CN107237122A - The durable antibiotic noniron finish liquid and finishing technique of a kind of cotton fabric - Google Patents
The durable antibiotic noniron finish liquid and finishing technique of a kind of cotton fabric Download PDFInfo
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- CN107237122A CN107237122A CN201710505234.5A CN201710505234A CN107237122A CN 107237122 A CN107237122 A CN 107237122A CN 201710505234 A CN201710505234 A CN 201710505234A CN 107237122 A CN107237122 A CN 107237122A
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- cotton fabric
- extract
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- liquid
- durable antibiotic
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- 239000007788 liquid Substances 0.000 title claims abstract description 59
- 229920000742 Cotton Polymers 0.000 title claims abstract description 53
- 239000004744 fabric Substances 0.000 title claims abstract description 52
- 230000003115 biocidal effect Effects 0.000 title claims abstract description 30
- 238000000034 method Methods 0.000 title claims abstract description 12
- 235000013717 Houttuynia Nutrition 0.000 claims abstract description 26
- 241000283690 Bos taurus Species 0.000 claims abstract description 21
- 235000014360 Punica granatum Nutrition 0.000 claims abstract description 21
- 230000000844 anti-bacterial effect Effects 0.000 claims abstract description 21
- 229920001661 Chitosan Polymers 0.000 claims abstract description 17
- GWEVSGVZZGPLCZ-UHFFFAOYSA-N Titan oxide Chemical class O=[Ti]=O GWEVSGVZZGPLCZ-UHFFFAOYSA-N 0.000 claims abstract description 13
- OGIDPMRJRNCKJF-UHFFFAOYSA-N titanium oxide Inorganic materials [Ti]=O OGIDPMRJRNCKJF-UHFFFAOYSA-N 0.000 claims abstract description 13
- 235000010489 acacia gum Nutrition 0.000 claims abstract description 12
- 239000001785 acacia senegal l. willd gum Substances 0.000 claims abstract description 12
- 238000002386 leaching Methods 0.000 claims abstract description 7
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Chemical compound O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 31
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 claims description 30
- 241000758769 Houttuynia Species 0.000 claims description 25
- 241000219991 Lythraceae Species 0.000 claims description 20
- 238000005119 centrifugation Methods 0.000 claims description 15
- 238000000605 extraction Methods 0.000 claims description 15
- 238000010992 reflux Methods 0.000 claims description 15
- 239000003795 chemical substances by application Substances 0.000 claims description 12
- 238000010409 ironing Methods 0.000 claims description 12
- 239000004902 Softening Agent Substances 0.000 claims description 11
- 229920002134 Carboxymethyl cellulose Polymers 0.000 claims description 10
- 239000001768 carboxy methyl cellulose Substances 0.000 claims description 10
- 235000010948 carboxy methyl cellulose Nutrition 0.000 claims description 10
- 239000008112 carboxymethyl-cellulose Substances 0.000 claims description 10
- 238000001035 drying Methods 0.000 claims description 10
- 238000002360 preparation method Methods 0.000 claims description 9
- 241000205585 Aquilegia canadensis Species 0.000 claims description 7
- 238000007730 finishing process Methods 0.000 claims description 7
- 229920001296 polysiloxane Polymers 0.000 claims description 6
- 230000000740 bleeding effect Effects 0.000 claims description 5
- 238000001816 cooling Methods 0.000 claims description 5
- 239000008367 deionised water Substances 0.000 claims description 5
- 229910021641 deionized water Inorganic materials 0.000 claims description 5
- 238000010298 pulverizing process Methods 0.000 claims description 5
- 239000002994 raw material Substances 0.000 claims description 5
- 238000007789 sealing Methods 0.000 claims description 5
- 239000007921 spray Substances 0.000 claims description 5
- 238000003756 stirring Methods 0.000 claims description 5
- 150000002148 esters Chemical class 0.000 claims description 4
- 239000000835 fiber Substances 0.000 claims description 4
- 150000003242 quaternary ammonium salts Chemical class 0.000 claims description 4
- 241000894006 Bacteria Species 0.000 claims description 3
- 241000251468 Actinopterygii Species 0.000 claims 1
- 244000025254 Cannabis sativa Species 0.000 claims 1
- HCHKCACWOHOZIP-UHFFFAOYSA-N Zinc Chemical compound [Zn] HCHKCACWOHOZIP-UHFFFAOYSA-N 0.000 claims 1
- 238000011010 flushing procedure Methods 0.000 claims 1
- PCHJSUWPFVWCPO-UHFFFAOYSA-N gold Chemical compound [Au] PCHJSUWPFVWCPO-UHFFFAOYSA-N 0.000 claims 1
- 239000010931 gold Substances 0.000 claims 1
- 229910052737 gold Inorganic materials 0.000 claims 1
- 239000001575 punica granatum l. bark extract Substances 0.000 claims 1
- 235000020995 raw meat Nutrition 0.000 claims 1
- 238000009738 saturating Methods 0.000 claims 1
- 239000004575 stone Substances 0.000 claims 1
- 239000011701 zinc Substances 0.000 claims 1
- 229910052725 zinc Inorganic materials 0.000 claims 1
- WSFSSNUMVMOOMR-UHFFFAOYSA-N Formaldehyde Chemical compound O=C WSFSSNUMVMOOMR-UHFFFAOYSA-N 0.000 abstract description 6
- 230000000845 anti-microbial effect Effects 0.000 abstract description 4
- 230000037303 wrinkles Effects 0.000 abstract description 4
- 230000000694 effects Effects 0.000 abstract description 3
- 239000004753 textile Substances 0.000 abstract description 3
- 230000007613 environmental effect Effects 0.000 abstract description 2
- 241000411851 herbal medicine Species 0.000 abstract description 2
- 125000002887 hydroxy group Chemical group [H]O* 0.000 abstract description 2
- 231100000252 nontoxic Toxicity 0.000 abstract description 2
- 230000003000 nontoxic effect Effects 0.000 abstract description 2
- 125000002924 primary amino group Chemical group [H]N([H])* 0.000 abstract description 2
- 238000013268 sustained release Methods 0.000 abstract description 2
- 239000012730 sustained-release form Substances 0.000 abstract description 2
- 150000001875 compounds Chemical class 0.000 abstract 2
- 240000000691 Houttuynia cordata Species 0.000 abstract 1
- 244000294611 Punica granatum Species 0.000 abstract 1
- 239000000654 additive Chemical class 0.000 abstract 1
- 230000000996 additive effect Effects 0.000 abstract 1
- 239000003242 anti bacterial agent Substances 0.000 abstract 1
- 230000001153 anti-wrinkle effect Effects 0.000 abstract 1
- SOQBVABWOPYFQZ-UHFFFAOYSA-N oxygen(2-);titanium(4+) Chemical compound [O-2].[O-2].[Ti+4] SOQBVABWOPYFQZ-UHFFFAOYSA-N 0.000 abstract 1
- 241000588724 Escherichia coli Species 0.000 description 4
- 241000191967 Staphylococcus aureus Species 0.000 description 4
- 230000002401 inhibitory effect Effects 0.000 description 4
- 239000000203 mixture Substances 0.000 description 4
- 238000012360 testing method Methods 0.000 description 3
- 238000005406 washing Methods 0.000 description 3
- 206010053615 Thermal burn Diseases 0.000 description 2
- 238000013329 compounding Methods 0.000 description 2
- 238000005516 engineering process Methods 0.000 description 2
- 238000002156 mixing Methods 0.000 description 2
- 229920000728 polyester Polymers 0.000 description 2
- 230000002421 anti-septic effect Effects 0.000 description 1
- 239000012752 auxiliary agent Substances 0.000 description 1
- 229920001222 biopolymer Polymers 0.000 description 1
- 230000007547 defect Effects 0.000 description 1
- 150000004676 glycans Chemical class 0.000 description 1
- 230000002045 lasting effect Effects 0.000 description 1
- 229920001282 polysaccharide Polymers 0.000 description 1
- 239000005017 polysaccharide Substances 0.000 description 1
- 241000894007 species Species 0.000 description 1
Classifications
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M13/00—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06B—TREATING TEXTILE MATERIALS USING LIQUIDS, GASES OR VAPOURS
- D06B3/00—Passing of textile materials through liquids, gases or vapours to effect treatment, e.g. washing, dyeing, bleaching, sizing, impregnating
- D06B3/10—Passing of textile materials through liquids, gases or vapours to effect treatment, e.g. washing, dyeing, bleaching, sizing, impregnating of fabrics
- D06B3/18—Passing of textile materials through liquids, gases or vapours to effect treatment, e.g. washing, dyeing, bleaching, sizing, impregnating of fabrics combined with squeezing, e.g. in padding machines
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M11/00—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with inorganic substances or complexes thereof; Such treatment combined with mechanical treatment, e.g. mercerising
- D06M11/32—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with inorganic substances or complexes thereof; Such treatment combined with mechanical treatment, e.g. mercerising with oxygen, ozone, ozonides, oxides, hydroxides or percompounds; Salts derived from anions with an amphoteric element-oxygen bond
- D06M11/36—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with inorganic substances or complexes thereof; Such treatment combined with mechanical treatment, e.g. mercerising with oxygen, ozone, ozonides, oxides, hydroxides or percompounds; Salts derived from anions with an amphoteric element-oxygen bond with oxides, hydroxides or mixed oxides; with salts derived from anions with an amphoteric element-oxygen bond
- D06M11/44—Oxides or hydroxides of elements of Groups 2 or 12 of the Periodic Table; Zincates; Cadmates
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M11/00—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with inorganic substances or complexes thereof; Such treatment combined with mechanical treatment, e.g. mercerising
- D06M11/32—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with inorganic substances or complexes thereof; Such treatment combined with mechanical treatment, e.g. mercerising with oxygen, ozone, ozonides, oxides, hydroxides or percompounds; Salts derived from anions with an amphoteric element-oxygen bond
- D06M11/36—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with inorganic substances or complexes thereof; Such treatment combined with mechanical treatment, e.g. mercerising with oxygen, ozone, ozonides, oxides, hydroxides or percompounds; Salts derived from anions with an amphoteric element-oxygen bond with oxides, hydroxides or mixed oxides; with salts derived from anions with an amphoteric element-oxygen bond
- D06M11/46—Oxides or hydroxides of elements of Groups 4 or 14 of the Periodic Table; Titanates; Zirconates; Stannates; Plumbates
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M15/00—Treating fibres, threads, yarns, fabrics, or fibrous goods made from such materials, with macromolecular compounds; Such treatment combined with mechanical treatment
- D06M15/01—Treating fibres, threads, yarns, fabrics, or fibrous goods made from such materials, with macromolecular compounds; Such treatment combined with mechanical treatment with natural macromolecular compounds or derivatives thereof
- D06M15/03—Polysaccharides or derivatives thereof
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M15/00—Treating fibres, threads, yarns, fabrics, or fibrous goods made from such materials, with macromolecular compounds; Such treatment combined with mechanical treatment
- D06M15/01—Treating fibres, threads, yarns, fabrics, or fibrous goods made from such materials, with macromolecular compounds; Such treatment combined with mechanical treatment with natural macromolecular compounds or derivatives thereof
- D06M15/03—Polysaccharides or derivatives thereof
- D06M15/05—Cellulose or derivatives thereof
- D06M15/09—Cellulose ethers
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M2101/00—Chemical constitution of the fibres, threads, yarns, fabrics or fibrous goods made from such materials, to be treated
- D06M2101/02—Natural fibres, other than mineral fibres
- D06M2101/04—Vegetal fibres
- D06M2101/06—Vegetal fibres cellulosic
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- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M2101/00—Chemical constitution of the fibres, threads, yarns, fabrics or fibrous goods made from such materials, to be treated
- D06M2101/16—Synthetic fibres, other than mineral fibres
- D06M2101/30—Synthetic polymers consisting of macromolecular compounds obtained otherwise than by reactions only involving carbon-to-carbon unsaturated bonds
- D06M2101/32—Polyesters
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- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M2200/00—Functionality of the treatment composition and/or properties imparted to the textile material
- D06M2200/20—Treatment influencing the crease behaviour, the wrinkle resistance, the crease recovery or the ironing ease
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M2200/00—Functionality of the treatment composition and/or properties imparted to the textile material
- D06M2200/50—Modified hand or grip properties; Softening compositions
Landscapes
- Engineering & Computer Science (AREA)
- Textile Engineering (AREA)
- Treatments For Attaching Organic Compounds To Fibrous Goods (AREA)
Abstract
The invention belongs to the durable antibiotic noniron finish liquid and finishing technique of textiles antibacterial finishing technical field, more particularly to a kind of cotton fabric.Dressing liquid uses chitosan, Chinese herbal medicine extract, nano zine oxide, nano titanium oxide and other additive compounds, chitosan Nantural non-toxic is degradable, good biocompatibility, anti-microbial property are excellent, substantial amounts of hydroxyl and amino isoreactivity group are contained in surface, are conducive to anti-wrinkle shrink-proof；Arabic gum film forming parcel Honegsukle flower P.E, houttuynia extract, pomegranate rind extract and nano zine oxide, nano titanium dioxide anti-bacterial agent, reach the effect of sustained release and durable antibiotic, compound chitosan, the good wrinkle resistance of cotton fabric, easy-care properties, anti-microbial property are imparted, cotton fabric feel, strength and washability is improved；Finishing technique two is rolled using two leachings, and content of formaldehyde is up to standard, environmental protection, safety, noresidue, it is collated after fabric antibiotic property, patience, wrinkle resistance and easy-care properties it is good, take comfortably.
Description
Technical field
The invention belongs to textiles antibacterial finishing technical field, more particularly to a kind of durable antibiotic of cotton fabric are non-ironing whole
Manage liquid and finishing technique.
Background technology
Cotton fabric has the advantages that comfortable and easy to wear, natural environmental-protective is very popular, but in dress and washing process
Middle to there is the defect such as easily wrinkle, be difficult to arrange, the life given people brings inconvenience.As quality of life and health are produced
The raising of product technology, people are more and more stronger to the lasting pursuit naturally with health-oriented products, and the feature such as antibacterial is most joyous by market
Meet.Antibacterial finishing agent species of the prior art is a lot, has inorganic antibacterial finishing agent, organic anti-bacterial finishing agent, biological antibiotic whole
Manage agent, natural antibacterial finishing agent etc..But the antibacterial finishing agent of current cotton fabric and the antibacterial effect of finishing technique are bad,
Staphylococcus aureus and Escherichia coli can not effectively be suppressed, washing fastness is poor, anti-microbial property can not persistently effectively, fabric
Wearability it is poor.
The content of the invention
Goal of the invention：In order to overcome problem above, exempt from it is an object of the invention to provide a kind of durable antibiotic of cotton fabric
Scald dressing liquid and finishing technique.
Technical scheme：It is an object of the present invention to provide a kind of durable antibiotic noniron finish liquid of cotton fabric, bag
Include the raw material of following parts by weight：20-30 parts of Honegsukle flower P.E, 20-30 parts of houttuynia extract, pomegranate rind extract 20-30
Part, 2-3 parts of Arabic gum, 5-10 parts of nano zine oxide, 5-10 parts of nano titanium oxide, 4-6 parts of chitosan, 3-5 parts of softening agent,
3-6 parts of carboxymethyl cellulose, 1-2 parts of bleeding agent.
Preferably, described Honegsukle flower P.E be honeysuckle dries pulverizing after with 20% ethanol solution in solid-liquid ratio 1:
10th, twice, each 1h merges extract solution concentration and produced temperature 60 C refluxing extraction after centrifugation.
Preferably, described houttuynia extract be cordate houttuynia segment after with 50% ethanol solution in solid-liquid ratio 1:10th, it is warm
Twice, each 1h merges extract solution concentration and produced refluxing extraction after centrifugation under the conditions of 50 DEG C of degree.
Preferably, described pomegranate rind extract is in solid-liquid ratio 1 after granatum is cut with 50% ethanol solution:10th, it is warm
Twice, each 1h merges extract solution concentration and produced refluxing extraction after centrifugation under the conditions of 50 DEG C of degree.
Preferably, described softening agent is silicone softening agent or ester based quaternary ammonium salt.
Preferably, described bleeding agent is nonionic penetrant JFC.
Preferably, the preparation method of described non-ironing and antibacteria liquid, comprises the following steps：
1) prepared by Honegsukle flower P.E, houttuynia extract and pomegranate rind extract；
2) Arabic gum is added to the solution for being made that concentration is 1% in deionized water, 45 DEG C of stirrings are completely dissolved and must mixed
Liquid；
3) nano zine oxide and nano titanium oxide are weighed by formula ratio, are dispersed in water rear and step 1) in
Honegsukle flower P.E, houttuynia extract and the pomegranate rind extract of preparation are together added to step 2) in mixed liquor in mix
Formula ratio chitosan, softening agent, carboxymethyl cellulose and bleeding agent is added after uniform to be thoroughly mixed and uniformly produce dressing liquid.
It is used for cotton another object of the present invention is to the durable antibiotic noniron finish liquid for providing cotton fabric described above
The durable antibiotic iron-free finishing process of matter fabric, comprises the following steps：Its water content is protected using spray method cotton fabric
Hold to be put into 90-100 DEG C of hot water after 30% and precook, then immerse in non-ironing and antibacteria liquid, bath raio is 1:30, arrange temperature
For 60-80 DEG C, finishing time is 15-30min；Two leachings two are rolled, pick-up 50%, 80 DEG C of -100 DEG C of preliminary drying 5-10min；100-
120 DEG C of baking 1-5min；20 DEG C of temperature, humidity cools down 15-25min for 65% constant temperature and humidity sealing cooling room；30-40 DEG C of temperature
Water is soaped, 90-100 DEG C of drying after cold water flush.
Preferably, described cotton fabric is pure-cotton fabric or cotton and fiber blended fabric, and the wherein content of cotton is 30-
100wt%.
Above-mentioned technical proposal can be seen that the present invention and have the advantages that：Cotton fabric of the present invention is held
Long non-ironing and antibacteria liquid, using chitosan and Chinese herbal medicine extract, nano zine oxide, nano titanium oxide and other auxiliary agents
Compounding is native biopolymer polysaccharide as dressing liquid, chitosan, and Nantural non-toxic is degradable, good biocompatibility, antibiotic property
Can be excellent, substantial amounts of hydroxyl and amino isoreactivity group are contained in chitosan surface, are conducive to improving the Shrinkproof crease-resistant effect of dressing liquid
Really；Arabic gum film forming parcel Honegsukle flower P.E, houttuynia extract, pomegranate rind extract and nano zine oxide, nanometer two
Titanium oxide antiseptic, reaches the effect of sustained release and durable antibiotic, adds chitosan compounding, imparts good crease-resistant of cotton fabric
Property, easy-care properties, anti-microbial property, improve cotton fabric feel, strength and washability；Antibacterial finishing process is rolled using two leachings two,
Content of formaldehyde is up to standard, environmental protection, safety, noresidue, it is collated after fabric antibiotic property, patience, wrinkle resistance and easy-care properties it is good, take
Comfortably.
Embodiment
With reference to specific embodiment, the present invention is furture elucidated.
Embodiment 1
A kind of durable antibiotic noniron finish liquid of cotton fabric, includes the raw material of following parts by weight：Honegsukle flower P.E 20
Part, 20 parts of houttuynia extract, 20 parts of pomegranate rind extract, 2 parts of Arabic gum, 5 parts of nano zine oxide, nano titanium oxide 5
Part, 4 parts of chitosan, 3 parts of silicone softening agent, 3 parts of carboxymethyl cellulose, 1 part of nonionic penetrant JFC.
Described Honegsukle flower P.E be honeysuckle dries pulverizing after with 20% ethanol solution in solid-liquid ratio 1:10th, temperature 60
Twice, each 1h merges extract solution concentration and produced after centrifugation for DEG C refluxing extraction.
Described houttuynia extract be cordate houttuynia segment after with 50% ethanol solution in solid-liquid ratio 1:10th, temperature 50 C bar
Twice, each 1h merges extract solution concentration and produced refluxing extraction after centrifugation under part.
Described pomegranate rind extract is in solid-liquid ratio 1 after granatum is cut with 50% ethanol solution:10th, temperature 50 C bar
Twice, each 1h merges extract solution concentration and produced refluxing extraction after centrifugation under part.
The preparation method of described non-ironing and antibacteria liquid, comprises the following steps：
1) prepared by Honegsukle flower P.E, houttuynia extract and pomegranate rind extract；
2) Arabic gum is added to the solution for being made that concentration is 1% in deionized water, 45 DEG C of stirrings are completely dissolved and must mixed
Liquid；
3) nano zine oxide and nano titanium oxide are weighed by formula ratio, are dispersed in water rear and step 1) in
Honegsukle flower P.E, houttuynia extract and the pomegranate rind extract of preparation are together added to step 2) in mixed liquor in mix
Formula ratio chitosan, silicone softening agent, carboxymethyl cellulose, nonionic penetrant JFC is added after uniform to be sufficiently stirred for mixing
Conjunction uniformly produces dressing liquid.
Above-mentioned non-ironing and antibacteria liquid is used for the durable antibiotic iron-free finishing process of cotton fabric, comprises the following steps：
Use spray method to make its water content be put into after being maintained at 30% in 90 DEG C of hot water cotton fabric to precook, then immerse antibacterial and exempt from
Scald in dressing liquid, bath raio is 1:30, it is 60 DEG C to arrange temperature, and finishing time is 30min；Two leachings two are rolled, pick-up 50%, 80 DEG C
Preliminary drying 10min；100 DEG C of baking 5min；20 DEG C of temperature, humidity cools down 15min for 65% constant temperature and humidity sealing cooling room；30℃
Warm water is soaped, 90 DEG C of drying after cold water flush.
Described cotton fabric is pure-cotton fabric.
Embodiment 2
A kind of durable antibiotic noniron finish liquid of cotton fabric, includes the raw material of following parts by weight：Honegsukle flower P.E 30
Part, 30 parts of houttuynia extract, 30 parts of pomegranate rind extract, 3 parts of Arabic gum, 10 parts of nano zine oxide, nano titanium oxide
10 parts, 6 parts of chitosan, 5 parts of ester based quaternary ammonium salt, 6 parts of carboxymethyl cellulose, JFC2 parts of nonionic penetrant.
Described Honegsukle flower P.E be honeysuckle dries pulverizing after with 20% ethanol solution in solid-liquid ratio 1:10th, temperature 60
Twice, each 1h merges extract solution concentration and produced after centrifugation for DEG C refluxing extraction.
Described houttuynia extract be cordate houttuynia segment after with 50% ethanol solution in solid-liquid ratio 1:10th, temperature 50 C bar
Twice, each 1h merges extract solution concentration and produced refluxing extraction after centrifugation under part.
Described pomegranate rind extract is in solid-liquid ratio 1 after granatum is cut with 50% ethanol solution:10th, temperature 50 C bar
Twice, each 1h merges extract solution concentration and produced refluxing extraction after centrifugation under part.
The preparation method of described non-ironing and antibacteria liquid, comprises the following steps：
1) prepared by Honegsukle flower P.E, houttuynia extract and pomegranate rind extract；
2) Arabic gum is added to the solution for being made that concentration is 1% in deionized water, 45 DEG C of stirrings are completely dissolved and must mixed
Liquid；
3) nano zine oxide and nano titanium oxide are weighed by formula ratio, are dispersed in water rear and step 1) in
Honegsukle flower P.E, houttuynia extract and the pomegranate rind extract of preparation are together added to step 2) in mixed liquor in mix
Formula ratio chitosan, ester based quaternary ammonium salt, carboxymethyl cellulose, nonionic penetrant JFC is added after uniform to be thoroughly mixed
Uniformly produce dressing liquid.
Non-ironing and antibacteria liquid described above is used for the durable antibiotic iron-free finishing process of cotton fabric, including following step
Suddenly：Make its water content be put into after being maintained at 30% in 100 DEG C of hot water using spray method cotton fabric to precook, then immerse anti-
In bacterium noniron finish liquid, bath raio is 1:30, it is 80 DEG C to arrange temperature, and finishing time is 15min；Two leachings two are rolled, pick-up 50%,
100 DEG C of preliminary drying 5min；120 DEG C of baking 1min；20 DEG C of temperature, humidity cools down 25min for 65% constant temperature and humidity sealing cooling room；
40 DEG C of warm water are soaped, 100 DEG C of drying after cold water flush.
Described cotton fabric is cotton and polyester fiber blended yarn weaved fabric, and the wherein content of cotton is 30wt%.
Embodiment 3
A kind of durable antibiotic noniron finish liquid of cotton fabric, includes the raw material of following parts by weight：Honegsukle flower P.E 25
Part, 25 parts of houttuynia extract, 25 parts of pomegranate rind extract, 2.5 parts of Arabic gum, 8 parts of nano zine oxide, nano titanium oxide
8 parts, 5 parts of chitosan, 4 parts of silicone softening agent, 5 parts of carboxymethyl cellulose, JFC1.5 parts of nonionic penetrant.
Described Honegsukle flower P.E be honeysuckle dries pulverizing after with 20% ethanol solution in solid-liquid ratio 1:10th, temperature 60
Twice, each 1h merges extract solution concentration and produced after centrifugation for DEG C refluxing extraction.
Described houttuynia extract be cordate houttuynia segment after with 50% ethanol solution in solid-liquid ratio 1:10th, temperature 50 C bar
Twice, each 1h merges extract solution concentration and produced refluxing extraction after centrifugation under part.
Described pomegranate rind extract is in solid-liquid ratio 1 after granatum is cut with 50% ethanol solution:10th, temperature 50 C bar
Twice, each 1h merges extract solution concentration and produced refluxing extraction after centrifugation under part.
The preparation method of described non-ironing and antibacteria liquid, comprises the following steps：
1) prepared by Honegsukle flower P.E, houttuynia extract and pomegranate rind extract；
2) Arabic gum is added to the solution for being made that concentration is 1% in deionized water, 45 DEG C of stirrings are completely dissolved and must mixed
Liquid；
3) nano zine oxide and nano titanium oxide are weighed by formula ratio, are dispersed in water rear and step 1) in
Honegsukle flower P.E, houttuynia extract and the pomegranate rind extract of preparation are together added to step 2) in mixed liquor in mix
Formula ratio chitosan, silicone softening agent, carboxymethyl cellulose, nonionic penetrant JFC is added after uniform to be sufficiently stirred for mixing
Conjunction uniformly produces dressing liquid.
Non-ironing and antibacteria liquid described above is used for the durable antibiotic iron-free finishing process of cotton fabric, including following step
Suddenly：Make its water content be put into after being maintained at 30% in 95 DEG C of hot water using spray method cotton fabric to precook, then immerse anti-
In bacterium noniron finish liquid, bath raio is 1:30, it is 70 DEG C to arrange temperature, and finishing time is 23min；Two leachings two are rolled, pick-up 50%,
90 DEG C of preliminary drying 8min；110 DEG C of baking 3min；20 DEG C of temperature, humidity cools down 20min for 65% constant temperature and humidity sealing cooling room；
35 DEG C of warm water are soaped, 95 DEG C of drying after cold water flush.
Described cotton fabric is cotton and polyester fiber blended yarn weaved fabric, and the wherein content of cotton is 65wt%.
Its ironing-free performance Testing index of cotton fabric and standard GB/T/T 18863- after being arranged to embodiment 1-3
2002《Non-ironing textile》Comparing result and install AATCC 79 test washing before and after water absorbing properties, as a result as shown in table 1；
It is as shown in table 2 below to the inhibiting rate of staphylococcus aureus and Escherichia coli.
The embodiment properties of product test index of table 1 and national standard contrast table
Inhibiting rate of the embodiment product of table 2 to staphylococcus aureus and Escherichia coli
| Staphylococcus aureus inhibiting rate | Escherichia coli inhibiting rate | |
| Embodiment 1 | 90.8% | 92.4% |
| Embodiment 2 | 93.5% | 92.8% |
| Embodiment 3 | 98.2% | 97.5% |
Described above is only the preferred embodiment of the present invention, it is noted that for the ordinary skill people of the art
For member, under the premise without departing from the principles of the invention, some improvement can also be made, these improvement also should be regarded as the present invention's
Protection domain.
Claims (9)
1. a kind of durable antibiotic noniron finish liquid of cotton fabric, it is characterised in that：Include the raw material of following parts by weight：Honeysuckle
It is 20-30 parts of extract, 20-30 parts of houttuynia extract, 20-30 parts of pomegranate rind extract, 2-3 parts of Arabic gum, nano oxidized
5-10 parts of zinc, 5-10 parts of nano titanium oxide, 4-6 parts of chitosan, 3-5 parts of softening agent, 3-6 parts of carboxymethyl cellulose, bleeding agent
1-2 parts.
2. a kind of durable antibiotic noniron finish liquid of cotton fabric according to claim 1, it is characterised in that：Described gold
Honeysuckle flower extract be honeysuckle dries pulverizing after with 20% ethanol solution in solid-liquid ratio 1:10th, temperature 60 C refluxing extraction twice, often
Secondary 1h, merges extract solution concentration and produces after centrifugation.
3. a kind of durable antibiotic noniron finish liquid of cotton fabric according to claim 1, it is characterised in that：Described fish
Raw meat grass extract be cordate houttuynia segment after with 50% ethanol solution in solid-liquid ratio 1:10th, under the conditions of temperature 50 C refluxing extraction twice,
Each 1h, merges extract solution concentration and produces after centrifugation.
4. a kind of durable antibiotic noniron finish liquid of cotton fabric according to claim 1, it is characterised in that：Described stone
Pomegranate bark extract is in solid-liquid ratio 1 after granatum is cut with 50% ethanol solution:10th, under the conditions of temperature 50 C refluxing extraction twice,
Each 1h, merges extract solution concentration and produces after centrifugation.
5. a kind of durable antibiotic noniron finish liquid of cotton fabric according to claim 1, it is characterised in that：Described is soft
Soft dose is silicone softening agent or ester based quaternary ammonium salt.
6. a kind of durable antibiotic noniron finish liquid of cotton fabric according to claim 1, it is characterised in that：Described oozes
Saturating agent is nonionic penetrant JFC.
7. a kind of durable antibiotic noniron finish liquid of cotton fabric according to claim 1, it is characterised in that：Described is anti-
The preparation method of bacterium noniron finish liquid, comprises the following steps：
1）It is prepared by Honegsukle flower P.E, houttuynia extract and pomegranate rind extract；
2）Arabic gum is added to the solution for being made that concentration is 1% in deionized water, 45 DEG C of stirrings are completely dissolved to obtain mixed liquor；
3）Nano zine oxide and nano titanium oxide are weighed by formula ratio, rear and step 1 is dispersed in water）It is middle to prepare
Honegsukle flower P.E, houttuynia extract and pomegranate rind extract be together added to step 2）In mixed liquor in be well mixed
Formula ratio chitosan, softening agent, carboxymethyl cellulose and bleeding agent is added afterwards to be thoroughly mixed and uniformly produce dressing liquid.
8. a kind of durable antibiotic noniron finish liquid of cotton fabric as described in claim any one of 1-7 is used for cotton fabric
Durable antibiotic iron-free finishing process, it is characterised in that：Its water content is set to be put after being maintained at 30% using spray method cotton fabric
Enter into 90-100 DEG C of hot water and precook, then immerse in non-ironing and antibacteria liquid, bath raio is 1:30, it is 60-80 DEG C to arrange temperature, whole
The reason time is 15-30min；Two leachings two are rolled, pick-up 50%, 80 DEG C of -100 DEG C of preliminary drying 5-10min；100-120 DEG C of baking 1-
5min；20 DEG C of temperature, humidity cools down 15-25min for 65% constant temperature and humidity sealing cooling room；30-40 DEG C of warm water is soaped, cold water
90-100 DEG C of drying after flushing.
9. the durable antibiotic iron-free finishing process of cotton fabric according to claim 8, it is characterised in that：Described cotton
Fabric is pure-cotton fabric or cotton and fiber blended fabric, and the wherein content of cotton is 30-100wt%.
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| CN111411510B (en) * | 2020-04-28 | 2022-10-21 | 同曦集团有限公司 | Antibacterial, anti-mite and antiviral finishing agent, plush fabric and preparation method and application thereof |
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| CN113445312A (en) * | 2021-07-13 | 2021-09-28 | 南通帝沙纺织有限公司 | Preparation method of whitening antibacterial finishing fabric and whitening antibacterial finishing fabric |
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| CN114575143A (en) * | 2022-03-22 | 2022-06-03 | 杭州朝盛塑业有限公司 | High-temperature-resistant antibacterial non-woven fabric |
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