CN102922178B - 一种免清洗液体铝助焊剂及其制备方法 - Google Patents
一种免清洗液体铝助焊剂及其制备方法 Download PDFInfo
- Publication number
- CN102922178B CN102922178B CN201210430506.7A CN201210430506A CN102922178B CN 102922178 B CN102922178 B CN 102922178B CN 201210430506 A CN201210430506 A CN 201210430506A CN 102922178 B CN102922178 B CN 102922178B
- Authority
- CN
- China
- Prior art keywords
- cleaning liquid
- fluoride
- scaling powder
- weight percent
- liquid aluminium
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
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- 229910052782 aluminium Inorganic materials 0.000 title claims abstract description 52
- XAGFODPZIPBFFR-UHFFFAOYSA-N aluminium Chemical compound [Al] XAGFODPZIPBFFR-UHFFFAOYSA-N 0.000 title claims abstract description 52
- 238000004140 cleaning Methods 0.000 title claims abstract description 48
- 239000007788 liquid Substances 0.000 title claims abstract description 43
- 238000002360 preparation method Methods 0.000 title claims abstract description 17
- 230000004907 flux Effects 0.000 title abstract description 7
- 238000007716 flux method Methods 0.000 title 1
- AVXURJPOCDRRFD-UHFFFAOYSA-N Hydroxylamine Chemical compound ON AVXURJPOCDRRFD-UHFFFAOYSA-N 0.000 claims abstract description 28
- 239000002904 solvent Substances 0.000 claims abstract description 23
- 230000007797 corrosion Effects 0.000 claims abstract description 20
- 238000005260 corrosion Methods 0.000 claims abstract description 20
- 229910052751 metal Inorganic materials 0.000 claims abstract description 20
- 239000002184 metal Substances 0.000 claims abstract description 20
- 150000003839 salts Chemical class 0.000 claims abstract description 19
- 239000000843 powder Substances 0.000 claims description 45
- 239000004411 aluminium Substances 0.000 claims description 43
- 239000011149 active material Substances 0.000 claims description 38
- 239000000203 mixture Substances 0.000 claims description 33
- KFZMGEQAYNKOFK-UHFFFAOYSA-N Isopropanol Chemical compound CC(C)O KFZMGEQAYNKOFK-UHFFFAOYSA-N 0.000 claims description 27
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 claims description 22
- 238000003756 stirring Methods 0.000 claims description 22
- 238000000034 method Methods 0.000 claims description 20
- 239000012190 activator Substances 0.000 claims description 18
- LYCAIKOWRPUZTN-UHFFFAOYSA-N Ethylene glycol Chemical compound OCCO LYCAIKOWRPUZTN-UHFFFAOYSA-N 0.000 claims description 16
- KRHYYFGTRYWZRS-UHFFFAOYSA-N Fluorane Chemical compound F KRHYYFGTRYWZRS-UHFFFAOYSA-N 0.000 claims description 16
- GLUUGHFHXGJENI-UHFFFAOYSA-N Piperazine Chemical compound C1CNCCN1 GLUUGHFHXGJENI-UHFFFAOYSA-N 0.000 claims description 14
- PQXKHYXIUOZZFA-UHFFFAOYSA-M lithium fluoride Chemical compound [Li+].[F-] PQXKHYXIUOZZFA-UHFFFAOYSA-M 0.000 claims description 14
- PUZPDOWCWNUUKD-UHFFFAOYSA-M sodium fluoride Chemical compound [F-].[Na+] PUZPDOWCWNUUKD-UHFFFAOYSA-M 0.000 claims description 14
- JIAARYAFYJHUJI-UHFFFAOYSA-L zinc dichloride Chemical compound [Cl-].[Cl-].[Zn+2] JIAARYAFYJHUJI-UHFFFAOYSA-L 0.000 claims description 14
- BHHYHSUAOQUXJK-UHFFFAOYSA-L zinc fluoride Chemical compound F[Zn]F BHHYHSUAOQUXJK-UHFFFAOYSA-L 0.000 claims description 14
- 239000007795 chemical reaction product Substances 0.000 claims description 10
- 239000002253 acid Substances 0.000 claims description 9
- CBPYOHALYYGNOE-UHFFFAOYSA-M potassium;3,5-dinitrobenzoate Chemical compound [K+].[O-]C(=O)C1=CC([N+]([O-])=O)=CC([N+]([O-])=O)=C1 CBPYOHALYYGNOE-UHFFFAOYSA-M 0.000 claims description 9
- ILWRPSCZWQJDMK-UHFFFAOYSA-N triethylazanium;chloride Chemical compound Cl.CCN(CC)CC ILWRPSCZWQJDMK-UHFFFAOYSA-N 0.000 claims description 9
- HZAXFHJVJLSVMW-UHFFFAOYSA-N 2-Aminoethan-1-ol Chemical compound NCCO HZAXFHJVJLSVMW-UHFFFAOYSA-N 0.000 claims description 8
- PIICEJLVQHRZGT-UHFFFAOYSA-N Ethylenediamine Chemical compound NCCN PIICEJLVQHRZGT-UHFFFAOYSA-N 0.000 claims description 8
- GSEJCLTVZPLZKY-UHFFFAOYSA-N Triethanolamine Chemical compound OCCN(CCO)CCO GSEJCLTVZPLZKY-UHFFFAOYSA-N 0.000 claims description 8
- ZBCBWPMODOFKDW-UHFFFAOYSA-N diethanolamine Chemical compound OCCNCCO ZBCBWPMODOFKDW-UHFFFAOYSA-N 0.000 claims description 8
- 229940043237 diethanolamine Drugs 0.000 claims description 8
- WGCNASOHLSPBMP-UHFFFAOYSA-N hydroxyacetaldehyde Natural products OCC=O WGCNASOHLSPBMP-UHFFFAOYSA-N 0.000 claims description 8
- 230000008569 process Effects 0.000 claims description 8
- ULWHHBHJGPPBCO-UHFFFAOYSA-N propane-1,1-diol Chemical class CCC(O)O ULWHHBHJGPPBCO-UHFFFAOYSA-N 0.000 claims description 8
- 238000010792 warming Methods 0.000 claims description 8
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 8
- -1 zinc fluoroborate Chemical compound 0.000 claims description 8
- TXUICONDJPYNPY-UHFFFAOYSA-N (1,10,13-trimethyl-3-oxo-4,5,6,7,8,9,11,12,14,15,16,17-dodecahydrocyclopenta[a]phenanthren-17-yl) heptanoate Chemical compound C1CC2CC(=O)C=C(C)C2(C)C2C1C1CCC(OC(=O)CCCCCC)C1(C)CC2 TXUICONDJPYNPY-UHFFFAOYSA-N 0.000 claims description 7
- IRPGOXJVTQTAAN-UHFFFAOYSA-N 2,2,3,3,3-pentafluoropropanal Chemical compound FC(F)(F)C(F)(F)C=O IRPGOXJVTQTAAN-UHFFFAOYSA-N 0.000 claims description 7
- KLZUFWVZNOTSEM-UHFFFAOYSA-K Aluminum fluoride Inorganic materials F[Al](F)F KLZUFWVZNOTSEM-UHFFFAOYSA-K 0.000 claims description 7
- 229910021626 Tin(II) chloride Inorganic materials 0.000 claims description 7
- JHXKRIRFYBPWGE-UHFFFAOYSA-K bismuth chloride Chemical compound Cl[Bi](Cl)Cl JHXKRIRFYBPWGE-UHFFFAOYSA-K 0.000 claims description 7
- ORUIBWPALBXDOA-UHFFFAOYSA-L magnesium fluoride Chemical compound [F-].[F-].[Mg+2] ORUIBWPALBXDOA-UHFFFAOYSA-L 0.000 claims description 7
- 229910001635 magnesium fluoride Inorganic materials 0.000 claims description 7
- 235000013024 sodium fluoride Nutrition 0.000 claims description 7
- 239000011775 sodium fluoride Substances 0.000 claims description 7
- 235000011150 stannous chloride Nutrition 0.000 claims description 7
- 239000001119 stannous chloride Substances 0.000 claims description 7
- ANOBYBYXJXCGBS-UHFFFAOYSA-L stannous fluoride Chemical compound F[Sn]F ANOBYBYXJXCGBS-UHFFFAOYSA-L 0.000 claims description 7
- 229960002799 stannous fluoride Drugs 0.000 claims description 7
- YUOWTJMRMWQJDA-UHFFFAOYSA-J tin(iv) fluoride Chemical compound [F-].[F-].[F-].[F-].[Sn+4] YUOWTJMRMWQJDA-UHFFFAOYSA-J 0.000 claims description 7
- 235000005074 zinc chloride Nutrition 0.000 claims description 7
- 239000011592 zinc chloride Substances 0.000 claims description 7
- 238000003466 welding Methods 0.000 abstract description 26
- 239000013543 active substance Substances 0.000 abstract 3
- 238000010438 heat treatment Methods 0.000 abstract 1
- 239000003112 inhibitor Substances 0.000 abstract 1
- 238000005303 weighing Methods 0.000 abstract 1
- 229910000679 solder Inorganic materials 0.000 description 10
- 239000000047 product Substances 0.000 description 5
- 238000005516 engineering process Methods 0.000 description 4
- 239000000463 material Substances 0.000 description 4
- 238000005476 soldering Methods 0.000 description 3
- RYGMFSIKBFXOCR-UHFFFAOYSA-N Copper Chemical compound [Cu] RYGMFSIKBFXOCR-UHFFFAOYSA-N 0.000 description 2
- 229910052802 copper Inorganic materials 0.000 description 2
- 239000010949 copper Substances 0.000 description 2
- 230000000694 effects Effects 0.000 description 2
- 230000007613 environmental effect Effects 0.000 description 2
- YCKRFDGAMUMZLT-UHFFFAOYSA-N Fluorine atom Chemical compound [F] YCKRFDGAMUMZLT-UHFFFAOYSA-N 0.000 description 1
- CBENFWSGALASAD-UHFFFAOYSA-N Ozone Chemical compound [O-][O+]=O CBENFWSGALASAD-UHFFFAOYSA-N 0.000 description 1
- ATJFFYVFTNAWJD-UHFFFAOYSA-N Tin Chemical compound [Sn] ATJFFYVFTNAWJD-UHFFFAOYSA-N 0.000 description 1
- 150000007513 acids Chemical class 0.000 description 1
- 239000003518 caustics Substances 0.000 description 1
- 230000008859 change Effects 0.000 description 1
- 125000001309 chloro group Chemical group Cl* 0.000 description 1
- 239000012459 cleaning agent Substances 0.000 description 1
- 230000006378 damage Effects 0.000 description 1
- 229910052731 fluorine Inorganic materials 0.000 description 1
- 239000011737 fluorine Substances 0.000 description 1
- 238000005187 foaming Methods 0.000 description 1
- 230000036541 health Effects 0.000 description 1
- 150000002430 hydrocarbons Chemical class 0.000 description 1
- 230000006872 improvement Effects 0.000 description 1
- 238000005507 spraying Methods 0.000 description 1
- 231100000331 toxic Toxicity 0.000 description 1
- 230000002588 toxic effect Effects 0.000 description 1
- 238000005493 welding type Methods 0.000 description 1
Landscapes
- Detergent Compositions (AREA)
- Cleaning And De-Greasing Of Metallic Materials By Chemical Methods (AREA)
Abstract
Description
Claims (9)
Priority Applications (1)
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CN201210430506.7A CN102922178B (zh) | 2012-11-01 | 2012-11-01 | 一种免清洗液体铝助焊剂及其制备方法 |
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CN201210430506.7A CN102922178B (zh) | 2012-11-01 | 2012-11-01 | 一种免清洗液体铝助焊剂及其制备方法 |
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CN102922178A CN102922178A (zh) | 2013-02-13 |
CN102922178B true CN102922178B (zh) | 2014-10-08 |
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Cited By (1)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN104607826A (zh) * | 2014-12-09 | 2015-05-13 | 华南理工大学 | 一种用于铝低温软钎焊的免清洗固态助焊剂及制备方法 |
Families Citing this family (8)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN103182612B (zh) * | 2013-03-28 | 2015-09-02 | 天津市恒固科技有限公司 | 一种热镀锡和锡合金的自析熔剂及其制备方法 |
CN103192201A (zh) * | 2013-03-28 | 2013-07-10 | 天津市恒固科技有限公司 | 一种用于铝及铝合金软钎焊的固态助焊剂及其制备方法 |
CN105081618A (zh) * | 2014-05-06 | 2015-11-25 | 烟台市固光焊接材料有限责任公司 | 低温无腐蚀易清洗铜铝钎剂及其制备方法 |
CN105081617A (zh) * | 2014-05-06 | 2015-11-25 | 烟台市固光焊接材料有限责任公司 | 一种铝钎焊膏及制备方法、用途 |
BE1022204B1 (fr) * | 2014-08-28 | 2016-02-29 | Qingdao Intek Tin Technology Co. Ltd | Un flux a souder d'aluminium liquide non lavable et son procede de preparation |
LU92531B1 (fr) * | 2014-08-28 | 2016-02-29 | Qingdao Intek Tin Tech Co Ltd | Un flux à souder d'aluminium liquide non lavable et son procédé de préparation |
CN106392377A (zh) * | 2016-10-07 | 2017-02-15 | 常州市鼎升环保科技有限公司 | 一种免清洗助焊剂的制备方法 |
CN106378549B (zh) * | 2016-11-08 | 2019-04-19 | 金锚电力控股有限公司 | 一种用于铜铝钎焊的免洗助焊剂 |
Family Cites Families (7)
Publication number | Priority date | Publication date | Assignee | Title |
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JPS5922632B2 (ja) * | 1980-05-19 | 1984-05-28 | メツク株式会社 | プリント配線基板ハンダ付用水溶性フラツクス |
US6059894A (en) * | 1998-04-08 | 2000-05-09 | Hewlett-Packard Company | High temperature flip chip joining flux that obviates the cleaning process |
US6887319B2 (en) * | 2002-04-16 | 2005-05-03 | Senju Metal Industry Co., Ltd. | Residue-free solder paste |
CN100479975C (zh) * | 2007-07-17 | 2009-04-22 | 西安理工大学 | 一种用于锡铅焊膏的低松香免清洗助焊剂及其制备方法 |
CN101480764B (zh) * | 2009-02-05 | 2013-11-06 | 深圳市亿铖达工业有限公司 | 水溶性铝及铝合金软钎焊钎剂及其制备方法 |
JP2012055922A (ja) * | 2010-09-08 | 2012-03-22 | Tetsuo Harada | 蝋付け用フラックス及び蝋付け法 |
CN102139425B (zh) * | 2011-04-13 | 2013-02-06 | 广州瀚源电子科技有限公司 | 一种铝软钎焊用高可靠性助焊剂 |
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Cited By (1)
Publication number | Priority date | Publication date | Assignee | Title |
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CN104607826A (zh) * | 2014-12-09 | 2015-05-13 | 华南理工大学 | 一种用于铝低温软钎焊的免清洗固态助焊剂及制备方法 |
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Denomination of invention: No-cleaning liquid aluminum flux and preparation method thereof Effective date of registration: 20150731 Granted publication date: 20141008 Pledgee: Qingdao Huitong Chinese financing Company limited by guarantee Pledgor: Qingdao Ying Taikexi industry Science and Technology Ltd. Registration number: 2015990000626 |
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Denomination of invention: No-cleaning liquid aluminum flux and preparation method thereof Effective date of registration: 20170228 Granted publication date: 20141008 Pledgee: Qingdao high technology financing Company limited by guarantee Pledgor: Qingdao Ying Taikexi industry Science and Technology Ltd. Registration number: 2017370010001 |
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Date of cancellation: 20180424 Granted publication date: 20141008 Pledgee: Qingdao high technology financing Company limited by guarantee Pledgor: Qingdao Ying Taikexi industry Science and Technology Ltd. Registration number: 2017370010001 |
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