CN103924463A - Technology for dyeing middle dark cotton/brocade fabric by one-bath one-step method - Google Patents
Technology for dyeing middle dark cotton/brocade fabric by one-bath one-step method Download PDFInfo
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Abstract
The invention discloses a technology for dyeing a middle dark cotton/brocade fabric by a one-bath one-step method. According to the technology, a reactive direct dye and a neutral dye are used; meanwhile, a water softening agent, pure alkali and edible salt are added and are used as auxiliaries; by the adoption of the dyeing technology based on the one-bath one-step method, the cotton/brocade fabric dyeing production time is greatly shortened, the energy consumption is greatly reduced, and the production cost is greatly lowered; the dark color dyeing property is achieved, and particularly deep dark color dyeing can be realized; the modern low-carbon and environment-friendly development idea can be met really.
Description
Technical field
The present invention relates to the colouring method of a kind of cotton/bright and beautiful fabric, particularly a kind of one bathe the technique that one-step method is dyed middle dark cotton/bright and beautiful fabric.
Background technology
The moisture absorption of the existing cotton of cotton/bright and beautiful fabric is breathed freely, the soft glutinous performance of feel, has again the elastic force of polyamide fibre, wear-resisting durable good characteristic, as garment material, liked by consumers in general.But due to cotton completely different with the dyeability of polyamide fibre; so normally with the dyeing of two one-bath two-step process; with the method dyeing, to carry out secondary dye bath; multistep technique, consume a large amount of steam, electric power and water, and the more material of dying; process route is long and numerous and diverse; power consumption is large, blowdown is many, yield poorly, cost is high, unfavorable greatly to environmental protection, is not suitable for the idea of development of modern low-carbon environment-friendly.Current domestic printing and dyeing circle, for addressing the above problem, have been invented employing heat curing-type REACTIVE DYES and neutral dye one bath one-step method cotton/bright and beautiful staining technique.These technology are because heat curing-type Dyeing of Cotton Fabric with Reactive Dyes has good level-dyeing property, the wet good feature of fastness improves staining technique greatly, but these dyestuff depths are poor, can only dye some light fabrics, cannot really solve a bath one-step method and dye cotton/bright and beautiful fabric problem, and because depth, dye-uptake problem have been brought a series of environmental issue.
Realize cotton/bright and beautiful kind fabric one is bathed to one-step method dyeing, particularly solve dark heavy colour problem, key point has three: one, dye cotton dye with dye bright and beautiful dyestuff to dyeing temperature require identical; Its two, dye cotton dye and dye bright and beautiful dyestuff the adaptability of the pH value of dye bath is wanted well; Its three, dye cotton dye and dye bright and beautiful dyestuff and be subject to electrolytical impact to want consistent.
It is better that direct dyes are dyed cotton depth, but that COLOR FASTNESS is compared with REACTIVE DYES is poor.Reactive direct dyes are the new products that in recent years come out, and both having had REACTIVE DYES can form chemical bonds with cellulose fibre, and the feature that set fastness is good has again direct dyes degree of exhaustion high, and dyeability is good, the advantage that heat-resistant stability is good.Therefore, the dyefastness of reactive direct dyes is significantly higher than common direct dyes, the binding pattern of itself and cellulose fibre is similar to the feature of REACTIVE DYES, and every fastness of the sample that causes dyeing (wet friction, soap, water logging, perspiration fastness etc.) is best in quality.After testing; reactive direct dyes are dyed cotton, and the best dyeing temperature of whole structure is 100 ℃, though polyamide fibre belongs to hydrophobic fibre; but structure is more loose than terylene; water imbibition is large compared with terylene, easy swelling in water, and vitrification point is low; therefore; no matter be that neutral dye or DISPERSE DYES are dyed brocade, under the 100 ℃ of conditions of temperature of boiling, dye, just can obtain optimum dyeing effect.Specifically in Table 1-1,1-2,1-3.
The relations of dependence of the amount of dying and dyeing temperature in the reactive direct dyes in table 1-1
Note: (1) prescription: dyestuff 2% (owf), calgon 1.5g/L,, soda ash 1g/L, salt 70g/l.
(2) technique: bath raio 1:25, heating rate 2%/min, 70 ℃, 80 ℃, 90 ℃, 100 ℃ insulation dyeing 50min respectively, wash, soap, wash, dry.
(3) detect: with Datacolor SF600X colour photometer, detect.
Table 1-2 DISPERSE DYES is dyed the relative color depth that obtains of polyamide fibre coloured differently temperature
Note: (1) prescription: dyestuff 2% (o.w.f), calgon 1.5g/L,, high temperature levelling agent 1.5g/L (raffinate PH=4.11).
(2) condition: bath raio 1:20,2.5 ℃/min of heating rate, rotating speed 45r/min, is incubated respectively dyeing 30min with institute's coloured differently temperature in showing.
(3) detect: with 100 ℃ of coloration results, make standard, relatively.Datacolor SF600X colour photometer detects.
Table 1-3 neutral dye dyes the relative color depth that obtains of polyamide fibre coloured differently temperature
Note: (1) prescription: dyestuff 2% (o.w.f), calgon 1.5g/L,, ammonium sulfate 2g/L, polyamide fibre levelling agent 9511.5g/L.
(2) technique: bath raio 1:25, heating rate is 2 ℃/min, with dyeing temperature listed in showing, is incubated respectively dyeing 30min, PH=6~6.5.
(3) detect: the relative of 100 ℃ of dyeing of take must the degree of depth be 100%, adopts Datacolor SF600X colour photometer to detect.
Reactive direct dyes and REACTIVE DYES are similar, in its molecular structure, with reactive group, under alkali condition, the crosslinked combination of chemistry can occur with cellulose, thereby obtain dyefastness.After testing, reactive direct dyes and DISPERSE DYES, dye and can obtain optimum dyeing effect at the similar point of pH value (pH=10.08) with nylon fabric cotton respectively; And neutral dye dyes polyamide fibre, dye bath pH value is little on coloration result (degree of depth, coloured light) impact, so, reactive direct dyes and DISPERSE DYES or neutral dye o'clock dye cotton and polyamide fibre with bathing in PH=10~11, and its character meets the requirement with bath property, specifically in Table 2-1,2-2,2-3.
The relative dependency that obtains color depth and dye bath pH value of table 2-1 gram jail clone AA type dye
Note: (1) prescription: dyestuff 1% (owf), calgon 1.5g/L,, salt 60g/L, soda ash 0.05~1.4g/L.
(2) technique: bath raio 1:25,2 ℃/min100 of heating rate ℃ insulation dyeing 40min, washing, soaps for twice.
(3) detect: pH value is detected by the Hangzhou thunder magnetic analysis instrument PHS-25 of factory type digital display acidometer, relative that color depth detects with Datacolor SF600X colour photometer.
Table 2-2 DISPERSE DYES is dyed the relative color depth that obtains of the different dye bath pH values of polyamide fibre
Note: (1) prescription: dyestuff 1.25% (o.w.f), calgon 1.5g/L,, salt (acid bath, neutral-bath dyeing do not add, and Dyeing in Alkali Bath adds 60g/L), pH value regulates with soda ash and acetic acid.
(2) technique: bath raio 1:30,2 ℃/min100 of heating rate ℃ insulation dyeing 40min, washes, soaps.
(3) detect: with table 2-1.
Table 2-3 neutral dye dyes the relative color depth that obtains of the different dye bath pH values of polyamide fibre
Note: testing conditions is with table 2-2.
Reactive direct dyes are dyed cotton, and electrolyte is larger than direct dyes, REACTIVE DYES on the impact of tinctorial yield.Simultaneously, electrolytical adding, stability on the DISPERSE DYES with bathing can produce certain impact, centering dyeing, level-dyeing property, covering, blending can have a certain impact, after testing, different depth of colors is given different appropriate, can solve with bath property problem, specifically, in Table 3-1, show 3-2.
The amount of dying and the electrolytical relations of dependence in the reactive direct dyes in table 3-1
Note: (1) prescription: dyestuff 2% (owf), calgon 1.5g/L,, soda ash 1g/L, salt 20~80g/L.
(2) technique: bath raio 1:25,2.5 ℃/min100 of heating rate ℃ insulation dyeing 50min, wash, soap, washing.
(3) detect: take relative the color depth that adds salt 80g/L as 100% relatively.Datacolor SF600X colour photometer detects.
Table 3-2 electrolyte is on dying the impact of polyamide fibre on DISPERSE DYES and neutral dye
Therefore, by experiment with practice, on the whole due to reactive direct dyes and neutral dye (or DISPERSE DYES), there is good co-bathing dyeing adaptability under certain condition, in order to a bath one-step method, dye cotton/bright and beautiful kind fabric, can obtain desirable Color, particularly can solve the colouring problem of dark dense property.In conjunction with above-mentioned discussion, we are simple in the urgent need to finding out a kind of colouring method, and can be applied in the dyeing that dyes the especially middle dark system of multiple colour system on cotton/bright and beautiful fabric.
Summary of the invention
The defect existing for prior art, the invention provides a kind of use that reactive direct dyes are combined with neutral dye one bathe the technique that one-step method is dyed middle dark cotton/bright and beautiful fabric, cotton/bright and beautiful textile dyeing production time is shortened greatly, energy resource consumption greatly reduces, production cost reduces greatly, solved dyeing depth problem, particularly dyed dark heavy colour fabric, from truly meeting the idea of development of modern low-carbon environment-friendly.
For solving the problems of the technologies described above, the technical solution used in the present invention is:
The technique that an a kind of bath one-step method is dyed middle dark cotton/bright and beautiful fabric is carried out according to following steps:
(1), under normal temperature, fabric is immersed to 10min in the dye liquor staining bath that contains a certain amount of auxiliary agent;
(2) then, add the mixture of a certain amount of reactive direct dyes and neutral dye to contaminate at normal temperatures 10~15min;
(3) speed of following with 1.5 ℃/min is warming up to 100 ℃, then at 100 ℃ of insulation 40~60min;
(4) finally by crossing, wash, soap, wash and can complete again.
As limitation of the invention: described auxiliary agent comprises soda ash, the 60~80g/L of the water softener of 1.0~1.5g/L, 0.4g/L.
As limitation of the invention further: the consumption of described reactive direct dyes is 0~4.5%o.w.f, and the consumption of neutral dye is 0~3.0%o.w.f.
Especially, of the present invention one bathes one-step method dyeing except can dying middle dark color, also can dye conventional shallow faint colour, and the processing step while dying shallow faint colour carries out in such a way:
(1), under normal temperature, fabric is immersed to 10min in the dye liquor staining bath that contains a certain amount of auxiliary agent;
(2) then, add the mixture of a certain amount of reactive direct dyes and DISPERSE DYES to contaminate at normal temperatures 10~15min;
(3) then start to be warming up to 60 ℃ with the speed of 1.5 ℃/min, in the time of 60 ℃, be incubated 10min; Then with the speed of 1.5 ℃/min, be warming up to 100 ℃ again, in the time of 100 ℃, be incubated 30~40min;
(4) finally by crossing, wash, soap, wash and can complete again.
Wherein, the consumption of auxiliary agent is with to dye middle dark color the same, and just the consumption of salt does not need so much, only need 20~30g/L, the consumption of reactive direct dyes is 0~0.5%o.w.f, and the consumption of DISPERSE DYES is 0~0.5%o.w.f, and other are all consistent when dying middle dark color.
Wherein, the consumption of water softener, soda ash is with to dye middle dark color the same, the consumption of salt does not need so much, only need 20~30g/L, another according to the depth of color and luster, when darker, will add diffusion agent N 1~1.5g/L, the consumption of reactive direct dyes is 0~0.5%o.w.f, and the consumption of DISPERSE DYES is 0~0.5%o.w.f.
For such scheme, there is following statement:
1. the aberration that mass discrepancy when polyamide fibre dyes shallow faint colour causes (being commonly called as through Ang, weft bar), if adopt the DISPERSE DYES temperature of boiling to dye polyamide fibre, covering, level dyeing performance are fine, but carry dark poor-performing, wet colour fastness is lower, and therefore, DISPERSE DYES is particularly suitable for dying the light color and luster of polyamide fibre.
2. because the DISPERSE DYES temperature of boiling is dyed polyamide fibre, by dying in hydrogen bond gravitation and Van der Waals force, there is not ionic bond combination, so add the almost not effect of polyamide fibre levelling agent, and can make a difference to dyeing tinctorial yield, can produce serious aberration, and the adding of diffusant, under (100 ℃) normal temperature and pressure conditions, the dispersion stabilization of DISPERSE DYES is good.
3. after testing, reactive direct dyes are dyed cotton, and electrolyte is larger than direct dyes, REACTIVE DYES on the impact of tinctorial yield.Meanwhile, due to the covering property of DISPERSE DYES by means of anion-proliferation agent, electrolytical existence, brings certain impact to dye stability again.When therefore shallow faint colour dyes, by adding in right amount salt and diffusion agent N, can address the above problem, generally be placed on 20~30g/L and be advisable.
4. when dark in dying cotton by reactive direct dyes, larger to electrolytical dependence, and neutral dye, because electrolytical solubility has affected level-dyeing property, covering, blending etc., so that amount of electrolyte is difficult for is too high, is generally placed on 60~80g/L and is advisable.
5. the vitrification point of polyamide fibre is low, and easy swelling in water, and DISPERSE DYES molecular mass is relatively little is dyed temperature while being greater than 60 ℃, and dye-uptake can be accelerated suddenly.Meanwhile, reactive direct dyes are dyed cotton, and in alkaline salt bath, affinity is higher, therefore when dyeing, control certain heating rate and temperature retention time, can obtain preferably Color.
6. after testing, in its molecular structure of reactive direct dyes, with reactive group, in PH=10~11, o'clock can obtain good dyefastness and certain dye level.DISPERSE DYES is dyed polyamide fibre, the chromatic adaptation of having illicit sexual relations in the alkalescence temperature of boiling in (PH=10.08) salt bath.And neutral dye dyes polyamide fibre, dye bath pH value is little on coloration result (degree of depth, coloured light) impact.Therefore, according to their feature, the cotton bright and beautiful fabric of shallow faint colour is dyed in the bath identical with DISPERSE DYES of reactivity direct dyes, and reactive direct dyes and neutral dye dye the cotton bright and beautiful fabric of middle dark color with bathing, and meets and dyes cotton dye and dye the condition that bright and beautiful dyestuff will be good to the adaptability of the pH value of dye bath.
Adopted after technique scheme, the present invention has following beneficial effect: this technique is except making the cotton bright and beautiful textile dyeing production time greatly shorten, and energy resource consumption greatly reduces, and outside production cost reduces greatly, also has advantage and the effect of three aspects:.The first, the depth of reactive direct dyes is good, has solved the middle deep colour dyeing problem of a bath one-step method, particularly especially remarkable for dark heavy colour effect.The second, general REACTIVE DYES dye-uptake is only 60%~65%, and reactive direct dyes more than 90% can go up on fiber and go, and dye utilization rate is high, and the pollutant of generation reduces widely, therefore, and good environmental protection.The 3rd, reactive direct dyes price is lower, and utilization rate is high, and its economy is also high, so the invention of this technique, meets idea of development high-quality and efficient, low-carbon environment-friendly.
The specific embodiment
For content of the present invention is more easily expressly understood, according to specific embodiment, the present invention is further detailed explanation below.
Embodiment 1
One bathes one-step method dyes navy
1. the cotton bright and beautiful elastic force poplin cloth 40 of fabric
s* 70
d+ 40
d/ 133 * 72
2. equipment adopts and sprays overflow machine dye bath ratio 1:12
3. dyeing prescription:
4. dyeing:
(1), under normal temperature, fabric is immersed in the dye liquor staining bath of the water softener, soda ash and the salt that are added with above-mentioned content
10min;
(2) then, add dyestuff to contaminate at normal temperatures 12min;
(3) speed of following with 1.5 ℃/min is warming up to 100 ℃, is then incubated 40min;
(4) finally by crossing, wash, soap, wash and can complete.
Embodiment 2
One bathes one-step method dyes coffee color
1. the cotton bright and beautiful elastic force poplin cloth 40 of fabric
s* 70
d+ 40
d/ 133 * 72
2. equipment adopts and sprays overflow machine dye bath ratio 1:12
3. dyeing prescription:
4. dyeing:
(1), under normal temperature, fabric is immersed and to be added with water softener, the soda ash of above-mentioned content, 10min in the dye liquor staining bath of salt;
(2) then, add dyestuff to contaminate at normal temperatures 15min;
(3) speed of following with 1.5 ℃/min is warming up to 100 ℃, is then incubated 40min;
(4) finally by crossing, wash, soap, wash and can complete.
Embodiment 3
One bathes one-step method dyes corvinus
1. the cotton bright and beautiful elastic force poplin cloth 40 of fabric
s* 70
d+ 40
d/ 133 * 72
2. equipment adopts and sprays overflow machine dye bath ratio 1:12
3. dyeing prescription:
4. dyeing:
(1) under normal temperature, in the dye liquor staining bath of the water softener that fabric immersion is contained to above-mentioned content, soda ash, salt
10min;
(2) then, add dyestuff to contaminate at normal temperatures 10min;
(3) speed of following with 1.5 ℃/min is warming up to 100 ℃, is then incubated 60min;
(4) then through washing, soaping, wash and can complete.
Embodiment 4
One bathes one-step method dyes salmon pink
1. the cotton bright and beautiful elastic force poplin cloth 40 of fabric
s* 70
d+ 40
d/ 133 * 72
2. equipment adopts and sprays overflow machine dye bath ratio 1:12
3. dyeing prescription:
4. dyeing:
(1), under normal temperature, fabric is immersed to 10min in the dye liquor staining bath that is added with water softener, soda ash, salt;
(2) then, add dyestuff to contaminate at normal temperatures 10min;
(3) then start to be warming up to 60 ℃ with the speed of 1.5 ℃/min;
(4) while arriving 60 ℃, insulation 10min;
(5) then start to be again warming up to 100 ℃ with the speed of 1.5 ℃/min;
(6), while arriving 100 ℃, insulation 30min, then through washing, soap, washing and complete again.
By above embodiment, not only the dyeing of the cotton of centering dark color/brocade is better can to see the dyeing arriving of the present invention, and also can dye to the cloth of shallow faint colour, is a kind of widely used dyeing.
Above-described specific embodiment; object of the present invention, technical scheme and beneficial effect are further described; institute is understood that; the foregoing is only specific embodiments of the invention; be not limited to the present invention; within the spirit and principles in the present invention all, any modification of making, be equal to replacement, improvement etc., within all should being included in protection scope of the present invention.
Claims (3)
1. one bathe the technique that one-step method is dyed middle dark cotton/bright and beautiful fabric, it is characterized in that this technique carries out according to following steps:
(1), under normal temperature, fabric is immersed to 10min in the dye liquor staining bath that contains a certain amount of auxiliary agent;
(2) then, add the mixture of a certain amount of reactive direct dyes and neutral dye to contaminate at normal temperatures 10~15min;
(3) speed of following with 1.5 ℃/min is warming up to 100 ℃, then at 100 ℃ of insulation 40~60min;
(4) finally by crossing, wash, soap, wash and can complete again.
2. according to claim 1 a kind of one bathe the technique that one-step method is dyed middle dark cotton/bright and beautiful fabric, it is characterized in that water softener, the soda ash of 0.4g/L and the salt of 60~80g/L that described auxiliary agent contains 1.0~1.5g/L.
3. according to claim 1 a kind of one bathe the technique that one-step method is dyed middle dark cotton/bright and beautiful fabric, it is characterized in that the consumption of described reactive direct dyes is 0~4.5%o.w.f, the consumption of neutral dye is 0~3.0%o.w.f.
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Cited By (6)
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---|---|---|---|---|
CN104313901A (en) * | 2014-09-30 | 2015-01-28 | 鲁泰纺织股份有限公司 | Pure cotton cheese dyeing method |
CN108708189A (en) * | 2018-05-21 | 2018-10-26 | 吴江桃源染料有限公司 | A kind of composite reactive crimson and its application |
CN108774906A (en) * | 2018-06-27 | 2018-11-09 | 彭伟民 | A method of with bath agent and its applied to dyeing |
CN111764039A (en) * | 2020-06-29 | 2020-10-13 | 山东华润厚木尼龙有限公司 | Production process of alginate fiber postoperative rehabilitation underpants and underpants thereof |
CN113550157A (en) * | 2021-08-23 | 2021-10-26 | 福建漳平协龙高新化纤有限公司 | Multi-component jacquard material one-bath process multicolor dyeing method |
CN116676796A (en) * | 2023-05-22 | 2023-09-01 | 浙江三元纺织有限公司 | Cotton-nylon blended one-bath dyeing method |
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Cited By (6)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN104313901A (en) * | 2014-09-30 | 2015-01-28 | 鲁泰纺织股份有限公司 | Pure cotton cheese dyeing method |
CN108708189A (en) * | 2018-05-21 | 2018-10-26 | 吴江桃源染料有限公司 | A kind of composite reactive crimson and its application |
CN108774906A (en) * | 2018-06-27 | 2018-11-09 | 彭伟民 | A method of with bath agent and its applied to dyeing |
CN111764039A (en) * | 2020-06-29 | 2020-10-13 | 山东华润厚木尼龙有限公司 | Production process of alginate fiber postoperative rehabilitation underpants and underpants thereof |
CN113550157A (en) * | 2021-08-23 | 2021-10-26 | 福建漳平协龙高新化纤有限公司 | Multi-component jacquard material one-bath process multicolor dyeing method |
CN116676796A (en) * | 2023-05-22 | 2023-09-01 | 浙江三元纺织有限公司 | Cotton-nylon blended one-bath dyeing method |
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