CN102783654A - Application of bunkanka saponin extract in weight losing and fat lowering fields - Google Patents
Application of bunkanka saponin extract in weight losing and fat lowering fields Download PDFInfo
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- CN102783654A CN102783654A CN201210321207XA CN201210321207A CN102783654A CN 102783654 A CN102783654 A CN 102783654A CN 201210321207X A CN201210321207X A CN 201210321207XA CN 201210321207 A CN201210321207 A CN 201210321207A CN 102783654 A CN102783654 A CN 102783654A
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Abstract
The invention aims to provide a bunkanka saponin extracting method that has the advantages of high efficiency, high yield, short time consumption, simple operation, low production cost and low device corrosion, and an extract with high-efficiency weight losing and fat lowering effects. The saponin can be used in weight losing and fat lowering fields, for example, the saponin can be added in health-care food according to a certain ratio to obtain the bunkanka saponin health-care food with good effect. The technical scheme is as follows: the extracting method comprises the steps of deoiling and crushing xanthoceras sorbifolia shells, extracting with a solution having a certain volume, filtering, then adding ethanol water having a certain volume to filter residue for extracting, filtering, combining the obtained filtrates, concentrating and lyophilizing to obtain the final product. The extract is added into food according to a certain ratio to prepare the functional food with weight losing and fat lowering effects.
Description
Technical field
The present invention provides the application of a kind of bunkankasaponin extract in the Weight-reducing and lipid-lowering field, belongs to agro-processing technology, relevant Weight-reducing and lipid-lowering such as health food field.
Background technology
Shiny-leaved yellowhorn belongs to the Sapindaceae shiny-leaved yellowhorn and belongs to, and also is referred to as civil official fruit, xanthoceras sobifolia bunge etc., is the woody seeds of the distinctive preciousness of China.It is very high that shinyleaf yellowhorn shell contains the saponin amount, and colorimetric estimation reaches 4%.Bunkankasaponin belongs to the oleanane type saponin, is prevalent in the plants such as pulse family, Araliaceae, Carrot family, Primulaceae, Curcurbitaceae.Oside compound aboundresources and be easy to extract extensively exists in organs such as the stem of plant, leaf, flower, fruit, be one group at structure and different in nature materials, the platymiscium secondary metabolite.The shinyleaf yellowhorn shell saponin has the effect of anti-anoxic, anti-oxidant, antifatigue.
Oside compound adopts solvent extraction usually.Mixed solvent such as methanol-water that the general available water of saponin, methyl alcohol, ethanol, acetone or polarity are bigger extract.Though technology is stablized feasible, efficient is low, length consuming time, and the reagent consumption is big, and solvent is prone to residual, and environment is had certain infringement.Pancreatic lipase is to absorb fatty most important enzyme in the digestive system; Food fat decomposes under the effect of pancreatic lipase in digesting and assimilating process, generates aliphatic acid and 2-acylglycerol; These steatolysis products mix with bile salt, and dispersion could be by little intestinal absorption after forming particulate.If can suppress the pancreatic lipase activity, just can postpone and reduce the absorption of small intestine, thereby reach anti-fat effect for reducing fat food fat.Research shows that plant sapogenin glycoside can make the absorption of fat reduce through suppressing the pancreatic lipase activity, thereby reaches the anti-fat effect of lipopenicillinase.For example panax quinquefolium saponin is 90% to the active inhibiting rate of pancreatic lipase, and panaxoside reaches 96%-100% to the pancreatic lipase maximum inhibition, and total saponin from platycodon grandiflorum reaches 41.7% to pancreatic lipase pancreatic lipase maximum inhibition.Pancreatic lipase is the most important enzyme of hydrolysis meals class fat, and isoelectric point is 5.0 acidic protein molecule.The food fat of hydrolyzable 50% ~ 70% is so can suppress high fat of blood through suppressing the pancreatic lipase activity.Yet, be that the Weight-reducing and lipid-lowering food of composition does not have report as yet at present with the bunkankasaponin.
Summary of the invention
The purpose of this invention is to provide that a kind of ability is efficient, yield is high, weak point consuming time, simple to operate, production cost is low, to saponin method for distilling in the low shinyleaf yellowhorn shell of equipment corrosion and extract with efficient lowering blood-fat and reducing weight effect; This saponin can be used for the Weight-reducing and lipid-lowering field; For example join by a certain percentage in the health food, can obtain respond well bunkankasaponin health food.Its technical scheme is:
A kind of bunkankasaponin extract is in the application in Weight-reducing and lipid-lowering field; It is characterized in that adopting following steps: (1) shinyleaf yellowhorn fruit shell is pulverized, and the volume that uses 20%-40% is shinyleaf yellowhorn shell opaque amount gram number 10-20 solution doubly milliliter, 70-75 ℃ of following lixiviate 60～90 minutes; Filter; Ethanolic solution lixiviate 30-60 minute that adds 30%-45% is again filtered, and twice filtrating is merged; (2) it is subsequent use filtrating to be condensed into paste, also can be Powdered with processing after the paste freeze-drying; (3) bunkankasaponin is in the application in Weight-reducing and lipid-lowering field: bunkankasaponin can significantly reduce the pancreatic lipase activity; Therefore it can join in the food in the ratio of 0.5%-1.1% (mass ratio); Food comprises bread and cheese and health food, products such as optional capsule, pulvis.
Described a kind of bunkankasaponin extract is in the application in Weight-reducing and lipid-lowering field, and shinyleaf yellowhorn shell is pulverized order and counted the 5-20 order in the step 1, and shinyleaf yellowhorn shell needs degreasing to carry oil.
Described a kind of bunkankasaponin extract contains 5%-10% methyl alcohol in the application in Weight-reducing and lipid-lowering field in the used solution in the step 1.
Described a kind of bunkankasaponin extract concentrates in the step 2 and can adopt decompression to concentrate in the application in Weight-reducing and lipid-lowering field, and the decompression thickening temperature is 60～70 ℃, under 0.1～0.7 atmospheric pressure, also can adopt the normal pressure heating.
Described a kind of bunkankasaponin extract is in the application in Weight-reducing and lipid-lowering field, wants mixing and stirring after adding health food in the step 3 to.
Described a kind of bunkankasaponin extract is in the application in Weight-reducing and lipid-lowering field, and the mode of this health products Weight-reducing and lipid-lowering is to be approach to suppress fat absorption in the step 3.
The present invention compared with prior art, the mixed solution that the technology that is adopted has used ethanol and methyl alcohol to form has reduced the consumption of methyl alcohol, has reduced dissolvent residual, has improved the extraction performance of solvent, has improved the recovery rate of saponin.Compare with traditional handicraft, technology is simple, recovery rate high (compare with simple ethanol extraction, recovery rate has increased about 26%); Yield high (compare with simple ethanol extraction, yield has improved about 20%), methanol usage significantly reduces (under the identical recovery rate, than simple methyl alcohol extraction; Methanol usage has reduced about 30%), production process is simple, and is easy to operate; Be prone to industrialization, mechanization, automated production.And the extract that the method obtains is active through suppressing pancreatic lipase, can realize fat-reducing and antihyperglycemic preferably.
Bunkankasaponin is through testing discovery to active inhibition of pancreatic lipase, and bunkankasaponin can suppress the pancreatic lipase activity and reach 68%, reduces fatty intake and reaches more than 60%.Can reduce the TG content 44% of high fat of blood mouse, prove tangible fat-reducing and antihyperglycemic.
Preferred forms
Embodiment 1:
Shinyleaf yellowhorn fruit shell is crushed to the 5-20 order after the degreasing, and with ethanol content 20%, 500 milliliters of the solution of methanol content 10% soak 50g shinyleaf yellowhorn shell powder, and 70 ℃ of following lixiviates 90 minutes are filtered, and adds 45% ethanolic solution lixiviate again 60 minutes, filters, and twice filtrating is merged; (2) will filtrate under the normal pressure after boiling removes about many milliliters of ethanol, water and methyl alcohol to 200, and changing decompression into and concentrating, it is 70 ℃ that decompression concentrates condition, 0.1 atmospheric pressure.Be condensed into the paste postlyophilization; (3) bunkankasaponin is in the application in Weight-reducing and lipid-lowering field: bunkankasaponin is joined mixing and stirring in the health product capsule of Weight-reducing and lipid-lowering in the ratio of 0.5% (mass ratio), can suppress the pancreatic lipase activity and reach 52%.
Embodiment 2:
Shinyleaf yellowhorn fruit shell is crushed to the 5-20 order after the degreasing, and with ethanol content 40%, 1000 milliliters of the solution of methanol content 5% soak 50g shinyleaf yellowhorn shell powder, and 70 ℃ of following lixiviates 60 minutes are filtered, and adds 30% ethanolic solution lixiviate again 30 minutes, filters, and twice filtrating is merged; (2) will filtrate under the normal pressure after boiling removes about many milliliters of ethanol, water and methyl alcohol to 200, and changing decompression into and concentrating, it is 70 ℃ that decompression concentrates condition, 0.1 atmospheric pressure.Be condensed into postlyophilization; (3) bunkankasaponin is in the application in Weight-reducing and lipid-lowering field: bunkankasaponin is joined mixing and stirring in the bread and cheese in the ratio of 1.1% (mass ratio), can suppress the pancreatic lipase activity and reach 61%.
Claims (6)
1. a bunkankasaponin extract is in the application in Weight-reducing and lipid-lowering field; It is characterized in that adopting following steps: (1) shinyleaf yellowhorn fruit shell is pulverized, and the volume that uses 20%-40% is shinyleaf yellowhorn shell opaque amount gram number 10-20 solution doubly milliliter, 70-75 ℃ of following lixiviate 60～90 minutes; Filter; Ethanolic solution lixiviate 30-60 minute that adds 30%-45% is again filtered, and twice filtrating is merged; (2) it is subsequent use filtrating to be condensed into paste, also can be Powdered with processing after the paste freeze-drying; (3) bunkankasaponin is in the application in Weight-reducing and lipid-lowering field: bunkankasaponin can significantly reduce the pancreatic lipase activity; Therefore it can join in the food in the ratio of 0.5%-1.1% (mass ratio); Food comprises bread and cheese and health food, products such as optional capsule, pulvis.
2. described a kind of bunkankasaponin extract is in the application in Weight-reducing and lipid-lowering field, and shinyleaf yellowhorn shell is pulverized order and counted the 5-20 order in the step 1, and shinyleaf yellowhorn shell needs degreasing to carry oil.
3. described a kind of bunkankasaponin extract contains 5%-10% methyl alcohol in the application in Weight-reducing and lipid-lowering field in the used solution in the step 1.
4. described a kind of bunkankasaponin extract concentrates in the step 2 and can adopt decompression to concentrate in the application in Weight-reducing and lipid-lowering field, and the decompression thickening temperature is 60～70 ℃, under 0.1～0.7 atmospheric pressure, also can adopt the normal pressure heating.
5. described a kind of bunkankasaponin extract is in the application in Weight-reducing and lipid-lowering field, wants mixing and stirring after adding health food in the step 3 to.
6. described a kind of bunkankasaponin extract is in the application in Weight-reducing and lipid-lowering field, and the mode of this health products Weight-reducing and lipid-lowering is to be approach to suppress fat absorption in the step 3.
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| Application Number | Priority Date | Filing Date | Title |
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| CN201210321207XA CN102783654A (en) | 2012-09-04 | 2012-09-04 | Application of bunkanka saponin extract in weight losing and fat lowering fields |
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| CN201210321207XA CN102783654A (en) | 2012-09-04 | 2012-09-04 | Application of bunkanka saponin extract in weight losing and fat lowering fields |
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Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1350001A (en) * | 2001-10-31 | 2002-05-22 | 杨柏珍 | Fruit shell capable of being used to extract shinyleaf yellowhorn general saponin, coarse fat, coarse protein and sugar |
| CN1626545A (en) * | 2004-07-07 | 2005-06-15 | 杨柏珍 | Compound extracted from hull and stem of yellow horn, extracting method and application |
| CN102250195A (en) * | 2011-07-05 | 2011-11-23 | 杨柏珍 | Method for producing xanthoceraside |
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2012
- 2012-09-04 CN CN201210321207XA patent/CN102783654A/en active Pending
Patent Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1350001A (en) * | 2001-10-31 | 2002-05-22 | 杨柏珍 | Fruit shell capable of being used to extract shinyleaf yellowhorn general saponin, coarse fat, coarse protein and sugar |
| CN1626545A (en) * | 2004-07-07 | 2005-06-15 | 杨柏珍 | Compound extracted from hull and stem of yellow horn, extracting method and application |
| CN102250195A (en) * | 2011-07-05 | 2011-11-23 | 杨柏珍 | Method for producing xanthoceraside |
Non-Patent Citations (6)
| Title |
|---|
| 《第二次世界中西医结合大会论文摘要集》 20021231 郑毅男等 西洋参皂甙的分离及其抑制胰脂肪酶活性的研究 第497页第1-8行 1 , * |
| 《食品科学》 20091231 李光勋等 正交试验优选文冠果壳中文冠果壳苷提取工艺 第59页左栏第4行-60页左栏16行 1 第30卷, 第2期 * |
| 刘继菊: "人参总皂苷提取工艺条件优化研究", 《中国中医药现代远程教育》, vol. 8, no. 14, 31 July 2010 (2010-07-31), pages 200 - 201 * |
| 李光勋等: "正交试验优选文冠果壳中文冠果壳苷提取工艺", 《食品科学》, vol. 30, no. 2, 31 December 2009 (2009-12-31) * |
| 王先科等: "植物皂甙降低机体胆固醇的作用及其机理研究进展", 《江西农业学报》, vol. 22, no. 1, 31 December 2010 (2010-12-31), pages 132 - 135 * |
| 郑毅男等: "西洋参皂甙的分离及其抑制胰脂肪酶活性的研究", 《第二次世界中西医结合大会论文摘要集》, 31 December 2002 (2002-12-31) * |
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Application publication date: 20121121 |