CN101338518A - One-bathing integrated finishing method for real silk fabric by natural extract - Google Patents
One-bathing integrated finishing method for real silk fabric by natural extract Download PDFInfo
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- CN101338518A CN101338518A CNA2008100418356A CN200810041835A CN101338518A CN 101338518 A CN101338518 A CN 101338518A CN A2008100418356 A CNA2008100418356 A CN A2008100418356A CN 200810041835 A CN200810041835 A CN 200810041835A CN 101338518 A CN101338518 A CN 101338518A
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Abstract
The invention discloses a method for real silk fabric functional finishing, especially relates to a method for one-bath multifunctional finishing of real silk fabric by utilizing natural extract, which pertains to textile dyeing and finishing technical field. The invention includes the following steps: placing real silk fabric in solution with 5-20%(o.w.f) natural extract, liquor ratio of 1:10 to 1:100 and PH value of 2-8, treating for 10-100min; then treating for 10-100min in solution with 3-15%(o.w.f.) metal salt, liquor ratio of 1:10 to 1:100 and PH value of 4-8; after washing, dehydrating and furnace drying, completing one-bath finishing with dyeing, antimicrobial and anti-ultraviolet function to real silk fabric. The invention reduces manufacturing procedure of real silk fabric, has effect of energy-saving and emission-reduction, improves cleaning production of textile processing, is harmless to human body and surroundings, and conforms to ecological textile processing requests.
Description
Technical field
The present invention relates to a kind of method of real silk fabric functional treatment, particularly a kind of method of utilizing the natural goods extract that real silk fabric is carried out one-bathing arrangement belongs to the textile dyeing and finishing technical field.
Background technology
In recent years, along with the raising and the science and technology development of living standards of the people, people grow with each passing day to the attention of environmental protection, human health.In the process of textiles, the whole world all requires the raw material of textiles processing and production technology to the minimum destruction of ecological tool.Think since the legislative assmeblies of in July, 1994 Germany and the textile dyeing meeting have been caused carcinogenic effect and since banning use of with diimide dyestuff or other dyestuffs, constantly there are synthetic dyestuffs and auxiliary agent product or its raw material to be found and work the mischief, be limited to be used for the processing of textiles the environment and the mankind.The potential danger factor that synthetic dyestuffs and auxiliary agent product are had has caused people's generally worry, and growing interest uses the security of dyestuff and auxiliary agent, and simultaneously, increasing people is at the natural sex of pursuing textile raw material.And along with the continuous development of detection technique, the rules of various countries' response are also strict step by step.Therefore, all meet ecology and require dyestuff and auxiliary agent considering how to develop this stage people, to satisfy present development trend.It is nontoxic, harmless extracting the composition with Color from natural goods, can be used in the processing of textiles at an easy rate, safely.At present, there is more composition to be used to be used for the dyeing of textiles in the extract of natural goods as natural colouring matter, pigment, mulberry red pigment, curcumin, mulberry pigment, lanigerin etc. in for example relevant big uranidin, red sorghum pigment, red yeast rice pigment, sophora bud pigment, the root of large-flowered skullcap, the existing report of above-mentioned natural goods extraction of effective components and application thereof.
On the other hand, in the environment of human survival, bacterium is ubiquitous, and people's various textiless used in everyday all are the suitable places of bacteria breed procreation and propagation as bed clothes, underwear, footgear, clothes, towel etc.Various bacteriums are breeding rapidly when condition is suitable, not only can make fibre variable color, mouldy, degraded etc., also can produce unusual stimulation and bring out various skin diseases human body skin, form all harm to the human lives, antibiotic be that people ensure healthy vital task all the time.Synthetic antibacterial agents is in the performance antibacterial action, and normal generation is to the harm of human body, and therefore the application of synthetic antibacterial agents on textiles in recent years is very restricted.Some some compositions that extract from natural goods have been found has antibacterial action, and nontoxic to human body, and skin is not had anaphylaxis and carcinogenic, has degradability and Environmental compatibility preferably.For example the extract of arhat pitch, aloe, heartleaf houttuynia, pine tree, Radix Glycyrrhizae, argy wormwood etc. has been in the news and has been used for the antibiotic finish of fabric.
Along with global warming, destruction with ozone layer, the ultraviolet protection effect of textiles has in recent years also caused people's attention, and organic uv commonly used at present prevents that agent from mainly containing salicylic acid, benzophenone class, benzotriazole, cyanoacrylate and triazines etc.Organic class ultraviolet ray prevents that agent from having certain influence to textile product life-span, ecological environment and properties of product.Therefore, the ultraviolet ray of selecting suitable textile treatment to use from the extract of natural goods prevents that active ingredient from also meriting attention.
At present, the technology of effective component extracting comparative maturity from natural goods, in the research of after natural extract is applied to functions of textile fabrics, putting in order, mainly stress aspect the research of special purpose, be about to the dyeing that a certain extract is used for textiles, perhaps a certain extract is used for antibiotic finish, perhaps a certain extract is used for anti-ultraviolet finishing, yet, according to the compatibility of various different natural goods extracts, fully utilize with regard to how, bring into play its synergistic effect, especially adopt optimum process condition, textiles is carried out one-bathing arrangement, promptly obtain dyeing simultaneously, antibiotic and research uvioresistant effect aspect yet there are no report.
Summary of the invention
In order to overcome the deficiency that prior art exists, the objective of the invention is to fully utilize different natural goods extracts, simple, the free of contamination silk fabric dyeing of a kind of technology, antibiotic, method that anti-ultraviolet function one is bathed processed are provided.
For achieving the above object, the technical solution adopted in the present invention is: the method that a kind of natural extract is put in order real silk fabric one one-bathing, effective component extracting from natural goods, carry out the multi-functional arrangement of following steps again:
1. real silk fabric being placed natural goods extract consumption is 5～20% (o.w.f), and bath raio is 1: 10～1: 100, and pH is that treatment temperature was 50～100 ℃ during 2～8 processing was bathed, and the processing time is 10～100min; Described natural goods extract comprises the lac extract, and is selected from the coptis, the root of large-flowered skullcap, granatum, cordate houttuynia or the Honegsukle flower P.E two or more, is selected from Chinese gall, bush, rheum officinale, mulberry fruit or the Turmeric P.E one or more;
2. be 3～15% (o.w.f.) by amount of metal salts, bath raio is 1: 10～1: 100, and pH is 4～8, the preparation metal salt compound is handled and is bathed, to put into wherein through the real silk fabric that above-mentioned steps was handled and handle, treatment temperature is 45～95 ℃, and the processing time is 10～100min;
3. real silk fabric being put into bath raio is 1: 10～1: 100 again, and temperature is to handle 2～3 times in 40～90 ℃ the hot water, and each processing time is 30～60min, after dehydration, oven dry, finishes the arrangement to silk fabric dyeing, antibiotic and uvioresistant function.
Described metal salt compound is a kind of in ferrous sulfate, calcium chloride, copper sulphate, aluminum sulfate or the ferric trichloride.
The present invention utilizes the function of different natural goods extracts in textile finishing, according to different extracts at the different-effect aspect painted, antibiotic and the uvioresistant effect, and the colorant match effect of different natural extracts, compatibility, synergistic effect, with bathing the feasibility of handling, adopt reasonable process conditions, realized the combination of multiple natural extract to real silk fabric dye, antibiotic, uvioresistant is with bathing the purpose of handling, compared with prior art, the present invention has following significant advantage:
1. the present invention adopts one-bathing arrangement real silk fabric, shortens the manufacturing procedure of real silk fabric, has the effect of energy-saving and emission-reduction, improves the cleaner production degree of textiles processing.
2. the present invention adopts multiple natural extract combination that real silk fabric is handled, and to human body and environmentally friendly, meets the requirement of ecological textile processing.
The specific embodiment
Below in conjunction with embodiment the present invention is further described:
Embodiment 1:
The natural extract that present embodiment adopts is formed and is comprised (in solid masses): 10 parts of Baical Skullcap root P.Es, 5 parts of coptis extracts, 2 parts of nutgall extractives, 8 parts of lac extracts.In actual the use, the natural goods extract comprises the lac extract, and in the coptis, the root of large-flowered skullcap, granatum, cordate houttuynia and the Honegsukle flower P.E two or more, one or more in Chinese gall, bush, rheum officinale, mulberry fruit and the Turmeric P.E; The component of each natural extract, the selection of ratio can be determined according to the index request of product color and uvioresistant, antibacterial functions.Above-mentioned natural extract is the active ingredient of extracting from its plant or other natural goods, extracting method is a prior art, and for example: the root of large-flowered skullcap and coptis extract available water are that solvent extracts the concentrate after the decompression distillation down at 100 ℃; Gallic extract method is the sodium hydroxide solution extraction under 60 ℃ with 20g/L, the concentrate after neutralization, decompression distillation; The lac extract is to use the dilute sodium carbonate extraction with aqueous solution, the product after neutralizing, concentrating.
Natural extract to the real silk fabric treatment process is: the extract consumption is 12% (o.w.f), and bath raio is 1: 30, handles and bathes pH=5,75 ℃ of treatment temperatures, processing time 40min.
Metal salt compound cooperates treatment process to be: the ferrous sulfate consumption is 6% (o.w.f.), and bath raio is 1: 40, handles and bathes pH=6,70 ℃ of treatment temperatures, processing time 30min.In actual the use, slaine can also adopt a kind of in calcium chloride, copper sulphate, aluminum sulfate and the ferric trichloride.
It is 1: 30 that fabric is put into bath raio, and temperature is to handle 2 times in 60 ℃ the hot water, and each processing time is 40min, and dehydration is dried under 80 ℃ of conditions then, and obtaining having antibiotic, uvioresistant function and color is the real silk fabric of gray purple.Adopt UV-1000F textiles uvioresistant factor tester (U.S. Labsphere company) to measure the UPF index resulting real silk fabric, go up the K/S value of measuring fabric at UlstrascanXE computer colour photometer (U.S. HunterLab company), adopt according to " disinfection technology standard " version test fabric in 2002 antibiotic property, the result is referring to table 1.
Embodiment 2:
The composition of the natural extract that present embodiment adopts comprises (in solid masses): 6 parts of pomegranate rind extracts, 5 parts of Baical Skullcap root P.Es, 6 parts of Honegsukle flower P.Es, 8 parts of Turmeric P.Es, 5 parts of lac extracts.Effective component extracting can adopt following extracting method from above-mentioned natural goods: granatum, the root of large-flowered skullcap and Honegsukle flower P.E are that water is that solvent extracts the concentrate after decompression distillation down at 100 ℃; The extract of turmeric is the ethanolic solution refluxing extraction in apparatus,Soxhlet's with 60%, the concentrate after decompression distillation; The lac extract is to use the dilute sodium carbonate extraction with aqueous solution, the product after neutralizing, concentrating.
Natural extract to the real silk fabric treatment process is: the extract consumption is 15% (o.w.f.), and bath raio is 1: 40, handles and bathes pH=4.5,85 ℃ of treatment temperatures, processing time 35min.
Metal salt compound cooperates treatment process to be: addition of aluminum sulfate is 8% (o.w.f.), and bath raio is 1: 40, handles and bathes pH=6,55 ℃ of treatment temperatures, processing time 40min.
It is 1: 30 that fabric is put into bath raio, and temperature is to handle 2 times in 60 ℃ the hot water, and each processing time is 40min, and dehydration is dried under 80 ℃ of conditions then, obtains having antibiotic, uvioresistant function and nearly coffee-like real silk fabric.Adopt UV-1000F textiles uvioresistant factor tester (U.S. Labsphere company) to measure the UPF index real silk fabric, go up the K/S value of measuring fabric at UlstrascanXE computer colour photometer (U.S. HunterLab company), adopt according to " disinfection technology standard " version test fabric in 2002 antibiotic property, the result is referring to table 1.
Table 1
As can be seen from Table 1, all greater than 70%, this explanation has bacteriostasis preferably to the real silk fabric of the technology of the present invention processing to staphylococcus aureus and colibacillary bacteriostasis rate; The UPF index of the real silk fabric of processing illustrates to have uvioresistant effect preferably all greater than 40; From handle the back fabric K/S value as can be known, the processing fabric obtain denseer color simultaneously.
Claims (2)
1. a natural extract is to the method for real silk fabric one one-bathing arrangement, and effective component extracting from natural goods is characterized in that carrying out the multi-functional arrangement of following steps again:
1. real silk fabric being placed natural goods extract consumption is 5～20% (o.w.f), and bath raio is 1: 10～1: 100, and pH is that treatment temperature was 50～100 ℃ during 2～8 processing was bathed, and the processing time is 10～100min; Described natural goods extract comprises the lac extract, and is selected from the coptis, the root of large-flowered skullcap, granatum, cordate houttuynia or the Honegsukle flower P.E two or more, is selected from Chinese gall, bush, rheum officinale, mulberry fruit or the Turmeric P.E one or more;
2. be 3～15% (o.w.f.) by amount of metal salts, bath raio is 1: 10～1: 100, and pH is that 4～8 preparation metal salt compounds are handled bath, real silk fabric is put into wherein handled, and treatment temperature is 45～95 ℃, and the processing time is 10～100min;
3. fabric being put into bath raio is 1: 10～1: 100, and temperature is to handle 2～3 times in 40～90 ℃ the hot water, and each processing time is 30～60min, through dehydration, oven dry, finishes the arrangement to silk fabric dyeing, antibiotic and uvioresistant function.
2. natural extract according to claim 1 is characterized in that the method for real silk fabric one one-bathing arrangement: described slaine is a kind of in ferrous sulfate, calcium chloride, copper sulphate, aluminum sulfate or the ferric trichloride.
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