CN103103757A - Preparation method of antibacterial finishing liquor for fabrics - Google Patents
Preparation method of antibacterial finishing liquor for fabrics Download PDFInfo
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- CN103103757A CN103103757A CN2012105396222A CN201210539622A CN103103757A CN 103103757 A CN103103757 A CN 103103757A CN 2012105396222 A CN2012105396222 A CN 2012105396222A CN 201210539622 A CN201210539622 A CN 201210539622A CN 103103757 A CN103103757 A CN 103103757A
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Abstract
The invention discloses a preparation method of antibacterial finishing liquor for fabrics. The method comprises the following process steps of: (1) adding reverse osmosis water to chitosan, and dripping several drops of acetic acid to the chitosan for dissolving the chitosan in the reverse osmosis water, thus forming a solution A; (2) adding reverse osmosis water to water-soluble wool fat, heating the solution in a water bath manner, and stirring for dissolving the water-soluble wool fat, thus forming a solution B; (3) adding reverse osmosis water to 3-chloromethyl propylmethoxysilane, an antibacterial agent and a nano-silver antibacterial agent for dissolving the substances, thus forming a solution C; (4) dissolving solid substances by ethanol, 2,4, 4'-trichlorine-2-hydroxy-diphenyl ether and PEG-40 hydrogenated castor oil, thus forming a solution D; and (5) mixing the solution A, the solution B, the solution C and the solution D, supplementing reverse osmosis water to the mixed solution till the total solution reach 100 weight parts, stirring the total solution, adding several drops of antifoaming agent to the total solution, and uniformly mixing the antifoaming agent and the total solution. The antibacterial finishing liquor has an antibacterial effect and a special effect of guaranteeing the original softness of the finished fabrics.
Description
Technical field
The present invention relates to the fabric finishing liquor field, be specifically related to a kind of preparation method of antibiotic finish of the fabric liquid.
Background technology
Some fabrics have gas permeability preferably, stronger absorbability, and good springiness, warmth retention property is good, feel is soft, human body is not had irritating advantage, so fabric is as the clothing more and more welcomed by the people of raw material.But it has been recognized that the especially microorganism such as the cellulose base fiber fabric such as the protein fibre such as silk, wool and linen-cotton meeting breed bacteria and mould of fabric, thereby stain, produce offending smell, and can discolour, reduce mechanical strength, affect application performance, therefore dress all needs antibiotic finish with textiles and industrial textile.
Summary of the invention
The object of the present invention is to provide a kind of preparation method of antibiotic finish of the fabric liquid, not only have antibiotic effect, can guarantee that the fabric that was organized keeps the special efficacy of original pliability but also have.
For achieving the above object, the invention provides a kind of preparation method of antibiotic finish of the fabric liquid, comprise following processing step:
1) get 0.3～1.5 weight portion shitosan, add the reverse osmosis water of 8 weight portions, drip several acetic acid shitosan is dissolved in reverse osmosis water, form A solution;
2) get 0.1～2.6 weight parts water dissolubility lanolin, add the reverse osmosis water of 12 weight portions, heating water bath stirs, and makes water-soluble lanolin dissolving, forms B solution;
3) get 2～6 weight portion 3-chloropropylmethyldimethoxysilanes, 0.2～2.6 weight portion antiseptic, 0.3～0.7 weight portion nano silver antimicrobials adds the reverse osmosis water of 11 weight portions, makes the above-mentioned substance dissolving, forms C solution;
4) get 7 parts by weight of ethanol, 0.2～0.8 weight portion 2,4,4 '-three chloro-2 hydroxyls-diphenyl ether, 2～8 weight portion Cremophor RH40s make the solid matter dissolving, form D solution;
5) A solution, B solution, C solution, D solution are mixed, and additional reverse osmosis water, making total solution is 100 weight portions, stirs and adds several defoamers, mixes.
Advantage of the present invention and beneficial effect are: a kind of preparation method of antibiotic finish of the fabric liquid is provided, not only has antibiotic effect, can guarantee that the fabric that was organized keeps the special efficacy of original pliability but also have.
The specific embodiment
Below in conjunction with specific embodiment, the invention will be further described.Following examples only are used for technical scheme of the present invention more clearly is described, and can not limit protection scope of the present invention with this.
Embodiment 1
A kind of preparation method of antibiotic finish of the fabric liquid comprises following processing step:
1) get 1 weight portion shitosan, add the reverse osmosis water of 8 weight portions, drip several acetic acid shitosan is dissolved in reverse osmosis water, form A solution;
2) get 1.6 weight parts water dissolubility lanolin, add the reverse osmosis water of 12 weight portions, heating water bath stirs, and makes water-soluble lanolin dissolving, forms B solution;
3) get 4 weight portion 3-chloropropylmethyldimethoxysilanes, 1.5 weight portion antiseptics, 0.5 weight portion nano silver antimicrobials adds the reverse osmosis water of 11 weight portions, makes the above-mentioned substance dissolving, forms C solution;
4) get 7 parts by weight of ethanol, 0.6 weight portion 2,4,4 '-three chloro-2 hydroxyls-diphenyl ether, 6 weight portion Cremophor RH40s make the solid matter dissolving, form D solution;
5) A solution, B solution, C solution, D solution are mixed, and additional reverse osmosis water, making total solution is 100 weight portions, stirs and adds several defoamers, mixes.
Embodiment 2
A kind of preparation method of antibiotic finish of the fabric liquid comprises following processing step:
1) get 0.3 weight portion shitosan, add the reverse osmosis water of 8 weight portions, drip several acetic acid shitosan is dissolved in reverse osmosis water, form A solution;
2) get 0.1 weight parts water dissolubility lanolin, add the reverse osmosis water of 12 weight portions, heating water bath stirs, and makes water-soluble lanolin dissolving, forms B solution;
3) get 2 weight portion 3-chloropropylmethyldimethoxysilanes, 0.2 weight portion antiseptic, 0.3 weight portion nano silver antimicrobials adds the reverse osmosis water of 11 weight portions, makes the above-mentioned substance dissolving, forms C solution;
4) get 7 parts by weight of ethanol, 0.2 weight portion 2,4,4 '-three chloro-2 hydroxyls-diphenyl ether, 2 weight portion Cremophor RH40s make the solid matter dissolving, form D solution;
5) A solution, B solution, C solution, D solution are mixed, and additional reverse osmosis water, making total solution is 100 weight portions, stirs and adds several defoamers, mixes.
Embodiment 3
A kind of preparation method of antibiotic finish of the fabric liquid comprises following processing step:
1) get 1.5 weight portion shitosans, add the reverse osmosis water of 8 weight portions, drip several acetic acid shitosan is dissolved in reverse osmosis water, form A solution;
2) get 2.6 weight parts water dissolubility lanolin, add the reverse osmosis water of 12 weight portions, heating water bath stirs, and makes water-soluble lanolin dissolving, forms B solution;
3) get 6 weight portion 3-chloropropylmethyldimethoxysilanes, 2.6 weight portion antiseptics, 0.7 weight portion nano silver antimicrobials adds the reverse osmosis water of 11 weight portions, makes the above-mentioned substance dissolving, forms C solution;
4) get 7 parts by weight of ethanol, 0.8 weight portion 2,4,4 '-three chloro-2 hydroxyls-diphenyl ether, 8 weight portion Cremophor RH40s make the solid matter dissolving, form D solution;
5) A solution, B solution, C solution, D solution are mixed, and additional reverse osmosis water, making total solution is 100 weight portions, stirs and adds several defoamers, mixes.
The above is only the preferred embodiment of the present invention; should be pointed out that for those skilled in the art, under the prerequisite that does not break away from the technology of the present invention principle; can also make some improvements and modifications, these improvements and modifications also should be considered as protection scope of the present invention.
Claims (1)
1. the preparation method of an antibiotic finish of the fabric liquid, is characterized in that, comprises following processing step:
1) get 0.3～1.5 weight portion shitosan, add the reverse osmosis water of 8 weight portions, drip several acetic acid shitosan is dissolved in reverse osmosis water, form A solution;
2) get 0.1～2.6 weight parts water dissolubility lanolin, add the reverse osmosis water of 12 weight portions, heating water bath stirs, and makes water-soluble lanolin dissolving, forms B solution;
3) get 2～6 weight portion 3-chloropropylmethyldimethoxysilanes, 0.2～2.6 weight portion antiseptic, 0.3～0.7 weight portion nano silver antimicrobials adds the reverse osmosis water of 11 weight portions, makes the above-mentioned substance dissolving, forms C solution;
4) get 7 parts by weight of ethanol, 0.2～0.8 weight portion 2,4,4 '-three chloro-2 hydroxyls-diphenyl ether, 2～8 weight portion Cremophor RH40s make the solid matter dissolving, form D solution;
5) A solution, B solution, C solution, D solution are mixed, and additional reverse osmosis water, making total solution is 100 weight portions, stirs and adds several defoamers, mixes.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN2012105396222A CN103103757A (en) | 2012-12-14 | 2012-12-14 | Preparation method of antibacterial finishing liquor for fabrics |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN2012105396222A CN103103757A (en) | 2012-12-14 | 2012-12-14 | Preparation method of antibacterial finishing liquor for fabrics |
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| CN103103757A true CN103103757A (en) | 2013-05-15 |
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| CN2012105396222A Pending CN103103757A (en) | 2012-12-14 | 2012-12-14 | Preparation method of antibacterial finishing liquor for fabrics |
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Cited By (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN103757921A (en) * | 2013-12-04 | 2014-04-30 | 常熟市福亿印花炼染有限公司 | Preparation method for fabric antibacterial finishing liquid |
| CN104032564A (en) * | 2014-06-16 | 2014-09-10 | 东华大学 | Sensitization-free and activation-free chemical silvering method for polyamide base body |
| CN104452281A (en) * | 2014-12-23 | 2015-03-25 | 常熟市周行毛巾厂 | Towel cloth finishing solution |
| CN104975504A (en) * | 2015-07-08 | 2015-10-14 | 陕西科技大学 | Method for preparing shoe antibacterial synthesis leather substrate and liner through O-carboxymethyl chitosan grafted nylon 66 fabric |
| CN105350278A (en) * | 2015-12-18 | 2016-02-24 | 成路凯尔服装（苏州）有限公司 | Preparation method of antibiotic finish liquid for fabric |
| CN105951437A (en) * | 2016-05-24 | 2016-09-21 | 无锡市长安曙光手套厂 | Antibacterial textile finishing agent and preparation method thereof |
Citations (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1948606A (en) * | 2006-10-20 | 2007-04-18 | 深圳清华大学研究院 | Textiles antibacterial finishing agent, its preparation method and application |
| CN102505467A (en) * | 2011-09-30 | 2012-06-20 | 天津市中科健新材料技术有限公司 | Finishing liquor for realizing antibiosis of fabrics and preparation method of finishing liquor |
-
2012
- 2012-12-14 CN CN2012105396222A patent/CN103103757A/en active Pending
Patent Citations (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1948606A (en) * | 2006-10-20 | 2007-04-18 | 深圳清华大学研究院 | Textiles antibacterial finishing agent, its preparation method and application |
| CN102505467A (en) * | 2011-09-30 | 2012-06-20 | 天津市中科健新材料技术有限公司 | Finishing liquor for realizing antibiosis of fabrics and preparation method of finishing liquor |
Cited By (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN103757921A (en) * | 2013-12-04 | 2014-04-30 | 常熟市福亿印花炼染有限公司 | Preparation method for fabric antibacterial finishing liquid |
| CN104032564A (en) * | 2014-06-16 | 2014-09-10 | 东华大学 | Sensitization-free and activation-free chemical silvering method for polyamide base body |
| CN104452281A (en) * | 2014-12-23 | 2015-03-25 | 常熟市周行毛巾厂 | Towel cloth finishing solution |
| CN104975504A (en) * | 2015-07-08 | 2015-10-14 | 陕西科技大学 | Method for preparing shoe antibacterial synthesis leather substrate and liner through O-carboxymethyl chitosan grafted nylon 66 fabric |
| CN105350278A (en) * | 2015-12-18 | 2016-02-24 | 成路凯尔服装（苏州）有限公司 | Preparation method of antibiotic finish liquid for fabric |
| CN105951437A (en) * | 2016-05-24 | 2016-09-21 | 无锡市长安曙光手套厂 | Antibacterial textile finishing agent and preparation method thereof |
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Application publication date: 20130515 |