CN102854157B - 一种测量碳素材料中Na含量的方法 - Google Patents
一种测量碳素材料中Na含量的方法 Download PDFInfo
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- CN102854157B CN102854157B CN201110182564.8A CN201110182564A CN102854157B CN 102854157 B CN102854157 B CN 102854157B CN 201110182564 A CN201110182564 A CN 201110182564A CN 102854157 B CN102854157 B CN 102854157B
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- 239000003575 carbonaceous material Substances 0.000 title claims abstract description 115
- 238000000034 method Methods 0.000 title claims abstract description 36
- 239000011734 sodium Substances 0.000 claims abstract description 90
- 238000001354 calcination Methods 0.000 claims abstract description 48
- DGAQECJNVWCQMB-PUAWFVPOSA-M Ilexoside XXIX Chemical compound C[C@@H]1CC[C@@]2(CC[C@@]3(C(=CC[C@H]4[C@]3(CC[C@@H]5[C@@]4(CC[C@@H](C5(C)C)OS(=O)(=O)[O-])C)C)[C@@H]2[C@]1(C)O)C)C(=O)O[C@H]6[C@@H]([C@H]([C@@H]([C@H](O6)CO)O)O)O.[Na+] DGAQECJNVWCQMB-PUAWFVPOSA-M 0.000 claims abstract description 38
- 229910052708 sodium Inorganic materials 0.000 claims abstract description 38
- 238000005259 measurement Methods 0.000 claims abstract description 8
- 239000000243 solution Substances 0.000 claims description 128
- VEXZGXHMUGYJMC-UHFFFAOYSA-N Hydrochloric acid Chemical compound Cl VEXZGXHMUGYJMC-UHFFFAOYSA-N 0.000 claims description 58
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Chemical compound O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 44
- 238000000227 grinding Methods 0.000 claims description 32
- 238000002835 absorbance Methods 0.000 claims description 31
- VLTRZXGMWDSKGL-UHFFFAOYSA-N perchloric acid Chemical compound OCl(=O)(=O)=O VLTRZXGMWDSKGL-UHFFFAOYSA-N 0.000 claims description 28
- BASFCYQUMIYNBI-UHFFFAOYSA-N platinum Chemical compound [Pt] BASFCYQUMIYNBI-UHFFFAOYSA-N 0.000 claims description 28
- 239000012085 test solution Substances 0.000 claims description 28
- 239000000203 mixture Substances 0.000 claims description 15
- 238000010521 absorption reaction Methods 0.000 claims description 14
- 239000012490 blank solution Substances 0.000 claims description 14
- 235000019504 cigarettes Nutrition 0.000 claims description 14
- 230000001186 cumulative effect Effects 0.000 claims description 14
- 239000008367 deionised water Substances 0.000 claims description 14
- 229910021641 deionized water Inorganic materials 0.000 claims description 14
- 238000001704 evaporation Methods 0.000 claims description 14
- 230000008020 evaporation Effects 0.000 claims description 14
- 238000010438 heat treatment Methods 0.000 claims description 14
- 229910052697 platinum Inorganic materials 0.000 claims description 14
- 239000002245 particle Substances 0.000 claims description 2
- 238000004458 analytical method Methods 0.000 abstract description 6
- OKTJSMMVPCPJKN-UHFFFAOYSA-N Carbon Chemical compound [C] OKTJSMMVPCPJKN-UHFFFAOYSA-N 0.000 abstract description 2
- 238000003556 assay Methods 0.000 abstract description 2
- 230000009286 beneficial effect Effects 0.000 abstract description 2
- 229910052799 carbon Inorganic materials 0.000 abstract description 2
- 239000003610 charcoal Substances 0.000 abstract description 2
- 239000003153 chemical reaction reagent Substances 0.000 abstract description 2
- 238000001914 filtration Methods 0.000 abstract description 2
- 239000002006 petroleum coke Substances 0.000 abstract description 2
- 239000000523 sample Substances 0.000 description 42
- 239000000463 material Substances 0.000 description 13
- 239000012086 standard solution Substances 0.000 description 4
- 238000002156 mixing Methods 0.000 description 1
- 238000002360 preparation method Methods 0.000 description 1
- 239000012488 sample solution Substances 0.000 description 1
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- Investigating Or Analyzing Non-Biological Materials By The Use Of Chemical Means (AREA)
- Investigating Or Analysing Materials By Optical Means (AREA)
Abstract
Description
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Priority Applications (1)
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CN201110182564.8A CN102854157B (zh) | 2011-07-01 | 2011-07-01 | 一种测量碳素材料中Na含量的方法 |
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CN201110182564.8A CN102854157B (zh) | 2011-07-01 | 2011-07-01 | 一种测量碳素材料中Na含量的方法 |
Publications (2)
Publication Number | Publication Date |
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CN102854157A CN102854157A (zh) | 2013-01-02 |
CN102854157B true CN102854157B (zh) | 2016-02-17 |
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CN201110182564.8A Active CN102854157B (zh) | 2011-07-01 | 2011-07-01 | 一种测量碳素材料中Na含量的方法 |
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Citations (1)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN1624454A (zh) * | 2003-12-03 | 2005-06-08 | 上海化工研究院 | 肥料中微量元素汞的测定方法 |
Family Cites Families (1)
Publication number | Priority date | Publication date | Assignee | Title |
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DE4011338A1 (de) * | 1990-04-07 | 1991-10-10 | Bodenseewerk Perkin Elmer Co | Verfahren und vorrichtung zur analyse von proben mittels atomabsorptions-spektrometer |
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2011
- 2011-07-01 CN CN201110182564.8A patent/CN102854157B/zh active Active
Patent Citations (1)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN1624454A (zh) * | 2003-12-03 | 2005-06-08 | 上海化工研究院 | 肥料中微量元素汞的测定方法 |
Non-Patent Citations (3)
Title |
---|
原子吸收光谱法测定石油焦中铁和钠;金珊;《理化检验-化学分册》;20001031;第36卷(第10期);第467页第1.3.1节第1段 * |
火焰原子吸收法测定石油焦中的铁、镍、钠;张春明 等;《光谱实验室》;20011130;第18卷(第6期);全文 * |
煤灰成分分析方法;中华人民共和国国家质量监督检验检疫总局 等;《中华人民共和国国家标准 GB/T 1574-2007》;20071101;第1页第5节第1段,第26页倒数第1段,第27页第11.3.5.1-11.3.5.3节 * |
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Address after: Sheng Tong Industrial Park No. 109 Venus 410200 Hunan province Changsha road in Wangcheng County Applicant after: Shengtong Science and Technology Group Co.,Ltd. Address before: Sheng Tong Industrial Park No. 109 Venus 410200 Hunan province Changsha road in Wangcheng County Applicant before: Hunan Sheng Tong Technology Group Co.,Ltd. |
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Free format text: CORRECT: APPLICANT; FROM: HUNAN SHENGTONG TECHNOLOGY GROUP CO., LTD. TO: SNTO TECHNOLOGY GROUP CO., LTD. |
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Inventor after: Zhang Cunzhong Inventor before: Wu Yuhua Inventor before: Zhang Ping Inventor before: Jin Hanqing |
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Effective date of registration: 20171228 Address after: 252100 Xin Fa Hope Industrial Park, Chiping County, Liaocheng City, Shandong Patentee after: SHANDONG XINFA HUAYUAN ALUMINUM CO.,LTD. Address before: Sheng Tong Industrial Park No. 109 Venus 410200 Hunan province Changsha road in Wangcheng County Patentee before: Shengtong Science and Technology Group Co.,Ltd. |
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Effective date of registration: 20240822 Address after: No. 747 Shunhe North Street, Xinfa Street, Chiping County, Liaocheng City, Shandong Province, China 252100 Patentee after: Xinfa Science and Technology Research Co.,Ltd. Country or region after: China Address before: 252100 Xinfa Hope Industrial Park, Chiping County, Liaocheng City, Shandong Province Patentee before: SHANDONG XINFA HUAYUAN ALUMINUM CO.,LTD. Country or region before: China |