CN105064011A - Method for performing antibiotic finishing on cotton fabric by use of granatum extract - Google Patents
Method for performing antibiotic finishing on cotton fabric by use of granatum extract Download PDFInfo
- Publication number
- CN105064011A CN105064011A CN201510569527.0A CN201510569527A CN105064011A CN 105064011 A CN105064011 A CN 105064011A CN 201510569527 A CN201510569527 A CN 201510569527A CN 105064011 A CN105064011 A CN 105064011A
- Authority
- CN
- China
- Prior art keywords
- cotton fabric
- pomegranate rind
- extract
- rind extract
- antibiotic finishing
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Pending
Links
Landscapes
- Agricultural Chemicals And Associated Chemicals (AREA)
- Treatments For Attaching Organic Compounds To Fibrous Goods (AREA)
- Medicines Containing Plant Substances (AREA)
Abstract
The invention relates to a method for performing antibiotic finishing on a cotton fabric and particularly relates to a method for performing antibiotic finishing on a cotton fabric by use of a granatum extract. The granatum extract is utilized as an antibacterial agent, aluminium potassium sulfate is utilized as a cross-linking agent, antibiotic finishing is performed on the cotton fabric by use of a post-finishing method, so that the air permeability of the obtained antibiotic cotton fabric is slightly improved, and the breaking strength is basically not damaged; after being subjected to standard water washing for 5 times, the cotton fabric still has the staphylococcus aureus inhibitive rate of 95-99% and the colibacillus inhibitive rate of 93-97%.
Description
Technical field
The present invention relates to a kind of antibiotic finishing method of COTTON FABRIC, be specifically related to the antibiotic finishing method of a kind of pomegranate rind extract to COTTON FABRIC, belong to the technical field of finishing functions of textile fabrics.
Background technology
Sweat, scurf etc. that human metabolism produces can provide nutriment for each bacterioid, make fabric become the hotbed of bacteria breed, and fabric can turn to be yellow by bacteria effect, mouldy, generation peculiar smell, even can bring out skin disease; As the preferred material of underclothes, COTTON FABRIC is the class textiles that in daily life, directly contact skin consumption is maximum, thus carries out antibiotic finish to COTTON FABRIC and seems particularly important.
At present, the method preparing antibiotic fabric mainly contains following two kinds: a kind of method adds antibacterial material in the raw material of fiber, anti-bacterial fibre is made after spinning, again anti-bacterial fibre is woven into antibiotic fabric, this method durable antibacterial effect, but with high content of technology, difficulty is large, and antiseptic requires high; Another kind method adds antibacterial finishing agent in fabric printing Final finishing process, then makes various antibacterial fabric, and this method processing process is comparatively simple, and washability and durable antibacterial effect poor.For pure cotton fabric, usually select the processing method of fabric post-treatment, and of paramount importance in hindlimb unload be namely the selection of antiseptic.Inorganic antiseptic and synthesis organic antibacterial agent, the fewer and feweri use due to its inevitable toxic and side effect, the research application of natural organic antibacterial agent is in the majority with shitosan, few to the research of other natural antibacterial agent.Modern scientific research confirms, natural organic antibacterial agent pomegranate rind extract has the effect of broad-spectrum antiseptic, has obvious inhibitory action to most of Gram-negative bacteria, gram-positive bacteria, various fungi and mould etc.In addition, granatum also has the advantages such as wide material sources, cheap, natural environmental-protective, thus pomegranate rind extract can be applied to COTTON FABRIC, exploitation ecological antibiotic COTTON FABRIC.
summary of the invention:
Technical problem to be solved by this invention is: how pomegranate rind extract is applied to COTTON FABRIC, make COTTON FABRIC have antibacterial functions, and toxic and side effect is little.
The technical solution adopted in the present invention is the antibiotic finishing method of pomegranate rind extract to COTTON FABRIC, carries out according to following step:
Step one, boiling water sterilization processing is carried out to COTTON FABRIC: get pure cotton fabric and drop into and be equipped with in deionized water, hydro-oxidation sodium regulates pH to 8-9, after boiling 10-20min, take out and wash in warm water, extract, the baking oven putting into 70-90 DEG C is dried, and under weak basic condition, carry out boiling water sterilization processing to COTTON FABRIC effectively can kill acid-proof bacteria, and is conducive to the pre-complexing of follow-up aluminium ion.
The pre-complexing COTTON FABRIC of step 2, aluminium ion: be in the aluminum potassium sulfate solution of 8%-10% by the mass percent concentration that the pH value that the COTTON FABRIC input dilute sulfuric acid processed through step one regulates is 3-4 according to bath raio 1:40 to 1:55,20-40min is soaked in the shaking water bath pot of 60-75 DEG C, extract, the baking oven putting into 70-90 DEG C is dried; Enhance COTTON FABRIC on the one hand to the absorption of pomegranate rind extract antibiotic finishing solution by the pre-complexing COTTON FABRIC of aluminium ion, aluminium ion enhances the bactericidal effect of pomegranate rind extract antibiotic finishing solution on the other hand.
Step 3, preparation pomegranate rind extract antibiotic finishing solution: be add pomegranate rind extract and sodium chloride in the methanol aqueous solution of 4% in percent by volume, be stirred to solid matter all to dissolve, forming pomegranate rind extract mass percent concentration is 8-12%, sodium chloride mass percent concentration is 1-2%, regulates pH to 4-7 to form pomegranate rind extract antibiotic finishing solution with NaOH; Add pomegranate rind extract antibiotic finishing solution and effectively can strengthen bactericidal effect, and be conducive to COTTON FABRIC pomegranate rind extract antibiotic finishing solution is adsorbed.
Step 4, antibiotic finish: under air-tight state, pomegranate rind extract antibiotic finishing solution step 3 prepared is placed in the ultrasonic oscillation water-bath of 60-70 DEG C, the COTTON FABRIC of step 2 process is added according to bath raio 1:15 to 1:30, dipping 30-60min, extract, dry at the environment lower open mouth of 70-90 DEG C.
As a kind of preferred embodiment: described pomegranate rind extract contains the pomegranate rind extract of ellagic acid 40%, polyphenol 40%, punicalagins 20% according to mass percent concentration, the pomegranate rind extract bactericidal effect of this composition is best.
Beneficial effect: the present invention is by natural environmental-protective, cheap, and the natural organic antibacterial agent pomegranate rind extract with broad-spectrum antibacterial action is applied in the Final finishing of COTTON FABRIC, not only increase effective utilization of resource, and after pomegranate rind extract process, the gas permeability of fabric slightly improves, fracture strength is not damaged substantially, after 5 standard washings, COTTON FABRIC still can reach 95-99% and 93-97% to staphylococcus aureus and colibacillary bacteriostasis rate, with directly with compared with the method for the aqueous solution process COTTON FABRIC of pomegranate rind extract, its anti-microbial property of dressing liquid process COTTON FABRIC is better.
Detailed description of the invention
Further illustrate the present invention below by embodiment, but be not limited to following examples.
Selected chemical substance material:
To carry out selected to the chemical substance material that preparation uses, and carry out quality purity, content control:
Pomegranate rind extract, brownish-yellow powder, ellagic acid 40%, polyphenol 40%, punicalagins 20%;
Methyl alcohol (CH
3oH), colourless liquid, purity is 99.9%;
Sodium chloride (NaCl), white crystal, purity is more than or equal to 99.5%;
Alum (KAl (SO
4)
212H
2o), colourless crystallization, purity is 99.9%;
NaOH (NaOH), white solid, purity is 99.9%;
Deionized water (H
2o), liquid liquid, purity is 99.9%.
Boiling water sterilization processing is carried out to COTTON FABRIC:
Getting pure cotton fabric input is equipped with in the beaker of deionized water, and hydro-oxidation sodium regulates pH to 8, after kiering 10min, take out, wash in warm water, extract, put into the baking oven dry for standby of 75 DEG C, the COTTON FABRIC of alkali condition is conducive to the pre-complexing of follow-up aluminium ion;
The pre-complexing COTTON FABRIC of aluminium ion:
The pre-complexing COTTON FABRIC of aluminium ion: be in the aluminum potassium sulfate solution of 8% by the mass percent concentration that the pH value that the COTTON FABRIC input dilute sulfuric acid processed through step one regulates is 4 according to bath raio 1:40,30min is soaked in the shaking water bath pot of 60-75 DEG C, extract, the baking oven putting into 70-90 DEG C is dried;
Preparation pomegranate rind extract antibiotic finishing solution:
Preparation pomegranate rind extract antibiotic finishing solution: be add pomegranate rind extract and sodium chloride in the methanol aqueous solution of 4% in percent by volume, be stirred to solid matter all to dissolve, forming pomegranate rind extract mass percent concentration is 8%, sodium chloride mass percent concentration is 1%, regulate pH to 5 to form pomegranate rind extract antibiotic finishing solution with NaOH, the alum carried is crosslinking agent;
Antibiotic finish:
Under air-tight state, pomegranate rind extract antibiotic finishing solution step 3 prepared is placed in the ultrasonic oscillation water-bath of 60 DEG C, adds the COTTON FABRIC of step 2 process according to bath raio 1:15, dipping 30-60min, extract, two leachings two are dried at the environment lower open mouth of 70-90 DEG C after rolling.
Detect and characterize:
Adopt antibacterial circle diameter method of testing to detect its anti-microbial property to the COTTON FABRIC after having processed, detect its gas permeability with the full-automatic air permeation volume gauge of YG461E-III, detect mechanical property with YG (B) 026D-500 type imported electronic fabric strength tester.
Result shows, after pomegranate rind extract process, the gas permeability of fabric slightly improves, and fracture strength does not become substantially, and after 5 standard washings, COTTON FABRIC can reach 98% and 96% to staphylococcus aureus and colibacillary bacteriostasis rate.
Claims (2)
1. pomegranate rind extract is to the antibiotic finishing method of COTTON FABRIC, it is characterized in that carrying out according to following step:
Step one, boiling water sterilization processing is carried out to COTTON FABRIC: get pure cotton fabric and drop into and be equipped with in deionized water, hydro-oxidation sodium regulates pH to 8-9, and after boiling 10-20min, take out and wash in warm water, extract, the baking oven putting into 70-90 DEG C is dried;
The pre-complexing COTTON FABRIC of step 2, aluminium ion: be in the aluminum potassium sulfate solution of 8%-10% by the mass percent concentration that the pH value that the COTTON FABRIC input dilute sulfuric acid processed through step one regulates is 3-4 according to bath raio 1:40 to 1:55,20-40min is soaked in the shaking water bath pot of 60-75 DEG C, extract, the baking oven putting into 70-90 DEG C is dried;
Step 3, preparation pomegranate rind extract antibiotic finishing solution: be add pomegranate rind extract and sodium chloride in the methanol aqueous solution of 4% in percent by volume, be stirred to solid matter all to dissolve, forming pomegranate rind extract mass percent concentration is 8-12%, sodium chloride mass percent concentration is 1-2%, regulates pH to 4-7 to form pomegranate rind extract antibiotic finishing solution with NaOH;
Step 4, antibiotic finish: under air-tight state, pomegranate rind extract antibiotic finishing solution step 3 prepared is placed in the ultrasonic oscillation water-bath of 60-70 DEG C, the COTTON FABRIC of step 2 process is added according to bath raio 1:15 to 1:30, dipping 30-60min, extract, dry at the environment lower open mouth of 70-90 DEG C.
2. pomegranate rind extract according to claim 1 is to the antibiotic finishing method of COTTON FABRIC, it is characterized in that: described pomegranate rind extract contains the pomegranate rind extract of ellagic acid 40%, polyphenol 40%, punicalagins 20% according to mass percent concentration.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201510569527.0A CN105064011A (en) | 2015-09-09 | 2015-09-09 | Method for performing antibiotic finishing on cotton fabric by use of granatum extract |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201510569527.0A CN105064011A (en) | 2015-09-09 | 2015-09-09 | Method for performing antibiotic finishing on cotton fabric by use of granatum extract |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN105064011A true CN105064011A (en) | 2015-11-18 |
Family
ID=54493499
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201510569527.0A Pending CN105064011A (en) | 2015-09-09 | 2015-09-09 | Method for performing antibiotic finishing on cotton fabric by use of granatum extract |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN105064011A (en) |
Cited By (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN105908331A (en) * | 2016-05-17 | 2016-08-31 | 长兴华海纺织有限公司 | Natural faint scent antibacterial warm-keeping easy-care shirt fabric and preparation method thereof |
| CN108295099A (en) * | 2017-06-30 | 2018-07-20 | 晋大纳米科技（厦门）有限公司 | A kind of antiseptic and its application |
| CN108703420A (en) * | 2018-06-25 | 2018-10-26 | 陈承基 | A kind of female mammary gland health-care brassiere Chinese medicine protection pad and preparation method thereof |
| CN110578250A (en) * | 2019-10-29 | 2019-12-17 | 江苏金荣泰新材料科技有限公司 | Antibacterial agent for nonwoven fabric |
| CN115976830A (en) * | 2023-02-13 | 2023-04-18 | 罗莱生活科技股份有限公司 | Long-acting antibacterial fabric and preparation method thereof |
Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101824758A (en) * | 2010-04-28 | 2010-09-08 | 江南大学 | Antibacterial and deodorizing health-care quilted stockings based on traditional Chinese medicinal granatum and preparation method thereof |
| CN102755360A (en) * | 2012-07-24 | 2012-10-31 | 西华大学 | Method for extracting pomegranate peel polyphenols from pomegranate peel |
| CN103265823A (en) * | 2013-05-04 | 2013-08-28 | 江门职业技术学院 | Pomegranate rind nature dye preparation and application of pomegranate rind nature dye in fabric |
| CN104831529A (en) * | 2015-05-27 | 2015-08-12 | 天津滨海大田纺织有限公司 | Antibacterial finishing agent for cotton fabrics and antibacterial finishing process |
-
2015
- 2015-09-09 CN CN201510569527.0A patent/CN105064011A/en active Pending
Patent Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101824758A (en) * | 2010-04-28 | 2010-09-08 | 江南大学 | Antibacterial and deodorizing health-care quilted stockings based on traditional Chinese medicinal granatum and preparation method thereof |
| CN102755360A (en) * | 2012-07-24 | 2012-10-31 | 西华大学 | Method for extracting pomegranate peel polyphenols from pomegranate peel |
| CN103265823A (en) * | 2013-05-04 | 2013-08-28 | 江门职业技术学院 | Pomegranate rind nature dye preparation and application of pomegranate rind nature dye in fabric |
| CN104831529A (en) * | 2015-05-27 | 2015-08-12 | 天津滨海大田纺织有限公司 | Antibacterial finishing agent for cotton fabrics and antibacterial finishing process |
Non-Patent Citations (4)
| Title |
|---|
| 刘劭钢等: "《科学消毒 有益健康》", 28 February 2004, 湖南科学技术出版社 * |
| 李婕姝等: ""石榴的生物活性成分及其药理作用研究进展"", 《中国现代中药》 * |
| 楼方岑: "《传染病手册》", 30 September 1984, 人民卫生出版社出版 * |
| 艾儒棣: "《中医外科特色制剂》", 31 October 2008, 中国中医药出版社 * |
Cited By (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN105908331A (en) * | 2016-05-17 | 2016-08-31 | 长兴华海纺织有限公司 | Natural faint scent antibacterial warm-keeping easy-care shirt fabric and preparation method thereof |
| CN108295099A (en) * | 2017-06-30 | 2018-07-20 | 晋大纳米科技（厦门）有限公司 | A kind of antiseptic and its application |
| CN108703420A (en) * | 2018-06-25 | 2018-10-26 | 陈承基 | A kind of female mammary gland health-care brassiere Chinese medicine protection pad and preparation method thereof |
| CN110578250A (en) * | 2019-10-29 | 2019-12-17 | 江苏金荣泰新材料科技有限公司 | Antibacterial agent for nonwoven fabric |
| CN115976830A (en) * | 2023-02-13 | 2023-04-18 | 罗莱生活科技股份有限公司 | Long-acting antibacterial fabric and preparation method thereof |
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| CN105064011A (en) | Method for performing antibiotic finishing on cotton fabric by use of granatum extract | |
| CN105011391B (en) | A kind of natural antibacterial bamboo fiber socks | |
| CN103835124B (en) | Carry silver-colored COTTON FABRIC anti-biotic material and preparation method thereof | |
| CN103147288B (en) | Method for preparing halamine antibacterial material based on cyanuric chloride | |
| CN104695203B (en) | Anti-wrinkle treatment process of wool and linen yarns | |
| CN104589445A (en) | Rattan softening method | |
| CN112227067A (en) | Preparation process of non-soaked antibacterial deodorant cotton | |
| CN107354716A (en) | A kind of preparation method of the mould proof bafta of long acting antibiotic | |
| CN102418267A (en) | Traditional Chinese medicinal antibacterial finishing agent | |
| CN102352568A (en) | Arrangement method for down feathers with antibacterial function | |
| CN103437173A (en) | Preparation method of silver/chitosan composite antibiotic finishing agent | |
| CN101886338A (en) | Biological antibiotic cotton fibers or cotton cloth and method for preparing same | |
| CN106811972A (en) | A kind of preparation method of permanent seal cooling fabric antimicrobial finishing agent | |
| CN108708060A (en) | A kind of preparation method of low-cost and high-performance antibiotic fabric | |
| CN108708160A (en) | A kind of antibacterial blended yarn weaved fabric | |
| CN104313776A (en) | Production method of seamless knitted underwear with healthcare function | |
| CN103103757A (en) | Preparation method of antibacterial finishing liquor for fabrics | |
| CN104452266B (en) | A kind of antibacterial modified method of towel | |
| CN101153460B (en) | Ecological antimicrobial fabric and method for producing the same | |
| CN104109972A (en) | Nano-antibacterial finishing process of cashmere knitwear | |
| CN107158030A (en) | A kind of new silver-containing antibacterial product and preparation method thereof | |
| CN106702741A (en) | Antibacterial finishing liquid containing modified sericin protein and preparation method of antibacterial finishing liquid | |
| CN103498248B (en) | Tencel bamboo fiber shirt fabric | |
| CN104420057A (en) | Antibacterial and health-care fabric | |
| CN105780194A (en) | Novel antibacterial alginate fiber and preparation method thereof |
Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| C06 | Publication | ||
| PB01 | Publication | ||
| C10 | Entry into substantive examination | ||
| SE01 | Entry into force of request for substantive examination | ||
| RJ01 | Rejection of invention patent application after publication |
Application publication date: 20151118 |
|
| RJ01 | Rejection of invention patent application after publication |