CN102774951A - Water body detoxication anti-stress agent for aquaculture and preparation method and application thereof - Google Patents
Water body detoxication anti-stress agent for aquaculture and preparation method and application thereof Download PDFInfo
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- CN102774951A CN102774951A CN201210287763XA CN201210287763A CN102774951A CN 102774951 A CN102774951 A CN 102774951A CN 201210287763X A CN201210287763X A CN 201210287763XA CN 201210287763 A CN201210287763 A CN 201210287763A CN 102774951 A CN102774951 A CN 102774951A
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Abstract
The invention discloses a pollution-free water body detoxication anti-stress agent for aquaculture and a preparation method and an application thereof, belonging to the technical field of aquaculture. The water body detoxication anti-stress agent for aquaculture comprises the following components in parts by weight: 2-5 parts of citric acid, 0.5-3 parts of tartaric acid, 0.5-2 parts of lauric acid, 1-5 parts of sodium salicylate, 0.5-3 parts of synergist, 0.5-2 parts of stabilizer and 80-90 parts of clean water. By the water body detoxication anti-stress agent for aquaculture, the water body buffer capability and anti-stress capability of aquatic animals can be improved, heavy metal ions can be rapidly complexed and degraded, toxicity of heavy metal ions and pesticide to aquatic animals is eliminated, content and toxicity of harmful substances such as ammonia nitrogen, nitrite and hydrogen sulfide in the water body are reduced, the damage of algae toxin to the aquatic animals is relieved and eliminated, a proper pH value of the water body is maintained, multiplied propagation of bacteria and virus is restrained or killed, the immune and disease resistance of aquatic animals can be rapidly enhanced, the anti-stress capability of aquatic animals is improved, and the functions of calling food, prompting appetite and enhancing the vigor of fish and prawn are realized.
Description
Technical field
The present invention relates to a kind of water body detoxifcation antistress agent, particularly a kind of water body of used for aquiculture detoxifcation antistress agent and preparation method thereof and application.
Background technology
Along with aquaculture develops to high-density, high intensive culture, a large amount of bait throwing in and excess fertilising become the raiser and culture one of common technology.But consequences such as the body eutrophication that brings thus, water quality deterioration, illness outbreak are just being destroyed the healthy benign Sustainable development of culture fishery.How to solve these contradictions in the aquaculture, the composite organic acid technology becomes one of big promising utilisation technology.
Under the state of nature; Water body can be kept the koinomatter circulation of water quality through self-purification; But along with the development of high bait throwing in, the aquaculture of high fertilising formula, organic matters such as the residual bait in the water body, ight soil, corpse have surpassed water body environment maximum load ability, and the material cycle decomposition course is obstructed.Do not become water body greatest contamination source in a large number by the organic matter of effective and reasonable utilization; Mass consumption dissolved oxygen during oxygenolysis; Cause oxygen debt to occur in advance and raise, further suppress the organism complete oxidation again, thereby generate incomplete oxidation product such as ammonia nitrogen, nitrite and hydrogen sulfide etc.These materials are very big to aquatic animal existence and growth harm influence, can cause the chronic or acute poisoning of aquatic animal.A large amount of organic matters provide the necessary carbon source of algal grown and cause a large amount of breedings as the eutrophy source; The a large amount of breedings of algae that low value harm is bigger such as blue-green algae green alga break out appearance " wawter bloom "; In order to control algae reproduction; The raiser uses high heavy metal ion medicines such as pesticide such as copper sulfate in a large number, makes heavy metal ion content rising in the water body, in the aquatic animal body, enrichment occurs.Dissolved oxygen is low to cause that the potential of hydrogen daily amplitude is big; Bacterium, mikrobe, parasite are in active state; Fish dignity is faced the low multiple stimulation that holds oxygen, high ammonia nitrogen, high nitrite and Micobial Disease, be in that immune resistibility is the most weak, subhealth state and high stress state, be very easy to take place disease.After disease such as parasite occurring, the raiser can use and contain the high agricultural chemicals of heavy metal ion and splash, and causes enrichments in the aquatic animal body such as heavy metal ion zinc, copper, harm fishery products safety and consumer health.
The single means of main employing are handled on the cultural technique at present, as to aquatic animal heavy metal poisoning situation, produce the EDTA that generally splashes and come the chelating heavy metal ion, but effect is unstable, the spinoff that pH raises also can occur; And when changing to ammonia nitrogen, nitrite content is too high or water quality reddens suddenly blackening etc., then can use products such as vitamins C or organic acid, but exist usage quantity few, take effect and wait problem slowly.Therefore still lack a kind of effective ways on producing; Complexation heavy metal ion degraded heavy metal toxicity rapidly when removing ammonia nitrogen, the too high poisoning of amounts of nitrous acid rapidly; And can many-sidedly reduce various stressed conditions in the water body, make the growth of aquatic animal safety and Health.
In recent years; Because situation such as water quality deterioration that the aquatic animal high-density breeding brings and heavy metal poisoning happen occasionally; The research electricity that this respect is handled in therefore relevant aquaculture system detoxifcation increases gradually; Such as, name is called " a kind of used for aquiculture water body splash type antistress agent ", publication number is Chinese invention patent applications such as CN102106863A.These patents or be staple with organic acid, active components of plants, tensio-active agent are sent to a place under guard the removing heavy metals toxic action, or are staple with vitamins C, amino acid and glucose, work aquatic animal physiology and the immunity function effect of recovering.But still do not have and a kind ofly can from many aspects, comprehensively remove water body each side stressor and toxic product, as bacterial micro-organism stress, low dissolved oxygen stress, ammonia nitrogen toxicity, toxicity of pesticide, heavy metal ion toxicity or the like.
Summary of the invention
In view of this; The objective of the invention is in order to overcome the deficiency that prior art exists; From the composite angle of poly-basic organic acid a kind of used for aquiculture water body detoxifcation antistress agent is provided, reduces water pH value, degradation of ammonia nitrogen, the too high toxicity of nitrite; Unwanted bacteria and microorganism growth in the control water body reduce aquatic animal by the risk of cause of disease invasion and attack; It is the heavy metal ion in complexing and the chelating water body rapidly, removes heavy metal toxicity fast, reduces the danger of heavy metal enrichment in the aquatic animal body.Based on this, the present invention also provides a kind of preparation method of used for aquiculture water body detoxifcation antistress agent, and the application of a kind of used for aquiculture water body detoxifcation antistress agent in aquaculture.
For solving the problems of the technologies described above, technical scheme of the present invention is:
A kind of used for aquiculture water body detoxifcation antistress agent; Meter comprises following component: 2～5 parts of Hydrocerol As, 0.5～3 part of tartaric acid, 0.5～2 part of LAURIC ACID 99 MIN, 1～5 part of SS, 0.5～3 part of synergistic agent, 0.5～2 part of stablizer, 80～90 parts in peace and quiet water by weight.
Preferably, meter comprises following component: 2～3 parts of Hydrocerol As, 0.5～2 part of tartaric acid, 0.5～1.5 part of LAURIC ACID 99 MIN, 1～3 part of SS, 0.5～1.5 part of synergistic agent, 0.5～1.5 part of stablizer, 80～85 parts in peace and quiet water by weight.
Preferably, meter comprises following component: 4～5 parts of Hydrocerol As, 1～2.5 part of tartaric acid, 1～1.5 part of LAURIC ACID 99 MIN, 2～4 parts of SSs, 1.5～2.5 parts of synergistic agent, 1～2 part of stablizer, 82～88 parts in peace and quiet water by weight.
Preferably, the Hydrocerol A effective ingredient is greater than 2% in the said component, and the SS effective ingredient is greater than 1%.
Preferably, described synergistic agent is any one or the two or more mixture in taurine, vitamin c, the Sodium salts humic acids.
Preferably, said stablizer is any one or the two or more mixture in EDTA, N.F,USP MANNITOL, tetramethylolmethane, the phosphorous acid ester.
The preparation method of a kind of used for aquiculture water body detoxifcation antistress agent of the present invention comprises the steps:
1) get Hydrocerol A, tartaric acid, LAURIC ACID 99 MIN, SS and peace and quiet water, press 2～5 parts of Hydrocerol As, 0.5～3 part of tartaric acid, 0.5～2 part of LAURIC ACID 99 MIN, 1～5 part of SS, the ratio that peace and quiet water is 80～90 parts is mixed stirring with aforesaid liquid and is obtained mixture;
2) again in 0.5～3 part ratio adding synergistic agent, add stablizer in 0.5～2 part ratio, stirring promptly gets.
Preferably, step 2) in, use rotating speed to stir 10-20 minute as the low-speed mixer that PM 30-80 changes.
Preferably, step 2) in, use rotating speed to stir 10-20 minute as the low-speed mixer that PM 30-80 changes.
The application of aquaculture system detoxifcation antistress agent in aquaculture of a kind of aforementioned aquaculture system detoxifcation antistress agent of the present invention and aforementioned preparing method's gained; By the every mu of used water body detoxifcation of water body antistress agent 250～300ml; With water body detoxify antistress agent with 100 times of water dilutions more than the volume after, direct full pool spilling head; Or directly splash near oxygenating machine, the mechanical stirring through oxygenating machine is uniformly distributed in the aquaculture water.
Compared with prior art, the present invention has the following advantages:
The water body detoxifcation antistress agent of used for aquiculture of the present invention; From the composite angle of poly-basic organic acid; Utilize various actual productions to prove that effective organic acid monomer carries out compound proportioning according to suitable ratio; Add synergistic agent and stablizer, mix as carrier with the peace and quiet water of easy acquisition and obtain, it has the following advantages:
1, reduce water pH value, degradation of ammonia nitrogen, the too high toxicity of nitrite, unwanted bacteria and microorganism growth in the control water body reduce aquatic animal by the risk of cause of disease invasion and attack;
2, the heavy metal ion in rapid complexing and the chelating water body is removed heavy metal toxicity fast, reduces the danger of heavy metal enrichment in the aquatic animal body.
3, comprehensively remove various stressors and toxic harm in the water body all sidedly, reach the effect of detoxifcation anti-stress.And because natural tartaric acid is distinguished the flavor of in the product of the present invention, have the function of food calling appetizing, can strengthen the fishes and shrimps vigor, reduce the generation of disease.
Embodiment
Basic design of the present invention is: poly-basic organic acid provided by the invention is that two or more organic acidulants is composited by a certain percentage; Utilize the complementation synergy between the different acids; Can improve water body surge capability and aquatic animal anti-stress ability; Complexing degraded heavy metal ion is eliminated the toxicity hazard of chemical pollutions such as heavy metal ion and agricultural chemicals to hydrocoles rapidly; Can reduce content of harmful and toxicity such as ammonia nitrogen in the water body, nitrite, hydrogen sulfide, alleviate and eliminate the harm that algae toxin causes aquatic animal; Can keep the suitable pH pH of water body, the procreation of inhibition and kill bacteria and virus is propagated; Can promote aquatic animal immunological competence and resistance against diseases fast, improve the aquatic animal anti-stress ability; And the food calling appetizing is arranged, strengthen the effect of fishes and shrimps vigor; The present invention produces and is easy to use, does not receive the limitations affect of envrionment conditions, and result of use is rapid and stable.
In order to make those skilled in the art understand technical scheme of the present invention better, the present invention is described in further detail below by specific embodiment.
Embodiment one
The used for aquiculture water body of present embodiment detoxifcation antistress agent comprises the component of following weight part:
2 parts of Hydrocerol As, 1.5 parts of tartaric acid, 0.8 part of LAURIC ACID 99 MIN, 1.5 parts of SSs, 1.2 parts of taurines, EDTA1 part, 92 parts in peace and quiet water.
The used for aquiculture water body detoxifcation antistress agent of present embodiment, its preparation method is following:
Get Hydrocerol A, tartaric acid, LAURIC ACID 99 MIN, SS and peace and quiet water, press 2 parts of Hydrocerol As, 1.5 parts of tartaric acid; 0.8 part of LAURIC ACID 99 MIN, 1.5 parts of SSs, the ratio that peace and quiet water is 92 parts is mixed stirring with aforesaid liquid and is obtained mixture; Add 1.2 parts of taurines again; Add EDTA1 part, continue to stir, the low-speed mixer that uses PM 30-80 to change continues churning time and is 10-20 minute.With liquid mixture pack into according to quantity 2kg packing bag and vacuum sealed package.
The used for aquiculture water body detoxifcation antistress agent of present embodiment, its method of use is:
Get the used for aquiculture water body detoxifcation antistress agent that present embodiment makes; By every mu of water body (1 meter of the depth of water) consumption 250～300ml,, or directly splash near oxygenating machine with the direct full pool spilling head in water dilution back more than 100 times; Mechanical stirring through oxygenating machine is uniformly distributed in the aquaculture water.
Embodiment two
The used for aquiculture water body of present embodiment detoxifcation antistress agent comprises the component of following weight part:
2.5 parts of Hydrocerol As, 1.6 parts of tartaric acid, 1.2 parts of LAURIC ACID 99 MIN, 2.0 parts of SSs, 1.5 parts of taurines, EDTA1.2 part, 90 parts in peace and quiet water.
The used for aquiculture water body detoxifcation antistress agent of present embodiment, its preparation method is following:
Get Hydrocerol A, tartaric acid, LAURIC ACID 99 MIN, SS and peace and quiet water, press 2.5 parts of Hydrocerol As, 1.6 parts of tartaric acid; 1.2 parts of LAURIC ACID 99 MIN, 2.0 parts of SSs, the ratio that peace and quiet water is 90 parts is mixed stirring with aforesaid liquid and is obtained mixture; Add 1.5 parts of taurines again; Add EDTA1.2 part, continue to stir, the low-speed mixer that uses PM 30-80 to change continues churning time and is 10-20 minute.With liquid mixture pack into according to quantity 2kg packing bag and vacuum sealed package.
The used for aquiculture water body detoxifcation antistress agent of present embodiment, its method of use is:
Get product of the present invention by every mu of water body (1 meter of the depth of water) consumption 250～300ml, with the direct full pool spilling head in water dilution back more than 100 times, or directly splash near oxygenating machine, the mechanical stirring through oxygenating machine is uniformly distributed in the aquaculture water.
Embodiment three
The used for aquiculture water body of present embodiment detoxifcation antistress agent comprises the component of following weight part:
3 parts of Hydrocerol As, 1.8 parts of tartaric acid, 1 part of LAURIC ACID 99 MIN, 2.2 parts of SSs, 1.5 parts of taurines, EDTA1.5 part, 89 parts in peace and quiet water.
The used for aquiculture water body detoxifcation antistress agent of present embodiment, its preparation method is following:
Get Hydrocerol A, tartaric acid, LAURIC ACID 99 MIN, SS and peace and quiet water, press 3 parts of Hydrocerol As, 1.8 parts of tartaric acid; 1 part of LAURIC ACID 99 MIN, 2.2 parts of SSs, the ratio that peace and quiet water is 89 parts is mixed stirring with aforesaid liquid and is obtained mixture; Add 1.5 parts of taurines again; Add EDTA1.5 part, continue to stir, the low-speed mixer that uses PM 30-80 to change continues churning time and is 10-20 minute.With liquid mixture pack into according to quantity 2kg packing bag and vacuum sealed package.
The used for aquiculture water body detoxifcation antistress agent of present embodiment, its method of use is:
Get product of the present invention by every mu of water body (1 meter of the depth of water) consumption 250～300ml, with the direct full pool spilling head in water dilution back more than 100 times, or directly splash near oxygenating machine, the mechanical stirring through oxygenating machine is uniformly distributed in the aquaculture water.
The prescription of used for aquiculture water body detoxifcation antistress agent of the present invention can also adopt following embodiment (each component is a weight part):
| Sequence number | Hydrocerol A | Tartaric acid | LAURIC ACID 99 MIN | SS | Taurine | EDTA | Peace and quiet water |
| Embodiment four | 2 | 3 | 2 | 1 | 2 | 1 | 85 |
| Embodiment five | 4 | 2 | 1 | 3 | 3 | 0.5 | 80 |
| Embodiment six | 3 | 1.5 | 0.9 | 4 | 2 | 2 | 88 |
| Embodiment seven | 5 | 1 | 1.5 | 5 | 0.5 | 1.5 | 82 |
| Embodiment eight | 2.5 | 2.5 | 0.5 | 4 | 1.5 | 1 | 84 |
Among the above embodiment; The synergistic agent that provides is a taurine; This is a kind of preferred scheme, in actual implementation process, also can adopt any one or two kinds in vitamin c, the Sodium salts humic acids as synergistic agent; Also can be with any one or two or more mixing the in taurine and vitamin c, the Sodium salts humic acids, as synergistic agent.
Among the above embodiment; Used stablizer is EDTA, and in other embodiments, stablizer also can be N.F,USP MANNITOL, tetramethylolmethane; In the phosphorous acid ester any one or two or more mixtures; Also can be with EDTA and N.F,USP MANNITOL, tetramethylolmethane, any one in the phosphorous acid ester or two or more mixing are as stablizer.
Below through concrete test the implementation result of used for aquiculture water body of the present invention detoxifcation antistress agent is verified:
Test one: in the sluice gate jewfish cultivating pool of Guangdong, use 8.2 mu of areas.The pond water colour is color of soy sauce, and algal grown is the trend of ruining.Analyze discovery through water quality detection, dissolved oxygen is 3.5mg/L in the water body, and the pH value is 9.5, and copper content is 0.1mg/L, and breed jewfish appetite is low, and feeding intake, it is poor to rob food.Be selected in fine day point in the mornings 9 during use, used for aquiculture water body of the present invention is detoxified antistress agent in accordance with method of use, by every mu of water body (1 meter of the depth of water) consumption 270ml, with direct full pool spilling head after the water dilution more than 100 times.Used 3 days continuously.Detected water quality on the 4th day, dissolved oxygen is upgraded to 5.5mg/L, and the pH value reduces to 8.0, and copper content is reduced to 0.01mg/L.Water colour transfers green to, and algae is main with diatom and chlorella growth, and the breed jewfish feeds intake and robs the food ferociousness.
Test two: in Guangdong Jiangmen tilapia cultivating pool, use 6.5 mu of areas.Pond waters is muddy, overfertilization, and transparency is low, has blue brown oil film to cover, and the naked eyes visible bubble in bubble is up emitted at the bottom of the pond, and can smell fishy odor at pool side.Tilapia gill filament raisin, color is dark red not bright-coloured.Ammonia nitrogen chronic poisoning situation appears in the ammonia-nitrogen content severe overweight.Analyze discovery through water quality detection, dissolved oxygen is 3.0mg/L in the water body, and the pH value is 11, and ammonia nitrogen is 2.8mg/L, and cultivating tilapia appetite descends, and tilapia occurs less when feeding intake.Be selected in fine day point in the mornings 10 during use, used for aquiculture water body of the present invention is detoxified antistress agent in accordance with method of use, by every mu of water body (1 meter of the depth of water) consumption 350ml, with direct full pool spilling head after the water dilution more than 100 times.Used 3 days continuously.Detected water quality on the 4th day, dissolved oxygen is upgraded to 5.2mg/L, and the pH value reduces to 7.4, and ammonia-nitrogen content is reduced to 0.2mg/L.Water colour transfers green to, and the tilapia gill filament is scarlet, and color is bright-coloured, and cultivating tilapia feeds intake and robs the dyspepsia utmost point.
Test three: in the grass carp cultivating pool of yiyang, hunan Nan County, use 10.5 mu of areas.This pond is a cement pit, 1.5 meters of the depth of waters, and water colour is pearl.The water quality dissolved oxygen is 3.1mg/L, and the pH value is 9.1, and ammonia-nitrogen content is 1.2mg/L, occurs dead movement pattern of fish condition when drawing in the net fish, dead altogether 1745 jin of grass carp, silver carp and bighead.Used for aquiculture water body detoxifcation antistress agent of the present invention is abideed by method of use, press every mu of water body (1 meter of the depth of water) consumption 300ml in the fine morning 9, dilute directly full pool spilling head of back with water more than 100 times.Used 3 days continuously.Detected water quality on the 4th day, dissolved oxygen is upgraded to 5.0mg/L, and the pH value reduces to 7.5, and ammonia-nitrogen content is reduced to 0.1mg/L.Death does not appear in grass carp and bighead when drawing in the net to fish, and only silver carp is dead 25 jin.
More than the present invention has been carried out detailed introduction, use concrete example in the literary composition principle of the present invention and embodiment set forth, the explanation of above embodiment just is used for helping to understand method of the present invention and core concept thereof.Should be pointed out that for those skilled in the art, under the prerequisite that does not break away from the principle of the invention, can also carry out some improvement and modification to the present invention, these improvement and modification also fall in the protection domain of claim of the present invention.
Claims (10)
1. used for aquiculture water body detoxifcation antistress agent; It is characterized in that: count by weight, comprise following component: 2～5 parts of Hydrocerol As, 0.5～3 part of tartaric acid, 0.5～2 part of LAURIC ACID 99 MIN, 1～5 part of SS, 0.5～3 part of synergistic agent, 0.5～2 part of stablizer, 80～90 parts in peace and quiet water.
2. used for aquiculture water body detoxifcation antistress agent according to claim 1; It is characterized in that; Meter comprises following component: 2～3 parts of Hydrocerol As, 0.5～2 part of tartaric acid, 0.5～1.5 part of LAURIC ACID 99 MIN, 1～3 part of SS, 0.5～1.5 part of synergistic agent, 0.5～1.5 part of stablizer, 80～85 parts in peace and quiet water by weight.
3. used for aquiculture water body detoxifcation antistress agent according to claim 1; It is characterized in that; Meter comprises following component: 4～5 parts of Hydrocerol As, 1～2.5 part of tartaric acid, 1～1.5 part of LAURIC ACID 99 MIN, 2～4 parts of SSs, 1.5～2.5 parts of synergistic agent, 1～2 part of stablizer, 82～88 parts in peace and quiet water by weight.
4. used for aquiculture water body detoxifcation antistress agent according to claim 1 is characterized in that Hydrocerol A effective constituent is greater than 2% in the said component, and SS effective constituent is greater than 1%.
5. used for aquiculture water body according to claim 1 detoxifcation antistress agent is characterized in that, said synergistic agent is any one or the two or more mixture in taurine, vitamin c, the Sodium salts humic acids.
6. used for aquiculture water body according to claim 1 detoxifcation antistress agent is characterized in that, said stablizer is any one or the two or more mixture in EDTA, N.F,USP MANNITOL, tetramethylolmethane, the phosphorous acid ester.
7. the preparation method of a used for aquiculture water body detoxifcation antistress agent is characterized in that, comprises the steps:
1) get Hydrocerol A, tartaric acid, LAURIC ACID 99 MIN, SS and peace and quiet water, press 2～5 parts of Hydrocerol As, 0.5～3 part of tartaric acid, 0.5～2 part of LAURIC ACID 99 MIN, 1～5 part of SS, the ratio that peace and quiet water is 80～90 parts is mixed stirring with aforesaid liquid and is obtained mixture;
2) again in 0.5～3 part ratio adding synergistic agent, add stablizer in 0.5～2 part ratio, stirring promptly gets.
8. the preparation method of used for aquiculture water body detoxifcation antistress agent according to claim 7 is characterized in that step 2) in, use rotating speed to stir 10-20 minute as the low-speed mixer that PM 30-80 changes.
9. the preparation method of used for aquiculture water body detoxifcation antistress agent according to claim 7 is characterized in that step 2) in, use rotating speed to stir 15 minutes as the low-speed mixer that PM 30-80 changes.
10. the application of aquaculture system detoxifcation antistress agent in aquaculture like preparing method's gained of claim 1～6 aquaculture system detoxifcation antistress agent and claim 7～9; It is characterized in that; By the used water body detoxifcation of every mu of water body antistress agent 250～300ml, with water body detoxify antistress agent with 100 times of water dilutions more than the volume after, near direct full pool spilling head or directly splash oxygenating machine; Mechanical stirring through oxygenating machine is uniformly distributed in the aquaculture water.
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| CN113277604A (en) * | 2021-06-11 | 2021-08-20 | 潍坊加易加生物科技有限公司 | Method for improving water quality and inhibiting vibrio in aquaculture and preparation |
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