CN102021846A - Process method for dying flax fabric by vegetable dye - Google Patents
Process method for dying flax fabric by vegetable dye Download PDFInfo
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- CN102021846A CN102021846A CN2009101767683A CN200910176768A CN102021846A CN 102021846 A CN102021846 A CN 102021846A CN 2009101767683 A CN2009101767683 A CN 2009101767683A CN 200910176768 A CN200910176768 A CN 200910176768A CN 102021846 A CN102021846 A CN 102021846A
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Abstract
The invention relates to the technical field of textiles, in particular to a process method for dying a flax fabric by a vegetable dye. The process method is characterized by comprising the following steps of: firstly, carrying out bioenzyme degumming and ultrasonic pretreatment on the flax fabric; secondly, carrying out the subsequent dyeing treatment including ultrasonic pretreatment in dye liquor and the temperature-rise dyeing treatment on the fabric; carrying out cold water washing, soaping and hot water washing; and finally carrying out cold water washing, drying and other steps to obtain the finished product of the flax fabric. Compared with the prior art, the fabric to be dyed cannot be damaged in the dyeing process, the performance of the vegetable dye is improved and the dyeing uniformity and stability are improved; and the finished fabric meets the requirements for greenness and environmental protection.
Description
Technical field
The present invention relates to field of fabric producing technology, particularly, relate to the process that a kind of vegetable colour dyes flax lining.
Background technology
Along with human living standard's raising day by day, people are to environmental protection and healthy more and more attention.The textiles of chemical dye dyeing uses the phenol formaldehyde (PF) color-fixing agent for strengthening COLOR FASTNESS, and use formaldehyde to carry out the back arrangement, some azo dyess in the chemical dye can also be decomposed into poisonous aromatic amine, pentachloro-, chlorophenol etc. simultaneously, these have caused national governments and scientist's great attention to the mankind's harm, but the way that solves also just limits the printing and dyeing enterprise sewage discharge and limits the content of formaldehyde of textiles, forbidding azo dyes, heavy metal etc., and these ways can not fundamentally solve the problem of chemical dye serious environment pollution and injury human health.
And vegetable colour dyeing just can fundamentally solve the chemical contamination problem, and this is the traditional colouring method of China, meets the requirement of present ecological textile.But textile fabric is various in style at present, own characteristic at different linings, plant dyeing also faces different problems, wherein at flax lining, subject matter is: the dyestuff dye-uptake is low, and dyefastness is lower, and inhomogeneous and poor stability dyes, above shortcoming has had a strong impact on the quality of flax lining, has also limited its development simultaneously.
Summary of the invention
The objective of the invention is at above-mentioned defective of the prior art, provide a kind of vegetable colour to dye the process of flax lining, in dyeing course, can not cause damage to dying lining, improved the plant dyeing performance, improved dyeing uniformity, stability, the finished product lining meets requirements of green environmental protection.
The technical scheme that realizes above-mentioned purpose is as follows:
A kind of vegetable colour dyes the process of flax lining, adopts following steps:
The first step is carried out biological enzyme degumming and ultrasonic wave pre-treatment to flax lining
Required processing lining is inserted in the pre-treatment pond, add entry; bath raio 1: 15～60, add biology enzyme again, consumption 0.5～3g/L; pH value 5～9; under the condition of 50～80 ℃ of temperature, soaked 1～3 hour, dehydration; add water treatment 0.5～1 hour then in supersonic wave cleaning machine, dehydration is dried again;
Second step, follow-up mordant dyeing look was handled
(1) add entry in supersonic wave cleaning machine, evenly add mordant again, the materials ratio is 1.0～25g/L, adds vegetable colour again, and the materials ratio is 10～100g/L, uses the ultrasonic Treatment dye liquor then 0.5～1 hour;
(2) in dying the pond, dye the pond placing through flax lining of pre-treatment, add the dye liquor of crossing through step (1) ultrasonic Treatment, bath raio 1: 10～50 is warming up to 65～95 ℃, handles 1～1.5 hour, and heating rate is 2～4 ℃/minute;
(3) will carry out cold wash through the lining that handled step (2): bath raio 1: 15～45,20～30 ℃ of water temperatures were handled 15～40 minutes, repeated 3～5 times;
(4) will soap through the lining that handled step (3): bath raio 1: 25～60,30～45 ℃ of water temperatures were handled 10～20 minutes, repeated 2～3 times;
(5) will carry out hot water wash through the lining that handled step (4): bath raio 1: 30～50,75～90 ℃ of water temperatures, 1～2 ℃/minute of programming rate was handled 40～60 minutes;
(6) lining cold wash 2～3 times that will handle through step (5) again, 20～30 ℃ of water temperatures were handled 20～40 minutes at every turn;
(7) oven dry: 90～120 ℃ of temperature.
Further, the biology enzyme in the described first step pre-treatment is protease or amylase.
Further, the mordant in described second rapid step by step (1) is a kind of in plant ash, lime, alunite or the red water.
Further, the vegetable colour in described second rapid step by step (1) is turmeric uranidin or cork tree uranidin.
Used industrial soap content is 0.5～2% when soaping in described second rapid step by step (4) further.
Compared with the prior art the present invention has following advantage:
(1) utilizes vegetable colour that flax lining is dyeed, proposed a kind of new environmental protection colouring method, pollution-free generation in dyeing course.
(2) have peptizaiton because the microjet that the ultrasonic cavitation effect forms is assembled dyestuff, make more the polychromatophilia material be the unimolecule state and exist, more help the absorption of fiber, improved dye-uptake, improved dyefastness.
(3) utilize biology enzyme and ultrasonic wave that flax lining is carried out pre-treatment, effectively protect lining injury-free in dyeing course.Simultaneously, improve dyeability, guaranteed the stability and the uniformity of dyeing, thereby guaranteed the quality of dyeing back lining.
The specific embodiment
Embodiment 1
1, flax lining is carried out biological enzyme degumming and ultrasonic wave pre-treatment
Required processing lining is inserted in the pre-treatment pond, add entry, bath raio 1: 15 adds protease again, consumption 0.5g/L, pH value 5 under the condition of 50 ℃ of temperature, was soaked 1 hour, dehydration adds water treatment 0.5 hour then in large-scale single groove ultrasonic cleaning machine, dehydration is dried again;
2, follow-up mordant dyeing look is handled
(1) add entry in large-scale single groove ultrasonic cleaning machine, evenly add the mordant alunite again, materials add vegetable colour turmeric uranidin again than for 1.0g/L, and materials were used the ultrasonic Treatment dye liquor 0.5 hour then than for 10g/L;
(2) in dying the pond, dye the pond placing through flax lining of pre-treatment, add the dye liquor of crossing through step (1) ultrasonic Treatment, bath raio 1: 10 is warming up to 65 ℃, handles 1 hour, and heating rate is 2 ℃/minute;
(3) cold wash: bath raio 1: 15,20 ℃ of water temperatures were handled 15 minutes, repeated 3 times;
(4) lining that step (3) was handled is soaped: bath raio 1: 25, and 30 ℃ of water temperatures were handled 10 minutes, repeated 2 times, and used industrial soap content is 0.5% when wherein soaping;
(5) lining that step (4) was handled carries out hot water wash: bath raio 1: 30, and 75 ℃ of water temperatures, 1 ℃/minute of programming rate was handled 40 minutes;
(6) use cold wash again 2 times, 20 ℃ of water temperatures were handled 20 minutes at every turn;
(7) oven dry: 90 ℃ of temperature;
(8) conventional preshrunk, tentering, packing.
Embodiment 2
1, flax lining is carried out biological enzyme degumming and ultrasonic wave pre-treatment
Required processing lining is inserted in the pre-treatment pond, add entry, bath raio 1: 60 adds amylase again, consumption 3g/L, pH value 9 under the condition of 80 ℃ of temperature, was soaked 3 hours, dehydration adds water treatment 0.8 hour then in large-scale single groove ultrasonic cleaning machine, dehydration is dried again;
2, follow-up mordant dyeing look is handled
(1) add entry in large-scale single groove ultrasonic cleaning machine, evenly add mordant lime again, materials add vegetable colour cork tree uranidin again than for 25g/L, and materials were used the ultrasonic Treatment dye liquor 1 hour then than for 100g/L;
(2) in dying the pond, dye the pond placing through flax lining of pre-treatment, add the dye liquor of crossing through step (1) ultrasonic Treatment, bath raio 1: 50 is warming up to 95 ℃, handles 1.5 hours, and heating rate is 4 ℃/minute;
(3) cold wash: bath raio 1: 45,30 ℃ of water temperatures were handled 40 minutes, repeated 5 times;
(4) lining that step (3) was handled is soaped: bath raio 1: 60, and 45 ℃ of water temperatures were handled 20 minutes, repeated 3 times;
(5) lining that step (4) was handled carries out hot water wash: bath raio 1: 50, and 90 ℃ of water temperatures, 2 ℃/minute of programming rates were handled 60 minutes;
(6) use cold wash again 3 times, 30 ℃ of water temperatures were handled 40 minutes at every turn;
(7) oven dry: 120 ℃ of temperature;
(8) conventional preshrunk, tentering, packing.
Embodiment 3
1, flax lining is carried out biological enzyme degumming and ultrasonic wave pre-treatment
Required processing lining is inserted in the pre-treatment pond, add entry, bath raio 1: 30 adds protease again, consumption 2g/L, pH value 7 under the condition of 65 ℃ of temperature, was soaked 2 hours, dehydration adds water treatment 1 hour then in large-scale single groove ultrasonic cleaning machine, dehydration is dried again;
2, follow-up mordant dyeing look is handled
(1) add entry in large-scale single groove ultrasonic cleaning machine, evenly add mordant plant ash again, materials add vegetable colour turmeric uranidin again than for 15g/L, and materials were used the ultrasonic Treatment dye liquor 0.8 hour then than for 50g/L;
(2) in dying the pond, dye the pond placing through flax lining of pre-treatment, add the dye liquor of crossing through step (1) ultrasonic Treatment, bath raio 1: 30 is warming up to 80 ℃, handles 1.2 hours, and heating rate is 3 ℃/minute;
(3) cold wash: bath raio 1: 30,25 ℃ of water temperatures were handled 25 minutes, repeated 4 times;
(4) lining that step (3) was handled is soaped: bath raio 1: 40, and 35 ℃ of water temperatures were handled 15 minutes, repeated 2 times;
(5) lining that step (4) was handled carries out hot water wash: bath raio 1: 40, and 80 ℃ of water temperatures, 1.5 ℃/minute of programming rates were handled 50 minutes;
(6) use cold wash again 2 times, 25 ℃ of water temperatures were handled 30 minutes at every turn;
(7) oven dry: 110 ℃ of temperature;
(8) conventional preshrunk, tentering, packing.
Embodiment 4
1, flax lining is carried out biological enzyme degumming and ultrasonic wave pre-treatment
Required processing lining is inserted in the pre-treatment pond, add entry, bath raio 1: 45 adds amylase again, consumption 1g/L, pH value 8 under the condition of 70 ℃ of temperature, was soaked 2 hours, dehydration adds water treatment 1 hour then in large-scale single groove ultrasonic cleaning machine, dehydration is dried again;
2, follow-up mordant dyeing look is handled:
(1) add entry in large-scale single groove ultrasonic cleaning machine, evenly add mordant red water again, materials add vegetable colour cork tree uranidin again than for 8g/L, and materials were used the ultrasonic Treatment dye liquor 0.8 hour then than for 80g/L;
(2) in dying the pond, dye the pond placing through flax lining of pre-treatment, add the dye liquor of crossing through step (1) ultrasonic Treatment, bath raio 1: 40 is warming up to 75 ℃, handles 1.2 hours, and heating rate is 3 ℃/minute;
(3) cold wash: bath raio 1: 40,25 ℃ of water temperatures were handled 30 minutes, repeated 4 times;
(4) lining that step (3) was handled is soaped: bath raio 1: 50, and 40 ℃ of water temperatures were handled 15 minutes, repeated 2 times;
(5) lining that step (4) was handled carries out hot water wash: bath raio 1: 40, and 85 ℃ of water temperatures, 1.5 ℃/minute of programming rates were handled 50 minutes;
(6) use cold wash again 2 times, 25 ℃ of water temperatures were handled 30 minutes at every turn;
(7) oven dry: 100 ℃ of temperature;
(8) conventional preshrunk, tentering, packing.
Claims (4)
1. the process that vegetable colour dyes flax lining is characterized in that, adopts following steps:
The first step is carried out biological enzyme degumming and ultrasonic wave pre-treatment to flax lining
Required processing lining is inserted in the pre-treatment pond, add entry; bath raio 1: 15～60, add biology enzyme again, consumption 0.5～3g/L; pH value 5～9; under the condition of 50～80 ℃ of temperature, soaked 1～3 hour, dehydration; add water treatment 0.5～1 hour then in supersonic wave cleaning machine, dehydration is dried again;
Second step, follow-up mordant dyeing look was handled
(1) add entry in supersonic wave cleaning machine, evenly add mordant again, the materials ratio is 1.0～25g/L, adds vegetable colour again, and the materials ratio is 10～100g/L, uses the ultrasonic Treatment dye liquor then 0.5～1 hour;
(2) in dying the pond, dye the pond placing through flax lining of pre-treatment, add the dye liquor of crossing through step (1) ultrasonic Treatment, bath raio 1: 10～50 is warming up to 65～95 ℃, handles 1～1.5 hour, and heating rate is 2～4 ℃/minute;
(3) will carry out cold wash through the lining that handled step (2): bath raio 1: 15～45,20～30 ℃ of water temperatures were handled 15～40 minutes, repeated 3～5 times;
(4) will soap through the lining that handled step (3): bath raio 1: 25～60,30～45 ℃ of water temperatures were handled 10～20 minutes, repeated 2～3 times;
(5) will carry out hot water wash through the lining that handled step (4): bath raio 1: 30～50,75～90 ℃ of water temperatures, 1～2 ℃/minute of programming rate was handled 40～60 minutes;
(6) lining cold wash 2～3 times that will handle through step (5) again, 20～30 ℃ of water temperatures were handled 20～40 minutes at every turn;
(7) oven dry: 90～120 ℃ of temperature.
2. a kind of vegetable colour according to claim 1 dyes the process of flax lining, it is characterized in that, the biology enzyme in the described first step pre-treatment is protease or amylase.
3. a kind of vegetable colour according to claim 1 dyes the process of flax lining, it is characterized in that, the mordant in described second rapid step by step (1) is a kind of in plant ash, lime, alunite or the red water.
4. a kind of vegetable colour according to claim 1 dyes the process of flax lining, it is characterized in that, the vegetable colour in described second rapid step by step (1) is turmeric uranidin or cork tree uranidin.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN2009101767683A CN102021846A (en) | 2009-09-21 | 2009-09-21 | Process method for dying flax fabric by vegetable dye |
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| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN2009101767683A CN102021846A (en) | 2009-09-21 | 2009-09-21 | Process method for dying flax fabric by vegetable dye |
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Cited By (14)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN102677189A (en) * | 2012-05-11 | 2012-09-19 | 铜陵市霞飞新材料有限责任公司 | Method for extracting linen fiber from linen waste by biological enzyme |
| CN102733205A (en) * | 2012-06-15 | 2012-10-17 | 桐乡闻道纺织有限公司 | Preparation method for linen |
| CN102758350A (en) * | 2011-04-29 | 2012-10-31 | 李晓柯 | Textile product printing and dyeing method |
| CN103361830A (en) * | 2013-08-06 | 2013-10-23 | 太仓市珠江线带厂 | Flax fabric |
| CN103993488A (en) * | 2014-04-23 | 2014-08-20 | 江苏华艺服饰有限公司 | Environmentally friendly printing and dyeing method |
| CN105239430A (en) * | 2015-10-22 | 2016-01-13 | 江南大学 | Application of ultrasonic technology to hemp fiber dyeing |
| CN105586790A (en) * | 2016-02-16 | 2016-05-18 | 德州恒丰纺织有限公司 | Vegetable dye staining series yarn and preparation method thereof |
| CN105780531A (en) * | 2014-12-22 | 2016-07-20 | 王洪波 | Cymbaria dahurica cloth dyeing technology |
| CN105780530A (en) * | 2014-12-22 | 2016-07-20 | 宋雅男 | Rose flower cloth dyeing technology |
| CN105780532A (en) * | 2014-12-22 | 2016-07-20 | 董绍光 | Process for dyeing cloth with Chinese gall |
| CN106087469A (en) * | 2016-06-15 | 2016-11-09 | 贵州省黎平县筑绿康农业发展贸易有限公司 | A kind of technique utilizing plant making to dye cloth |
| CN106835773A (en) * | 2017-03-09 | 2017-06-13 | 睢亚历 | The dyeing and printing products and its dyeing method of a kind of linen |
| CN109056376A (en) * | 2018-06-01 | 2018-12-21 | 辽东学院 | A kind of upper dyeing method of natural cationic dye liquor and tussah silk |
| WO2019109694A1 (en) * | 2017-12-06 | 2019-06-13 | 何炽斌 | Novel method of producing completely natural dyed fabric |
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2009
- 2009-09-21 CN CN2009101767683A patent/CN102021846A/en active Pending
Cited By (18)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN102758350A (en) * | 2011-04-29 | 2012-10-31 | 李晓柯 | Textile product printing and dyeing method |
| CN102758350B (en) * | 2011-04-29 | 2014-12-10 | 李晓柯 | Textile product printing and dyeing method |
| CN102677189A (en) * | 2012-05-11 | 2012-09-19 | 铜陵市霞飞新材料有限责任公司 | Method for extracting linen fiber from linen waste by biological enzyme |
| CN102733205A (en) * | 2012-06-15 | 2012-10-17 | 桐乡闻道纺织有限公司 | Preparation method for linen |
| CN103361830A (en) * | 2013-08-06 | 2013-10-23 | 太仓市珠江线带厂 | Flax fabric |
| CN103993488A (en) * | 2014-04-23 | 2014-08-20 | 江苏华艺服饰有限公司 | Environmentally friendly printing and dyeing method |
| CN105780531A (en) * | 2014-12-22 | 2016-07-20 | 王洪波 | Cymbaria dahurica cloth dyeing technology |
| CN105780530A (en) * | 2014-12-22 | 2016-07-20 | 宋雅男 | Rose flower cloth dyeing technology |
| CN105780532A (en) * | 2014-12-22 | 2016-07-20 | 董绍光 | Process for dyeing cloth with Chinese gall |
| CN105239430A (en) * | 2015-10-22 | 2016-01-13 | 江南大学 | Application of ultrasonic technology to hemp fiber dyeing |
| CN105586790A (en) * | 2016-02-16 | 2016-05-18 | 德州恒丰纺织有限公司 | Vegetable dye staining series yarn and preparation method thereof |
| CN106087469A (en) * | 2016-06-15 | 2016-11-09 | 贵州省黎平县筑绿康农业发展贸易有限公司 | A kind of technique utilizing plant making to dye cloth |
| CN106087469B (en) * | 2016-06-15 | 2018-05-29 | 贵州省黎平县筑绿康农业发展贸易有限公司 | It is a kind of that the technique dyed cloth is made using plant |
| CN106835773A (en) * | 2017-03-09 | 2017-06-13 | 睢亚历 | The dyeing and printing products and its dyeing method of a kind of linen |
| CN106835773B (en) * | 2017-03-09 | 2018-12-25 | 睢亚历 | A kind of dyeing and printing products and its dyeing method of linen |
| WO2019109694A1 (en) * | 2017-12-06 | 2019-06-13 | 何炽斌 | Novel method of producing completely natural dyed fabric |
| CN109056376A (en) * | 2018-06-01 | 2018-12-21 | 辽东学院 | A kind of upper dyeing method of natural cationic dye liquor and tussah silk |
| CN109056376B (en) * | 2018-06-01 | 2020-12-15 | 辽东学院 | Natural cationic dye liquor and tussah silk dyeing method |
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Application publication date: 20110420 |