CN102712516B - 用于制备中空微球体的方法 - Google Patents

用于制备中空微球体的方法 Download PDF

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Publication number
CN102712516B
CN102712516B CN201080058694.4A CN201080058694A CN102712516B CN 102712516 B CN102712516 B CN 102712516B CN 201080058694 A CN201080058694 A CN 201080058694A CN 102712516 B CN102712516 B CN 102712516B
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CN
China
Prior art keywords
feed
weight
hollow microspheres
hollow
inner tube
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired - Fee Related
Application number
CN201080058694.4A
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English (en)
Chinese (zh)
Other versions
CN102712516A (zh
Inventor
戚钢
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
3M Innovative Properties Co
Original Assignee
3M Innovative Properties Co
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by 3M Innovative Properties Co filed Critical 3M Innovative Properties Co
Publication of CN102712516A publication Critical patent/CN102712516A/zh
Application granted granted Critical
Publication of CN102712516B publication Critical patent/CN102712516B/zh
Expired - Fee Related legal-status Critical Current
Anticipated expiration legal-status Critical

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Classifications

    • C—CHEMISTRY; METALLURGY
    • C03—GLASS; MINERAL OR SLAG WOOL
    • C03C—CHEMICAL COMPOSITION OF GLASSES, GLAZES OR VITREOUS ENAMELS; SURFACE TREATMENT OF GLASS; SURFACE TREATMENT OF FIBRES OR FILAMENTS MADE FROM GLASS, MINERALS OR SLAGS; JOINING GLASS TO GLASS OR OTHER MATERIALS
    • C03C11/00—Multi-cellular glass ; Porous or hollow glass or glass particles
    • C03C11/002—Hollow glass particles
    • C—CHEMISTRY; METALLURGY
    • C03—GLASS; MINERAL OR SLAG WOOL
    • C03B—MANUFACTURE, SHAPING, OR SUPPLEMENTARY PROCESSES
    • C03B19/00—Other methods of shaping glass
    • C03B19/10—Forming beads
    • C03B19/107—Forming hollow beads
    • C—CHEMISTRY; METALLURGY
    • C03—GLASS; MINERAL OR SLAG WOOL
    • C03B—MANUFACTURE, SHAPING, OR SUPPLEMENTARY PROCESSES
    • C03B19/00—Other methods of shaping glass
    • C03B19/10—Forming beads
    • C03B19/107—Forming hollow beads
    • C03B19/1075—Forming hollow beads by blowing, pressing, centrifuging, rolling or dripping
    • C—CHEMISTRY; METALLURGY
    • C03—GLASS; MINERAL OR SLAG WOOL
    • C03B—MANUFACTURE, SHAPING, OR SUPPLEMENTARY PROCESSES
    • C03B9/00—Blowing glass; Production of hollow glass articles
    • C03B9/20—Blowing glass; Production of hollow glass articles in "vacuum blowing" or in "vacuum-and-blow" machines
    • C—CHEMISTRY; METALLURGY
    • C03—GLASS; MINERAL OR SLAG WOOL
    • C03C—CHEMICAL COMPOSITION OF GLASSES, GLAZES OR VITREOUS ENAMELS; SURFACE TREATMENT OF GLASS; SURFACE TREATMENT OF FIBRES OR FILAMENTS MADE FROM GLASS, MINERALS OR SLAGS; JOINING GLASS TO GLASS OR OTHER MATERIALS
    • C03C3/00—Glass compositions
    • C03C3/04—Glass compositions containing silica
    • C03C3/076—Glass compositions containing silica with 40% to 90% silica, by weight
    • C03C3/078—Glass compositions containing silica with 40% to 90% silica, by weight containing an oxide of a divalent metal, e.g. an oxide of zinc
    • C—CHEMISTRY; METALLURGY
    • C03—GLASS; MINERAL OR SLAG WOOL
    • C03C—CHEMICAL COMPOSITION OF GLASSES, GLAZES OR VITREOUS ENAMELS; SURFACE TREATMENT OF GLASS; SURFACE TREATMENT OF FIBRES OR FILAMENTS MADE FROM GLASS, MINERALS OR SLAGS; JOINING GLASS TO GLASS OR OTHER MATERIALS
    • C03C3/00—Glass compositions
    • C03C3/04—Glass compositions containing silica
    • C03C3/076—Glass compositions containing silica with 40% to 90% silica, by weight
    • C03C3/11—Glass compositions containing silica with 40% to 90% silica, by weight containing halogen or nitrogen
    • C03C3/112—Glass compositions containing silica with 40% to 90% silica, by weight containing halogen or nitrogen containing fluorine
    • C03C3/115—Glass compositions containing silica with 40% to 90% silica, by weight containing halogen or nitrogen containing fluorine containing boron
    • Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02P—CLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
    • Y02P40/00—Technologies relating to the processing of minerals
    • Y02P40/50—Glass production, e.g. reusing waste heat during processing or shaping
    • Y02P40/57—Improving the yield, e-g- reduction of reject rates

Landscapes

  • Chemical & Material Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Materials Engineering (AREA)
  • Organic Chemistry (AREA)
  • Manufacturing & Machinery (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • General Chemical & Material Sciences (AREA)
  • Geochemistry & Mineralogy (AREA)
  • Glass Compositions (AREA)
  • Manufacturing Of Micro-Capsules (AREA)
CN201080058694.4A 2009-12-21 2010-12-14 用于制备中空微球体的方法 Expired - Fee Related CN102712516B (zh)

Applications Claiming Priority (3)

Application Number Priority Date Filing Date Title
US12/643,606 2009-12-21
US12/643,606 US8261577B2 (en) 2009-12-21 2009-12-21 Method for making hollow microspheres
PCT/US2010/060229 WO2011084407A2 (en) 2009-12-21 2010-12-14 Method for making hollow microspheres

Publications (2)

Publication Number Publication Date
CN102712516A CN102712516A (zh) 2012-10-03
CN102712516B true CN102712516B (zh) 2015-04-22

Family

ID=44151907

Family Applications (1)

Application Number Title Priority Date Filing Date
CN201080058694.4A Expired - Fee Related CN102712516B (zh) 2009-12-21 2010-12-14 用于制备中空微球体的方法

Country Status (8)

Country Link
US (1) US8261577B2 (enExample)
EP (1) EP2516338A4 (enExample)
JP (1) JP5731537B2 (enExample)
KR (1) KR101902587B1 (enExample)
CN (1) CN102712516B (enExample)
BR (1) BR112012015180A2 (enExample)
EA (1) EA025991B1 (enExample)
WO (1) WO2011084407A2 (enExample)

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BR112013013237A2 (pt) * 2010-12-20 2016-09-06 3M Innovative Properties Co método de formação de microesferas ocas, microesferas ocas e aparelho para formação de microesferas ocas de vidro
CN105392742B (zh) 2013-07-18 2018-05-11 3M创新有限公司 玻璃微泡、粗制产品及其制备方法
FR3015474B1 (fr) 2013-12-19 2016-01-01 Bostik Sa Composition d'enduit pour mur et plafond ayant des proprietes d'isolation thermique
GB201415005D0 (en) * 2014-08-22 2014-10-08 Univ Nottingham Porous and non-pourous bodies
US9809493B2 (en) * 2015-04-27 2017-11-07 Ford Global Technologies, Llc Surface treatment of glass bubbles
CN104926137A (zh) * 2015-07-01 2015-09-23 合肥鼎亮光学科技有限公司 一种pc反光膜用玻璃微珠及其制备方法
CN105036555A (zh) * 2015-07-13 2015-11-11 安徽天堂唯高塑业科技有限公司 一种用于汽车车牌级反光膜的玻璃微珠及其制备方法
CN105060706A (zh) * 2015-07-29 2015-11-18 蚌埠高华电子股份有限公司 一种反光布用耐压玻璃微珠及其制备方法
CN105152538B (zh) * 2015-08-27 2018-11-09 东阿县鼎盛玻璃球有限公司 一种代替不锈钢球的节能环保玻璃球
RS57226B1 (sr) 2015-12-21 2018-07-31 Adf Mat Gmbh Hemijska supstanca za proizvodnju šupljih sfernih staklenih čestica sa visokom kompresivnom snagom
JP2019112283A (ja) * 2017-12-26 2019-07-11 日本電気硝子株式会社 ガラスフィラーの製造方法
CN110054396B (zh) * 2018-01-18 2021-10-15 宁波大学 一种2s2g硫系玻璃微球制作装置
PL3826969T3 (pl) * 2018-07-26 2024-08-19 Omya International Ag Puste w środku kuliste cząstki ze szkła
US12006394B2 (en) 2018-10-03 2024-06-11 Sika Technology Ag Curable composition of low density
CN109877330B (zh) * 2019-03-20 2023-09-05 北京科技大学 一种生产3d打印用球形金属粉体的装置及使用方法
WO2020198919A1 (en) * 2019-03-29 2020-10-08 Dow Global Technologies Llc Pellet containing additives
BR112022014385A2 (pt) 2020-01-24 2022-09-20 Basf Se Processo para preparar partículas de vidro esféricas ocas, e, dispositivo de aquecimento
WO2021203232A1 (en) * 2020-04-07 2021-10-14 Corning Incorporated Porous structure such as for filters, and making the same
KR102308504B1 (ko) * 2020-12-31 2021-10-01 황인동 중공비드를 포함하는 콘크리트 조성물 및 그 제조방법
US20230406993A1 (en) 2021-02-02 2023-12-21 Sika Technology Ag Two-component polyurethane filler having an adjustable pot life
CN116604810B (zh) * 2023-05-25 2024-01-16 惠州市顺美医疗科技有限公司 一种导管鞘表面成型设备及其成型工艺

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US4133854A (en) * 1977-06-16 1979-01-09 The United States Of America As Represented By The United States Department Of Energy Method for producing small hollow spheres
US4142969A (en) * 1971-05-17 1979-03-06 Funk Richard S Composition and process for selectively removing oleaginous products from water
US4257798A (en) * 1979-07-26 1981-03-24 The United States Of America As Represented By The United States Department Of Energy Method for introduction of gases into microspheres
US4661137A (en) * 1984-06-21 1987-04-28 Saint Gobain Vitrage Process for producing glass microspheres
US4698317A (en) * 1984-04-24 1987-10-06 Kanto Kagaku Kabushiki Kaisha Porous cordierite ceramics, a process for producing same and use of the porous cordierite ceramics
US5501871A (en) * 1992-10-30 1996-03-26 Innovation Associates, Inc. Thermal insulating material and method of manufacturing same

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US3365315A (en) * 1963-08-23 1968-01-23 Minnesota Mining & Mfg Glass bubbles prepared by reheating solid glass partiles
US3673101A (en) * 1969-12-08 1972-06-27 Grace W R & Co Process for preparing improved carbide microspheres from ion exchange resins
US4279632A (en) * 1979-05-08 1981-07-21 Nasa Method and apparatus for producing concentric hollow spheres
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US4767726A (en) * 1987-01-12 1988-08-30 Minnesota Mining And Manufacturing Company Glass microbubbles
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US5217928A (en) * 1988-08-24 1993-06-08 Potters Industries, Inc. Hollow glass spheres
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DK165090D0 (da) 1990-07-09 1990-07-09 Kem En Tec As Konglomererede partikler
CA2111141A1 (en) * 1992-12-11 1994-06-12 Kazuo Sunahara Process for producing crystalline microballoons
JP3633091B2 (ja) * 1996-04-09 2005-03-30 旭硝子株式会社 微小無機質球状中実体の製造方法
EP1156021A1 (en) * 2000-05-19 2001-11-21 Asahi Glass Co., Ltd. Hollow aluminosilicate glass microspheres and process for their production
US6983797B2 (en) * 2003-05-22 2006-01-10 Halliburton Energy Services, Inc. Lightweight high strength particles and methods of their use in wells
US7449503B2 (en) * 2004-10-18 2008-11-11 Potters Industries Inc. Glass microspheres with multiple bubble inclusions
JP4949657B2 (ja) * 2004-11-09 2012-06-13 大研化学工業株式会社 高耐摩耗性ジルコニア微小球とその製造方法
US20060122049A1 (en) 2004-12-03 2006-06-08 3M Innovative Properties Company Method of making glass microbubbles and raw product
EP1877348A1 (en) 2005-04-29 2008-01-16 3M Innovative Properties Company Glass microbubble-containing syntactic foams, explosives, and method of making
GB2427170A (en) * 2005-06-17 2006-12-20 3M Innovative Properties Co Fluoropolymer film having glass microspheres
EP1953184B1 (en) * 2005-09-16 2018-08-01 Matsumoto Yushi-Seiyaku Co., Ltd. Thermally expanded microsphere and process for production thereof
WO2007050062A1 (en) 2005-10-26 2007-05-03 University Of North Dakota Methods for the production of low-density microspheres

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* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US4142969A (en) * 1971-05-17 1979-03-06 Funk Richard S Composition and process for selectively removing oleaginous products from water
US4133854A (en) * 1977-06-16 1979-01-09 The United States Of America As Represented By The United States Department Of Energy Method for producing small hollow spheres
US4257798A (en) * 1979-07-26 1981-03-24 The United States Of America As Represented By The United States Department Of Energy Method for introduction of gases into microspheres
US4698317A (en) * 1984-04-24 1987-10-06 Kanto Kagaku Kabushiki Kaisha Porous cordierite ceramics, a process for producing same and use of the porous cordierite ceramics
US4661137A (en) * 1984-06-21 1987-04-28 Saint Gobain Vitrage Process for producing glass microspheres
US5501871A (en) * 1992-10-30 1996-03-26 Innovation Associates, Inc. Thermal insulating material and method of manufacturing same

Also Published As

Publication number Publication date
EP2516338A2 (en) 2012-10-31
WO2011084407A3 (en) 2011-10-20
EA201200772A1 (ru) 2013-02-28
JP2013514965A (ja) 2013-05-02
CN102712516A (zh) 2012-10-03
US20110152056A1 (en) 2011-06-23
EP2516338A4 (en) 2014-07-09
US8261577B2 (en) 2012-09-11
WO2011084407A2 (en) 2011-07-14
KR101902587B1 (ko) 2018-09-28
JP5731537B2 (ja) 2015-06-10
BR112012015180A2 (pt) 2016-03-29
EA025991B1 (ru) 2017-02-28
KR20120102779A (ko) 2012-09-18

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C06 Publication
PB01 Publication
C10 Entry into substantive examination
SE01 Entry into force of request for substantive examination
C14 Grant of patent or utility model
GR01 Patent grant
CF01 Termination of patent right due to non-payment of annual fee
CF01 Termination of patent right due to non-payment of annual fee

Granted publication date: 20150422

Termination date: 20191214