CN101824758A - Antibacterial and deodorizing health-care quilted stockings based on traditional Chinese medicinal granatum and preparation method thereof - Google Patents
Antibacterial and deodorizing health-care quilted stockings based on traditional Chinese medicinal granatum and preparation method thereof Download PDFInfo
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Abstract
The invention relates to antibacterial and deodorizing health-care quilted stockings based on traditional Chinese medicinal granatum and a preparation method thereof. In the preparation method, hot water is used as a solvent, an extract of the traditional Chinese medicinal granatum not only has a dyeing function, but also has antibacterial and deodorizing functions, and a pigment extract of the granatum is adopted to carry out pre-mordant dyeing on 100 percent of cotton yarns which are frequently used for weaving stockings or 100 percent of quilted stockings so as to prepare the antibacterial and deodorizing health-care quilted stockings. The preparation method mainly comprises the following four steps of: (1) extracting granatum pigment; (2) carrying out pre-mordant dyeing on the cotton yarns or the quilted stockings by adopting aluminum ions and iron ions; (3) putting the cotton yarns or the quilted stockings, which are subjected to the pre-mordant dyeing, into dye bath of the granatum pigment for carrying out a step integrating dyeing and antibacterial and deodorizing processing; and (4) preparing the dyed cotton yarns into quilted stockings by adopting a traditional method. The antibacterial and deodorizing health-care quilted stockings have the advantages of safety, effectiveness, low cost, no toxic or side effects and have no adverse influences on favorable properties of moisture permeability, moisture absorption and flexibility of cotton fibers.
Description
Technical field
The present invention relates to a kind of antibiotic, deodorization health quilted stockings and preparation method thereof, especially relate to a kind of antibiotic, deodorization health quilted stockings based on the traditional Chinese medicine granatum and preparation method thereof, function of dominant textile material technical field.
Background technology
Along with the enhancing of people's health care consciousness, cleaning, health care, the maintenance of foot are paid attention to more.Traditional Chinese medicine thinks that pin is second " heart " of human body, the strong earlier foot of body-building, and foot is healthy and strong from strong.In people's walking process, foot's load is big, perspires easily.But compare with clothing, footwear ventilative, wet ability is far short of what is expected thoroughly, pin usually is in moist microenvironment, easily breed bacteria.Therefore, saturating wet, antibiotic, the deodorizing to footwear, socks just proposed very high requirement.
At present, the production of antibiotic fabric mainly contains two kinds of methods both at home and abroad: a kind of is to make anti-bacterial fibre earlier, and then makes antibiotic fabric; Another kind is that fabric is carried out antibiotic finish and obtains anti-microbial property.The antibacterial action that anti-bacterial fibre obtained is lasting, and washing resistance is good, but its production technology more complicated, to the requirement of antiseptic also than higher, the general resistant to elevated temperatures inorganic antiseptic of multiselect.The antibiotic finish processing technology is fairly simple, and the range of choice of antiseptic is wide, but the washing resistance of antibacterial effect is relatively poor.
Bamboo-carbon fibre is a kind of anti-bacterial fibre of industrialization in recent years, and its production technology is: 1. the bamboo with perennation becomes bamboo charcoal through 1000 ℃ of anaerobic high-temperature firings; 2. adopt methods such as air-flow pulverizing that bamboo charcoal powder is broken into ultramicro powder; 3. the bamboo charcoal particle that crushes is evenly dispersed in the polyester support, is processed into the bamboo charcoal dacron master grain of high-load, wherein bamboo charcoal content is about 40%; 4. according to the different requirements of product, in terylene chips, add different proportion bamboo charcoal dacron master grain, obtain the bamboo charcoal terylene through melt spinning.Bamboo charcoal in the bamboo charcoal terylene (having antibiotic, deodorization and high temperature resistant) content the highlyest is no more than 7% generally about 3%.Patent of invention " a kind of preparation method of pineapple leaf fiber antibiosis health-protection socks " (application number: 200910039617.3) think that natural arghan has antibiotic property itself, with arghan (10～60%) and other fiber (40～90%) blending, can be made into health promoting socks with antibacterial action.At present, nano titanium oxide silver antibacterial agent powder also is a main inorganic antiseptic of producing anti-bacterial fibre, its main component is a nano titanium oxide silver permutoid, the cost height, simultaneously because particle diameter minimum (only being 30nm), be easy to stripping from the anti-bacterial fibre body and might enter human body, its security is still needed and will further be studied.
Textile antimicrobial agent at present commonly used has tens of kinds, and wherein organic class accounts for 90%, comprises natural and 2 synthetic big classes.Natural organic antibacterial agent mainly from animal and plant refining refinement form, weatherability is good, toxicity is low, safe in utilization.Synthetic organic antibacterial agent has advantages such as quick-acting, that sterilizing power is strong, but can produce the microorganism drug resistance.In recent years, the synthetic antimicrobial finishing agent has been subjected to all circles' attention to the security of human body.The data introduction is arranged, and used antibacterial finishing agent has only the DC-5700 organosilicon quaternary ammonium salt antibacterial finishing agent of Dow corning chemical company to obtain the blanket approval of Environmental Protection Agency USA (EPA) at present.Therefore, having only DC-5700 to be acknowledged as is anti-bacteium deodorization finishing agent non-stripping property, nontoxic to the mankind.(application number: 200510016705.3) adopt homemade WS-8810 sanitary finish agent that the socks that contain cotton 80%～100% are carried out antibiotic finish, the inventor thinks that this antiseptic can not produce the bacterial drug resistance and the resistance to the action of a drug to patent of invention " antibacterial odour oliminating health care stocks ".
The textile material of making socks requires to have very strong moisture absorption, wet ability thoroughly, and synthetic anti-bacterial fibre is because natural cotton fiber is generally adopted in moisture absorption, water vapour permeability difference and seldom adopt.But, can only adopt afterfinish method to reach antibacterial functions for natural cotton fiber.Simultaneously, people in the process of walking, socks bottoms is subjected to very big pressure, periphery is subjected to very big friction, causes wherein antiseptic to be easy to come off and enters human body by foot, therefore, the security of socks antibacterial finishing agent is just had higher requirement.
Edible, medicinal and ornamental value that pomegranate has, extensively cultivated in recent years, mainly be distributed in Hebei, Henan, Shandong, Jiangsu, Anhui, Zhejiang, Jiangxi, Fujian, Taiwan, Hunan, Hubei, Guangdong, Guangxi, Guizhou, Sichuan etc. and economize (autonomous region).Granatum is a kind of important traditional Chinese medicine, and the main chemical compositions pomegranate glycosides (punicalagin) (content reaches 8.24%) of granatum promptly is the main pigment composition of granatum, also is main active constituents of medicine, and soluble in water.In vitro test shows that the granatum water decoction all has killing action to staphylococcus aureus, proteus, corynebacterium diphtheriae, typhoid fever and paratyphoid, comma bacillus, Pseudomonas aeruginosa, shigella dysenteriae, tubercle bacillus etc. all there is the obvious suppression effect, the various skin fungi there is in various degree inhibitory action, so blue formula trichobacteria, yellow trichobacteria, barber's itch trichobacteria, trichophyton ferrugium, Du's big belly formula sporidiole bacteria difficult to understand, acrothesium floccosum etc.Experimental study shows the granatum dyed cotton fabric, especially adopts the COTTON FABRIC after environment-friendly type mordant aluminium ion, the pre-mordant dyeing of iron ion to have excellent antibiotic, deodorization.
Summary of the invention
The present invention is intended to adopt extraction from the pigment of aboundresources, low-cost natural by-product granatum cotton yarn or quilted stockings to be dyeed, and has quilted stockings antibiotic, deodorization functions with preparation.The present invention is antibiotic, the deodorizing quilted stockings compared with the prior art, safe and effective, cost is low, and is without any side effects, and saturating wet, moisture absorption and softness that cotton fiber is good are not had any harmful effect.
Technology path of the present invention mainly comprises following four aspects: the extraction of (1) granatum pigment; (2) adopt aluminium ion, iron ion that cotton yarn or quilted stockings are carried out pre-mordant dyeing; (3) cotton yarn after the pre-mordant dyeing or quilted stockings are dropped into dyeing and antibiotic, the deodorizing arrangement that is integrated in one in the dye bath of granatum pigment; (4) adopt conventional method, dyed cotton yarn is made quilted stockings.
The extraction of granatum pigment of the present invention comprises following process:
(1) hot water extracting granatum pigment
Under the normal temperature, the granatum of suitably pulverizing is added in the 20-40 times of water gaging, be heated to temperature 80-100 ℃, constant temperature extracts pigment 1-2h, extracts 2-3 time;
(2) adopt the metallic sieve coarse filtration
Adopt 100-200 order metallic sieve while hot the pigment solution that extracts to be filtered, expect slag to remove, and each time filtrate is merged, make brown granatum pigment extract;
(3) centrifuge separates
Will be through the further centrifugation of brown granatum pigment extract of metallic sieve filtration, to remove fine impurities.Centrifuge speed 3000-6000r/min, centrifugation time 20-40min.
(4) concentrated, spray drying
The method that adopts decompression to concentrate to the upper strata granatum pigment stillness of night after centrifugal concentrates, and spray drying, gets powder granatum pigment.
Adopt aluminium ion, iron ion as follows to the method that cotton yarn or quilted stockings carry out pre-mordant dyeing:
Adopt normal temperature type dyeing sample machine, water-bath etc., 100% cotton yarn or quilted stockings are carried out pre-mordant dyeing.Mordant adopts environment-friendly type mordants such as aluminium ion, iron ion.The pre-mordant dyeing technology of aluminium ion mordant: mordant KAl (SO
4)
212H
2O, mordant consumption 1%-6% (o.w.f), bath raio (25-50): 1,30 ℃ is dyed, and heating rate 1-2 ℃/min, is warming up to 60-80 ℃, insulation 40-60min.The pre-mordant dyeing technology of iron ion mordant: mordant FeSO
47H
2O, mordant consumption 0.5-3%, bath raio (25-50): 1,30 ℃ is risen and to dye, and heating rate 1-2 ℃/min, is warming up to 40-60 ℃ and be incubated 30-60min.
Colouring method of the present invention is as follows:
Can adopt the granatum pigment extract directly cotton yarn or quilted stockings to be dyeed, also can adopt through spray-dired powder granatum pigment through dyeing after the dissolving once more.
To drop in the granatum dye solution through the cotton yarn or the quilted stockings of pre-mordant dyeing; bath raio (25-50): 1, granatum dye dosage 10-50% (o.w.f) (dye dosage calculates the cotton fiber consumption with the granatum consumption) or granatum dye dosage 1-5% (o.w.f) (dye dosage calculates the cotton fiber consumption with the powder granatum dye dosage that extracts); 30 ℃ are dyed; heating rate 1-2 ℃/mi n; be warming up to 60 ℃-90 ℃, insulation 60-120min.Sample after the dyeing adopts the neutral soap lotion of 0.5g/L to wash 10-30min under 30-50 ℃ of condition, adopts clear water to clean then.Because the granatum pigment solution promptly is a dyestuff, has antibiotic, deodorant activities again, therefore, this process promptly is to dye and is antibiotic, deodorization functions arrangement.
Through the cotton yarn or the quilted stockings process dyeing back color difference of different mordant dyeing agent mordant dyeing in advance, the pre-mordant dyeing of aluminium ion gets yellow or yellowish-brown, and the pre-mordant dyeing of iron ion gets coffee-like or grey black.
Specific embodiment:
Antibiotic, deodorization health quilted stockings preparation example 1 based on the natural by-product granatum:
The granatum pigment extracts: under the normal temperature, the granatum of suitably pulverizing is added in 20 times of water gagings, be heated to 100 ℃ of temperature, constant temperature extracts pigment 1h, extracts 2 times; Adopt 100 order metallic sieves while hot the pigment solution that extracts to be filtered, expect slag to remove, and each time filtrate is merged, make brown granatum pigment extract.The pre-mordant dyeing of 100% cotton yarn: adopt aluminium ion mordant KAl (SO
4)
212H
2O carries out pre-mordant dyeing to 100% cotton yarn, mordant consumption 3% (o.w.f), and bath raio 25: 1,30 ℃ are dyed, and 1 ℃/min of heating rate is warming up to 60 ℃, insulation 30min.Dyeing: adopt above-mentioned granatum pigment extract directly the cotton yarn after the pre-mordant dyeing to be dyeed; bath raio 50: 1, granatum dye dosage 20% (o.w.f) (dye dosage calculates the cotton yarn consumption with the granatum consumption); 30 ℃ are dyed; 1 ℃/min of heating rate; be warming up to 70 ℃, insulation dyeing 60min.Clean: the cotton yarn after the dyeing adopts the neutral soap lotion of 0.5g/L to wash 10min under 30 ℃ of conditions, adopts clear water to clean then.Knit socks: adopt conventional method, dyed cotton yarn is made into quilted stockings, promptly obtain having dyeing quilted stockings antibiotic, health-care deodorized function.
Antibiotic, deodorization health quilted stockings preparation example 2 based on the natural by-product granatum:
The granatum pigment extracts: under the normal temperature, the granatum of suitably pulverizing is added in 30 times of water gagings, be heated to 100 ℃ of temperature, constant temperature extracts pigment 1h, extracts 2 times; Adopt 200 order metallic sieves while hot the pigment solution that extracts to be filtered, expect slag to remove, and each time filtrate is merged, make brown granatum pigment extract; Adopt centrifuge further the feed liquid after filtering to be separated, to remove fine impurities, centrifuge speed 4000r/min, centrifugation time 30min; The method that adopts decompression to concentrate to the upper strata granatum pigment stillness of night after centrifugal concentrates, and spray drying, gets powder granatum dyestuff.Iron ion carries out pre-mordant dyeing to quilted stockings: adopt normal temperature type to dye model machine, iron ion mordant FeSO
47H
2O, mordant consumption 1%, bath raio 30: 1,30 ℃ are dyed, and 1 ℃/min of heating rate is warming up to 70 ℃, insulation 40min.Dyeing: adopt the Pomegranate Rind dyestuff, dye dosage 2% (o.w.f), bath raio 50: 1,30 ℃ are dyed, and 1 ℃/min of heating rate is warming up to 80 ℃ and insulation dyeing 90min.Clean: the quilted stockings after the dyeing adopts the neutral soap lotion of 0.5g/L to wash 20min under 30 ℃ of conditions, adopts clear water to clean then, obtains having health care quilted stockings antibiotic, deodorization functions.
Claims (3)
1. one kind based on antibiotic, deodorization health quilted stockings of traditional Chinese medicine granatum and preparation method thereof, and it is characterized in that adopting with hot water is cotton yarn or quilted stockings antibiotic, the deodorization functions arrangement and dyeing that are integrated in one of the pigment solution of solvent extraction in traditional Chinese medicine granatum after to environment-friendly metal mordant aluminium ion, the pre-mordant dyeing of iron ion.
2. a kind of antibiotic, deodorization health quilted stockings based on the natural by-product granatum according to claim 1 and preparation method thereof mainly comprises following four aspects: the extraction of (1) granatum pigment; (2) adopt aluminium ion, iron ion that cotton yarn or quilted stockings are carried out pre-mordant dyeing; (3) cotton yarn after the mordant dyeing or quilted stockings are dropped into dyeing and antibiotic, the deodorizing arrangement that is integrated in one in the dye bath of granatum pigment; (4) adopt conventional method, dyed cotton yarn is made quilted stockings.
3. according to claim 1 is that the pigment solution of solvent extraction in traditional Chinese medicine granatum can be thought the pigment solution of direct extraction from granatum with hot water, also can for the pigment solution that extracts powder granatum dyestuff through concentrating, preparing after the spray drying through the pigment solution after dissolving once more.
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Cited By (11)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN102628227A (en) * | 2012-03-29 | 2012-08-08 | 江南大学 | Grape-seed-based ecological preparation method for ultravioresistant woolen and silk textiles |
| CN102634994A (en) * | 2012-03-29 | 2012-08-15 | 江南大学 | Ecological preparation method for anti-ultraviolet wool and silk textile based on granatum |
| CN102758350A (en) * | 2011-04-29 | 2012-10-31 | 李晓柯 | Textile product printing and dyeing method |
| CN103265823A (en) * | 2013-05-04 | 2013-08-28 | 江门职业技术学院 | Pomegranate rind nature dye preparation and application of pomegranate rind nature dye in fabric |
| CN104452335A (en) * | 2014-12-15 | 2015-03-25 | 常熟市启弘纺织实业有限公司 | Environment-friendly printing and dyeing method for textile |
| CN104775312A (en) * | 2014-01-14 | 2015-07-15 | 新疆大学 | Nature pomegranate peel dye tie-dyeing pure-cotton fabric preparation method |
| CN105064011A (en) * | 2015-09-09 | 2015-11-18 | 太原理工大学 | Method for performing antibiotic finishing on cotton fabric by use of granatum extract |
| CN108774902A (en) * | 2018-06-01 | 2018-11-09 | 何炽斌 | A kind of production method carrying out garment dyeing using fruit natural dye |
| CN109023958A (en) * | 2018-07-03 | 2018-12-18 | 威海惠高生物科技有限公司 | A kind of manufacture craft of natural antibacterial fabric |
| CN109943936A (en) * | 2019-03-27 | 2019-06-28 | 安徽省亮亮纺织有限公司 | A kind of antibacterial cotton fabric and preparation method thereof |
| CN115074884A (en) * | 2022-06-10 | 2022-09-20 | 浙江今日风纺织有限公司 | Elastic yarn and processing method thereof |
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| Publication number | Priority date | Publication date | Assignee | Title |
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| CN102758350A (en) * | 2011-04-29 | 2012-10-31 | 李晓柯 | Textile product printing and dyeing method |
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| CN102628227A (en) * | 2012-03-29 | 2012-08-08 | 江南大学 | Grape-seed-based ecological preparation method for ultravioresistant woolen and silk textiles |
| CN102634994A (en) * | 2012-03-29 | 2012-08-15 | 江南大学 | Ecological preparation method for anti-ultraviolet wool and silk textile based on granatum |
| CN103265823A (en) * | 2013-05-04 | 2013-08-28 | 江门职业技术学院 | Pomegranate rind nature dye preparation and application of pomegranate rind nature dye in fabric |
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| CN105064011A (en) * | 2015-09-09 | 2015-11-18 | 太原理工大学 | Method for performing antibiotic finishing on cotton fabric by use of granatum extract |
| CN108774902A (en) * | 2018-06-01 | 2018-11-09 | 何炽斌 | A kind of production method carrying out garment dyeing using fruit natural dye |
| CN109023958A (en) * | 2018-07-03 | 2018-12-18 | 威海惠高生物科技有限公司 | A kind of manufacture craft of natural antibacterial fabric |
| CN109943936A (en) * | 2019-03-27 | 2019-06-28 | 安徽省亮亮纺织有限公司 | A kind of antibacterial cotton fabric and preparation method thereof |
| CN115074884A (en) * | 2022-06-10 | 2022-09-20 | 浙江今日风纺织有限公司 | Elastic yarn and processing method thereof |
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Open date: 20100908 |