CN102527066B - Multifunctional hot reflux extracting and concentrating unit - Google Patents

Multifunctional hot reflux extracting and concentrating unit Download PDF

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Publication number
CN102527066B
CN102527066B CN201210041987.2A CN201210041987A CN102527066B CN 102527066 B CN102527066 B CN 102527066B CN 201210041987 A CN201210041987 A CN 201210041987A CN 102527066 B CN102527066 B CN 102527066B
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concentration
hot reflux
tank
extractor
reflux extracting
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CN201210041987.2A
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CN102527066A (en
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李晓云
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Abstract

The invention discloses a multifunctional hot reflux extracting and concentrating unit which comprises an extracting tank, a concentrating tank, an alcohol recycling tank and a condensing unit, wherein a gas outlet on the top of the extracting tank and a gas outlet on the top of the concentrating tank are respectively communicated with fluid at a to-be-condensed gas inlet of the condensing unit, a condensate outlet of the condensing device is communicated with fluid at a fluid inlet of the alcohol recycling tank, and a liquid medicine outlet at the bottom of the extracting tank is communicated with fluid at a liquid medicine inlet at the top of the condensing tank through a liquid medicine transmission pipeline. The multifunctional hot reflux extracting and concentrating unit provided by the invention has the advantages that extraction, condensation and recycle are integrated to reach the purposes of time saving, labor saving and cost reducing; and meanwhile, the extraction purity is high and the concentration ratio is large.

Description

Multi-functional hot reflux extracting-concentration machine group
Technical field
The present invention relates to the extraction enrichment facility of chemical and field of medicaments, particularly a kind of multi-functional hot reflux extracting-concentration machine group.
Background technology
In chemical and field of medicaments, often need to extract some specific materials, and obtain the mixture that content is higher after concentrated.But in the prior art, extraction equipment and concentrator normally work alone respectively, consuming time, consumption power and cost are high; And in prior art, the extraction effect of extraction equipment is poor, and DNA purity is low; The concentrating capacity of concentrator is poor, causes concentrated smaller.
Summary of the invention
For the deficiencies in the prior art, the object of the present invention is to provide a kind of extraction, concentrated and reclaim the multi-functional hot reflux extracting-concentration machine group of integrated work, reach save time, laborsaving and cost-saving object, and DNA purity is high, cocnentration factor is large.
Technical scheme of the present invention is achieved in that multi-functional hot reflux extracting-concentration machine group, comprise extractor, concentration tank, alcohol recycling can and condensing unit, the gas vent at the gas vent at described extractor top and described concentration tank top respectively with described condensing unit treat the conducting of condensed gas inlet fluid, the liquid inlet fluid communication of the condensate outlet of described condensing unit and described alcohol recycling can, the medicine liquid outlet of described extractor bottom is by the liquid inlet fluid conducting at liquid conveyance conduit and described concentration tank top.
Above-mentioned multi-functional hot reflux extracting-concentration machine group, is provided with liquor piping pump on described liquid conveyance conduit.
Above-mentioned multi-functional hot reflux extracting-concentration machine group, all has heat-insulation layer on the lateral wall of described extractor and described concentration tank.
Above-mentioned multi-functional hot reflux extracting-concentration machine group, has conduction oil between described extractor inwall and described heat-insulation layer and between described concentration tank inwall and described heat-insulation layer, in described conduction oil, has electric heater.
Above-mentioned multi-functional hot reflux extracting-concentration machine group, is provided with stirring motor on described extractor.
Above-mentioned multi-functional hot reflux extracting-concentration machine group, is all provided with Pressure gauge, oil level pipe and heat conductive oil inlet on described extractor and described concentration tank.
Above-mentioned multi-functional hot reflux extracting-concentration machine group, described alcohol recycling can is connected with vavuum pump by vacuum tube, and described alcohol recycling can and described concentration tank are by suction tube fluid communication, on described suction tube, valve are installed.
The invention has the beneficial effects as follows: multi-functional hot reflux extracting-concentration machine group advantage of the present invention is to extract, concentrated and reclaim integrated work, can reach save time, laborsaving and cost-saving object, and DNA purity is high, cocnentration factor is large.
Brief description of the drawings
Fig. 1 is the structural representation of the multi-functional hot reflux extracting-concentration machine group of the present invention.
In figure: 1-extractor, 2-concentration tank, 3-alcohol recycling can, 4-condensing unit, 5-liquid conveyance conduit, 6-vacuum tube, 7-liquor piping pump, 8-heat-insulation layer, 9-conduction oil, 10-electric heater, 11-stirring motor, 12-Pressure gauge, 13-oil level pipe, 14-heat conductive oil inlet, 15-water inlet, 16-delivery port, 17-suction tube, 18-valve.
Detailed description of the invention
The present invention is described further by reference to the accompanying drawings:
The multi-functional hot reflux extracting-concentration machine group of the present embodiment, comprise extractor 1, concentration tank 2, alcohol recycling can 3 and condensing unit 4, the gas vent at described extractor 1 top and the gas vent at described concentration tank 2 tops respectively with described condensing unit 4 treat the conducting of condensed gas inlet fluid, the liquid inlet fluid communication of the condensate outlet of described condensing unit 1 and described alcohol recycling can 3.The gas volatilizing away from described extractor 1 and described concentration tank 2 becomes liquid and flows in described alcohol recycling can 3 and collect and can again utilize after described condensing unit 4 is cooling; Realize cost-saving object.
The medicine liquid outlet of described extractor 1 bottom is the liquid inlet fluid conducting with described concentration tank 2 tops by liquid conveyance conduit 5, after can making like this to extract, the extract that obtains is delivered directly in described concentration tank 2 and concentrates, thereby has realized extraction and concentration institutional operation.Described alcohol recycling can 3 is connected with vavuum pump by vacuum tube 6, to described alcohol recycling can 3 is vacuumized, and described alcohol recycling can 3 passes through suction tube 17 fluid communication with described concentration tank 2, on described suction tube 17, valve 18 is installed, can make like this gas pumping producing in the inherent concentration process of described concentration tank 2 to described alcohol recycling can 3, can solve that gas in described concentration tank 2 can not enter into described condensing unit 1 in time and the problem of the concentrated speed of impact [alcohol gas that concentration process produces is stranded in described concentration tank 2 and can not discharges in time, a part becomes liquid again, thereby the concentrated speed of impact], the gas producing in concentration process is divided to rapidly in described condensing unit 4 and described alcohol recycling can 3, accelerate concentrated process, shorten concentration time.On described liquid conveyance conduit 5, liquor piping pump 7 is installed, can realizes the smooth delivery of power of extract.On the lateral wall of described extractor 1 and described concentration tank 2, all there is heat-insulation layer 8, between described extractor 1 inwall and described heat-insulation layer 8 and between described concentration tank 2 inwalls and described heat-insulation layer 8, have conduction oil 9, in described conduction oil 9, have electric heater 10; Can heat described conduction oil 9 by described electric heater 10, thereby realize, the concentrate in extract and described concentration tank 2 in described extractor 1 be heated, be conducive to the carrying out of extraction and concentration.On described extractor 1, stirring motor 11 is installed, by stirring motor 11, the material in described extractor 1 is carried out, make extraction rate faster, DNA purity is higher.Pressure gauge 12, oil level pipe 13 and heat conductive oil inlet 14 are all installed on described extractor 1 and described concentration tank 2, can observe easily the pressure in described extractor 1 and described concentration tank 2 by described Pressure gauge 12, guarantee that extraction and concentration carries out smoothly; The amount that can observe conduction oil by described oil level pipe 13, to add conduction oil by described heat conductive oil inlet 14 in time.
The multi-functional hot reflux extracting-concentration machine group of the present embodiment is particularly useful in the production of heart disease curing drop pill, the active ingredient of Ligusticum wallichii and the red sage root being extracted, and DNA purity is high, and cocnentration factor is large.
The multi-functional hot reflux extracting-concentration machine group of the present invention is applicable to the extraction of heat sensitive material, concentrated and receipts cream, and is applicable to volatile oil extraction and reclaims.Technique advanced person, extracts, concentrates and reclaim and can carry out simultaneously, saves time, laborsaving, cost-saving.DNA purity is high, and cocnentration factor is large.
Above-described embodiment is only for the invention example is clearly described, and the not restriction to the invention detailed description of the invention.For those of ordinary skill in the field, can also make other changes in different forms on the basis of the above description.Here without also giving exhaustive to all embodiments.And the apparent variation of being extended out thus or variation are still among the protection domain in the invention claim.

Claims (6)

1. multi-functional hot reflux extracting-concentration machine group, it is characterized in that, comprise extractor (1), concentration tank (2), alcohol recycling can (3) and condensing unit (4), the gas vent at the gas vent at described extractor (1) top and described concentration tank (2) top respectively with described condensing unit (4) treat the conducting of condensed gas inlet fluid, the liquid inlet fluid communication of the condensate outlet of described condensing unit (4) and described alcohol recycling can (3), the liquid inlet fluid conducting with described concentration tank (2) top by liquid conveyance conduit (5) of the medicine liquid outlet of described extractor (1) bottom, described alcohol recycling can (3) is connected with vavuum pump by vacuum tube (6), and described alcohol recycling can (3) and described concentration tank (2) pass through suction tube (17) fluid communication, and valve (18) is installed on described suction tube (17).
2. multi-functional hot reflux extracting-concentration machine group according to claim 1, is characterized in that, liquor piping pump (7) is installed on described liquid conveyance conduit (5).
3. multi-functional hot reflux extracting-concentration machine group according to claim 1, is characterized in that, on the lateral wall of described extractor (1) and described concentration tank (2), all has heat-insulation layer (8).
4. multi-functional hot reflux extracting-concentration machine group according to claim 3, it is characterized in that, between described extractor (1) inwall and described heat-insulation layer (8) and between described concentration tank (2) inwall and described heat-insulation layer (8), there is conduction oil (9), in described conduction oil (9), have electric heater (10).
5. multi-functional hot reflux extracting-concentration machine group according to claim 1, is characterized in that, stirring motor (11) is installed on described extractor (1).
6. according to the arbitrary described multi-functional hot reflux extracting-concentration machine group of claim 1-5, it is characterized in that, Pressure gauge (12), oil level pipe (13) and heat conductive oil inlet (14) are all installed on described extractor (1) and described concentration tank (2).
CN201210041987.2A 2012-02-23 2012-02-23 Multifunctional hot reflux extracting and concentrating unit Expired - Fee Related CN102527066B (en)

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CN102527066B true CN102527066B (en) 2014-09-17

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Families Citing this family (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN103007571B (en) * 2012-12-19 2014-09-10 汪振朴 Alcohol-recyclable medicine extracting device and process thereof
CN105998126A (en) * 2016-05-18 2016-10-12 安徽瑞思威尔科技有限公司 Method for preparing Bozhou chrysanthemum general flavone extracting solution and concentrated solution by extraction and concentration machine

Citations (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN2329428Y (en) * 1998-02-13 1999-07-21 石家庄市星烁实业公司 Reactor for preparing liquid crystal high polymer
CN2596984Y (en) * 2003-01-18 2004-01-07 刘燕湫 Chinese medicine extraction and concentration machine
WO2007042542A1 (en) * 2005-10-12 2007-04-19 Boehringer Ingelheim Pharma Gmbh & Co. Kg Improved method for the production of betulinic acid
CN102342304A (en) * 2011-08-10 2012-02-08 河南华泰粮油机械工程有限公司 Production method for extracting pyrethrin from pyrethrum

Patent Citations (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN2329428Y (en) * 1998-02-13 1999-07-21 石家庄市星烁实业公司 Reactor for preparing liquid crystal high polymer
CN2596984Y (en) * 2003-01-18 2004-01-07 刘燕湫 Chinese medicine extraction and concentration machine
WO2007042542A1 (en) * 2005-10-12 2007-04-19 Boehringer Ingelheim Pharma Gmbh & Co. Kg Improved method for the production of betulinic acid
CN102342304A (en) * 2011-08-10 2012-02-08 河南华泰粮油机械工程有限公司 Production method for extracting pyrethrin from pyrethrum

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