CN102888155A - Preparation method of odorless environment-friendly humidifying antibacterial paint - Google Patents

Preparation method of odorless environment-friendly humidifying antibacterial paint Download PDF

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Publication number
CN102888155A
CN102888155A CN2012104182052A CN201210418205A CN102888155A CN 102888155 A CN102888155 A CN 102888155A CN 2012104182052 A CN2012104182052 A CN 2012104182052A CN 201210418205 A CN201210418205 A CN 201210418205A CN 102888155 A CN102888155 A CN 102888155A
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environmental protection
agent
nano
emulsion
powder
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CN2012104182052A
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Chinese (zh)
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CN102888155B (en
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许钧强
康伦国
欧永杰
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合众(佛山)化工有限公司
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Abstract

The invention relates to a preparation method of an odorless environment-friendly humidifying antibacterial paint. The odorless environment-friendly humidifying antibacterial paint basically comprises 12-40% of emulsion, 5-20% of titanium white, 12-20% of kieselguhr, 2-6% of attapulgite, 4-8% of bamboo charcoal powder, 3-10% of nano TiO2/anion powder additive, 5-10% of light calcium carbonate, 5-10% of kaolin, 1-5% of propanediol, 2-5% of assistant and 10-30% of deionized water. The multifunctional humidifying antimicrobial internal wall paint completely satisfies various indexes specified in GB/T9756-2001, has the effects of temperature control, energy saving, environmental protection, moisture absorption and release, humidification, dewing resistance, air refreshing, no odor, deodorization, bacteria and mold inactivation and the like, and is widely used in inner wall application of habitable rooms, classrooms, offices, hospitals and the like.

Description

A kind of preparation method of clean flavor environmental protection moisture adjustable antibiotic paint
Technical field
The present invention relates to a kind of preparation method of humidity controlling coating, relate in particular to and be applicable to various indoor a kind of clean flavor environmental protection moisture adjustable antibiotic paints.
Background technology
Humidity is closely related with human productive life, and humidity is crossed the low or too high orthobiosis that all can affect people.When indoor humidity was lower than 40%, Person's skin was chapped, the respiratory system resistibility descends, and bacterium, virus can be taken advantage of a weak point, and furniture can be out of shape explosion, and coating, mural painting efflorescence are accelerated, and easily cause again static electric fire; When being higher than 60%, environment is too moist, and microbial reproduction is accelerated, and article easily go mouldy, rot or corrosion.Therefore, the control indoor humidity all seems very important to productive life, and especially to humidity and arid area, adjusting humidity is particularly important.Indoor damping is adopted initiatively and passive mode usually.The former mainly refers to air-conditioning, and the method investment is large, energy consumption is high, easily produce noise pollution, causes problems such as " architecture indoor air conditioner comprehensive diseases ", unsuitable life-time service.The moisture adsorption and releasing characteristic of the latter renewable energy source or material is regulated humidity, need not to consume any artificial energy source, be a kind of ecological property regulating and controlling method, usually adopt humidity adjusting material and humidity controlling coating, its purposes extensively become one of modern architecture and the indispensable material of house fitting.
Clean flavor coating also claims the special efficacy air purifying coating, has the function of photocatalyst, 1. purifies air: harmful element such as formaldehyde, triphen etc. in the air can be decomposed into water and carbonic acid gas equistability element, play the effect that purifies air.2. antibiotic, sterilization, mildew-resistant: have superpower redox ability, the bacterium (microorganisms such as intestinal bacteria, streptococcus aureus, penicillin staphylococcus, mould) around can effectively killing plays the effect of antibacterial and mouldproof.3. smelly eliminating: can decompose the odour element of the cigarettes such as acetaldehyde around being adsorbed on, acetic acid, ammonia in smelly, play the effect of eliminating residual smell in the air.4. antifouling, self-cleaning: oily dirt can be broken down into water and other stabilizing gas after being attracted to its surface in the air, plays antifouling, self-cleaning effect.5. environmental protection, pollution-free: the active oxygen anion of generation without any detrimentally affect, is free of contamination environmentfriendly products to human body.
The development of interior wall material of construction is on the basis of original decoration functions, future development towards " multifunction, environmental harmony ", " multifunction " refers to except decoration functions, have simultaneously healthy functions such as " energy-conservation, regulate humidity, antibacterial and mouldproof, purify air, sound insulation, shielding unwanted electromagnetic wave ", this will greatly improve the human settlement, improve human life quality and health level.
Summary of the invention
The present invention selects diatomite, attapulgite, bamboo charcoal to form composite humidity adjusting material, with nano-TiO 2/ negative ion powder is antibiotic material for air purification.
Diatomite is a kind of aqueous silicon dioxide mineral dust, density is very little, be microvoid structure and the duct is interconnected, porosity reaches more than 85%, and specific surface area is large, and water-retaining capacity is strong, Young's modulus is high, have heat insulating, regulate humidity, absorption toxic gas, antisweat, noise reduction, adhesion strength be strong, and acid resistance, preservative property, flame retardant resistance, good dispersity are the main components of humidity adjusting material of the present invention.
Attapulgite be a kind of have a chain laminate structure contain Shuifu County's magnesium silicate clay, have special fibrous texture and unusual absorption property, also have simultaneously thickening, anti-settling, sag prevention performance.
Bamboo charcoal has the various functions such as superpower absorption, damping, deodorizing, insect protected, remove various objectionable impuritiess such as formaldehyde, benzene,toluene,xylene and ammonia etc. after the new house finishing is fitted up with room smell, strong adsorption, increase the space anion concentration, reach and purify air and the far-infrared health-care effect.
Nano-TiO 2/ negative ion antibiotic additive can forever discharge hydroxyl group anion by filming, and then obnoxious flavour, bacterium and microorganism are passed through to coat the processes such as sedimentation, neutralization, electric field Current Decomposition and chemical reaction, reaches the purpose that purifies air with bacteriostasis antibiosis.
In order to solve technical problem recited above, the present invention takes following technical scheme: the present invention relates to a kind of clean flavor environmental protection moisture adjustable antibiotic paint, its basic recipe is: emulsion 12%~40%, titanium dioxide 5%~20%, diatomite 12%~20%, attapulgite 2%~6%, bamboo charcoal powder 4%~8%, nano-TiO 2/ negative ion powder additive 3%~10%, light calcium carbonate 5%~10%, kaolin 5%~10%, propylene glycol 1%~5%, auxiliary agent 2%~5%, deionized water 10%~30%.
Wherein, emulsion is selected one or more combination of benzene emulsion, ACRYLIC EMULSION, organosilicon crylic acid latex, acrylate and vinyl acetate emulsion, chlorine partial emulsion, uncle's acrylic emulsion or silicon sol.
Titanium dioxide is selected one or more combination of rutile titanium white powder or anatase thpe white powder.
Diatomite is selected through 600~800 ℃ of calcinings, specific surface area>500,000 cm 2The 800 purpose powders of/g.
Attapulgite is selected canescence, contains attapulgite hybrid amount 〉=75%, has 800 purpose powders of fiber needle pencil.
Bamboo charcoal powder is chosen and is used through 700 ℃ of calcinings, carbon content at 800 purpose powders more than 85%.
Nano-TiO 2It is that 30nm~80nm, solid content are 15% nano-TiO that/negative ion powder additive is selected particle diameter 2With the compound dispersed paste of 15% negative ion powder.
Auxiliary agent comprises one or more combination of dispersion agent, wetting agent, defoamer, PH multifunctional assistant, flow agent, the anti-stick dirty agent of nanometer, thickener rheology agent or film coalescence aid at least.
Nano-TiO of the present invention 2/ negative ion powder additive preparation technology: by formulation weight per-cent, add successively entry, macromolecule dispersing agent, silane coupling agent and add and disperse to stir in the cylinder, then slowly add while stirring nano-TiO 2Powder and negative ion powder, powder add rear high speed dispersion 60min, open nano-level grinder, carry out circular grinding, and milling time is approximately 12h~15h, obtain the meta particle diameter between 40nm~80nm, solid content is 30% nano-dispersed slurry.
The preparation method preparation technology that the present invention proposes a kind of clean flavor environmental protection moisture adjustable antibiotic paint is as follows: by the formulation weight ratio, deionized water is added in the Scattered Kettle, stir lower add auxiliary agent, damping powder, color stuffing, nano-TiO 2/ negative ion powder additive, high speed dispersion 30~40min reaches 50 μ m form slurry through mesh-of-grind; Ground slurry is squeezed in the paint mixing tank, and middling speed stirs lower adding emulsion, defoamer, flow agent, thickener rheology agent, then at the uniform velocity adds film coalescence aid, and the good viscosity of stirring and adjusting and pH value namely make a kind of clean flavor environmental protection moisture adjustable antibiotic paint.
The clean flavor environmental protection moisture adjustable antibiotic paint that the present invention makes is except the indices that meets GB/T9756-2001 regulation fully, also have the effects such as temperature adjustment temperature control, energy-conserving and environment-protective, humidity absorption and release, damping antisweat, clear bright air, deodorizing, anion ecological, kill bacteria mould, can be widely used in the interior wall applications such as room, classroom, office, hospital.
Embodiment
Preparing material according to the component prescription of table 1 implements.
Table 1: three embodiment component prescription mass parts
Material name Example 1 Example 2 Example 3
Deionized water 17 13 15
Propylene glycol 3 3 3
Wetting agent 0.3 0.3 0.3
Dispersion agent 1.5 1.5 1.5
Titanium dioxide 15 12 12
Light calcium carbonate 6 8 8
Kaolin 6 8 8
Diatomite 15 16 16
Attapulgite 3 3 3
Bamboo charcoal powder 5 5 5
The nano-antibacterial additive 5 5 5
ACRYLIC EMULSION 20 -- --
Benzene emulsion -- 22 --
Organosilicon crylic acid latex -- -- 20
Film coalescence aid 1.2 1.2 1.0
The PH conditioning agent 0.5 0.5 0.5
Flow agent 0.2 0.2 0.2
Thickening material 1.0 1.0 1.0
Defoamer 0.3 0.3 0.3
Embodiment 1:
Deionized water is added in the Scattered Kettle by the formulation weight ratio according to example in the table 11, stir lower auxiliary agent, damping powder, color stuffing, the nano-TiO of adding 2/ negative ion powder additive, high speed dispersion 30~40min reaches 50 μ m form slurry through mesh-of-grind; Ground slurry is squeezed in the paint mixing tank, and middling speed stirs lower adding emulsion, defoamer, thickener rheology agent, then at the uniform velocity adds film coalescence aid, and flow agent, the good viscosity of stirring and adjusting and pH value namely make a kind of clean flavor environmental protection moisture adjustable antibiotic paint.
Embodiment 2, and embodiment 3 preparation processes are with reference to embodiment 1.
According to relevant national standard, the performance of clean flavor environmental protection moisture adjustable antibiotic paint of the present invention is detected, test result is as shown in table 2.
The clean flavor of table 2 environmental protection moisture adjustable antibiotic paint the performance test results
Test event Test result
At condition in container Without lump, uniform state
Application property Brush two roads accessible
Contrast ratio/% ≥0.91
Low-temperature stability By
Paint film appearance Normally
Alkali resistance 24h Without unusual
Abrasion resistance/time 300
VOC content/gkg -1 ≤30
Free formaldehyde/gkg-1 0.01
Formaldehyde, ammonia clearance (96h)/% ≥92
Germ resistance/% ≥99.5
Antibiotic weather resistance ≥99.0
Antifungal/level 0
Antifungal weather resistance/level 0
Moisture uptake/gm-2 72
Moisture releasing amount/gm-2 70
A negative ion burst size/cm-3 ≥1200
Dissoluble lead/ppm ≤20
Soluble cadmium/ppm ≤15
Soluble chromium/ppm ≤10
Soluble mercury/ppm Do not detect
Although the present invention has done to describe in detail and quoted embodiment as proof, for those of ordinary skill in the art, various schemes, modification and the change that obviously can make according to above-mentioned explanation all should be included within the scope of claim.

Claims (10)

1. a clean flavor environmental protection moisture adjustable antibiotic paint is characterized in that: by weight percentage, comprise following component: emulsion 12%~40%, titanium dioxide 5%~20%, diatomite 12%~20%, attapulgite 2%~6%, bamboo charcoal powder 4%~8%, nano-TiO 2/ negative ion powder additive 3%~10%, light calcium carbonate 5%~10%, kaolin 5%~10%, propylene glycol 1%~5%, auxiliary agent 2%~5%, deionized water 10%~30%.
2. a kind of clean flavor environmental protection moisture adjustable antibiotic paint as claimed in claim 1 is characterized in that: said emulsion is selected one or more combination of benzene emulsion, ACRYLIC EMULSION, organosilicon crylic acid latex, acrylate and vinyl acetate emulsion, chlorine partial emulsion, uncle's acrylic emulsion or silicon sol.
3. a kind of clean flavor environmental protection moisture adjustable antibiotic paint as claimed in claim 1 is characterized in that: said titanium dioxide is selected one or more combination of rutile titanium white powder or anatase thpe white powder.
4. a kind of clean flavor environmental protection moisture adjustable antibiotic paint as claimed in claim 1, it is characterized in that: said diatomite is selected through 600~800 ℃ of calcinings, specific surface area>500,000 cm 2The 800 purpose powders of/g.
5. a kind of clean flavor environmental protection moisture adjustable antibiotic paint as claimed in claim 1, it is characterized in that: said attapulgite is selected canescence, contains attapulgite hybrid amount 〉=75%, has 800 purpose powders of fiber needle pencil.
6. a kind of clean flavor environmental protection moisture adjustable antibiotic paint as claimed in claim 1, it is characterized in that: said bamboo charcoal powder is chosen and is used through 700 ℃ of calcinings, carbon content at 800 purpose powders more than 85%.
7. a kind of clean flavor environmental protection moisture adjustable antibiotic paint as claimed in claim 1 is characterized in that: said nano-TiO 2It is that 30nm~80nm, solid content are 15% nano-TiO that/negative ion powder additive is selected particle diameter 2With the compound dispersed paste of 15% negative ion powder.
8. a kind of clean flavor environmental protection moisture adjustable antibiotic paint as claimed in claim 1 is characterized in that: said auxiliary agent comprises one or more combination of dispersion agent, wetting agent, defoamer, PH multifunctional assistant, flow agent, the anti-stick dirty agent of nanometer, thickener rheology agent or film coalescence aid at least.
9. one kind such as claim 1,7 described nano-TiOs 2The preparation method of/negative ion powder additive, it is characterized in that: described preparation method comprises: by formulation weight per-cent, add successively entry, macromolecule dispersing agent, silane coupling agent and add and disperse to stir in the cylinder, then slowly add while stirring nano-TiO 2Powder and negative ion powder, powder add rear high speed dispersion 60min, open nano-level grinder, carry out circular grinding, and milling time is approximately 12h~15h, obtain the meta particle diameter between 40nm~80nm, solid content is 30% nano-dispersed slurry.
10. the preparation method of an a kind of clean flavor environmental protection moisture adjustable antibiotic paint as claimed in claim 1, it is characterized in that: described preparation method comprises: by the formulation weight ratio, deionized water is added in the Scattered Kettle, stir lower add auxiliary agent, damping powder, color stuffing, nano-TiO 2/ negative ion powder additive, high speed dispersion 30~40min reaches 50 μ m form slurry through mesh-of-grind; Ground slurry is squeezed in the paint mixing tank, and middling speed stirs lower adding emulsion, defoamer, flow agent, thickener rheology agent, then at the uniform velocity adds film coalescence aid, and the good viscosity of stirring and adjusting and pH value namely make a kind of clean flavor environmental protection moisture adjustable antibiotic paint.
CN201210418205.2A 2012-10-26 2012-10-26 A kind of preparation method of clean taste environmental protection moisture adjustable antibiotic paint Active CN102888155B (en)

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CN104559494A (en) * 2013-10-10 2015-04-29 天长市开林化工有限公司 Sound absorbing and noise reducing seaweed mud indoor coating and production technology thereof
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CN103525232A (en) * 2013-10-24 2014-01-22 镇江威信广厦模块建筑有限公司 Preparation method of mildewproof waterborne coating
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Denomination of invention: Preparation method of odorless environment-friendly humidifying antibacterial paint

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