CN103099285A - Preparation method of dendrobium huoshanense composite fresh juice and oral liquid thereof - Google Patents
Preparation method of dendrobium huoshanense composite fresh juice and oral liquid thereof Download PDFInfo
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Abstract
The invention discloses a preparation method of dendrobium huoshanense composite fresh juice and an oral liquid thereof, wherein the formula comprises the following raw materials in parts by weight: 100 parts of dendrobium huoshanense fresh slices, 10-15 parts of roxburgh anoectochilus terminal bud fresh grass, 5-10 parts of mulberry fresh fruits, 4-8 parts of dragon fruit fresh skin and 10-15 parts of functional oligosaccharide. Composite fresh juice is obtained by the techniques of microwave extraction, biological enzyme decomposition, membrane separation and the like on traditional Chinese medicine, namely dendrobium huoshanense fresh slices which is taken as a raw material, and then the composite fresh juice and the functional oligosaccharide are mixed uniformly, and the oral liquid is prepared through filling and sealing, and high-temperature instant sterilization. According to the preparation method, the additional value of dendrobium huoshanense can be increased; the upgrading of dendrobium huoshanense processing industry can be improved; nutritional health care products with health care effect of dendrobium huoshanense are developed; the health level and the immune function of human beings can be directly improved; the economic benefit of the enterprise is mobilized; and enterprises can develop rapidly and sustainably by assistance.
Description
Technical field
The present invention relates to the processing of its a kind of herbal health care product, particularly relate to the preparation method of the compound bright juice of its a kind of Dendrobidium huoshanness and oral liquid thereof, belong to health food processing technique field.
Background technology
Dendrobidium huoshanness (formal name used at school: the wild Dendrobidium huoshanness of the title of " medicine circle giant panda " Dendrobium huoshanense), is arranged in the world, have another name called a meter dry measure used in former times, apart from the history of modern existing more than 200 year.Originating in the ground such as China Huoshan, is the first protection kind in great special more than 200 Rare Kinds in imminent danger of National modern Chinese medicine.Being the superfine product in medicinal dendrobium, is also the rare traditional Chinese medicine that Huoshan County is exclusive, have the original producton location geographical sign, is described as in history " first of Chinese nine immortal grass ", " healthy soft gold "." legendary god of farming's book on Chinese herbal medicine ", Compendium of Material Medica are all on the books.The contained polysaccharide of Dendrobidium huoshanness can increase substantially the main matter that in human body, SOD(delays senility), at aspects such as strengthening immunity, antifatigue, delay senility and promote cancer cell-apoptosis, obvious effect is arranged, thereby reach the effect of health-care.Except Dendrobidium huoshanness, other medicinal dendrobium (as Huoshan dendrobium candidum and Huoshan Dendrobium Moniliforme etc.) also has similar health care and medical value.
Summary of the invention
The object of the invention is to for the not anti-permanent storage of Dendrobidium huoshanness fresh goods and the situation of taking the loaded down with trivial details decoction of needs, the compound bright juice of a kind of Dendrobidium huoshanness and oral liquid are provided, produce the Normal juice local flavor that namely keeps Dendrobidium huoshanness, have again the oral liquid of health care.
The technical solution used in the present invention is as follows:
The compound bright juice of a kind of Dendrobidium huoshanness and oral liquid thereof is characterized in that: in its formula, the weight portion of each raw material is: the bright bar 100 of Dendrobidium huoshanness, roxburgh anoectochilus terminal bud bright careless 10-15, mulberries fresh fruit 5-10, dragon fruit fresh hide 4-8, functional oligose 10-15.
The preparation method of the compound bright juice of a kind of Dendrobidium huoshanness and oral liquid thereof carries out according to the following step;
(1) choose the bright bar of fresh Dendrobidium huoshanness, the bright grass of roxburgh anoectochilus terminal bud, mulberries fresh fruit, dragon fruit fresh hide, remove foreign material and earth, with drying after clear water rinsing totally, add etc. weight mineral water, send into grinder and carry out break process;
(2) the compound bright juice of the Dendrobidium huoshanness after fragmentation is put into the microwave abstracting tank and extract, the microwave frequency of extraction is 2400-2500MHz, and extraction time is controlled at 5-l0min;
(3) put into the stainless steel enzymatic vessel through the compound bright juice of Dendrobidium huoshanness of microwave abstracting, when adjustment is arrived 55-60 ℃, the neutral cellulase that is 0.1-0.5% that adds compound bright juice weight ratio, the neutral xylanase of 0.1-0.2% and the neutral pectase of 0.1-0.2%, enzymolysis time 120-180min stirs lentamente to compound bright juice in enzymolysis process;
(4) the compound bright juice of Dendrobidium huoshanness after adopting centrifugal separator to enzymolysis carries out separating of compound bright juice and the dregs of a decoction, and the centrifugal separator rotating speed is controlled at 3000-4500r/min, separates and collects without the compound bright juice of the Dendrobidium huoshanness of slag;
(5) solution after separating is under 55-60 ℃ of condition in temperature, under the pressure of 1-2Mpa, the multi-pipeline bundle type micro-hole filter membrane that is 0.2-1.0 μ m with the aperture filters, and removes the macromolecular mass such as remaining albuminate, microorganism, obtains the compound bright juice of Dendrobidium huoshanness of clarification;
(6) get the compound bright juice of Dendrobidium huoshanness and functional oligose mixing of clarification after, with bottle placer can under aseptic environment, compound bright juice can is sealed in the coloured glass bottle of 10 mL, adopt the flash pasteurization machine that the compound bright juice of bottled Dendrobidium huoshanness is sterilized, sterilising temp 115-120 ℃, use steam pressure＜0.78MPa, high-temperature heating time 4-10s namely gets the Dendrobidium huoshanness oral liquid.
Described functional oligose is selected from a kind of in FOS, xylo-oligosaccharide, galactooligosaccharide, oligoisomaltose, iMOS, oligomeric dragon gallbladder sugar and soyabean oligosaccharides.
The preparation method's of the compound bright juice of Dendrobidium huoshanness of the present invention and oral liquid thereof primary raw material is the bright bar of Dendrobidium huoshanness, but is not limited to Dendrobidium huoshanness, also is applicable to the bright bar of other medicinal dendrobiums such as dendrobium candidum and Dendrobium Moniliforme.
The present invention adopts and the bright bar of Dendrobidium huoshanness etc. to be carried out microwave abstracting, biological enzymolysis and the technology such as film separates obtains the compound bright juice of Dendrobidium huoshanness, more compound bright juice is completed the making of oral liquid by technology such as flash pasteurizations.
The present invention adopts microwave-assisted extraction technique in preparation process, utilize frequency electromagnetic waves to penetrate the extraction medium, arrives the inside be extracted material, is dissolved in extraction solution at lower temperature, then obtains to extract material by further filtering and separating.Be extracted the material composition and accelerate to the extractant interfacial diffusion under microwave irradiation effect, thereby make extraction rate improve several times, also reduced simultaneously extraction temperature, guarantee to greatest extent original quality of extraction feed.
Adopted the combination of enzymolysis and membrane separation technique in preparation process, use multiple biology enzyme compounded technology under neutrallty condition, Chinese herbal medicine Dendrobidium huoshanness cell membrane to be hydrolyzed, destroy cell wall structure and make its active ingredient expose, dissolve, be suspended in solvent, thereby reach the purpose of extracting active ingredient in cell.Adopted the micro-filtration technology in preparation process, utilized the Selective Separation of film, hold back albuminate in compound bright juice, bacterium with and other large molecular impurities, with the purpose that reaches purification, separates.
The present invention adopts microwave-assisted extraction technique, biological enzymolysis technology, membrane separation technique to obtain the compound bright juice of Dendrobidium huoshanness.The microwave abstracting time is short, and active ingredient is easy to separate, purifying, and the extraction process cost is low, and has guaranteed that the active ingredient of product is not destroyed; Cellulose, hemicellulose and the pectin of the composite enzymolysis of plants cell of multiple biology enzyme can obviously improve the dissolution rate of Dendrobidium huoshanness physiologically active polysaccharide, and enzymolysis do not change the structure of physiologically active polysaccharide substantially under neutrallty condition; The centrifugal mocromembrane filter process that adds does not need filter aid, and technical process is short, and expense is low, is comparatively cost-effective health drink defecation method.
The present invention is conducive to promote the added value of Dendrobidium huoshanness, promote the upgrading of Dendrobidium huoshanness secondary industry, exploitation Dendrobidium huoshanness nutrient and healthcare products with health role, can directly improve the mankind's the general level of the health and immunologic function, more drive Business Economic Benefit, help Promoting Enterprise fast-developing sustainably.
The specific embodiment
Embodiment: the preparation of the compound bright juice of Dendrobidium huoshanness and oral liquid thereof
Take off the raw material (g) of column weight amount: the bright bar 100g of Dendrobidium huoshanness, roxburgh anoectochilus terminal bud bright careless 12g, mulberries fresh fruit 8g, dragon fruit fresh hide 6g, iMOS 10g.
The preparation method of the compound bright juice of Dendrobidium huoshanness carries out according to the following step;
(1) choose the bright bar of fresh Dendrobidium huoshanness, the bright grass of roxburgh anoectochilus terminal bud, mulberries fresh fruit, dragon fruit fresh hide, remove foreign material and earth, with drying after clear water rinsing totally, add etc. weight mineral water, send into grinder and carry out break process;
(2) the compound bright juice of the Dendrobidium huoshanness after fragmentation is put into the microwave abstracting tank and extract, the microwave frequency of extraction is 2450MHz, and extraction time is controlled at 8min;
(3) put into the stainless steel enzymatic vessel through the compound bright juice of Dendrobidium huoshanness of microwave abstracting, during adjustment to 55 ℃, adding compound bright juice weight ratio is 0.3% neutral cellulase, 0.15% neutral xylanase and 0.2% neutral pectase, enzymolysis time 160min stirs lentamente to compound bright juice in enzymolysis process;
(4) the compound bright juice of Dendrobidium huoshanness after adopting centrifugal separator to enzymolysis carries out separating of compound bright juice and the dregs of a decoction, and the centrifugal separator rotating speed is controlled at 4500r/min, separates and collects without the compound bright juice of the Dendrobidium huoshanness of slag;
(5) solution after separating is under 60 ℃ of conditions in temperature, under the pressure of 1.5Mpa, the multi-pipeline bundle type micro-hole filter membrane that is 0.45 μ m with the aperture filters, and removes the macromolecular mass such as remaining albuminate, microorganism, obtains the compound bright juice of Dendrobidium huoshanness of clarification;
(6) get the compound bright juice of Dendrobidium huoshanness and functional oligose mixing of clarification after, with bottle placer can under aseptic environment, compound bright juice can is sealed in the coloured glass bottle of 10 mL, adopt the flash pasteurization machine that the compound bright juice of bottled Dendrobidium huoshanness is sterilized, 120 ℃ of sterilising temps, use steam pressure 0.65MPa, high-temperature heating time 6s namely gets the Dendrobidium huoshanness oral liquid.
Case 1:
Huang, the man, 42 years old, the discomforts such as, lassitude in loin and legs idle in sense malaise, four limbs in 2011, lassitude were once repeatedly removed the examination in hospital health, did not all find any organic disease, can be exactly often to feel fatigue and weak.After 3 months, conscious fatigue and weak, lassitude in loin and legs etc. are uncomfortable obviously to be improved, and feels energetic through long-term taking oral liquid of the present invention.So far there are no above-mentioned malaise symptoms.
Case 2:
Zeng, the man, 19 years old, in May, 2011, the discomforts such as sensation general fatigue, four limbs burnout, soreness of waist and knee, lassitude, repeated cold, impotence, seminal emission.Repeatedly see a doctor in, doctor trained in Western medicine hospital, through experiment
The chamber checks does not find any organic disease, and doctor's final diagnosis is: immunity function is low, takes chinese-western medicine preparation and treats rear poor effect and take the compound bright juice of Dendrobidium huoshanness of the present invention.Through take this product after half a year spirit be clearly better, the diseases such as impotence, seminal emission are clearly better, the transference cure of repeated cold.
Case 3:
Lee, the female, 31 years old, in September, 2011, the sensation general fatigue was unable, drowsiness, the malaise symptoms such as pale complexion, One's spirits are drooping, irregular menstruation.Through taking the compound bright juice of Dendrobidium huoshanness of the present invention after about half a year, its complexion turns ruddy, spiritual amelioration, and the irregular menstruation situation is obviously improved, and other malaise symptoms all disappear.
Claims (4)
1. the compound bright juice of Dendrobidium huoshanness and oral liquid thereof, it is characterized in that: in its formula, the weight portion of each raw material is: the bright bar 100 of Dendrobidium huoshanness, roxburgh anoectochilus terminal bud bright careless 10-15, mulberries fresh fruit 5-10, dragon fruit fresh hide 4-8, functional oligose 10-15.
2. the preparation method of the compound bright juice of Dendrobidium huoshanness as claimed in claim 1 and oral liquid thereof, is characterized in that comprising the steps:
(1) choose the bright bar of fresh Dendrobidium huoshanness, the bright grass of roxburgh anoectochilus terminal bud, mulberries fresh fruit, dragon fruit fresh hide, remove foreign material and earth, with drying after clear water rinsing totally, add etc. weight mineral water, send into grinder and carry out break process;
(2) the compound bright juice of the Dendrobidium huoshanness after fragmentation is put into the microwave abstracting tank and extract, the microwave frequency of extraction is 2400-2500MHz, and extraction time is controlled at 5-l0min;
(3) put into the stainless steel enzymatic vessel through the compound bright juice of Dendrobidium huoshanness of microwave abstracting, when adjustment is arrived 55-60 ℃, the neutral cellulase that is 0.1-0.5% that adds compound bright juice weight ratio, the neutral xylanase of 0.1-0.2% and the neutral pectase of 0.1-0.2%, enzymolysis time 120-180min stirs lentamente to compound bright juice in enzymolysis process;
(4) the compound bright juice of Dendrobidium huoshanness after adopting centrifugal separator to enzymolysis carries out separating of compound bright juice and the dregs of a decoction, and the centrifugal separator rotating speed is controlled at 3000-4500r/min, separates and collects without the compound bright juice of the Dendrobidium huoshanness of slag;
(5) solution after separating is under 55-60 ℃ of condition in temperature, under the pressure of 1-2Mpa, the multi-pipeline bundle type micro-hole filter membrane that is 0.2-1.0 μ m with the aperture filters, and removes the macromolecular mass such as remaining albuminate, microorganism, obtains the compound bright juice of Dendrobidium huoshanness of clarification;
(6) get the compound bright juice of Dendrobidium huoshanness and functional oligose mixing of clarification after, with bottle placer can under aseptic environment, compound bright juice can is sealed in the coloured glass bottle of 10 mL, adopt the flash pasteurization machine that the compound bright juice of bottled Dendrobidium huoshanness is sterilized, sterilising temp 115-120 ℃, use steam pressure＜0.78MPa, high-temperature heating time 4-10s namely gets the Dendrobidium huoshanness oral liquid.
3. the preparation method of the compound bright juice of Dendrobidium huoshanness according to claim 1 and oral liquid thereof, it is characterized in that, described functional oligose is selected from a kind of in FOS, xylo-oligosaccharide, galactooligosaccharide, oligoisomaltose, iMOS, oligomeric dragon gallbladder sugar and soyabean oligosaccharides.
4. the preparation method of the compound bright juice of described a kind of Dendrobidium huoshanness and oral liquid thereof according to claim 1, it is characterized in that: the preparation method's of the compound bright juice of described a kind of Dendrobidium huoshanness and oral liquid thereof primary raw material is the bright bar of Dendrobidium huoshanness, but be not limited to Dendrobidium huoshanness, also the applicable geography symbol product-dendrobium candidum that Huoshan County, Dendrobidium huoshanness original producton location produces and bright bar of Dendrobium Moniliforme.
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Cited By (9)
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| CN104306732A (en) * | 2014-08-18 | 2015-01-28 | 漳州美利德生物工程有限公司 | A roxburgh anoectochilus terminal bud-dendrobium officinale soft capsule and a preparing method thereof |
| CN105029439A (en) * | 2015-07-30 | 2015-11-11 | 天津农科食品生物科技有限公司 | Processing method for fresh dendrobium officinale oral liquid with effect of reducing blood glucose |
| CN105077272A (en) * | 2015-07-16 | 2015-11-25 | 天津绿新低温科技有限公司 | Preparation method of dendrobium plasmogen oral liquid |
| CN105505666A (en) * | 2014-09-27 | 2016-04-20 | 梁振权 | Brewing method of wine containing dendrobium officinale and mulberries |
| CN106244390A (en) * | 2016-08-05 | 2016-12-21 | 锬酃藏虫草生物科技(深圳)有限公司 | A kind of Herba Dendrobii Cordyceps fermentation original plasm wine and preparation method thereof |
| CN106266614A (en) * | 2016-08-31 | 2017-01-04 | 福建永耕农业开发有限公司 | A kind of Herba Dendrobii health care oral liquid and preparation method thereof |
| CN110432414A (en) * | 2019-08-26 | 2019-11-12 | 九仙尊霍山石斛股份有限公司 | A kind of Dendrobidium huoshanness combined beverage and preparation method thereof adjusting function of human body |
| CN111110642A (en) * | 2020-01-03 | 2020-05-08 | 西安医学院 | Anoectochilus roxburghii polysaccharide dispersible tablet and preparation method thereof |
| CN116035145A (en) * | 2022-12-30 | 2023-05-02 | 安徽迎驾山泉股份有限公司 | Dendrobium huoshanense beverage and preparation method thereof |
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Cited By (10)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN104306732A (en) * | 2014-08-18 | 2015-01-28 | 漳州美利德生物工程有限公司 | A roxburgh anoectochilus terminal bud-dendrobium officinale soft capsule and a preparing method thereof |
| CN104306732B (en) * | 2014-08-18 | 2017-11-07 | 漳州美利德生物工程有限公司 | A kind of golden dry measure used in former times soft capsule and preparation method thereof |
| CN105505666A (en) * | 2014-09-27 | 2016-04-20 | 梁振权 | Brewing method of wine containing dendrobium officinale and mulberries |
| CN105077272A (en) * | 2015-07-16 | 2015-11-25 | 天津绿新低温科技有限公司 | Preparation method of dendrobium plasmogen oral liquid |
| CN105029439A (en) * | 2015-07-30 | 2015-11-11 | 天津农科食品生物科技有限公司 | Processing method for fresh dendrobium officinale oral liquid with effect of reducing blood glucose |
| CN106244390A (en) * | 2016-08-05 | 2016-12-21 | 锬酃藏虫草生物科技(深圳)有限公司 | A kind of Herba Dendrobii Cordyceps fermentation original plasm wine and preparation method thereof |
| CN106266614A (en) * | 2016-08-31 | 2017-01-04 | 福建永耕农业开发有限公司 | A kind of Herba Dendrobii health care oral liquid and preparation method thereof |
| CN110432414A (en) * | 2019-08-26 | 2019-11-12 | 九仙尊霍山石斛股份有限公司 | A kind of Dendrobidium huoshanness combined beverage and preparation method thereof adjusting function of human body |
| CN111110642A (en) * | 2020-01-03 | 2020-05-08 | 西安医学院 | Anoectochilus roxburghii polysaccharide dispersible tablet and preparation method thereof |
| CN116035145A (en) * | 2022-12-30 | 2023-05-02 | 安徽迎驾山泉股份有限公司 | Dendrobium huoshanense beverage and preparation method thereof |
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