CN102660140A - 多种色调甜菜红色素的制备方法 - Google Patents
多种色调甜菜红色素的制备方法 Download PDFInfo
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- CN102660140A CN102660140A CN2012101547346A CN201210154734A CN102660140A CN 102660140 A CN102660140 A CN 102660140A CN 2012101547346 A CN2012101547346 A CN 2012101547346A CN 201210154734 A CN201210154734 A CN 201210154734A CN 102660140 A CN102660140 A CN 102660140A
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- beet red
- beet
- red pigment
- liters
- pigment
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Links
- 235000016068 Berberis vulgaris Nutrition 0.000 title claims abstract description 74
- 241000335053 Beta vulgaris Species 0.000 title claims abstract description 74
- 239000001054 red pigment Substances 0.000 title claims abstract description 65
- 238000002360 preparation method Methods 0.000 title claims abstract description 15
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims abstract description 32
- 239000011347 resin Substances 0.000 claims abstract description 21
- 229920005989 resin Polymers 0.000 claims abstract description 21
- 238000001035 drying Methods 0.000 claims abstract description 16
- 238000000108 ultra-filtration Methods 0.000 claims abstract description 15
- 238000010828 elution Methods 0.000 claims abstract description 13
- 235000019646 color tone Nutrition 0.000 claims abstract description 4
- 238000000605 extraction Methods 0.000 claims abstract 2
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 claims description 44
- 239000000843 powder Substances 0.000 claims description 35
- 239000007788 liquid Substances 0.000 claims description 30
- 239000000243 solution Substances 0.000 claims description 25
- 239000000049 pigment Substances 0.000 claims description 19
- 239000000203 mixture Substances 0.000 claims description 18
- 239000007864 aqueous solution Substances 0.000 claims description 15
- QTBSBXVTEAMEQO-UHFFFAOYSA-N Acetic acid Chemical compound CC(O)=O QTBSBXVTEAMEQO-UHFFFAOYSA-N 0.000 claims description 14
- 239000012141 concentrate Substances 0.000 claims description 14
- 238000005507 spraying Methods 0.000 claims description 14
- 239000003112 inhibitor Substances 0.000 claims description 13
- 238000002156 mixing Methods 0.000 claims description 11
- GVJHHUAWPYXKBD-UHFFFAOYSA-N (±)-α-Tocopherol Chemical compound OC1=C(C)C(C)=C2OC(CCCC(C)CCCC(C)CCCC(C)C)(C)CCC2=C1C GVJHHUAWPYXKBD-UHFFFAOYSA-N 0.000 claims description 10
- XEEYBQQBJWHFJM-UHFFFAOYSA-N Iron Chemical compound [Fe] XEEYBQQBJWHFJM-UHFFFAOYSA-N 0.000 claims description 10
- 230000002378 acidificating effect Effects 0.000 claims description 9
- 238000005538 encapsulation Methods 0.000 claims description 9
- KRKNYBCHXYNGOX-UHFFFAOYSA-N citric acid Chemical compound OC(=O)CC(O)(C(O)=O)CC(O)=O KRKNYBCHXYNGOX-UHFFFAOYSA-N 0.000 claims description 8
- JVTAAEKCZFNVCJ-UHFFFAOYSA-N lactic acid Chemical compound CC(O)C(O)=O JVTAAEKCZFNVCJ-UHFFFAOYSA-N 0.000 claims description 6
- VYPSYNLAJGMNEJ-UHFFFAOYSA-N Silicium dioxide Chemical compound O=[Si]=O VYPSYNLAJGMNEJ-UHFFFAOYSA-N 0.000 claims description 5
- 229930003427 Vitamin E Natural products 0.000 claims description 5
- 238000010521 absorption reaction Methods 0.000 claims description 5
- 239000008367 deionised water Substances 0.000 claims description 5
- 238000004090 dissolution Methods 0.000 claims description 5
- 239000004744 fabric Substances 0.000 claims description 5
- WIGCFUFOHFEKBI-UHFFFAOYSA-N gamma-tocopherol Natural products CC(C)CCCC(C)CCCC(C)CCCC1CCC2C(C)C(O)C(C)C(C)C2O1 WIGCFUFOHFEKBI-UHFFFAOYSA-N 0.000 claims description 5
- 238000000265 homogenisation Methods 0.000 claims description 5
- 239000012535 impurity Substances 0.000 claims description 5
- 229910052742 iron Inorganic materials 0.000 claims description 5
- 230000007935 neutral effect Effects 0.000 claims description 5
- 229920006395 saturated elastomer Polymers 0.000 claims description 5
- 238000000926 separation method Methods 0.000 claims description 5
- 238000007873 sieving Methods 0.000 claims description 5
- 238000001179 sorption measurement Methods 0.000 claims description 5
- 229940046009 vitamin E Drugs 0.000 claims description 5
- 235000019165 vitamin E Nutrition 0.000 claims description 5
- 239000011709 vitamin E Substances 0.000 claims description 5
- 229920000858 Cyclodextrin Polymers 0.000 claims description 4
- 239000001116 FEMA 4028 Substances 0.000 claims description 4
- 239000005913 Maltodextrin Substances 0.000 claims description 4
- 229920002774 Maltodextrin Polymers 0.000 claims description 4
- WHGYBXFWUBPSRW-FOUAGVGXSA-N beta-cyclodextrin Chemical compound OC[C@H]([C@H]([C@@H]([C@H]1O)O)O[C@H]2O[C@@H]([C@@H](O[C@H]3O[C@H](CO)[C@H]([C@@H]([C@H]3O)O)O[C@H]3O[C@H](CO)[C@H]([C@@H]([C@H]3O)O)O[C@H]3O[C@H](CO)[C@H]([C@@H]([C@H]3O)O)O[C@H]3O[C@H](CO)[C@H]([C@@H]([C@H]3O)O)O3)[C@H](O)[C@H]2O)CO)O[C@@H]1O[C@H]1[C@H](O)[C@@H](O)[C@@H]3O[C@@H]1CO WHGYBXFWUBPSRW-FOUAGVGXSA-N 0.000 claims description 4
- 235000011175 beta-cyclodextrine Nutrition 0.000 claims description 4
- 229960004853 betadex Drugs 0.000 claims description 4
- 229940035034 maltodextrin Drugs 0.000 claims description 4
- 239000004310 lactic acid Substances 0.000 claims description 3
- 235000014655 lactic acid Nutrition 0.000 claims description 3
- PPASLZSBLFJQEF-RKJRWTFHSA-M sodium ascorbate Substances [Na+].OC[C@@H](O)[C@H]1OC(=O)C(O)=C1[O-] PPASLZSBLFJQEF-RKJRWTFHSA-M 0.000 claims description 3
- 229960005055 sodium ascorbate Drugs 0.000 claims description 3
- 239000003463 adsorbent Substances 0.000 claims 1
- 238000000034 method Methods 0.000 abstract description 6
- 238000004440 column chromatography Methods 0.000 abstract description 5
- 238000001914 filtration Methods 0.000 abstract description 5
- 239000002994 raw material Substances 0.000 abstract description 3
- 235000009328 Amaranthus caudatus Nutrition 0.000 abstract 1
- 240000001592 Amaranthus caudatus Species 0.000 abstract 1
- 235000021537 Beetroot Nutrition 0.000 abstract 1
- 235000012735 amaranth Nutrition 0.000 abstract 1
- 239000004178 amaranth Substances 0.000 abstract 1
- 239000003963 antioxidant agent Substances 0.000 abstract 1
- 230000003078 antioxidant effect Effects 0.000 abstract 1
- 238000005406 washing Methods 0.000 abstract 1
- 238000004140 cleaning Methods 0.000 description 8
- 239000000523 sample Substances 0.000 description 8
- 239000000284 extract Substances 0.000 description 6
- 229930006000 Sucrose Natural products 0.000 description 4
- CZMRCDWAGMRECN-UGDNZRGBSA-N Sucrose Chemical compound O[C@H]1[C@H](O)[C@@H](CO)O[C@@]1(CO)O[C@@H]1[C@H](O)[C@@H](O)[C@H](O)[C@@H](CO)O1 CZMRCDWAGMRECN-UGDNZRGBSA-N 0.000 description 4
- 229960000583 acetic acid Drugs 0.000 description 4
- 230000008901 benefit Effects 0.000 description 4
- 238000004519 manufacturing process Methods 0.000 description 4
- 238000002791 soaking Methods 0.000 description 4
- 239000005720 sucrose Substances 0.000 description 4
- 239000003643 water by type Substances 0.000 description 4
- 238000005516 engineering process Methods 0.000 description 3
- 241000196324 Embryophyta Species 0.000 description 2
- VMHLLURERBWHNL-UHFFFAOYSA-M Sodium acetate Chemical compound [Na+].CC([O-])=O VMHLLURERBWHNL-UHFFFAOYSA-M 0.000 description 2
- 238000006243 chemical reaction Methods 0.000 description 2
- 238000009776 industrial production Methods 0.000 description 2
- 239000001632 sodium acetate Substances 0.000 description 2
- 235000017281 sodium acetate Nutrition 0.000 description 2
- BHZOKUMUHVTPBX-UHFFFAOYSA-M sodium acetic acid acetate Chemical compound [Na+].CC(O)=O.CC([O-])=O BHZOKUMUHVTPBX-UHFFFAOYSA-M 0.000 description 2
- 239000000654 additive Substances 0.000 description 1
- 239000003513 alkali Substances 0.000 description 1
- 238000004364 calculation method Methods 0.000 description 1
- 239000003153 chemical reaction reagent Substances 0.000 description 1
- 230000008878 coupling Effects 0.000 description 1
- 238000010168 coupling process Methods 0.000 description 1
- 238000005859 coupling reaction Methods 0.000 description 1
- 238000013016 damping Methods 0.000 description 1
- 230000018044 dehydration Effects 0.000 description 1
- 238000006297 dehydration reaction Methods 0.000 description 1
- 230000008021 deposition Effects 0.000 description 1
- 238000000151 deposition Methods 0.000 description 1
- 238000001514 detection method Methods 0.000 description 1
- 238000007599 discharging Methods 0.000 description 1
- 239000003814 drug Substances 0.000 description 1
- 230000000694 effects Effects 0.000 description 1
- JEIPFZHSYJVQDO-UHFFFAOYSA-N ferric oxide Chemical compound O=[Fe]O[Fe]=O JEIPFZHSYJVQDO-UHFFFAOYSA-N 0.000 description 1
- 239000012847 fine chemical Substances 0.000 description 1
- 238000005189 flocculation Methods 0.000 description 1
- 230000016615 flocculation Effects 0.000 description 1
- 239000012530 fluid Substances 0.000 description 1
- 235000013305 food Nutrition 0.000 description 1
- 235000013373 food additive Nutrition 0.000 description 1
- 239000002778 food additive Substances 0.000 description 1
- 239000012362 glacial acetic acid Substances 0.000 description 1
- 238000010438 heat treatment Methods 0.000 description 1
- 238000006386 neutralization reaction Methods 0.000 description 1
- 231100000252 nontoxic Toxicity 0.000 description 1
- 230000003000 nontoxic effect Effects 0.000 description 1
- 239000012488 sample solution Substances 0.000 description 1
- 239000007974 sodium acetate buffer Substances 0.000 description 1
- 230000001954 sterilising effect Effects 0.000 description 1
- 238000004659 sterilization and disinfection Methods 0.000 description 1
- 239000002699 waste material Substances 0.000 description 1
- 239000002351 wastewater Substances 0.000 description 1
- 238000005303 weighing Methods 0.000 description 1
Landscapes
- Coloring Foods And Improving Nutritive Qualities (AREA)
- Cosmetics (AREA)
Abstract
Description
实施例1 | 实施例2 | 实施例3 | 实施例4 | 实施例5 | 实施例6 | |
色调 | 4种 | 4种 | 4种 | 2种 | 4种 | 2种 |
平均色价 | 81.3 | 81.1 | 81.1 | 61.1 | 81.1 | 40.5 |
产率 | 1.35% | 1.34% | 1.33% | 0.77% | 1.34% | 0.66% |
热损失率 | 2.5% | 2.6% | 2.8% | 2.5% | 17.5% | 29.3% |
光损失率 | 1.3% | 1.5% | 1.6% | 1.3% | 16.2% | 27.9% |
Claims (7)
Priority Applications (1)
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CN201210154734.6A CN102660140B (zh) | 2012-05-18 | 2012-05-18 | 多种色调甜菜红色素的制备方法 |
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CN201210154734.6A CN102660140B (zh) | 2012-05-18 | 2012-05-18 | 多种色调甜菜红色素的制备方法 |
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Publication Number | Publication Date |
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CN102660140A true CN102660140A (zh) | 2012-09-12 |
CN102660140B CN102660140B (zh) | 2014-04-16 |
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CN201210154734.6A Expired - Fee Related CN102660140B (zh) | 2012-05-18 | 2012-05-18 | 多种色调甜菜红色素的制备方法 |
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Cited By (6)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN102993769A (zh) * | 2012-12-24 | 2013-03-27 | 晨光生物科技集团股份有限公司 | 改善甜菜红色素色调的方法 |
CN104130591A (zh) * | 2014-08-19 | 2014-11-05 | 天津市尖峰天然产物研究开发有限公司 | 一种从红甜菜浓缩汁中提取纯化甜菜红色素的方法 |
WO2015091354A1 (de) * | 2013-12-20 | 2015-06-25 | Sensient Colors Europe Gmbh | Zum menschlichen verzehr geeignete farbstoffzusammensetzungen |
CN107874070A (zh) * | 2017-11-08 | 2018-04-06 | 南京喜之郎食品有限公司 | 一种甜菜红色素乳化工艺 |
CN112011192A (zh) * | 2020-09-09 | 2020-12-01 | 江西丹霞生物科技股份有限公司 | 一种脱味甜菜红的制备工艺及其制品 |
CN115637059A (zh) * | 2022-11-01 | 2023-01-24 | 云南博瑞生物科技有限公司 | 一种偏黄色调甜菜红的生产方法 |
Citations (7)
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JPS52142725A (en) * | 1976-05-25 | 1977-11-28 | Sanei Kagaku Kogyo Kk | Method of stabilization of betanin series coloring matters |
US4238518A (en) * | 1978-04-28 | 1980-12-09 | Laboratoire L. Lafon | Process for the preparation of a stable Beta vulgaris extract |
US4409254A (en) * | 1980-09-29 | 1983-10-11 | General Foods Corporation | Process for concentrating and isolating a beet colorant |
JPH0411895A (ja) * | 1990-04-27 | 1992-01-16 | Shimadzu Corp | ベタニンの製造法 |
CN1191877A (zh) * | 1997-02-27 | 1998-09-02 | 吉林省农业科学院原子能利用研究所 | 甜菜红色素的制备 |
CN101305797A (zh) * | 2008-07-17 | 2008-11-19 | 江西国亿生物科技有限公司 | 一种胡萝卜色素的制备方法及其胡萝卜色素制品 |
CN102093747A (zh) * | 2010-12-22 | 2011-06-15 | 晨光生物科技集团股份有限公司 | 一种利用大孔树脂生产高色价甜菜红色素的工艺 |
Family Cites Families (1)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
JP4011895B2 (ja) * | 2001-11-22 | 2007-11-21 | キヤノン株式会社 | 画像形成装置 |
-
2012
- 2012-05-18 CN CN201210154734.6A patent/CN102660140B/zh not_active Expired - Fee Related
Patent Citations (7)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
JPS52142725A (en) * | 1976-05-25 | 1977-11-28 | Sanei Kagaku Kogyo Kk | Method of stabilization of betanin series coloring matters |
US4238518A (en) * | 1978-04-28 | 1980-12-09 | Laboratoire L. Lafon | Process for the preparation of a stable Beta vulgaris extract |
US4409254A (en) * | 1980-09-29 | 1983-10-11 | General Foods Corporation | Process for concentrating and isolating a beet colorant |
JPH0411895A (ja) * | 1990-04-27 | 1992-01-16 | Shimadzu Corp | ベタニンの製造法 |
CN1191877A (zh) * | 1997-02-27 | 1998-09-02 | 吉林省农业科学院原子能利用研究所 | 甜菜红色素的制备 |
CN101305797A (zh) * | 2008-07-17 | 2008-11-19 | 江西国亿生物科技有限公司 | 一种胡萝卜色素的制备方法及其胡萝卜色素制品 |
CN102093747A (zh) * | 2010-12-22 | 2011-06-15 | 晨光生物科技集团股份有限公司 | 一种利用大孔树脂生产高色价甜菜红色素的工艺 |
Non-Patent Citations (1)
Title |
---|
罗金岳,安鑫南: "《植物精油和天然色素加工工艺》", 30 September 2005, 北京:化学工业出版社 * |
Cited By (8)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN102993769A (zh) * | 2012-12-24 | 2013-03-27 | 晨光生物科技集团股份有限公司 | 改善甜菜红色素色调的方法 |
WO2015091354A1 (de) * | 2013-12-20 | 2015-06-25 | Sensient Colors Europe Gmbh | Zum menschlichen verzehr geeignete farbstoffzusammensetzungen |
CN104130591A (zh) * | 2014-08-19 | 2014-11-05 | 天津市尖峰天然产物研究开发有限公司 | 一种从红甜菜浓缩汁中提取纯化甜菜红色素的方法 |
CN104130591B (zh) * | 2014-08-19 | 2016-06-08 | 天津市尖峰天然产物研究开发有限公司 | 一种从红甜菜浓缩汁中提取纯化甜菜红色素的方法 |
CN107874070A (zh) * | 2017-11-08 | 2018-04-06 | 南京喜之郎食品有限公司 | 一种甜菜红色素乳化工艺 |
CN112011192A (zh) * | 2020-09-09 | 2020-12-01 | 江西丹霞生物科技股份有限公司 | 一种脱味甜菜红的制备工艺及其制品 |
CN115637059A (zh) * | 2022-11-01 | 2023-01-24 | 云南博瑞生物科技有限公司 | 一种偏黄色调甜菜红的生产方法 |
CN115637059B (zh) * | 2022-11-01 | 2024-03-22 | 云南博瑞生物科技有限公司 | 一种偏黄色调甜菜红的生产方法 |
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