CN105463876B - A kind of reducing dye bathes ready-made clothes dyeing technology together with water-soluble sulfur dye - Google Patents
A kind of reducing dye bathes ready-made clothes dyeing technology together with water-soluble sulfur dye Download PDFInfo
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- CN105463876B CN105463876B CN201510994883.7A CN201510994883A CN105463876B CN 105463876 B CN105463876 B CN 105463876B CN 201510994883 A CN201510994883 A CN 201510994883A CN 105463876 B CN105463876 B CN 105463876B
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- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06P—DYEING OR PRINTING TEXTILES; DYEING LEATHER, FURS OR SOLID MACROMOLECULAR SUBSTANCES IN ANY FORM
- D06P1/00—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed
- D06P1/22—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed using vat dyestuffs including indigo
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- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06P—DYEING OR PRINTING TEXTILES; DYEING LEATHER, FURS OR SOLID MACROMOLECULAR SUBSTANCES IN ANY FORM
- D06P1/00—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed
- D06P1/30—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed using sulfur dyes
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06P—DYEING OR PRINTING TEXTILES; DYEING LEATHER, FURS OR SOLID MACROMOLECULAR SUBSTANCES IN ANY FORM
- D06P1/00—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed
- D06P1/44—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed using insoluble pigments or auxiliary substances, e.g. binders
- D06P1/52—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed using insoluble pigments or auxiliary substances, e.g. binders using compositions containing synthetic macromolecular substances
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- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06P—DYEING OR PRINTING TEXTILES; DYEING LEATHER, FURS OR SOLID MACROMOLECULAR SUBSTANCES IN ANY FORM
- D06P1/00—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed
- D06P1/44—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed using insoluble pigments or auxiliary substances, e.g. binders
- D06P1/64—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed using insoluble pigments or auxiliary substances, e.g. binders using compositions containing low-molecular-weight organic compounds without sulfate or sulfonate groups
- D06P1/642—Compounds containing nitrogen
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- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06P—DYEING OR PRINTING TEXTILES; DYEING LEATHER, FURS OR SOLID MACROMOLECULAR SUBSTANCES IN ANY FORM
- D06P1/00—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed
- D06P1/44—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed using insoluble pigments or auxiliary substances, e.g. binders
- D06P1/673—Inorganic compounds
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- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06P—DYEING OR PRINTING TEXTILES; DYEING LEATHER, FURS OR SOLID MACROMOLECULAR SUBSTANCES IN ANY FORM
- D06P5/00—Other features in dyeing or printing textiles, or dyeing leather, furs, or solid macromolecular substances in any form
- D06P5/02—After-treatment
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06P—DYEING OR PRINTING TEXTILES; DYEING LEATHER, FURS OR SOLID MACROMOLECULAR SUBSTANCES IN ANY FORM
- D06P5/00—Other features in dyeing or printing textiles, or dyeing leather, furs, or solid macromolecular substances in any form
- D06P5/02—After-treatment
- D06P5/04—After-treatment with organic compounds
- D06P5/08—After-treatment with organic compounds macromolecular
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- Textile Engineering (AREA)
- Chemical & Material Sciences (AREA)
- Inorganic Chemistry (AREA)
- Coloring (AREA)
Abstract
The invention discloses a kind of reducing dye and water-soluble sulfur dye with ready-made clothes dyeing technology is bathed, ready-made clothes to be dyed is carried out to pretreatment procedure → dyeing process → soap washing → sodium hypochlorite washing process → cellulase successively and washes process；The dyeing working reagent used in dyeing process includes accounting for the water-soluble sulfur dye and account for the reducing dye that ready-made clothes percentage by weight is 0.5~4% that ready-made clothes percentage by weight is 1~5%；Ready-made clothes after dyeing remains the style of missing old times or old friends of traditional garment dyeing, the physical index such as more traditional its light fastness of garment dyeing product of product, crock fastness greatly improves simultaneously, ready-made clothes through the technique productions can be especially suitable for all kinds of garment productions, dyeing producer carries out the needs of dyeing and finishing processing to clothes through follow-up deep processing.
Description
Technical field
The present invention relates to the dyeing and finishing technique field of Textile Manufacturing Industry, vulcanizes more particularly, to a kind of reducing dye with water-soluble
One-bath dyeing ready-made clothes dyeing technology.
Background technology
Garment dyeing is with its small lot, multi items, special pseudo-classic effect, the style of existing cowboy, and various with its color
The features such as changing and being better than cowboy adapts to the multi-demandses that market increasingly changes, and is paid attention to by people.But ready-made clothes in the market
There is certain drawback in dyeing, such as weathering color fastness, colorfastness to rubbing is bad.Using the good colouring method of fastness, ready-made clothes
Pseudo-classic imitative old feature unobvious are dyed, unsightly；Using the colouring method of fastness difference, though pseudo-classic feature is obvious, fabric color jail
Very undesirable, fugitive color is spent, can also take into account the color dye attractive in appearance with the ready-made clothes of dyefastness well without a kind of in the prior art
Color technique.
The content of the invention
It is an object of the invention in place of overcome the deficiencies in the prior art, there is provided a kind of reducing dye vulcanizes with water-soluble
One-bath dyeing ready-made clothes dyeing technology, it both can guarantee that fabric with good pseudo-classic imitative old effect, ensured that fabric has well again
Color fastness index.
The technical solution adopted for the present invention to solve the technical problems is：
A kind of reducing dye bathes ready-made clothes dyeing technology together with water-soluble sulfur dye, before ready-made clothes to be dyed is carried out successively
Treatment process → dyeing process → soap washing → sodium hypochlorite washing process → cellulase washes process；In the dyeing process
The dyeing working reagent used includes accounting for the water-soluble sulfur dye and account for ready-made clothes weight percent that ready-made clothes percentage by weight is 1~5%
Than the reducing dye for 0.5~4%.
Wherein：The water-soluble sulfur dye is Shanghai Zhan and the black S-H of ASATHIOSOL water-soluble sulfur dyes, orange S-2R
At least one of with brown S-BR；The reducing dye is reducing dye BR palm fibres, B is green, G is yellow and at least one of the green T of olive；Respectively
The color that the ratio of dyestuff can contaminate as needed determines.
The pretreatment procedure is：
Pre-treatment working reagent is added at room temperature, and 90~100 DEG C are warming up to by 2 DEG C/min heating rate, reaction 10~
20 min；80~90 DEG C are cooled to by 2 DEG C/min rate of temperature fall, 80~90 DEG C of 3~8min of washing；Add glacial acetic acid regulation pH
It is worth to 6.0~7.0；Room temperature washes 8~12 min；
The pre-treatment working reagent includes：
The g/L of soda ash 3~5；
The g/L of refining agent 4~6.
The refining agent is development of evil in febrile disease refining agent TF-108.
The dyeing process is：
Dyeing working reagent is added at room temperature, and 85~95 DEG C are warming up to by 1~2 DEG C/min heating rate, dyeing 25~
35min；Overflow washing is cooled to 45~55 DEG C, 45~55 DEG C of 10~20min of washing；Add 2~4 g/L glacial acetic acid and 4~6
G/L hydrogen peroxide, 65~75 DEG C are warming up to by 2 DEG C/min heating rate, aoxidizes 10~20min；Room temperature washing 8~12
min；
The dyeing working reagent also includes：
The g/L of thiourea dioxide 2~4；
The g/L of soda ash 4~6；
The g/L of akali sulphide 11~13；
The g/L of solid sodium hydroxide 4~6；
The g/L of wetting softener 3~7；
The g/L of levelling agent 1~2.
It is described add dyeing working reagent the step of be：
Soda ash, solid sodium hydroxide are sequentially added at room temperature, stirs 1~3min, add thiourea dioxide and 1/2 vulcanization
Alkali, water-soluble sulfur dye and reducing dye are added, stir 6~10 min, be eventually adding the akali sulphide of residue 1/2；In bath
Softening agent adds with levelling agent before water-soluble sulfur dye and reducing dye；Thiourea dioxide is white powder crystal,
The aqueous solution is in faintly acid；Stablize in an acidic solution, easily decompose in the basic conditions, the very strong sulfinic acid of generation reproducibility, tool
Reduction can be controlled by having；Compared with sodium hydrosulfite, there is higher reduction potential, and the decrease speed of reduction potential is slow,
Only sodium hydrosulfite reduction potential reduces the 1/5 of number, has a safety feature, pollution-free when producing and using, and mainly plays reducing dye dye
Chromatic rendition acts on；Akali sulphide mainly plays water-soluble sulfur dye dyeing reduction；Wetting softener is advantageous to prevent fabric from existing
Dye scratching caused by operation process；The level-dyeing property that levelling agent can increase textile dyeing prevents dyeing defect phenomenon from producing.
The wetting softener is RT polyester complexes dispersions；The levelling agent is answered for DS aliphatic amine polyoxyethylene ethers
With thing.
The soap washing is：
Working reagent of soaping is added at 90~100 DEG C, soap 15~25 min；Room temperature washes 8~12min；
The working reagent of soaping includes：
The g/L of soda ash 1~3；
The g/L of detergent 209 1~3.
The sodium hypochlorite washes process：
Sodium hypochlorite washing working reagent is added at room temperature, handles 8~12min；Room temperature washes 10~20min；
The sodium hypochlorite washing working reagent includes：
The g/L of 10% sodium hypochlorite 15~20.
The cellulase washes process：
Vinegar acid for adjusting pH is added at room temperature to 4.0~5.0；The cellulase for accounting for that ready-made clothes percentage by weight is 2~4% is added,
50~55 DEG C are warming up to by 2 DEG C/min heating rate, the min of insulation reaction 20~30；90~100 DEG C of 8~12 min of washing；
Room temperature washes 8~12 min.
The cellulase is dolantin chemical industry cellulase DM8628.
A kind of reducing dye also includes with water-soluble sulfur dye with bath ready-made clothes dyeing technology：The processing work before ready-made clothes is carried out
First ready-made clothes is cleaned before sequence；After process of cellulase washing terminates, ready-made clothes is dehydrated, dried.
The ready-made clothes is pure cotton or blending material, and the blending is term of art, refers to chemical fibre and cotton, hair, silk, fiber crops
The fabric of weaving gained, the chemical fibre such as terylene, polyamide fibre, acrylic fibers, spandex, viscose rayon, vinegar ester are mixed Deng natural fiber
Fiber etc., is not limited thereto.
Room temperature of the present invention is 20~35 DEG C, namely the temperature that heating is also not required to cooling is not required in conventional environment.
Compared with background technology, it has the following advantages that the technical program：
Traditional dyeing be difficult to take into account ready-made clothes after dyeing color is attractive in appearance and dyefastness, how to develop one can
Ensure that fabric has good pseudo-classic imitative old effect, and can ensures that fabric has the ready-made clothes dyeing technology of good color fastness index
An always big technical barrier in garment dyeing field, because being not that the dyestuff of various different advantages is combined into dyeing just
Good effect can be obtained, its dyeing process of different types of dyestuff is different.The present invention breaches the skill of traditional dyeing
Art difficulty, using property and the approximate water-soluble sulfur dye of dyeing theory and reducing dye, and provide a kind of water-soluble sulphur
Change dyestuff with reducing dye with ready-made clothes dyeing technology is bathed, realize the common dyeing of water-soluble sulfur dye and reducing dye, together
Traditional garment dyeing method is compared, and the ready-made clothes after dyeing imitates that old pseudo-classic effect is more obvious, and chromatogram is more complete, and article
The multi-term physical indexes such as Exposure to Sunlight, colorfastness to rubbing increase substantially, and meet the requirement that market is increasingly improved to such product,
Improve the international competitiveness of China's textile product.
Embodiment
Present disclosure is illustrated below by embodiment：
Embodiment 1
The ready-made clothes that half-bleached shirting is made；Specification：40×40/133×72；Composition：Cotton 100%.
Above-mentioned ready-made clothes is put into garment dyeing machine, carries out following process successively：
Pretreatment procedure
At room temperature toward addition pre-treatment working reagent in garment dyeing machine, 95 DEG C are warming up to by 2 DEG C/min heating rate,
React 15min；85 DEG C are cooled to by 2 DEG C/min rate of temperature fall, 85 DEG C of washing 5min；Add glacial acetic acid and adjust pH value to 6.5；
Room temperature washes 10 min；
The pre-treatment working reagent includes：
The g/L of soda ash 4；
The g/L of development of evil in febrile disease refining agent TF-108 5.
The g/L is the grams that liquid adds working reagent each component in every liter of garment dyeing machine（Similarly hereinafter）.
Dyeing process
At room temperature toward addition dyeing working reagent in garment dyeing machine, 90 DEG C are warming up to by 1.5 DEG C/min heating rate,
Dye 30min；Overflow washing is cooled to 50 DEG C, 50 DEG C of washing 15min；3 g/L glacial acetic acid and 5 g/L hydrogen peroxide are added,
70 DEG C are warming up to by 2 DEG C/min heating rate, aoxidizes 15min；Room temperature washes 10 min；
The dyeing working reagent includes：
The black S-H 2% of ASATHIOSOL water-soluble sulfur dyes；
ASATHIOSOL water-soluble sulfur dye oranges S-2R 1.5%；
Reducing dye BR palm fibres 1%；
Reducing dye B green 1.3%；
The g/L of thiourea dioxide 3；
The g/L of soda ash 5；
The g/L of akali sulphide 12；
The g/L of solid sodium hydroxide 5；
The g/L of wetting softener RT polyester complexes dispersion 4；
The g/L of compound 1 of levelling agent DS aliphatic amine polyoxyethylene ethers.
The percentage % is the percentage by weight that each component accounts for ready-made clothes.
It is described toward being the step of dyeing working reagent is added in garment dyeing machine：
Soda ash, solid sodium hydroxide are sequentially added at room temperature, stirs 2min, add thiourea dioxide and 1/2 akali sulphide,
Water-soluble sulfur dye and reducing dye are added, stirs 8min, is eventually adding the akali sulphide of residue 1/2；It is soft in the bath
Agent adds with levelling agent before water-soluble sulfur dye and reducing dye.
Soap washing
Toward working reagent of soaping is added in garment dyeing machine at 95 DEG C, soap 20min；Room temperature washes 10min；
The working reagent of soaping includes：
The g/L of soda ash 2；
The g/L of detergent 209 2.
Sodium hypochlorite washes process
At room temperature toward addition sodium hypochlorite washing working reagent in garment dyeing machine, 10min is handled；Room temperature washes 15min；
The sodium hypochlorite washing working reagent includes：
The g/L of 10% sodium hypochlorite 20.
Cellulase washes process
At room temperature toward adding vinegar acid for adjusting pH in garment dyeing machine to 4.5；Add the moral for accounting for that ready-made clothes percentage by weight is 3%
Beautify work cellulase DM8628, be warming up to 50 DEG C by 2 DEG C/min heating rate, insulation reaction 25min；95 DEG C of washings
10min；Room temperature washes 10 min.
After process of cellulase washing terminates, ready-made clothes is dehydrated by industry common process, dried, produce ready-made clothes after dyeing.
The color fastness of two kinds of different process of garment dyeing is relatively shown in Table 1.
Table 1
It is described above, only present pre-ferred embodiments, therefore the scope that the present invention is implemented can not be limited according to this, i.e., according to
The equivalent changes and modifications that the scope of the claims of the present invention and description are made, all should still it belong in the range of the present invention covers.
Claims (8)
1. a kind of reducing dye bathes ready-made clothes dyeing technology together with water-soluble sulfur dye, it is characterised in that：By ready-made clothes to be dyed
Pretreatment procedure → dyeing process → soap washing → sodium hypochlorite washing process → cellulase is carried out successively washes process；It is described
The dyeing working reagent used in dyeing process includes accounting for the water-soluble sulfur dye and account for into that ready-made clothes percentage by weight is 1~5%
Clothing percentage by weight is 0.5~4% reducing dye；
The dyeing process is：
Dyeing working reagent is added at room temperature, and 85~95 DEG C are warming up to by 1~2 DEG C/min heating rate, dyeing 25~
35min；Overflow washing is cooled to 45~55 DEG C, washes 10~20min；Add 2~4 g/L glacial acetic acid and 4~6 g/L pair
Oxygen water, 65~75 DEG C are warming up to by 1~3 DEG C/min heating rate, aoxidizes 10~20min；Room temperature washes 8~12 min；
The dyeing working reagent also includes：
The g/L of thiourea dioxide 2~4；
The g/L of soda ash 4~6；
The g/L of akali sulphide 11~13；
The g/L of solid sodium hydroxide 4~6；
The g/L of wetting softener 3~7；
The g/L of levelling agent 1~2；
It is described add dyeing working reagent the step of be：
Soda ash, solid sodium hydroxide are sequentially added at room temperature, stirs 1~3min, add thiourea dioxide and 1/2 akali sulphide,
Water-soluble sulfur dye and reducing dye are added, stirs 6~10 min, is eventually adding the akali sulphide of residue 1/2；In the bath
Softening agent adds with levelling agent before water-soluble sulfur dye and reducing dye；
The wetting softener is RT polyester complexes dispersions；The levelling agent is the compounding of DS aliphatic amine polyoxyethylene ethers
Thing.
2. a kind of reducing dye according to claim 1 bathes ready-made clothes dyeing technology together with water-soluble sulfur dye, its feature
It is：The water-soluble sulfur dye is Shanghai Zhan and the black S-H of ASATHIOSOL water-soluble sulfur dyes, orange S-2R, brown S-BR
At least one of；The reducing dye is reducing dye BR palm fibres, B is green, G is yellow, at least one of the green T of olive.
3. a kind of reducing dye according to claim 1 bathes ready-made clothes dyeing technology together with water-soluble sulfur dye, its feature
It is：The pretreatment procedure is：
Pre-treatment working reagent is added at room temperature, is warming up to 90~100 DEG C by 2 DEG C/min heating rate, reaction 10~20
min；80~90 DEG C are cooled to by 2 DEG C/min rate of temperature fall, 80~90 DEG C of 3~8min of washing；Add glacial acetic acid regulation pH value
To 6.0~7.0；Room temperature washes 8~12 min；
The pre-treatment working reagent includes：
The g/L of soda ash 3~5；
The g/L of refining agent 4~6；
The refining agent is development of evil in febrile disease refining agent TF-108.
4. a kind of reducing dye according to claim 1 bathes ready-made clothes dyeing technology together with water-soluble sulfur dye, its feature
It is：The soap washing is：
Working reagent of soaping is added at 90~100 DEG C, soap 15~25 min；Room temperature washes 8~12min；
The working reagent of soaping includes：
The g/L of soda ash 1~3；
The g/L of detergent 209 1~3.
5. a kind of reducing dye according to claim 1 bathes ready-made clothes dyeing technology together with water-soluble sulfur dye, its feature
It is：The sodium hypochlorite washes process：
Sodium hypochlorite washing working reagent is added at room temperature, handles 8~12min；Room temperature washes 10~20min；
The sodium hypochlorite washing working reagent includes：
The g/L of 10% sodium hypochlorite 15~25.
6. a kind of reducing dye according to claim 1 bathes ready-made clothes dyeing technology together with water-soluble sulfur dye, its feature
It is：The cellulase washes process：
Vinegar acid for adjusting pH is added at room temperature to 4.0~5.0；The cellulase for accounting for that ready-made clothes percentage by weight is 2~4% is added, by 2
DEG C/min heating rate is warming up to 50~55 DEG C, 20~30min of insulation reaction；90~100 DEG C of 8~12 min of washing；Room temperature
Wash 8~12 min；
The cellulase is dolantin chemical industry cellulase DM8628.
7. a kind of reducing dye according to claim 1 bathes ready-made clothes dyeing technology together with water-soluble sulfur dye, its feature
It is：Also include：First ready-made clothes is cleaned before ready-made clothes carries out pretreatment procedure；, will be into after process of cellulase washing terminates
Clothing dehydration, drying.
8. a kind of reducing dye according to any one of claim 1-7 is with water-soluble sulfur dye with bath garment dyeing work
Skill, it is characterised in that：The ready-made clothes is pure cotton or blending material.
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| CN109778460B (en) * | 2019-01-15 | 2021-04-02 | 嘉兴市腾旺染整有限公司 | Scratch-proof garment dyeing process |
| CN110453510B (en) * | 2019-03-28 | 2021-03-23 | 李瑞卿 | Composite reducing agent and reduction dyeing method |
| CN110106723B (en) * | 2019-05-16 | 2021-10-26 | 广东溢达纺织有限公司 | Garment dyeing method using vat dye or sulfur dye |
| CN110438823A (en) * | 2019-07-30 | 2019-11-12 | 韶关市北纺智造科技有限公司 | It is a kind of to vulcanize indigo co-bathing dyeing composition and One Bath Dyeing |
| CN115045120A (en) * | 2022-06-23 | 2022-09-13 | 浙江新舒纺织有限公司 | Production process of dyed yarn-dyed TR elastic cheese dyed cloth |
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| JP2007046190A (en) * | 2005-08-10 | 2007-02-22 | Okayama Prefecture | Dyeing method |
| CN101768876B (en) * | 2008-12-31 | 2012-08-22 | 福建协盛协丰印染实业有限公司 | Dyeing process using reducing and bleeding |
| CN103422368B (en) * | 2012-05-22 | 2015-06-17 | 江南大学 | Dyeing method of cotton product reduced dye with low bath ratio |
| CN104805706B (en) * | 2015-04-02 | 2017-02-22 | 北京服装学院 | Reduction system for vat dye or sulfur dyestuff dyeing and reduction method |
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