) | 2009-05-19 | 2012-08-17 | Oreal | Composition tinctoriale comprenant une base d'oxydation para-phenylene diamine secondaire et un coupleur benzenique selectionne |
| FR2945740B1 (fr) | 2009-05-19 | 2011-06-10 | Oreal | Composition tinctoriale comprenant une base d'oxydation para-phenylene diamine secondaire et une base d'oxydation diaminopyrazole |
| FR2945735B1 (fr) | 2009-05-19 | 2011-06-17 | Oreal | Composition tinctoriale comprenant une base d'oxydation para-phenylene diamine secondaire et un tensioactif non ionique particulier |
| WO2010133640A2 (en) | 2009-05-19 | 2010-11-25 | L'oreal | Dyeing composition comprising a secondary para-phenylenediamine oxidation base and a heterocyclic oxidation base |
| FR2945736B1 (fr) | 2009-05-19 | 2011-06-10 | Oreal | Composition tinctoriale comprenant une base d'oxydation para-phenylene diamine secondaire et une base d'oxydation para-phenylene diamine selectionnee |
| WO2010133639A1 (en) | 2009-05-19 | 2010-11-25 | L'oreal | Dyeing composition comprising a secondary para-phenylenediamine oxidation base and a selected para-phenylenediamine or para-aminophenol oxidation base |
| FR2945728B1 (fr) | 2009-05-19 | 2012-10-19 | Oreal | Composition tinctoriale comprenant une base d'oxydation para-phenylene diamine secondaire et un polymere anionique epaississant acrylique non associatif. |
| FR2945732B1 (fr) | 2009-05-19 | 2011-06-17 | Oreal | Composition tinctoriale comprenant une base d'oxydation para-phenylene diamine secondaire et un tensioactif a charge cationique. |
| FR2945733B1 (fr) | 2009-05-19 | 2012-08-10 | Oreal | Composition tinctoriale comprenant une base d'oxydation para-phenylene diamine secondaire et un acide ether carboxylique. |
| WO2010133803A1 (fr) | 2009-05-19 | 2010-11-25 | L'oreal | Composition tinctoriale comprenant une base d'oxydation para-phenylene diamine secondaire et un tensioactif particulier |
| FR2945738B1 (fr) | 2009-05-19 | 2011-07-22 | Oreal | Composition tinctoriale comprenant une base d'oxydation para-phenylene diamine secondaire et un acide amine |
| FR2945743B1 (fr) | 2009-05-19 | 2012-09-07 | Oreal | Composition tinctoriale comprenant une base d'oxydation para-phenylene diamine secondaire et un coupleur selectionne |
| WO2010139878A2 (fr) | 2009-05-19 | 2010-12-09 | L'oreal | Composition tinctoriale comprenant une base d'oxydation para-phenylene diamine secondaire et un coupleur selectionne |
| FR2945744B1 (fr) | 2009-05-19 | 2011-06-10 | Oreal | Composition tinctoriale comprenant une base d'oxydation para-phenylene diamine secondaire et un sel de 4-formyl-1-methylquinolinium |
| FR2945741B1 (fr) | 2009-05-19 | 2011-06-10 | Oreal | Composition tinctoriale comprenant une base d'oxydation para-phenylene diamine secondaire et une base diaminopyrazolinone |
| FR2945729B1 (fr) | 2009-05-19 | 2012-10-19 | Oreal | Composition tinctoriale comprenant une base d'oxydation para-phenylene diamine secondaire et un polymere non associatif non cationique a motifs sucres. |
| FR2945756B1 (fr) | 2009-05-20 | 2011-08-05 | Commissariat Energie Atomique | Materiau solide nanocomposite a base d'hexa-et octacyanometallates, son procede de preparation et procede de fixation de polluants mineraux le mettant en oeuvre. |
| FR2946647B1 (fr) | 2009-06-11 | 2011-06-24 | Oreal | Colorants directs azomethiniques ou precurseurs reduits de ces colorants obtenus a partir de para-phenylenediamines secondaires n-alkylaminees, procede de coloration capilaire a partir de ces colorants. |
| FR2946648A1 (fr) | 2009-06-11 | 2010-12-17 | Oreal | Colorants directs azomethiniques n-oxydes ou precurseurs reduits de ces colorants obtenus a partir de para-phenylenediamines secondaires n-alkylaminees, procede de coloration capilaire a partir de ces colorants. |
| US8759589B2 (en) | 2010-09-29 | 2014-06-24 | The Procter & Gamble Company | Methods of synthesizing 2-Methoxymethyl-1,4-benzenediamine |
| CN103124718A (zh) | 2010-09-29 | 2013-05-29 | 宝洁公司 | 合成2-取代的-1,4-二苯胺的方法 |
| MX2013006179A (es) | 2010-12-03 | 2013-07-15 | Procter & Gamble | Proceso para la preparacion de 2-metoximetil-1,4-bencenodiamina, sus derivados y sales de esta. |
| JP6436627B2 (ja) | 2011-02-22 | 2018-12-12 | ノクセル・コーポレーション | 1−ヘキシル−4,5−ジアミノピラゾール及びm−アミノフェノール及びその誘導体を含む酸化染色組成物 |
| JP6433124B2 (ja) | 2011-02-22 | 2018-12-05 | ノクセル・コーポレーション | 1−ヘキシル/ヘプチル−4,5−ジアミノピラゾール及びベンゾ[1,3]ジオキソール−5−イルアミン及びこれらの誘導体を含む、酸化染色組成物 |
| JP2014510053A (ja) | 2011-02-22 | 2014-04-24 | ザ プロクター アンド ギャンブル カンパニー | 1−ヘキシル/へプチル−4,5−ジアミノピラゾール及びベンゼン−1,3−ジアミン及びその誘導体を含む酸化的染色組成物 |
| WO2013058814A1 (en) | 2011-02-22 | 2013-04-25 | The Procter & Gamble Company | Oxidative dyeing compositions comprising an 1-hexyl/heptyl-4,5-diaminopyrazole and a benzene-1,3-diol and derivatives thereof |
| WO2013058816A1 (en) | 2011-02-22 | 2013-04-25 | The Procter & Gamble Company | Oxidative dyeing compositions comprising an 1-hexyl/heptyl-4,5-diaminopyrazole and a 2-aminophenol and derivatives thereof |
| CN103442682B (zh) | 2011-02-22 | 2016-08-31 | 宝洁公司 | 包含1-己基/庚基-4,5-二氨基吡唑和萘-1-酚及其衍生物的氧化性染色组合物 |
| MX2013009685A (es) | 2011-02-22 | 2013-10-28 | Procter & Gamble | Composiciones para teñido oxidativo que comprenden un 1-hexil/heptil-4,5-diaminopirazol y una piridina, y derivados de estos. |
| IN2014DN01618A (es) | 2011-09-30 | 2015-05-15 | Procter & Gamble | |
| US8597670B2 (en) | 2011-12-07 | 2013-12-03 | Avon Products, Inc. | Wash resistant compositions containing aminosilicone |
| MX374017B (es) | 2014-11-04 | 2020-03-25 | Wella Operations Us Llc | Procedimiento para la preparacion de 1,4-bencenodiaminas 2-sustituidas y sales de las mismas. |
| MX366190B (es) | 2014-11-04 | 2019-07-01 | Noxell Corp | Nueva sintesis telescopica de 2-metoximetil-p-fenilenediamina. |
| CN104744272B (zh) * | 2015-03-24 | 2016-09-14 | 浙江鼎龙科技有限公司 | 一种2-(甲氧基甲基)苯基-1,4-二胺的制备方法 |
-
2015
- 2015-10-29 MX MX2017005810A patent/MX366192B/es active IP Right Grant
- 2015-10-29 WO PCT/US2015/058046 patent/WO2016073276A1/en not_active Ceased
- 2015-10-29 US US14/926,163 patent/US9688609B2/en active Active
- 2015-10-29 CN CN201580059802.2A patent/CN107074739B/zh active Active
- 2015-10-29 JP JP2017524383A patent/JP6383492B2/ja active Active
- 2015-10-29 EP EP15791872.3A patent/EP3215484B1/en active Active
Also Published As
| Publication number | Publication date |
|---|---|
| EP3215484B1 (en) | 2019-05-08 |
| US20160122286A1 (en) | 2016-05-05 |
| EP3215484A1 (en) | 2017-09-13 |
| JP6383492B2 (ja) | 2018-08-29 |
| WO2016073276A1 (en) | 2016-05-12 |
| CN107074739A (zh) | 2017-08-18 |
| MX2017005810A (es) | 2017-08-02 |
| US9688609B2 (en) | 2017-06-27 |
| CN107074739B (zh) | 2019-07-26 |
| JP2017534641A (ja) | 2017-11-24 |
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