CN102758350A - Textile product printing and dyeing method - Google Patents
Textile product printing and dyeing method Download PDFInfo
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- CN102758350A CN102758350A CN2011101092651A CN201110109265A CN102758350A CN 102758350 A CN102758350 A CN 102758350A CN 2011101092651 A CN2011101092651 A CN 2011101092651A CN 201110109265 A CN201110109265 A CN 201110109265A CN 102758350 A CN102758350 A CN 102758350A
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- dyeing
- dyeing method
- modification
- fabrics printing
- natural fabric
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- 238000004043 dyeing Methods 0.000 title claims abstract description 50
- 238000000034 method Methods 0.000 title claims abstract description 31
- 238000007639 printing Methods 0.000 title claims abstract description 31
- 239000004753 textile Substances 0.000 title claims abstract description 29
- 230000004048 modification Effects 0.000 claims abstract description 26
- 238000012986 modification Methods 0.000 claims abstract description 26
- 239000003607 modifier Substances 0.000 claims abstract description 26
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims abstract description 16
- 229930182559 Natural dye Natural products 0.000 claims abstract description 14
- 239000000978 natural dye Substances 0.000 claims abstract description 14
- AZDRQVAHHNSJOQ-UHFFFAOYSA-N alumane Chemical class [AlH3] AZDRQVAHHNSJOQ-UHFFFAOYSA-N 0.000 claims abstract description 5
- 150000003839 salts Chemical class 0.000 claims abstract description 5
- 239000004744 fabric Substances 0.000 claims description 48
- 239000000975 dye Substances 0.000 claims description 31
- 238000010792 warming Methods 0.000 claims description 15
- RBTARNINKXHZNM-UHFFFAOYSA-K iron trichloride Chemical compound Cl[Fe](Cl)Cl RBTARNINKXHZNM-UHFFFAOYSA-K 0.000 claims description 14
- 159000000013 aluminium salts Chemical class 0.000 claims description 10
- 229910000329 aluminium sulfate Inorganic materials 0.000 claims description 10
- 150000002500 ions Chemical class 0.000 claims description 10
- 238000009413 insulation Methods 0.000 claims description 9
- DIZPMCHEQGEION-UHFFFAOYSA-H aluminium sulfate (anhydrous) Chemical compound [Al+3].[Al+3].[O-]S([O-])(=O)=O.[O-]S([O-])(=O)=O.[O-]S([O-])(=O)=O DIZPMCHEQGEION-UHFFFAOYSA-H 0.000 claims description 8
- 235000003891 ferrous sulphate Nutrition 0.000 claims description 8
- 239000011790 ferrous sulphate Substances 0.000 claims description 8
- BAUYGSIQEAFULO-UHFFFAOYSA-L iron(2+) sulfate (anhydrous) Chemical compound [Fe+2].[O-]S([O-])(=O)=O BAUYGSIQEAFULO-UHFFFAOYSA-L 0.000 claims description 8
- 229910000359 iron(II) sulfate Inorganic materials 0.000 claims description 8
- 238000010438 heat treatment Methods 0.000 claims description 7
- 239000000835 fiber Substances 0.000 abstract description 7
- 238000005562 fading Methods 0.000 abstract description 2
- UFHFLCQGNIYNRP-UHFFFAOYSA-N Hydrogen Chemical compound [H][H] UFHFLCQGNIYNRP-UHFFFAOYSA-N 0.000 abstract 1
- 229910052739 hydrogen Inorganic materials 0.000 abstract 1
- 239000001257 hydrogen Substances 0.000 abstract 1
- 230000001105 regulatory effect Effects 0.000 abstract 1
- 244000163122 Curcuma domestica Species 0.000 description 10
- 235000003392 Curcuma domestica Nutrition 0.000 description 10
- 235000003373 curcuma longa Nutrition 0.000 description 10
- 230000007935 neutral effect Effects 0.000 description 10
- 235000013976 turmeric Nutrition 0.000 description 10
- 241000219991 Lythraceae Species 0.000 description 9
- 235000014360 Punica granatum Nutrition 0.000 description 9
- 230000007613 environmental effect Effects 0.000 description 5
- 230000000536 complexating effect Effects 0.000 description 4
- -1 iron ion Chemical class 0.000 description 4
- 238000005406 washing Methods 0.000 description 4
- XEEYBQQBJWHFJM-UHFFFAOYSA-N iron Substances [Fe] XEEYBQQBJWHFJM-UHFFFAOYSA-N 0.000 description 3
- 229910052742 iron Inorganic materials 0.000 description 3
- 102000004190 Enzymes Human genes 0.000 description 2
- 108090000790 Enzymes Proteins 0.000 description 2
- 239000003795 chemical substances by application Substances 0.000 description 2
- 238000004140 cleaning Methods 0.000 description 2
- 238000010586 diagram Methods 0.000 description 2
- 238000005516 engineering process Methods 0.000 description 2
- 229910001385 heavy metal Inorganic materials 0.000 description 2
- 238000004519 manufacturing process Methods 0.000 description 2
- 238000007670 refining Methods 0.000 description 2
- 239000000344 soap Substances 0.000 description 2
- 241000370738 Chlorion Species 0.000 description 1
- 229920000742 Cotton Polymers 0.000 description 1
- 244000020551 Helianthus annuus Species 0.000 description 1
- 235000003222 Helianthus annuus Nutrition 0.000 description 1
- MHAJPDPJQMAIIY-UHFFFAOYSA-N Hydrogen peroxide Chemical compound OO MHAJPDPJQMAIIY-UHFFFAOYSA-N 0.000 description 1
- 241000200487 Rhigozum obovatum Species 0.000 description 1
- 229910052782 aluminium Inorganic materials 0.000 description 1
- REDXJYDRNCIFBQ-UHFFFAOYSA-N aluminium(3+) Chemical compound [Al+3] REDXJYDRNCIFBQ-UHFFFAOYSA-N 0.000 description 1
- 238000004040 coloring Methods 0.000 description 1
- 238000010276 construction Methods 0.000 description 1
- 230000018044 dehydration Effects 0.000 description 1
- 238000006297 dehydration reaction Methods 0.000 description 1
- 239000000986 disperse dye Substances 0.000 description 1
- 210000004209 hair Anatomy 0.000 description 1
- 239000000543 intermediate Substances 0.000 description 1
- 239000006210 lotion Substances 0.000 description 1
- 239000002932 luster Substances 0.000 description 1
- 150000002736 metal compounds Chemical class 0.000 description 1
- 238000012856 packing Methods 0.000 description 1
- 239000010957 pewter Substances 0.000 description 1
- 229910000498 pewter Inorganic materials 0.000 description 1
- 231100000614 poison Toxicity 0.000 description 1
- 230000007096 poisonous effect Effects 0.000 description 1
- 238000002203 pretreatment Methods 0.000 description 1
- 239000000985 reactive dye Substances 0.000 description 1
- 241000894007 species Species 0.000 description 1
- 239000000126 substance Substances 0.000 description 1
- 210000002268 wool Anatomy 0.000 description 1
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Abstract
The invention provides a textile product printing and dyeing method including: subjecting natural fibers to ionic modification; adding aluminum salt or ferric salt modifiers when the water temperature in a dyeing vat is 45-55 DEG C, increasing the temperature to 70-90 DEG C and holding; dyeing the modified natural fibers; and adding natural dye when the water temperature in the dyeing vat is 40-60 DEG C, regulating the pH (potential of hydrogen) to 3-10, increasing the temperature to 70-99 DEG C and holding. Textile products printed and dyed by the textile product printing and dyeing method are environment-friendly and uniform in dyeing without fading.
Description
Technical field
The present invention relates to the fabrics printing and dyeing field, relate in particular to a kind of method of fabrics printing and dyeing.
Background technology
Textiles is human essential daily necessities, and the character of employed dyestuff and other chemical articles directly influences people's the health and the development of society in the fabrics printing and dyeing process.Along with the develop rapidly of textile industry, a large amount of dye species bright in colour, that coloring intensity is high, dyeability is excellent, fastness is good constantly are developed, and have also increased high-grade dyestuffs such as reducing dye, REACTIVE DYES, DISPERSE DYES simultaneously.But these dyestuffs many intermediates in process of production are poisonous.The raising of Along with people's environmental consciousness, the pollution problem that synthetic dyestuffs are brought in production and application process more and more causes people's attention, people begin to abandon synthetic dyestuffs, and are to use natural dye that textiles is dyeed.
Use natural dye that textiles is dyeed in the prior art, need repeatedly use modifier and dyeing auxiliaries, technological process is complicated, and cost is higher; And how the modifier that uses all contains heavy metal, bigger to human harm; And Color and bad, shortcoming such as it is inhomogeneous to tend to occur fading, dye.
Summary of the invention
The method that the purpose of this invention is to provide a kind of fabrics printing and dyeing, the textiles environmental protection of printing and dyeing, and even dyeing, do not fade.
A kind of fabrics printing and dyeing method provided by the invention is achieved in that
A kind of fabrics printing and dyeing method comprises step:
The natural fabric ion modification: during water temperature to 45 in dye vat～55 ℃, add aluminium salt or molysite modifier, intensification 70-90 ℃, insulation;
Natural fabric to after the modification dyes: during water temperature to 40 in dye vat～60 ℃, add natural dye, PH is adjusted to 3～10, is warming up to 70-99 ℃, insulation.
Optional, aluminum salt modified dose of said adding is aluminum sulfate, the molysite modifier of said adding is ferrous sulfate.
Optional, said textiles after the modification is dyeed, PH is adjusted to 4～5 or 9～10, is warming up to 70～90 ℃.
Optional, during said adding natural dye, also add salt.
Optional, said natural fabric after the modification is dyeed, PH is adjusted to 3～5, is warming up to 80～99 ℃.
Optional, said natural fabric after the modification is dyeed, PH is adjusted to 4～5, is warming up to 70～80 ℃.
Optional, said natural fabric after the modification is dyeed, the heating rate that is warming up to 60-99 ℃ is 1～3 ℃/min.
Optional, in the said natural fabric ion modification, being warming up to, 70-90 ℃ heating rate is 1～5 ℃/min.
Optional, the bath raio in the said natural fabric ion modification is: 1: 8～20.
Optional, said bath raio during natural fabric after the modification is dyeed is: 1: 5～30.
The present invention uses aluminium salt or molysite as modifier, and as modifier, environmental protection of the present invention is polluted little with respect to the available technology adopting heavy metal compound.And the present invention has only added modifier in textile fiber ion modification step, all need add modifier with respect to a plurality of steps in the prior art, and technological process is simple, and cost is low.When the textiles of the present invention after to modification dyes, add natural dye, regulate pH value to 3～10 simultaneously, with respect to the dyestuff that repeatedly uses modifier in the prior art, the textile coloration of printing and dyeing out is even, does not fade after the washing.
Further, the present invention is directed to string, when adding natural dye, also add salt, the textiles color and luster brightness of printing and dyeing is high.
Description of drawings
Fig. 1 is a fabrics printing and dyeing method flow diagram provided by the invention.
The specific embodiment
Fabrics printing and dyeing method provided by the invention; In natural fabric ion modification step, add molysite or aluminum salt modified dose, make natural fabric ion and molysite or the complexing of aluminium salt; Cleaning textiles then; Again further to complexing iron ion or aluminum ions natural fabric dye, dyeing is accomplished in the further complexing of natural dye and iron ion or aluminium ion.For specifying the present invention, provide detailed operating process that fabrics printing and dyeing method provided by the invention is described as follows.
As shown in Figure 1 is fabrics printing and dyeing method flow diagram provided by the invention, comprising:
The textiles natural fabric is carried out the refining enzyme handle, refining enzyme 1～2g/L, hydrogen peroxide solution 3～6g/L, insulation is 40 minutes in 80～90 ℃ of water, bath raio 1: 8-20.Insulation is put 1-3g/L environment-friendly soap lotion after finishing, and with textiles cloth cover wash clean, keeps textiles natural fabric pH to neutral.
Be specially: bath raio is 1: 8-20; The amount that aluminum salt modified dose or molysite modifier add: with the percentage by weight of natural fabric be 0.1-50%.Dissolve in the water with 40 ℃ of aluminium salt or molysite modifier, during water temperature to 45 in dye vat～55 ℃, add the aluminium salt or the molysite modifier that dissolve; Be warming up to 70-90 ℃ according to different natural fibre construction; Heating rate is 1-5 ℃/min, and insulation 30-40min is after modification time finishes; With complexing iron ion or chlorion the cold wash of textiles elder generation once, hot water wash is once again.
Needing explanation is that those skilled in the art can confirm according to different textile fiber structures: bath raio, the amount of the percentage by weight of adding modifier and fiber is confirmed the intensification temperature, confirms heating rate.
Specifically: bath raio 1: 5-30, natural dye is dissolved in 30～50 ℃ water, during water temperature to 40 in dye vat～60 ℃, add natural dye, if textiles is that string also adds salt 1～10g/L simultaneously, pH regulator is to 3-5, between the neutral or 9-10.Begin the dyeing that heats up then, heating rate is 1-3 ℃/min, is warming up to 70～99 ℃, insulation 30-40min, and dyeing finishes.
Need to prove that those skilled in the art can confirm bath raio according to different textile fiber structures, the characteristic of different natural dyes confirms to add the temperature of natural dye.
Elder generation's cold wash is once washed 10min; Use 70-80 ℃ hot water wash again; Use 50-60 ℃ hot water again, use the industry environmental protection soaping agent 0.1-1g/L 10-20min that soaps; And then once with hot water wash; After cleaning with cold water again, be warming up to the fastness modifying agent of 30～40 ℃ of addings and textiles weight ratio 1%～3%, insulation 30min.
Specifically: the textiles after will washing carries out soft finish → dehydration → oven dry preshrunk typing → packing, finished product.
Use the textiles environmental protection of fabrics printing and dyeing method provided by the invention printing and dyeing, pollute for a short time, and technological process is simple, and cost is low, and the textile coloration of printing and dyeing out is even, does not fade after the washing.
For illustrating further fabrics printing and dyeing method provided by the invention, concrete embodiment is provided below.
Embodiment one
This embodiment uses cotton fiber as the dyeing object, uses aluminium salt or molysite as modifier respectively, with turmeric and pomegranate respectively as dyestuff.Specifically shown in table one and table two.
Table one
Table two
Embodiment two
This embodiment uses wool class textiles as the dyeing object, uses aluminium salt or molysite as modifier respectively, with turmeric and pomegranate respectively as dyestuff, specifically shown in table three, table four.
| Dyestuff | Modifier | Dyeing temperature | PH value, dye the back color |
| Pomegranate | Aluminum sulfate | 80～99 | 3～5 or neutral: yellow careless look |
| Pomegranate | Ferrous sulfate | 80～99 | 3～5 or neutral: celadon |
Table three
| Dyestuff | Modifier | Dyeing temperature | PH value, dye the back color |
| Turmeric | Aluminum sulfate | 80～99 | 3～5 or neutral: gorgeous yellow |
| Turmeric | Ferrous sulfate | 80～99 | 3～5 or neutral: yellowish orange |
Table four
Embodiment three
This embodiment uses silk class textiles as the dyeing object, uses aluminium salt or molysite as modifier respectively, with turmeric and pomegranate respectively as dyestuff, specifically shown in table five, table six.
| Dyestuff | Modifier | Dyeing temperature | PH value, dye the back color |
| Turmeric | Aluminum sulfate | 70～80 | 4～5 or neutral: sunflower is yellow |
| Turmeric | Ferrous sulfate | 70～80 | 4～5 or neutral: yellowish orange |
Table five
| Dyestuff | Modifier | Dyeing temperature | PH value, dye the back color |
| Pomegranate | Aluminum sulfate | 70～80 | 4～5 or neutral: bright careless look |
| Pomegranate | Ferrous sulfate | 70～80 | 4～5 or neutral: pewter |
Table six
Embodiment four
This embodiment uses the hair bleached as the dyeing object, uses aluminium salt or molysite as modifier respectively, with turmeric and pomegranate respectively as dyestuff, specifically shown in table seven, table eight.
| Dyestuff | Modifier | Dyeing temperature | PH value, dye the back color |
| Turmeric | Aluminum sulfate | 70～80 | 3-5: deadgress |
| Turmeric | Ferrous sulfate | 70～80 | 3-5: yellowish orange |
Table seven
| Dyestuff | Modifier | Dyeing temperature | PH value, dye the back color |
| Pomegranate | Aluminum sulfate | 70～80 | 3-5: gorgeous yellow |
| Pomegranate | Ferrous sulfate | 70～80 | 3-5: field gray |
Table eight
The above is merely preferred embodiment of the present invention, not in order to restriction the present invention, all any modifications of within spirit of the present invention and principle, being done, is equal to and replaces and improvement etc., all should be included within protection scope of the present invention.
Claims (10)
1. a fabrics printing and dyeing method is characterized in that, comprises step:
The natural fabric ion modification: during water temperature to 45 in dye vat～55 ℃, add aluminium salt or molysite modifier, intensification 70-90 ℃, insulation;
Natural fabric to after the modification dyes: during water temperature to 40 in dye vat～60 ℃, add natural dye, PH is adjusted to 3～10, is warming up to 70-99 ℃, insulation.
2. fabrics printing and dyeing method according to claim 1 is characterized in that, aluminum salt modified dose of said adding is aluminum sulfate, and the molysite modifier of said adding is ferrous sulfate.
3. fabrics printing and dyeing method according to claim 2 is characterized in that, said textiles after the modification is dyeed, and PH is adjusted to 4～5 or 9～10, be warming up to 70～90 ℃.
4. fabrics printing and dyeing method according to claim 3 is characterized in that, during said adding natural dye, also adds salt.
5. fabrics printing and dyeing method according to claim 2 is characterized in that, said natural fabric after the modification is dyeed, and PH is adjusted to 3～5, be warming up to 80～99 ℃.
6. fabrics printing and dyeing method according to claim 2 is characterized in that, said natural fabric after the modification is dyeed, and PH is adjusted to 4～5, be warming up to 70～80 ℃.
7. fabrics printing and dyeing method according to claim 1 is characterized in that, said natural fabric after the modification is dyeed, and the heating rate that is warming up to 70-99 ℃ is 1～3 ℃/min.
8. fabrics printing and dyeing method according to claim 1 is characterized in that, in the said natural fabric ion modification, is warming up to, and 70-90 ℃ heating rate is 1～5 ℃/min.
9. fabrics printing and dyeing method according to claim 1 is characterized in that, the bath raio in the said natural fabric ion modification is: 1: 8～20.
10. fabrics printing and dyeing method according to claim 1 is characterized in that, said bath raio during natural fabric after the modification is dyeed is: 1: 5～30.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201110109265.1A CN102758350B (en) | 2011-04-29 | 2011-04-29 | Textile product printing and dyeing method |
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| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201110109265.1A CN102758350B (en) | 2011-04-29 | 2011-04-29 | Textile product printing and dyeing method |
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| Publication Number | Publication Date |
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| CN102758350A true CN102758350A (en) | 2012-10-31 |
| CN102758350B CN102758350B (en) | 2014-12-10 |
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Cited By (10)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN103643546A (en) * | 2013-11-27 | 2014-03-19 | 常熟市琴达针织印染有限公司 | Textile dyeing and printing method |
| CN104389198A (en) * | 2014-12-15 | 2015-03-04 | 常熟市启弘纺织实业有限公司 | Environment-friendly dyeing method of textile |
| CN104389197A (en) * | 2014-12-15 | 2015-03-04 | 常熟市启弘纺织实业有限公司 | Fabric printing and dyeing method |
| CN104389200A (en) * | 2014-12-15 | 2015-03-04 | 常熟市启弘纺织实业有限公司 | Dyeing method of textile |
| CN104389199A (en) * | 2014-12-15 | 2015-03-04 | 常熟市启弘纺织实业有限公司 | Uniform fabric printing and dyeing method |
| CN104404789A (en) * | 2014-12-15 | 2015-03-11 | 常熟市启弘纺织实业有限公司 | Uniform printing and dyeing method for fabric |
| CN104452335A (en) * | 2014-12-15 | 2015-03-25 | 常熟市启弘纺织实业有限公司 | Environment-friendly printing and dyeing method for textile |
| CN104499309A (en) * | 2014-12-15 | 2015-04-08 | 常熟市启弘纺织实业有限公司 | Environment-friendly printing and dyeing method of fabric |
| CN105332290A (en) * | 2015-10-12 | 2016-02-17 | 浙江纺织服装职业技术学院 | Iron rust and plant dyeing creative fabric production method |
| CN111235912A (en) * | 2019-05-22 | 2020-06-05 | 姚发礼 | Printing and dyeing finishing method for food-grade textiles and application thereof |
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| Publication number | Priority date | Publication date | Assignee | Title |
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| CN103643546A (en) * | 2013-11-27 | 2014-03-19 | 常熟市琴达针织印染有限公司 | Textile dyeing and printing method |
| CN104389198A (en) * | 2014-12-15 | 2015-03-04 | 常熟市启弘纺织实业有限公司 | Environment-friendly dyeing method of textile |
| CN104389197A (en) * | 2014-12-15 | 2015-03-04 | 常熟市启弘纺织实业有限公司 | Fabric printing and dyeing method |
| CN104389200A (en) * | 2014-12-15 | 2015-03-04 | 常熟市启弘纺织实业有限公司 | Dyeing method of textile |
| CN104389199A (en) * | 2014-12-15 | 2015-03-04 | 常熟市启弘纺织实业有限公司 | Uniform fabric printing and dyeing method |
| CN104404789A (en) * | 2014-12-15 | 2015-03-11 | 常熟市启弘纺织实业有限公司 | Uniform printing and dyeing method for fabric |
| CN104452335A (en) * | 2014-12-15 | 2015-03-25 | 常熟市启弘纺织实业有限公司 | Environment-friendly printing and dyeing method for textile |
| CN104499309A (en) * | 2014-12-15 | 2015-04-08 | 常熟市启弘纺织实业有限公司 | Environment-friendly printing and dyeing method of fabric |
| CN105332290A (en) * | 2015-10-12 | 2016-02-17 | 浙江纺织服装职业技术学院 | Iron rust and plant dyeing creative fabric production method |
| CN111235912A (en) * | 2019-05-22 | 2020-06-05 | 姚发礼 | Printing and dyeing finishing method for food-grade textiles and application thereof |
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|---|---|
| CN102758350B (en) | 2014-12-10 |
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