CN102906072B - 吡唑羧酸酰胺的制备方法 - Google Patents

吡唑羧酸酰胺的制备方法 Download PDF

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Publication number
CN102906072B
CN102906072B CN201180019785.1A CN201180019785A CN102906072B CN 102906072 B CN102906072 B CN 102906072B CN 201180019785 A CN201180019785 A CN 201180019785A CN 102906072 B CN102906072 B CN 102906072B
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formula
compound
reacting
bromine
chlorine
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Chinese (zh)
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CN102906072A (zh
Inventor
R·迪默尼耶
F·施莱斯
T·维蒂格
M·洛米尔
S·特拉
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Syngenta Crop Protection AG Switzerland
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Syngenta Participations AG
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    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07D—HETEROCYCLIC COMPOUNDS
    • C07D231/00—Heterocyclic compounds containing 1,2-diazole or hydrogenated 1,2-diazole rings
    • C07D231/02—Heterocyclic compounds containing 1,2-diazole or hydrogenated 1,2-diazole rings not condensed with other rings
    • C07D231/10—Heterocyclic compounds containing 1,2-diazole or hydrogenated 1,2-diazole rings not condensed with other rings having two or three double bonds between ring members or between ring members and non-ring members
    • C07D231/14—Heterocyclic compounds containing 1,2-diazole or hydrogenated 1,2-diazole rings not condensed with other rings having two or three double bonds between ring members or between ring members and non-ring members with hetero atoms or with carbon atoms having three bonds to hetero atoms with at the most one bond to halogen, e.g. ester or nitrile radicals, directly attached to ring carbon atoms
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C17/00—Preparation of halogenated hydrocarbons
    • C07C17/23—Preparation of halogenated hydrocarbons by dehalogenation
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C17/00—Preparation of halogenated hydrocarbons
    • C07C17/26—Preparation of halogenated hydrocarbons by reactions involving an increase in the number of carbon atoms in the skeleton
    • C07C17/30—Preparation of halogenated hydrocarbons by reactions involving an increase in the number of carbon atoms in the skeleton by a Diels-Alder synthesis
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C209/00—Preparation of compounds containing amino groups bound to a carbon skeleton
    • C07C209/04—Preparation of compounds containing amino groups bound to a carbon skeleton by substitution of functional groups by amino groups
    • C07C209/06—Preparation of compounds containing amino groups bound to a carbon skeleton by substitution of functional groups by amino groups by substitution of halogen atoms
    • C07C209/10—Preparation of compounds containing amino groups bound to a carbon skeleton by substitution of functional groups by amino groups by substitution of halogen atoms with formation of amino groups bound to carbon atoms of six-membered aromatic rings or from amines having nitrogen atoms bound to carbon atoms of six-membered aromatic rings
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C25/00—Compounds containing at least one halogen atom bound to a six-membered aromatic ring
    • C07C25/24—Halogenated aromatic hydrocarbons with unsaturated side chains
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C29/00—Preparation of compounds having hydroxy or O-metal groups bound to a carbon atom not belonging to a six-membered aromatic ring
    • C07C29/132—Preparation of compounds having hydroxy or O-metal groups bound to a carbon atom not belonging to a six-membered aromatic ring by reduction of an oxygen containing functional group
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C35/00—Compounds having at least one hydroxy or O-metal group bound to a carbon atom of a ring other than a six-membered aromatic ring
    • C07C35/48—Halogenated derivatives
    • C07C35/52—Alcohols with a condensed ring system
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C45/00—Preparation of compounds having >C = O groups bound only to carbon or hydrogen atoms; Preparation of chelates of such compounds
    • C07C45/27—Preparation of compounds having >C = O groups bound only to carbon or hydrogen atoms; Preparation of chelates of such compounds by oxidation
    • C07C45/29—Preparation of compounds having >C = O groups bound only to carbon or hydrogen atoms; Preparation of chelates of such compounds by oxidation of hydroxy groups
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07D—HETEROCYCLIC COMPOUNDS
    • C07D303/00—Compounds containing three-membered rings having one oxygen atom as the only ring hetero atom
    • C07D303/02—Compounds containing oxirane rings
    • C07D303/12—Compounds containing oxirane rings with hydrocarbon radicals, substituted by singly or doubly bound oxygen atoms
    • C07D303/16—Compounds containing oxirane rings with hydrocarbon radicals, substituted by singly or doubly bound oxygen atoms by esterified hydroxyl radicals
    • C07D303/17—Compounds containing oxirane rings with hydrocarbon radicals, substituted by singly or doubly bound oxygen atoms by esterified hydroxyl radicals containing oxirane rings condensed with carbocyclic ring systems having three or more relevant rings
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C2603/00—Systems containing at least three condensed rings
    • C07C2603/56—Ring systems containing bridged rings
    • C07C2603/58—Ring systems containing bridged rings containing three rings
    • C07C2603/60—Ring systems containing bridged rings containing three rings containing at least one ring with less than six members
    • C07C2603/66—Ring systems containing bridged rings containing three rings containing at least one ring with less than six members containing five-membered rings

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  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
  • Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)
  • Catalysts (AREA)
  • Epoxy Compounds (AREA)
CN201180019785.1A 2010-04-20 2011-04-14 吡唑羧酸酰胺的制备方法 Active CN102906072B (zh)

Applications Claiming Priority (3)

Application Number Priority Date Filing Date Title
EP10160438.7 2010-04-20
EP10160438 2010-04-20
PCT/EP2011/055871 WO2011131545A1 (en) 2010-04-20 2011-04-14 Process for the preparation of pyrazole carboxylic acid amides

Publications (2)

Publication Number Publication Date
CN102906072A CN102906072A (zh) 2013-01-30
CN102906072B true CN102906072B (zh) 2014-07-02

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CN201180019785.1A Active CN102906072B (zh) 2010-04-20 2011-04-14 吡唑羧酸酰胺的制备方法

Country Status (13)

Country Link
US (1) US8519152B2 (https=)
EP (1) EP2560959B1 (https=)
JP (1) JP5684896B2 (https=)
CN (1) CN102906072B (https=)
AR (1) AR080922A1 (https=)
BR (1) BR112012026631B1 (https=)
ES (1) ES2513540T3 (https=)
IL (1) IL222398A (https=)
MX (1) MX2012012005A (https=)
PY (1) PY1115670A (https=)
TW (1) TWI428325B (https=)
UY (1) UY33340A (https=)
WO (1) WO2011131545A1 (https=)

Families Citing this family (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
EP2560960B1 (en) * 2010-04-20 2014-02-26 Syngenta Participations AG Process for the preparation of pyrazole carboxylic acid amides
TWI534126B (zh) * 2011-01-25 2016-05-21 先正達合夥公司 用於製備吡唑羧酸醯胺之方法
GB201403438D0 (en) * 2014-02-27 2014-04-16 Syngenta Participations Ag Polymorphs
KR20250036910A (ko) 2022-07-22 2025-03-14 신젠타 크롭 프로텍션 아게 이종환식 아미드 유도체의 고체 형태
CN116143635B (zh) * 2022-12-01 2025-02-25 江苏七洲绿色科技研究院有限公司 一种9-二氯亚甲基-5-氨基-苯并降冰片烯的制备方法
PY2503719A (es) 2024-01-26 2025-08-05 Syngenta Crop Protection Ag Proceso químico

Citations (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
WO2007048556A1 (en) * 2005-10-25 2007-05-03 Syngenta Participations Ag Heterocyclic amide derivatives useful as microbiocides

Family Cites Families (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JPH075487B2 (ja) 1985-11-14 1995-01-25 住友化学工業株式会社 １―ブロモ―２―クロロ―４―フルオロベンゼンの製造法
US5093347A (en) 1991-01-28 1992-03-03 Monsanto Company 3-difluoromethylpyrazolecarboxamide fungicides, compositions and use
US7223879B2 (en) 1998-07-10 2007-05-29 Massachusetts Institute Of Technology Ligands for metals and improved metal-catalyzed processes based thereon
WO2007124907A2 (en) 2006-04-27 2007-11-08 Syngenta Participations Ag Heterocyclyl-carboxylic acid (benzonorbornene-5-yl)amide derivatives as fungicides for agrochemical use
CN101528034B (zh) 2006-10-25 2011-11-09 辛根塔有限公司 生产经取代的溴苯的方法
BRPI0923527A2 (pt) * 2008-12-24 2016-08-09 Syngenta Ltd métodos de preparo de fungicidas

Patent Citations (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
WO2007048556A1 (en) * 2005-10-25 2007-05-03 Syngenta Participations Ag Heterocyclic amide derivatives useful as microbiocides

Non-Patent Citations (1)

* Cited by examiner, † Cited by third party
Title
Bicyclo[2,2,1]heptadiene in the Diels–Alder reaction;K. Mackenzie;《Journal of the Chemical Society》;19601231;473-483 *

Also Published As

Publication number Publication date
AR080922A1 (es) 2012-05-16
TWI428325B (zh) 2014-03-01
US8519152B2 (en) 2013-08-27
CN102906072A (zh) 2013-01-30
IL222398A (en) 2017-01-31
BR112012026631A2 (pt) 2015-09-15
US20130035496A1 (en) 2013-02-07
TW201204704A (en) 2012-02-01
JP2013525317A (ja) 2013-06-20
JP5684896B2 (ja) 2015-03-18
WO2011131545A1 (en) 2011-10-27
BR112012026631B1 (pt) 2017-07-25
EP2560959A1 (en) 2013-02-27
EP2560959B1 (en) 2014-08-20
PY1115670A (es) 2014-09-01
MX2012012005A (es) 2012-12-17
UY33340A (es) 2011-12-01
ES2513540T3 (es) 2014-10-27

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